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Reference 65 Page 1
ACRONYMS USED IN THIS DOCUMENT
Terra Environmental Corporation seeks to use terminology that is conventional in environmental remediation science, and understandable to the reader. Recognizing that many acronyms have become standard in the environmental field, we have listed several terms that will be used throughout this document for the sake of clarity and readability. Companies EPA Environmental Protection Agency IDEM Indiana Department of Environmental Management Pace Pace Analytical Services, Inc. Terra Terra Environmental Corporation USGS United State Geological Survey
Groundwater Monitoring DO Dissolved Oxygen GW Groundwater MW Monitoring Well ORP Oxidation‐Reduction Potential (a.k.a. Redox Potential) TDS Total Dissolved Solids
Contaminants VOCs Volatile Organic Compounds PAHs Polynuclear Aromatic Hydrocarbons
Miscellaneous CAP Corrective Action Plan CAPA Corrective Action Plan Addendum COC(s) Chemical(s) of Concern DQO Data Quality Objectives ERC Environmental Restrictive Covenant FSI Further Site Investigation LEL Lower Explosive Limit (L)UST (Leaking) Underground Storage Tank LNAPL Light Non‐Aqueous Phase Liquid MDDR Minimum Data Documentation Requirements ORC Oxygen Releasing Compound PLSS Public Land Survey System PID Photo Ionization Detector PQL Practical Quantitative Limit MTG Migration to Groundwater RPG Remediation Program Guide RCG Remediation Closure Guide PPC Potential Petroleum Contaminant
Measurements ug/kg Micrograms per Kilogram (ppb) mg/kg Milligrams per Kilogram (ppm) mg/L Milligrams per Liter (ppm) ug/L Micrograms per Liter (ppb) ug/m3 Micrograms per cubic meter ppm Parts per Million ppb Parts per billion
Reference 65 Page 2
EXECUTIVE SUMMARY
Terra Environmental Corporation (Terra) was authorized by Mr. Charles Ingraham to perform a Phase II ESA at 1123 W. 21st Street, Indianapolis, Indiana. The purpose of the Phase II was to evaluate a recognized environmental condition (REC) identified in a Phase I ESA performed for the Subject Property. The REC was identified as an adjacent property (former Carrier‐Bryant) which was found in several Federal and State databases and a chlorinated solvent plume in the subsurface directly up‐gradient of the Subject Property. The data reviewed during the Phase I ESA indicated that the former Carrier‐Bryant property may have impacted the groundwater on the Subject Property.
The purpose of the Phase II was to evaluate this REC by collecting environmental data. Groundwater samples were collected during the Phase II investigation.
The groundwater samples were compared to the Indiana Department of Environmental Management (IDEM) Remediation Closure Guide March 2015 Screening Levels. These closure levels are used as a screening level to determine concentrations that may require to be cleaned up or may need a corrective action to protect human health and the environment.
The natural site stratigraphy consists predominantly of clay rich unconsolidated sediment from shallow surface to depths ranging from 4 to 8 feet below surface grade. Below the clay material sand and gravel were encountered. The sand and gravel materials were saturated at approximately 26 feet.
The groundwater samples were analyzed for VOCs. Certain VOCs were reported at screening levels exceeding the IDEM RCG (March 2015) tap water screening levels. Specifically Tetrachloroethylene (PCE) and Trichloroethylene (TCE) were reported at elevated levels.
The analytical results indicate exceedances for PCE and TCE in the groundwater at the site. These exceedances appear to be directly related to VOC contamination located in the groundwater at the Carrier‐Bryant site which is up‐gradient of the Subject Property. Terra recommends the pursuit of a comfort letter from the Indiana Brownfields program with regard to the chlorinated solvents identified during this investigation. A Comfort Letter will resolve the Recognized Environmental Condition (REC) associated with the chlorinated contaminant plume coming from an off‐site source.
Reference 65 Page 3
ACRONYMS USED IN THIS DOCUMENT ........................................................................................ 2
EXECUTIVE SUMMARY ................................................................................................................... 3
1. INTRODUCTION ..................................................................................................................... 6
2. BACKGROUND ....................................................................................................................... 6
Site Description and Features ............................................................................................ 6 A.
Physical Setting ................................................................................................................... 7 B.
1. Geological Setting ............................................................................................. 7
2. Site Vicinity Map Topographic Setting ............................................................. 7
3. Shallow Soil ....................................................................................................... 7
4. Aquifer System ................................................................................................. 7
Site History and Land Use .................................................................................................. 8 C.
Adjacent Property Land Use .............................................................................................. 8 D.
Summary of Previous Assessments ................................................................................... 9 E.
3. WORK PERFORMED AND RATIONALE .................................................................................. 9
Scope of Work .................................................................................................................... 9 A.
Methods .............................................................................................................................. 9 B.
Soil Samples ...................................................................................................................... 10 C.
Groundwater Samples ..................................................................................................... 10 D.
1. Grab Groundwater Samples from Soil Borings ............................................... 10
2. Sample Identification ...................................................................................... 10
Sample Analysis ................................................................................................................ 11 E.
3. Analytical Methods ......................................................................................... 11
4. RESULTS ................................................................................................................................ 11
Stratigraphy ...................................................................................................................... 11 A.
Soil Analytical Results ....................................................................................................... 11 B.
Groundwater analytical Results....................................................................................... 11 C.
1. Groundwater Flow .......................................................................................... 11
2. Grab Groundwater Samples ........................................................................... 11
5. EVALUATION OF POTENTIAL EXPOSURE PATHWAYS ....................................................... 12
Reference 65 Page 4
Direct Contact ................................................................................................................... 12 A.
Groundwater Ingestion .................................................................................................... 12 B.
Vapor Intrusion ................................................................................................................. 12 C.
6. CONCLUSIONS ..................................................................................................................... 13
Recognized Environmental Conditions ........................................................................... 13 A.
Adequacy of Investigations .............................................................................................. 13 B.
Limitations of this Assessment ........................................................................................ 13 C.
Conclusion ......................................................................................................................... 14 D.
7. RECOMMENDATIONS ......................................................................................................... 14
8. SUPPORTING DOCUMENTATION ....................................................................................... 14
9. QUALIFICATIONS ................................................................................................................. 15
10. APPENDIX ............................................................................................................................. 16
Figures ............................................................................................................................... 16 A.
1. Site Vicinity and Topographic Map ................................................................. 17
2. Site Map Showing Boring Locations ............................................................... 18
Tables ................................................................................................................................ 19 B.
1. Analytical Results ............................................................................................ 20
C. Boring Logs ........................................................................................................................... 21
D. Analytical Reports and Chain of Custody Documents ....................................................... 26
Reference 65 Page 5
PHASE II ESA REPORT 1123 West 21st Street Indianapolis, Indiana
Terra Project No. 15‐015
1. INTRODUCTION
Terra Environmental Corporation (Terra) was authorized by Mr. Charles Ingraham to perform
a Phase II ESA at 1123 W. 21st Street, Indianapolis, Indiana. The Phase II was conducted in
conformance with the scope and limitations of ASTM Practice E 1903‐11. The objective of
the Phase II was to evaluate a recognized environmental condition (REC) identified in the
Phase I ESA conducted by Terra for the Subject Property. The REC includes:
• An adjacent property (former Carrier‐Bryant) which was found in several Federal and
State databases and a chlorinated solvent plume in the subsurface directly up‐gradient of
the Subject Property. The data reviewed during the Phase I ESA indicated that the
former Carrier‐Bryant property may have impacted the groundwater on the Subject
Property.
