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SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski 1 , J. Langner 1 , R. Mirowski 1 , M. Sadowski 1 , S. Tazzari 2and J. Witkowski 1 1 The Andrzej Soltan Institute for Nuclear Studies, 05-400 Otwock/Swierk, Poland, e-mail: [email protected]¤ 2 The Tor Vergata University and INFN-Roma2, Roma, Italy Contribution to the 5 th International Workshop and Summer School “Towards Fusion Energy – Plasma Physics, Diagnostics, Spin-offs” Kudowa Zdroj, Poland Work supported by the European Community-Research Infrastructure Activity under the FP6 “Structuring the European Research Area” programme (CARE, contract number RII3-CT- 2003-506395). EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF 1

SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

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Page 1: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

SRF

MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING

AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES

P. Strzyzewski1, J. Langner1, R. Mirowski1, M. Sadowski1, S. Tazzari2● and J. Witkowski1

1 The Andrzej Soltan Institute for Nuclear Studies, 05-400 Otwock/Swierk, Poland, e-mail: [email protected]¤

2 The Tor Vergata University and INFN-Roma2, Roma, Italy

Contribution to the 5th International Workshop and Summer School “Towards Fusion Energy – Plasma Physics, Diagnostics, Spin-offs”

Kudowa Zdroj, Poland

Work supported by the European Community-Research Infrastructure Activity under the FP6 “Structuring the European Research Area” programme (CARE, contract number RII3-CT-2003-506395).

EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF

1

Page 2: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

Modelling of magnetic channels forModelling of magnetic channels formicro-droplets filteringmicro-droplets filtering

and tests of their efficiencyand tests of their efficiencyin UHV arc-dischargesin UHV arc-discharges

P.P. Strzyżewski Strzyżewski1)1), J., J. Langner Langner1)1), R., R. Mirowski Mirowski1)1), M.J., M.J. Sadowski Sadowski1)1),,S.S. Tazzari Tazzari2)2) and J. and J. Witkowski Witkowski1)1)

1) 1) TheThe Andrzej Soltan Andrzej Soltan Institute for Nuclear Studies (IPJ), 05-400 Institute for Nuclear Studies (IPJ), 05-400 Otwock Otwock--SwierkSwierk, Poland, e-mail: , Poland, e-mail: p.p.strzyzewskistrzyzewski@@ipjipj..govgov.pl.pl

2) 2) TheThe Tor Vergata Tor Vergata University and INFN-Roma2, Rome, Italy University and INFN-Roma2, Rome, Italy

Fifth International Workshop and Summer School“Towards Fusion Energy - Plasma Physics, Diagnostics, Spin-offs”

Kudowa Zdroj, Poland, June 6-10, 2005

EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF

2

Page 3: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

Vacuum arc dischargeVacuum arc discharge Physical properties:Physical properties:-- fullfull ionis ionisationation of the plasma of the plasma,,-- absence of a working gas sustaining the discharge,absence of a working gas sustaining the discharge,-- presence of multiple-charged ions,presence of multiple-charged ions,-- high kinetic energy of ions (18-150eV).high kinetic energy of ions (18-150eV).

Film properties:- very high density and smoothness (if filtered),- high quality – strongly reduced film defects (i.e. voids),- possibility of making pure metal films and compounds such as nitrides, oxides, carbonaceous,- possibility of deposition on components with sophisticated shape.

EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF

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Page 4: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

Vacuum arc in UHV conditionVacuum arc in UHV conditionIts a new concept proposedIts a new concept proposedrecentlyrecently by dr J by dr J.. LangnerLangner

The main The main goal goal –– to to obtain very obtain veryclean layer by excluding anyclean layer by excluding anysource of contaminantssource of contaminants..

Performing deposition by meansPerforming deposition by meansof the arc discharge in UHV isof the arc discharge in UHV iscomplicated due to:complicated due to:

- selection of appropriate - selection of appropriate materialsmaterials,, - - selection of appropriate triggeringselection of appropriate triggering

system,system, - baking of whole vacuum system - baking of whole vacuum system..

First results show that superconductorFirst results show that superconductor Nb Nb thin layer demonstrate thin layer demonstrate similarsimilar properties properties ((TTcc, RRR) , RRR) to pure bulkto pure bulk Nb Nb and are very promising in view of and are very promising in view of coating RF cavities for particle accelerators (i.e. TESLA)coating RF cavities for particle accelerators (i.e. TESLA)..

10-8 Torr

10-10Torr

Pressure below 10-10 Torr makes possiblethe practical elimination of impurities, like water vapours, nitrogen and CxHY

EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF

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Page 5: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

Vacuum arc vs. filtered vacuum arcVacuum arc vs. filtered vacuum arc

Surface of the Nb coating obtainedwithout magnetic filtering.

Surface of the Nb coating obtained with the use of the filtered UHV arc

The main disadvantage of the arc coating is the production of micro-droplets(macro-particles). It’s size ranges from 0.2 to 20µm. The adhesion of the micro-droplets to the substrate gets worse the uniformity of the film surfacesmoothness and consequently functions of the film. To eliminate the macro-particles from vacuum arc plasma, one could apply magnetic filters.

EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF

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Page 6: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

Magnetic filters for micro-dropletsMagnetic filters for micro-droplets

„Aksenov-type” „S-type” „T-type” 1)

1) Aksenov, I. et al., “High Efficiency Filtered Vacuum-Arc Plasma Source”, XXIth InternationalSymposium on Discharges end Electrical Insulation in Vacuum, Yalta, Ukraine, 2004, 491-494

The main purpose of the filters is to prevent line-of-sight of the macro-particles and to guide plasma efficiently to the substrate.

EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF

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Page 7: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

Magnetic filter suited for UHV conditionMagnetic filter suited for UHV conditionss

Difficulties in realization:--selection of appropriateselection of appropriate materialsmaterials,,--baking system,baking system,--cooling system.cooling system.

Pictures show the Aksenov-type magneticfilter in accordance with UHV technology.Its inner radius is 65mm.2 other filters have been designed and constructed at IPJ: the Aksenov-type with less curvature radius and the T-type.

EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF

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Page 8: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

Modelling of a magnetic field distributionModelling of a magnetic field distributionin the magnetic filtersin the magnetic filters – – partpart I I

•• Because, major plasma loss occurs in the curvilinear part of plasma ductBecause, major plasma loss occurs in the curvilinear part of plasma ductin the filter, it was essential to design the magnetic fields very carefullyin the filter, it was essential to design the magnetic fields very carefully..These losses are mainly due to contact of plasma stream with the filterThese losses are mainly due to contact of plasma stream with the filterwalls causedwalls caused by by gradient and centrifugal drifts. By local fields corrections gradient and centrifugal drifts. By local fields correctionsin the curved part of the filter one can noticeable reduce the drift losses.in the curved part of the filter one can noticeable reduce the drift losses.

•• Magnetic field distribution in the filters was calculated by means of aMagnetic field distribution in the filters was calculated by means of aMaxwell 2D program using Finite Element MethodologyMaxwell 2D program using Finite Element Methodology..

• A guiding magnetic field in the both Aksenov-type magnetic filters wasgenerated by current amounting to 20–200 A, which might flow in high-current cables wrapped around the plasma duct. Such approachensured better field uniformity in the curvature filter than the typical coils,which formed local magnetic bottles (in the region between these coils).

EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF

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Page 9: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

Modelling of a magnetic field distributionModelling of a magnetic field distributionin the magnetic filtersin the magnetic filters – – partpart II II

Magnetic field distribution in the Aksenov-type magnetic filters having different curvatureradius and in the T-type magnetic filter; 1 – cathode, 2 – anode, 3 – focusing coil, 4 –filter inlet, 5 – filter exit, 6 – high-current cable, 7 – ion collector position, 8 – plasma

stream, 9 - correcting coil.

Calculated magnetic filed strengths: - near-cathode region – 16 mT - magnetic duct region – 12 – 14 mT

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Page 10: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

Experimental efficiency of ion-transExperimental efficiency of ion-transpportortthrough considered filtersthrough considered filters

80 90 100 110 120

250

300

350

400

450

500

Ion

colle

ctor

cur

rent

(mA)

Arc curent (A)

(a) (b) (c)

Ion current collected in the magnetic filters outletfor 3 different value of arc discharge current. (a,b– the Aksenov-type filters with respectively high

and low curvature radius, c – the T-type magneticfilter).

The T-type filter is characterised by thebest efficiency of ion transport, whichis typically 30%-40% higher than bothAksenov-type filters.

The arc discharge is the most stablewhen Aksenov-type magnetic filter withless curvature radius is applied.

EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF

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Page 11: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

Efficiency of macro-droplets filteringEfficiency of macro-droplets filtering

Surfaces of thin niobium layer obtained after filtering in considered filtersin magnification of 500.

The Aksenov-type withbig curvature radius.

The Aksenov-type withsmall curvature radius.

The T-type

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Page 12: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

SummarySummaryTThree different prototypes of the magnetic filtershree different prototypes of the magnetic filters for the UHVfor the UHVrequirementsrequirements were were designed designed and made and made at the IPJ; two filters are of at the IPJ; two filters are ofthethe Aksenov Aksenov-type, but they have different curvature radius, and the-type, but they have different curvature radius, and thethirthird filter is the so-called T-type.d filter is the so-called T-type.After discussion two of considered three magnetic filters have beenAfter discussion two of considered three magnetic filters have beenselected for further study and improvements: theselected for further study and improvements: the Aksenov Aksenov-type with-type withless curvature radius and the T-type.less curvature radius and the T-type.

Plans for the future:Plans for the future: - 3D simulations of magnetic field distributions, - 3D simulations of magnetic field distributions, - positive biasing of the filters – to improve ions transport, - positive biasing of the filters – to improve ions transport, - set of fins and baffles - to improve micro-droplets filtering, - set of fins and baffles - to improve micro-droplets filtering, - - additional coil in the T-type filter – for better magnetic field bending additional coil in the T-type filter – for better magnetic field bending..

EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF

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Page 13: SRF - core.ac.uk · SRF MODELLING OF MAGNETIC CHANNELS FOR MICRO-DROPLETS FILTERING AND TESTS OF THEIR EFFICIENCY IN UHV ARC-DISCHARGES P. Strzyzewski1, J. Langner1, R. Mirowski1,

Thank you for attentionThank you for attention

and

Have a nice meal

EU contract number RII3CT-2003-506395 CARE Conf-05-038-SRF

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