The Phase II investigation was designed to evaluate the potential for impacts based on site
observations and Phase I research.
2. BACKGROUND
Site Description and Features A.
The site is identified as 1123 W. 21st Street, Indianapolis, Indiana The property is located on
the south side of West 21st Street at the northeast corner of the intersection of West 21st
Street and Rembrandt Street. 1.44 acres containing one (1) parcel which is identified as State
Parcel number 49‐06‐34‐115‐006.000‐101. The parcel is located in the northeast quarter of
Section 34, Township 16 North and Range 3 East, Center Township, Marion County, Indiana.
Figure 1 (Appendix A) locates the site on the Indianapolis West, Indiana, USGS Quadrangle
Topographic Map.
Reference 65 Page 6
Physical Setting B.
1. Geological Setting
The site is located in the Tipton Till Plain Physiographic Unit of Indiana. Unconsolidated
deposits are approximately 50 to 150 feet thick below the site (Gray, 1983). These
unconsolidated sediments are mapped at the surface as alluvium of Holocene Age and
undifferentiated outwash of Wisconsinan Age. The bedrock below the site is composed of
dolomite and limestone of the Muscatatuck Group of Devonian Age (Gray et al. 1987).
2. Site Vicinity Map Topographic Setting
According to the USGS topographic map, the site is approximately 712 feet above mean sea
level with a nearly flat topography. Runoff from the site appears to flow to the west and
southwest.
3. Shallow Soil
Information pertaining to soil characteristics in the project area was obtained from the
United States Department of Agriculture (USDA), Soil Conservation Service (SCS) and the
United States Geological Survey (USGS). A copy of the soil report for the site is contained in
Appendix 9.2 to this report. The soil in this area consists of Urban land–Fox complex with 0‐3
percent slopes. These soils consist of about 50 percent Urban land and 35 percent nearly
level, well drained fox soils on bottom land. Runoff is generally rapid on the Urban land and
slow on the Fox soils, and drainage is mostly via sewer systems, gutters and sometimes
surface ditches (USDA SCS, Marion County, Indiana).
4. Aquifer System
The site is located in the White River and Tributaries Outwash Aquifer System. This aquifer
system is mapped adjacent to the White River in the central portion of Marion County, and
the three tributaries entering the county from the northwest and northeast. This system
includes thick glacial outwash sands and gravels that are generally capped by a layer of clay
and silt deposits.
This aquifer system is capable of meeting the needs of both domestic and high‐capacity users
in Marion County. Saturated sand and gravel aquifer materials are commonly 10 to 35 feet
Reference 65 Page 7
thick with well depths ranging from 25 to 277 feet. Domestic well yields are typically up to
50 gpm. There are 37 registered significant groundwater withdrawal facilities (145 wells)
using the White River and Tributaries Outwash Aquifer System. These facilities are used for
energy production, public water supply, industry, irrigation, and miscellaneous. The reported
high‐capacity yields for the wells range from 70 to 3,040 gpm.
The White River and Tributaries Outwash Aquifer System typically is highly susceptible to
surface contamination where sand and gravel deposits are near the surface and have little or
no clay deposits. However, areas having relatively thick clays overlying the sand and gravel
deposits are moderately susceptible to contamination (Schmidt 2011).
Site History and Land Use C.
According to information obtained for the Marion County, Center Township Assessors Office
on February 3, 2015, the current owner of the property is Tranum Insulation Inc. The site is
currently occupied by Midwest Exterior Services and Marion County, Center Township
records classify the site as a commercial warehouse. Previously it was used for container
manufacturing (stone, packing materials, plywood), millwork, peanut and soybean
processing, among other uses.
Adjacent Property Land Use D.
Adjacent properties have been used for residential and a variety of industrial purposes
historically. A railroad right‐of‐way runs north south immediately east of the site. The
adjoining property to the east was utilized as a stone cutting facility in 1915. The property
was converted to a coal yard in the 1930s/40s and to a parking lot in between 1950 and 1956
associated with an industrial facility utilized for the processing of medical waste. The
adjoining property to the south was identified as a vinegar warehouse in 1950 through 1969.
The property is currently owned and operated by Harris Barrier Corp. Adjoining properties to
the west have been used historically for residential and industrial properties, however no
directories, photos or maps going back to 1914 showed any development on the industrial
zoned property. The adjoining property to the north has been utilized for industrial purposes
since at least 1914. The property was occupied by International Machine Tool Co. and
Reference 65 Page 8
Capital Gas Engine Co. in 1914. As of 1924 only International Machine Tool Co. was listed in
the city directories and this continued until 1943. From 1949 through 1990 various
companies have used the site for the manufacturing of appliances including washing
machines and furnaces. After 1990 the site was listed as vacant and currently consists of
vacant land owned by the City of Indianapolis, Department of Metropolitan Development.
Summary of Previous Assessments E.
Terra is not aware of any previous assessments conducted on the Subject Property. Reports
for adjacent properties were reviewed from the IDEM Virtual File Cabinet (VFC).
3. WORK PERFORMED AND RATIONALE
Scope of Work A.
The scope of the work included performance of soil borings on the north property line and
immediately south of the structure on the site to evaluate whether the site was impacted at
all, and if so, whether the building may also be impacted by vapor intrusion (see Figure 2 for
soil boring locations). Direct push soil borings were performed in these areas to collect
groundwater samples for analysis. In total three (3) soil borings were conducted.
Methods B.
The soil borings were performed using direct push sampling technology. Water samples
were obtained from a discrete interval via a 4 foot drop screen. The sample technology used
was a Geoprobe© Screen Point 15 (SP‐15) system. The SP‐15 sampling system procedure is
detailed in a SOP provided by Geoprobe©:
http://files.geoprobe.com/pdfs/sp15_sop_mk3141_1107_0.pdf
The SP‐15 sampling system is used for collecting water samples from the discrete screened
interval while the outer casing eliminates vertical communication. Borings were conducted
to a maximum depth of 32 feet.
Soil borings were blind‐drilled to depth as the contaminant plume identified in the
groundwater was the recognized environmental concern.
Reference 65 Page 9
Soil Samples C.
No soil samples were collected during this investigation.
The drilling equipment was decontaminated by a cold water soap and brush wash, and
double rinse.
Groundwater Samples D.
1. Grab Groundwater Samples from Soil Borings
Groundwater grab samples were collected from the SP‐15 system using a slotted stainless
steel screen which was exposed after retraction of the outer casing. The screen is exposed to
the water bearing formation during outer casing retraction. The outer casing eliminates
vertical communication, protecting and allowing a grab water sample from the discrete
screened interval. The borings are then grouted from the bottom up during removal of the
outer casing. The objective of the procedure is to collect a representative groundwater
sample at depth. Soil borings were conducted to a maximum depth of 32 feet.
2. Sample Identification
Terra has a unique sample identification scheme that includes information concerning the
location of the sample, sample matrix type, date and project identification. The sampling
scheme is as follows: (xxx‐xxdate‐xx#). The first part of the sample ID corresponds to the
location or boring number (e.g., SB1 = soil boring one), the next two letters after the hyphen
correspond to sample type (for example, GW groundwater, SD sediment). The next series of
numbers following sample type correspond to the sample date, than a hyphen and the initial
of the company (T for Terra), followed by the sample depth on the boring log (1A being 0 to
2.5 feet).
All sample custody was documented with the necessary paperwork that included the date
and time of sample collection and the appropriate chain‐of‐custody. The analytical samples
were cooled and maintained at a maximum of 4° Celsius and shipped to an analytical
laboratory.
Reference 65 Page 10
Sample Analysis E.
The groundwater samples were analyzed by Pace Analytical Services Inc. Pace is located at
7726 Moller Road, Indianapolis, IN 46268, phone number 317‐228‐3100. The results
conform to the most current NELAC standards, where applicable, unless otherwise narrated
in the body of the report.
3. Analytical Methods
The groundwater samples were analyzed for VOCs via EPA Method 8260.
4. RESULTS
Stratigraphy A.
The natural site stratigraphy consists predominantly of clay rich unconsolidated sediment
from shallow surface to depths ranging from 4 to 8 feet below surface grade (bsg). Below
the clay material sand and gravel were encountered. The sand and gravel materials were
saturated at approximately 26 feet. The boring logs are attached in Appendix C. The borings
were blind‐drilled to maximum depth of 32 feet bsg.
Soil Analytical Results B.
No soil samples were collected from the site during the current investigation.
Groundwater analytical Results C.
1. Groundwater Flow
The regional flow for the unconsolidated aquifer is to the south. The groundwater on site
was encountered at a depth of approximately 26 feet bsg, the elevation is estimated at
approximately 686 feet. The elevation of the regional White River and Tributaries Outwash
Aquifer System in the area of the site is between 690 and 680 feet, indicating that the
groundwater encountered and sampled in the borings was associated with the
unconsolidated White River and Tributaries Outwash Aquifer System.
2. Grab Groundwater Samples
Grab groundwater samples were collected from three borings SB‐1, SB‐2, and SB‐3. The
groundwater was encountered at a depth of approximately 26 feet bsg. The groundwater
Reference 65 Page 11
was encountered in a well‐defined sand and gravel formation associated with the White
River and Tributaries Outwash Aquifer System.
Tetrachloroethylene (PCE) and Trichloroethene (TCE) had exceedances in the groundwater
when compared to the IDEM RCG (March 2015) tap water screening levels. Neither
compound was found in exceedance of the vapor exposure criteria for industrial property.
Table 1 (Appendix B) details the results of the groundwater sampling. Appendix D contains
the laboratory analytical results and the chain of custody data.
5. EVALUATION OF POTENTIAL EXPOSURE PATHWAYS
Direct Contact A.
Soil impacts were not assessed as a part of the scope of work for this project.
Groundwater Ingestion B.
The groundwater was encountered in a well‐defined sand and gravel formation associated
with the White River and Tributaries Outwash Aquifer System. The groundwater did have
exceedances for PCE and TCE. The groundwater is associated with a drinking water source.
However the site and surrounding areas are currently provided drinking water from the
municipality. The IDNR identifies 4 significant withdrawal wells within approximately ½ mile
of the site. These wells are identified as being owned by Citizens Energy Group and are
reported at depths of 80 to 271 feet. They are used for public water supply. The impacted
groundwater zone may be underlain by a substantial clay that separates the impacted
groundwater from the aquifer resources at greater depth.
The concentrations of PCE and TCE are relatively low but do exceed the tap screening levels
and therefore are a risk to a drinking water resource.
Vapor Intrusion C.
No COCs were encountered in the groundwater which exceeded the screening levels for
vapor exposure for a commercial facility. Therefore vapor intrusion is not an exposure risk.
TCE does exceed the vapor exposure for residential use, however, and therefore the site
would not be eligible for residential use without mitigation.
Reference 65 Page 12
6. CONCLUSIONS
The objective of the Phase II was to evaluate certain recognized environmental conditions
(RECs) based on the Phase I conducted by Terra Environmental Corporation. The results are
detailed below.
Recognized Environmental Conditions A.
1. An adjacent property (former Carrier‐Bryant) was found in several Federal and State databases and a chlorinated solvent plume in the subsurface directly up‐gradient of the Subject Property. The data reviewed during the Phase I ESA indicated that the former Carrier‐Bryant property may have impacted the groundwater on the Subject Property.
The results of the groundwater analytical indicate that the groundwater exceeds the tap
water concentrations for PCE and TCE. These exceedances appear to be directly related to
the groundwater contamination located on the former Carrier‐Bryant site which is
immediately adjacent and up‐gradient of the Subject Property.
Adequacy of Investigations B.
The REC as identified in the Phase I was evaluated through the collection and analysis of
groundwater analytical data. This data was compared to the IDEM Remediation Closure
Guidelines March 2015 Screening Levels to identify specific contaminants that may require
remediation.
Exceedances for certain chlorinated compounds were encountered in the groundwater grab
samples taken from soil borings. The levels encountered on the site appear to be directly
related to the contamination located on the former Carrier‐Bryant site which is immediately
adjacent and up‐gradient of the Subject Property.
Limitations of this Assessment C.
This work plan was not designed to delineate the extent of impacts to the Subject Property.
This assessment was limited in scope in order to identify whether the groundwater at the
site had been impacted.
Reference 65 Page 13
Conclusion D.
Exceedances for certain chlorinated compounds, specifically tetrachloroethylene and
trichloroethylene were encountered in the groundwater. These chlorinated compounds
were encountered up‐gradient of the site in the groundwater at higher concentrations that
those encountered on the site. Therefore it seems conclusive that the impacts to the
groundwater are from an up‐gradient source flowing onto the property. The distribution and
concentrations of the chemicals of concern (COCs) indicate an off‐site source.
7. RECOMMENDATIONS
Terra recommends pursuit of a Bona Fide Prospective Purchaser (BFPP) comfort letter from
the IDEM Brownfields that would provide for the Contaminated Aquifer and Comfort Letter
Policies.
8. SUPPORTING DOCUMENTATION
Fetter, C. W. 1988. Applied Hydrogeology, Second Edition, Merrill Publishing Company, Columbus, OH, p. 592.
Gray, H. H., 1983. Map of Indiana showing thickness of unconsolidated deposits: Indiana Department of Natural Resources, Geological Survey Miscellaneous Map 37, scale 1:500,000.
Gray, H. H., Ault, C. H., and Keller, S. J., 1987, Bedrock geologic map of Indiana: Indiana Department of Natural Resources, Geological Survey Miscellaneous Map 49, scale 1:500000.
Gray, H. H., 1989. Quaternary geologic map of Indiana: Indiana Department of Natural Resources, Geological Survey Miscellaneous Map 49, scale 1:500,000.
Lewis, Richard, J., Sr. Hazardous Chemicals Desk Reference. Third Edition, Van Nostrand Reinhold, New York, NY 1993. p. 639.
Schneider, A. F., 1966, Physiography, in Lindsey, A. A., Ed, Natural features of Indiana: Indianapolis, Indiana Academy of Science, p. 40‐56.
Schmidt, Robert, K., 2011, Unconsolidated Aquifer Systems of Marion County, Indiana, IDNR, Division of Water, Resource Assessment Section.
Schmidt, Robert, K., 2011, Bedrock Aquifer Systems of Marion County, Indiana, IDNR, Division of Water, Resource Assessment Section.
Sittig, Marshal, Handbook of Toxic and Hazardous Chemicals and Carcinogens. Third Edition, V. 2, Noyles Publications, New Jersey, NY 1991, p 850‐852.
Reference 65 Page 14
U. S. Air Force. 1989. The Installation Restoration Toxicology Guide, Vols. 1‐5. Wright‐Patterson Air Force Base, OH.
9. QUALIFICATIONS
Our professional services have been performed, our findings obtained and our
recommendations prepared in accordance with customary principles and practices in the
fields of environmental science and geology. This warranty is in lieu of all other warranties
either expressed or implied. This corporation is not responsible for the independent
conclusions, opinions or recommendations made by others based on the field exploration
and information research presented in this report. In addition, this report is intended for the
sole use of Charles Ingraham and Midwest Exterior Services. Any use or re‐use of this
document or the findings, conclusions, or recommendations presented herein are at the sole
risk of said user.
Groundwater conditions were field investigated on a limited basis as part of this study and
other areas may differ from the conditions implied by the observations. Additionally, the
passage of time may result in a change in the environmental characteristics at this site and
surrounding properties.
It must be noted that no investigation can absolutely rule out the existence of any hazardous
materials at the given site. This Phase II ESA has been based upon prior site history,
observable conditions and activities and limited subsurface investigation and analytical
testing. Hazardous materials and contaminants can escape detection using these methods.
The results of this study suggest that the site has been environmentally impacted. If a higher
level of confidence is required than that expressed in this report, additional investigation
would, of course, be required. It is Terra’s professional opinion that this study was
appropriate for a Phase II ESA and that additional services are needed with regard to the
Subject Property.
Reference 65 Page 15
10. APPENDIX
Figures A.
1. Site Vicinity and Topographic Map
2. Site Map Showing Boring Locations
Reference 65 Page 16
Site Vicinity/Topographic Map1123 West 21st StreetIndianapolis, IndianaN
Job No. Figure 115-015
Site
Reference 65 Page 17
TCE = 11.1
TCE = 13.4
TCE = 18.2PCE = 10.2
PCE = 16.6
PCE = 12.4
Site Map Showing Boring Locations
Figure 2
1123 W. 21st Street, Indianapolis, IN
Scale: 1 inch = 50 ft
Fence
Property Line
Retention Area
Soil Pile
SiteBuilding
Monitoring Well Monitoring Well
Railroad
Rem
brandt St
West 21st St
SB-1
SB-2
SB-3
Legend
Soil Boring
Monitoring Well
Storm Sewer
Water Meter
Sewer
Water
Electric
Fence
Property Line
Railroad
Tetrachloroethylene
Trichloroethylene
PCE
TCE
Reference 65 Page 18
Tables B.
1. Analytical Results
Reference 65 Page 19
1,1
,1-T
rich
loro
eth
an
e
Ca
rbo
n t
etr
ach
lori
de
Te
tra
chlo
roe
the
ne
Tri
chlo
roe
the
ne
cis-
1,2
-Dic
hlo
roe
the
ne
Vin
yl c
hlo
rid
e
Be
nze
ne
Eth
ylb
en
zen
e
To
lue
ne
Xyl
en
e (
To
tal)
Na
ph
tha
len
e
SB1-GW040915-T 04/09/2015 11:05 ug/L ND ND 10.2 11.1 ND ND ND ND ND ND ND
SB2-GW040915-T 04/09/2015 11:55 ug/L ND ND 16.6 13.4 ND ND ND ND ND ND ND
SB3-GW040915-T 04/09/2015 12:50 ug/L ND ND 12.4 18.2 ND ND ND ND ND ND ND
TRIP 04/09/2015 08:00 ug/L ND ND ND ND ND ND ND ND ND ND ND
ug/L 200 5 5 5 70 2 5 700 1000 10000 1.7
ug/L 54000 28 470 38 - 35 120 - - - 460
IDEM RCG March 2015 Screening Levels
Table 1: Analytical Results
Groundwater Analytical Results
VOCs
Terra Project No. 15-0151123 W. 21st St., Indianapolis, Indiana
IDEM RCG Tap
Vapor Exposure Groundwater Concentration (Industrial/Commercial)
EPA 8260
Sa
mp
le I
D
Sa
mp
le T
ime
Un
its
Reference 65 Page 20
C. Boring Logs
Reference 65 Page 21
GW Well graded gravel or gravel sand mixtures little or no fines J‐plug
GP Poorly graded gravel or gravel sand mixtures, little or no fines
GM Sandy gravel gravel‐sand‐silt‐mixtures End Cap
GC Clayey gravel, gravel‐sand‐silt mixture
Cement
SW Well graded sand and/or gravelly sand, little fines
SP Poorly graded sand or gravelly sand, little fines Bentonite Seal
SM Silty sands, sand‐silt mixture
SC Inorganic silt and very fine sand slight plasticity Sand Pack
ML Inorganic silt silty or clayey fine sand, l‐plasticity Riser
CL Inorganic clay, gravelly‐sandy clay, m‐l plasticity
OL Organic silt and silty clay with low plasticity
MH Inorganic silt, micaceous or diatomaceous
CH Inorganic silt with high plasticity Flush Mount Cover
OH Organic clay and silt with high plasticity
Above Ground Cover
PT Peat
DS Discrete Soil Sample
ASPHALT Asphalt DT Dual Tube
CONCRETE Concrete MC Macro‐core
FILL Aggregate Engineering Material
Screen
Unified Soil Classification System
TERRA ENVIRONMENTAL CORPORATION
KEY TO BORING LOGS AND MONITORING WELL INSTALLATIONS
Monitoring Well Construction
Reference 65 Page 22
15‐0151123 W. 21st St., Indianapolis, IN
04/09/15 Ground Surface: Dip 90
Boring Method
Dep
th in feet
Unified SCS
Description
Strata Plot
Dep
th BSG
Munsell Color
Water
I D TYPE
Recovery
PID
Soil Analytical
Sample Dep
th
Casing
SP‐15
Casing
SB‐1
0 SURFACE GRADE 0
0.5 FL Aggregate Engineering Material 1 Gravel/stone 1.01 FL Blind Drilled to 30'2 1.25" tooling with expendable point23 3.0 Black
CL Inorganic clay, gravelly‐sandy clay, m‐l plasticity4 Silty to 4' then smooth clay
5 5.56 6.57 7.58 8.08.5 ML Inorganic silt silty or clayey fine sand, l‐plasticity9 Soft moist9.510 Dense, trace gravel 10.011 GM Sandy gravel gravel‐sand‐silt‐mixtures11 Wet 10.75
12 ML Inorganic silt silty or clayey fine sand, l‐plasticity12 Very dense, dry, trace gravel1313 1414 1515 16 16 1717 17.018 SW Well graded sand and/or gravelly sand, little fines Black18 Gravelly Red1919 2020 2121 21.022 ML Inorganic silt silty or clayey fine sand, l‐plasticity22 Dry crumbly2323 24 23.75
24 SM Silty sands, sand‐silt mixture25 Saturated25 25.026 ML Inorganic silt silty or clayey fine sand, l‐plasticity26 26'
2727 2828 No water. Offset and blind‐drilled to 30' SB1‐GW040915‐T
29 11:05
29 3030 30.0 30'
Total Depth: 30 feet Jeff Stone LT Environmental DrillingDrawn: JCS Terra Environmental Corporation
5B 1.5
6A
MC 100%
0.0
6B 0.0
4B 2.9
Brown
5A
MC 65%
6.1
Dark brown
3B 0.9
4A
DT 3.25"
100%
1.6
2B 0.0
3ADT 3.25"
100%
0.0
1B 0.0
Brown
2A
DT 3.25"
100%
0.0
Depth Scale SOIL PROFILE SAMPLES
GEO
PROBE
rk bro 1A
DT 3.25"
80%
0.0
TERRA ENVIRONMENTAL CORPORATION BORING LOGProject
SB‐1Groundwater Sampling
LocationBoring Date
Reference 65 Page 23
15‐0151123 W. 21st St., Indianapolis, IN
04/09/15 Ground Surface: Dip 90
Boring Method
Dep
th in feet
Unified SCS
Description
Strata Plot
Dep
th BSG
Munsell Color
Water
I D TYPE
Recovery
PID
Soil Analytical
Sample Dep
th
Casing
SP‐15
Casing
SB‐2
0 SURFACE GRADE 0
0.5 OL Organic silt and silty clay with low plasticity 1 Topsoil/grass 1.01 FL Blind Drilled to 32'2 1.25" tooling with expendable point23 3.0 Black
CL Inorganic clay, gravelly‐sandy clay, m‐l plasticity4 Silty to 4' then smooth clay
5 5.56 6.57 7.58 8.08.5 ML Inorganic silt silty or clayey fine sand, l‐plasticity9 Soft moist9.510 Dense, trace gravel 10.011 GM Sandy gravel gravel‐sand‐silt‐mixtures11 Wet 10.75
12 ML Inorganic silt silty or clayey fine sand, l‐plasticity12 Very dense, dry, trace gravel1313 1414 1515 16 16 1717 17.018 SW Well graded sand and/or gravelly sand, little fines Black18 Gravelly Red1919 2020 2121 21.022 ML Inorganic silt silty or clayey fine sand, l‐plasticity22 Dry crumbly2323 24 23.75
24 SM Silty sands, sand‐silt mixture25 Saturated25 25.026 ML Inorganic silt silty or clayey fine sand, l‐plasticity26 2727 2828 No water. Offset and blind‐drilled to 30' 28'
2929 3030
SB2‐GW040915‐T
31 11:55
32 32.0 32'
Total Depth: 32 feet Justin Miller LT Environmental DrillingDrawn: JCS Terra Environmental Corporation
0.0
6B 0.0
5B 1.5
Brown
5A
MC 65%
6.1
Dark brown 6A
MC 100%
4A
DT 3.25"
100%
1.6
4B 2.9
2B 0.0
3ADT 3.25"
100%
0.0
Brown
2A
DT 3.25"
100%
0.0
3B 0.9
Depth Scale SOIL PROFILE SAMPLES
rk bro 1A
DT 3.25"
80%
0.0
TERRA ENVIRONMENTAL CORPORATION BORING LOGProject
SB‐2Groundwater Sampling
LocationBoring Date
GEO
PROBE
7A
1B 0.0
Reference 65 Page 24
15‐0151123 W. 21st St., Indianapolis, IN
04/09/15 Ground Surface: Dip 90
Boring Method
Dep
th in feet
Unified SCS
Description
Strata Plot
Dep
th BSG
Munsell Color
Water
I D TYPE
Recovery
PID
Soil Analytical
Sample Dep
th
Casing
SP‐15
Casing
SB‐3
0 SURFACE GRADE 0
0.5 OL Organic silt and silty clay with low plasticity 1 Topsoil/grass 1.01 FL Blind Drilled to 32'2 1.25" tooling with expendable point23 3.0 Black
CL Inorganic clay, gravelly‐sandy clay, m‐l plasticity4 Silty to 4' then smooth clay
5 5.56 6.57 7.58 8.08.5 ML Inorganic silt silty or clayey fine sand, l‐plasticity9 Soft moist9.510 Dense, trace gravel 10.011 GM Sandy gravel gravel‐sand‐silt‐mixtures11 Wet 10.75
12 ML Inorganic silt silty or clayey fine sand, l‐plasticity12 Very dense, dry, trace gravel1313 1414 1515 16 16 1717 17.018 SW Well graded sand and/or gravelly sand, little fines Black18 Gravelly Red1919 2020 2121 21.022 ML Inorganic silt silty or clayey fine sand, l‐plasticity22 Dry crumbly2323 24 23.75
24 SM Silty sands, sand‐silt mixture25 Saturated25 25.026 ML Inorganic silt silty or clayey fine sand, l‐plasticity26 2727 2828 No water. Offset and blind‐drilled to 30' 28'
2929 3030
SB3‐GW040915‐T
31 12:50
32 32.0 32'
Total Depth: 32 feet Justin Miller LT Environmental DrillingDrawn: JCS Terra Environmental Corporation
6B 0.0
7A
5B 1.5
Dark brown 6A
MC 100%
0.0
4B 2.9
Brown
5A
MC 65%
6.1
3B 0.9
4A
DT 3.25"
100%
1.6
2B 0.0
3ADT 3.25"
100%
0.0
1B 0.0
Brown
2A
DT 3.25"
100%
0.0
Depth Scale SOIL PROFILE SAMPLES
GEO
PROBE
rk bro 1A
DT 3.25"
80%
0.0
TERRA ENVIRONMENTAL CORPORATION BORING LOGProject
SB‐3Groundwater Sampling
LocationBoring Date
Reference 65 Page 25
D. Analytical Reports and Chain of Custody Documents
Reference 65 Page 26
#=CL#
April 15, 2015
LIMS USE: FR - RUSTY WHEATLIMS OBJECT ID: 50116403
50116403Project:Pace Project No.:
RE:
Mr. Rusty WheatTerra Environmental20 Seumin StreetBrownsburg, IN 46112
1123 W 21st St 15-015
Dear Mr. Wheat:Enclosed are the analytical results for sample(s) received by the laboratory on April 10, 2015. Theresults relate only to the samples included in this report. Results reported herein conform to themost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unlessotherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Donna [email protected] Manager
Enclosures
cc: Mr. Jason Stephens, Terra EnvironmentalMr. Mike Wirt, Terra Environmental
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 1 of 25
Reference 65 Page 27
#=CP#
CERTIFICATIONS
Pace Project No.:Project:
501164031123 W 21st St 15-015
Indiana Certification IDs7726 Moller Road, Indianapolis, IN 46268Illinois Certification #: 200074Indiana Certification #: C-49-06Kansas Certification #:E-10177/ E-10247Kentucky UST Certification #: 0042Kentucky WW Certification #:98019Louisiana/NELAP Certification #: 04076
Ohio VAP Certification #: CL-0065Oklahoma Certification #: 2014-148Pennsylvania Certification #: 68-05340Texas Certification #: T104704355-15-8West Virginia Certification #: 330Wisconsin Certification #: 999788130USDA Soil Permit #: P330-10-00128
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 2 of 25
Reference 65 Page 28
#=SS#
SAMPLE SUMMARY
Pace Project No.:Project:
501164031123 W 21st St 15-015
Lab ID Sample ID Matrix Date Collected Date Received
50116403001 TRIP Water 04/09/15 08:00 04/10/15 10:50
50116403002 SB1-GW040915-T Water 04/09/15 11:05 04/10/15 10:50
50116403003 SB2-GW040915-T Water 04/09/15 11:55 04/10/15 10:50
50116403004 SB3-GW040915-T Water 04/09/15 12:50 04/10/15 10:50
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 3 of 25
Reference 65 Page 29
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:Project:
501164031123 W 21st St 15-015
Lab ID Sample ID MethodAnalytesReportedAnalysts
50116403001 TRIP EPA 8260 75RSW
50116403002 SB1-GW040915-T EPA 8260 75RSW
50116403003 SB2-GW040915-T EPA 8260 75RSW
50116403004 SB3-GW040915-T EPA 8260 75RSW
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 4 of 25
Reference 65 Page 30
#=HO#
SUMMARY OF DETECTION
Pace Project No.:Project:
501164031123 W 21st St 15-015
Parameters AnalyzedResultLab Sample ID
Report Limit QualifiersUnitsMethodClient Sample ID
50116403002 SB1-GW040915-TTetrachloroethene 10.2 ug/L 04/14/15 18:095.0EPA 8260Trichloroethene 11.1 ug/L 04/14/15 18:095.0EPA 8260
50116403003 SB2-GW040915-TTetrachloroethene 16.6 ug/L 04/14/15 19:175.0EPA 8260Trichloroethene 13.4 ug/L 04/14/15 19:175.0EPA 8260
50116403004 SB3-GW040915-TTetrachloroethene 12.4 ug/L 04/14/15 20:255.0EPA 8260Trichloroethene 18.2 ug/L 04/14/15 20:255.0EPA 8260
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 5 of 25
Reference 65 Page 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
501164031123 W 21st St 15-015
Sample: TRIP Lab ID: 50116403001 Collected: 04/09/15 08:00 Received: 04/10/15 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Indiana
Acetone ND ug/L 04/14/15 17:36 67-64-1100 1Acrolein ND ug/L 04/14/15 17:36 107-02-850.0 1Acrylonitrile ND ug/L 04/14/15 17:36 107-13-1100 1Benzene ND ug/L 04/14/15 17:36 71-43-25.0 1Bromobenzene ND ug/L 04/14/15 17:36 108-86-15.0 1Bromochloromethane ND ug/L 04/14/15 17:36 74-97-55.0 1Bromodichloromethane ND ug/L 04/14/15 17:36 75-27-45.0 1Bromoform ND ug/L 04/14/15 17:36 75-25-25.0 1Bromomethane ND ug/L 04/14/15 17:36 74-83-95.0 12-Butanone (MEK) ND ug/L 04/14/15 17:36 78-93-325.0 1n-Butylbenzene ND ug/L 04/14/15 17:36 104-51-85.0 1sec-Butylbenzene ND ug/L 04/14/15 17:36 135-98-85.0 1tert-Butylbenzene ND ug/L 04/14/15 17:36 98-06-65.0 1Carbon disulfide ND ug/L 04/14/15 17:36 75-15-010.0 1Carbon tetrachloride ND ug/L 04/14/15 17:36 56-23-55.0 1Chlorobenzene ND ug/L 04/14/15 17:36 108-90-75.0 1Chloroethane ND ug/L 04/14/15 17:36 75-00-35.0 1Chloroform ND ug/L 04/14/15 17:36 67-66-35.0 1Chloromethane ND ug/L 04/14/15 17:36 74-87-35.0 12-Chlorotoluene ND ug/L 04/14/15 17:36 95-49-85.0 14-Chlorotoluene ND ug/L 04/14/15 17:36 106-43-45.0 1Dibromochloromethane ND ug/L 04/14/15 17:36 124-48-15.0 11,2-Dibromoethane (EDB) ND ug/L 04/14/15 17:36 106-93-45.0 1Dibromomethane ND ug/L 04/14/15 17:36 74-95-35.0 11,2-Dichlorobenzene ND ug/L 04/14/15 17:36 95-50-15.0 11,3-Dichlorobenzene ND ug/L 04/14/15 17:36 541-73-15.0 11,4-Dichlorobenzene ND ug/L 04/14/15 17:36 106-46-75.0 1trans-1,4-Dichloro-2-butene ND ug/L 04/14/15 17:36 110-57-6100 1Dichlorodifluoromethane ND ug/L 04/14/15 17:36 75-71-85.0 11,1-Dichloroethane ND ug/L 04/14/15 17:36 75-34-35.0 11,2-Dichloroethane ND ug/L 04/14/15 17:36 107-06-25.0 11,1-Dichloroethene ND ug/L 04/14/15 17:36 75-35-45.0 1cis-1,2-Dichloroethene ND ug/L 04/14/15 17:36 156-59-25.0 1trans-1,2-Dichloroethene ND ug/L 04/14/15 17:36 156-60-55.0 11,2-Dichloropropane ND ug/L 04/14/15 17:36 78-87-55.0 11,3-Dichloropropane ND ug/L 04/14/15 17:36 142-28-95.0 12,2-Dichloropropane ND ug/L 04/14/15 17:36 594-20-75.0 11,1-Dichloropropene ND ug/L 04/14/15 17:36 563-58-65.0 1cis-1,3-Dichloropropene ND ug/L 04/14/15 17:36 10061-01-55.0 1trans-1,3-Dichloropropene ND ug/L 04/14/15 17:36 10061-02-65.0 1Ethylbenzene ND ug/L 04/14/15 17:36 100-41-45.0 1Ethyl methacrylate ND ug/L 04/14/15 17:36 97-63-2100 1Hexachloro-1,3-butadiene ND ug/L 04/14/15 17:36 87-68-35.0 1n-Hexane ND ug/L 04/14/15 17:36 110-54-35.0 12-Hexanone ND ug/L 04/14/15 17:36 591-78-625.0 1Iodomethane ND ug/L 04/14/15 17:36 74-88-410.0 1Isopropylbenzene (Cumene) ND ug/L 04/14/15 17:36 98-82-85.0 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 6 of 25
Reference 65 Page 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
501164031123 W 21st St 15-015
Sample: TRIP Lab ID: 50116403001 Collected: 04/09/15 08:00 Received: 04/10/15 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Indiana
p-Isopropyltoluene ND ug/L 04/14/15 17:36 99-87-65.0 1Methylene Chloride ND ug/L 04/14/15 17:36 75-09-25.0 11-Methylnaphthalene ND ug/L 04/14/15 17:36 90-12-0 N25.0 12-Methylnaphthalene ND ug/L 04/14/15 17:36 91-57-610.0 14-Methyl-2-pentanone (MIBK) ND ug/L 04/14/15 17:36 108-10-125.0 1Methyl-tert-butyl ether ND ug/L 04/14/15 17:36 1634-04-44.0 1Naphthalene ND ug/L 04/14/15 17:36 91-20-31.7 1n-Propylbenzene ND ug/L 04/14/15 17:36 103-65-15.0 1Styrene ND ug/L 04/14/15 17:36 100-42-55.0 11,1,1,2-Tetrachloroethane ND ug/L 04/14/15 17:36 630-20-65.0 11,1,2,2-Tetrachloroethane ND ug/L 04/14/15 17:36 79-34-55.0 1Tetrachloroethene ND ug/L 04/14/15 17:36 127-18-45.0 1Toluene ND ug/L 04/14/15 17:36 108-88-35.0 11,2,3-Trichlorobenzene ND ug/L 04/14/15 17:36 87-61-65.0 11,2,4-Trichlorobenzene ND ug/L 04/14/15 17:36 120-82-15.0 11,1,1-Trichloroethane ND ug/L 04/14/15 17:36 71-55-65.0 11,1,2-Trichloroethane ND ug/L 04/14/15 17:36 79-00-55.0 1Trichloroethene ND ug/L 04/14/15 17:36 79-01-65.0 1Trichlorofluoromethane ND ug/L 04/14/15 17:36 75-69-45.0 11,2,3-Trichloropropane ND ug/L 04/14/15 17:36 96-18-45.0 11,2,4-Trimethylbenzene ND ug/L 04/14/15 17:36 95-63-65.0 11,3,5-Trimethylbenzene ND ug/L 04/14/15 17:36 108-67-85.0 1Vinyl acetate ND ug/L 04/14/15 17:36 108-05-450.0 1Vinyl chloride ND ug/L 04/14/15 17:36 75-01-42.0 1Xylene (Total) ND ug/L 04/14/15 17:36 1330-20-710.0 1SurrogatesDibromofluoromethane (S) 109 %. 04/14/15 17:36 1868-53-779-116 14-Bromofluorobenzene (S) 94 %. 04/14/15 17:36 460-00-480-114 1Toluene-d8 (S) 94 %. 04/14/15 17:36 2037-26-581-110 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 7 of 25
Reference 65 Page 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
501164031123 W 21st St 15-015
Sample: SB1-GW040915-T Lab ID: 50116403002 Collected: 04/09/15 11:05 Received: 04/10/15 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Indiana
Acetone ND ug/L 04/14/15 18:09 67-64-1100 1Acrolein ND ug/L 04/14/15 18:09 107-02-850.0 1Acrylonitrile ND ug/L 04/14/15 18:09 107-13-1100 1Benzene ND ug/L 04/14/15 18:09 71-43-25.0 1Bromobenzene ND ug/L 04/14/15 18:09 108-86-15.0 1Bromochloromethane ND ug/L 04/14/15 18:09 74-97-55.0 1Bromodichloromethane ND ug/L 04/14/15 18:09 75-27-45.0 1Bromoform ND ug/L 04/14/15 18:09 75-25-25.0 1Bromomethane ND ug/L 04/14/15 18:09 74-83-95.0 12-Butanone (MEK) ND ug/L 04/14/15 18:09 78-93-325.0 1n-Butylbenzene ND ug/L 04/14/15 18:09 104-51-85.0 1sec-Butylbenzene ND ug/L 04/14/15 18:09 135-98-85.0 1tert-Butylbenzene ND ug/L 04/14/15 18:09 98-06-65.0 1Carbon disulfide ND ug/L 04/14/15 18:09 75-15-010.0 1Carbon tetrachloride ND ug/L 04/14/15 18:09 56-23-55.0 1Chlorobenzene ND ug/L 04/14/15 18:09 108-90-75.0 1Chloroethane ND ug/L 04/14/15 18:09 75-00-35.0 1Chloroform ND ug/L 04/14/15 18:09 67-66-35.0 1Chloromethane ND ug/L 04/14/15 18:09 74-87-35.0 12-Chlorotoluene ND ug/L 04/14/15 18:09 95-49-85.0 14-Chlorotoluene ND ug/L 04/14/15 18:09 106-43-45.0 1Dibromochloromethane ND ug/L 04/14/15 18:09 124-48-15.0 11,2-Dibromoethane (EDB) ND ug/L 04/14/15 18:09 106-93-45.0 1Dibromomethane ND ug/L 04/14/15 18:09 74-95-35.0 11,2-Dichlorobenzene ND ug/L 04/14/15 18:09 95-50-15.0 11,3-Dichlorobenzene ND ug/L 04/14/15 18:09 541-73-15.0 11,4-Dichlorobenzene ND ug/L 04/14/15 18:09 106-46-75.0 1trans-1,4-Dichloro-2-butene ND ug/L 04/14/15 18:09 110-57-6100 1Dichlorodifluoromethane ND ug/L 04/14/15 18:09 75-71-85.0 11,1-Dichloroethane ND ug/L 04/14/15 18:09 75-34-35.0 11,2-Dichloroethane ND ug/L 04/14/15 18:09 107-06-25.0 11,1-Dichloroethene ND ug/L 04/14/15 18:09 75-35-45.0 1cis-1,2-Dichloroethene ND ug/L 04/14/15 18:09 156-59-25.0 1trans-1,2-Dichloroethene ND ug/L 04/14/15 18:09 156-60-55.0 11,2-Dichloropropane ND ug/L 04/14/15 18:09 78-87-55.0 11,3-Dichloropropane ND ug/L 04/14/15 18:09 142-28-95.0 12,2-Dichloropropane ND ug/L 04/14/15 18:09 594-20-75.0 11,1-Dichloropropene ND ug/L 04/14/15 18:09 563-58-65.0 1cis-1,3-Dichloropropene ND ug/L 04/14/15 18:09 10061-01-55.0 1trans-1,3-Dichloropropene ND ug/L 04/14/15 18:09 10061-02-65.0 1Ethylbenzene ND ug/L 04/14/15 18:09 100-41-45.0 1Ethyl methacrylate ND ug/L 04/14/15 18:09 97-63-2100 1Hexachloro-1,3-butadiene ND ug/L 04/14/15 18:09 87-68-35.0 1n-Hexane ND ug/L 04/14/15 18:09 110-54-35.0 12-Hexanone ND ug/L 04/14/15 18:09 591-78-625.0 1Iodomethane ND ug/L 04/14/15 18:09 74-88-410.0 1Isopropylbenzene (Cumene) ND ug/L 04/14/15 18:09 98-82-85.0 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 8 of 25
Reference 65 Page 34
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
501164031123 W 21st St 15-015
Sample: SB1-GW040915-T Lab ID: 50116403002 Collected: 04/09/15 11:05 Received: 04/10/15 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Indiana
p-Isopropyltoluene ND ug/L 04/14/15 18:09 99-87-65.0 1Methylene Chloride ND ug/L 04/14/15 18:09 75-09-25.0 11-Methylnaphthalene ND ug/L 04/14/15 18:09 90-12-0 N25.0 12-Methylnaphthalene ND ug/L 04/14/15 18:09 91-57-610.0 14-Methyl-2-pentanone (MIBK) ND ug/L 04/14/15 18:09 108-10-125.0 1Methyl-tert-butyl ether ND ug/L 04/14/15 18:09 1634-04-44.0 1Naphthalene ND ug/L 04/14/15 18:09 91-20-31.7 1n-Propylbenzene ND ug/L 04/14/15 18:09 103-65-15.0 1Styrene ND ug/L 04/14/15 18:09 100-42-55.0 11,1,1,2-Tetrachloroethane ND ug/L 04/14/15 18:09 630-20-65.0 11,1,2,2-Tetrachloroethane ND ug/L 04/14/15 18:09 79-34-55.0 1Tetrachloroethene 10.2 ug/L 04/14/15 18:09 127-18-45.0 1Toluene ND ug/L 04/14/15 18:09 108-88-35.0 11,2,3-Trichlorobenzene ND ug/L 04/14/15 18:09 87-61-65.0 11,2,4-Trichlorobenzene ND ug/L 04/14/15 18:09 120-82-15.0 11,1,1-Trichloroethane ND ug/L 04/14/15 18:09 71-55-65.0 11,1,2-Trichloroethane ND ug/L 04/14/15 18:09 79-00-55.0 1Trichloroethene 11.1 ug/L 04/14/15 18:09 79-01-65.0 1Trichlorofluoromethane ND ug/L 04/14/15 18:09 75-69-45.0 11,2,3-Trichloropropane ND ug/L 04/14/15 18:09 96-18-45.0 11,2,4-Trimethylbenzene ND ug/L 04/14/15 18:09 95-63-65.0 11,3,5-Trimethylbenzene ND ug/L 04/14/15 18:09 108-67-85.0 1Vinyl acetate ND ug/L 04/14/15 18:09 108-05-450.0 1Vinyl chloride ND ug/L 04/14/15 18:09 75-01-42.0 1Xylene (Total) ND ug/L 04/14/15 18:09 1330-20-710.0 1SurrogatesDibromofluoromethane (S) 107 %. 04/14/15 18:09 1868-53-779-116 14-Bromofluorobenzene (S) 99 %. 04/14/15 18:09 460-00-480-114 1Toluene-d8 (S) 97 %. 04/14/15 18:09 2037-26-581-110 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 9 of 25
Reference 65 Page 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
501164031123 W 21st St 15-015
Sample: SB2-GW040915-T Lab ID: 50116403003 Collected: 04/09/15 11:55 Received: 04/10/15 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Indiana
Acetone ND ug/L 04/14/15 19:17 67-64-1100 1Acrolein ND ug/L 04/14/15 19:17 107-02-850.0 1Acrylonitrile ND ug/L 04/14/15 19:17 107-13-1100 1Benzene ND ug/L 04/14/15 19:17 71-43-25.0 1Bromobenzene ND ug/L 04/14/15 19:17 108-86-15.0 1Bromochloromethane ND ug/L 04/14/15 19:17 74-97-55.0 1Bromodichloromethane ND ug/L 04/14/15 19:17 75-27-45.0 1Bromoform ND ug/L 04/14/15 19:17 75-25-25.0 1Bromomethane ND ug/L 04/14/15 19:17 74-83-95.0 12-Butanone (MEK) ND ug/L 04/14/15 19:17 78-93-325.0 1n-Butylbenzene ND ug/L 04/14/15 19:17 104-51-85.0 1sec-Butylbenzene ND ug/L 04/14/15 19:17 135-98-85.0 1tert-Butylbenzene ND ug/L 04/14/15 19:17 98-06-65.0 1Carbon disulfide ND ug/L 04/14/15 19:17 75-15-010.0 1Carbon tetrachloride ND ug/L 04/14/15 19:17 56-23-55.0 1Chlorobenzene ND ug/L 04/14/15 19:17 108-90-75.0 1Chloroethane ND ug/L 04/14/15 19:17 75-00-35.0 1Chloroform ND ug/L 04/14/15 19:17 67-66-35.0 1Chloromethane ND ug/L 04/14/15 19:17 74-87-35.0 12-Chlorotoluene ND ug/L 04/14/15 19:17 95-49-85.0 14-Chlorotoluene ND ug/L 04/14/15 19:17 106-43-45.0 1Dibromochloromethane ND ug/L 04/14/15 19:17 124-48-15.0 11,2-Dibromoethane (EDB) ND ug/L 04/14/15 19:17 106-93-45.0 1Dibromomethane ND ug/L 04/14/15 19:17 74-95-35.0 11,2-Dichlorobenzene ND ug/L 04/14/15 19:17 95-50-15.0 11,3-Dichlorobenzene ND ug/L 04/14/15 19:17 541-73-15.0 11,4-Dichlorobenzene ND ug/L 04/14/15 19:17 106-46-75.0 1trans-1,4-Dichloro-2-butene ND ug/L 04/14/15 19:17 110-57-6100 1Dichlorodifluoromethane ND ug/L 04/14/15 19:17 75-71-85.0 11,1-Dichloroethane ND ug/L 04/14/15 19:17 75-34-35.0 11,2-Dichloroethane ND ug/L 04/14/15 19:17 107-06-25.0 11,1-Dichloroethene ND ug/L 04/14/15 19:17 75-35-45.0 1cis-1,2-Dichloroethene ND ug/L 04/14/15 19:17 156-59-25.0 1trans-1,2-Dichloroethene ND ug/L 04/14/15 19:17 156-60-55.0 11,2-Dichloropropane ND ug/L 04/14/15 19:17 78-87-55.0 11,3-Dichloropropane ND ug/L 04/14/15 19:17 142-28-95.0 12,2-Dichloropropane ND ug/L 04/14/15 19:17 594-20-75.0 11,1-Dichloropropene ND ug/L 04/14/15 19:17 563-58-65.0 1cis-1,3-Dichloropropene ND ug/L 04/14/15 19:17 10061-01-55.0 1trans-1,3-Dichloropropene ND ug/L 04/14/15 19:17 10061-02-65.0 1Ethylbenzene ND ug/L 04/14/15 19:17 100-41-45.0 1Ethyl methacrylate ND ug/L 04/14/15 19:17 97-63-2100 1Hexachloro-1,3-butadiene ND ug/L 04/14/15 19:17 87-68-35.0 1n-Hexane ND ug/L 04/14/15 19:17 110-54-35.0 12-Hexanone ND ug/L 04/14/15 19:17 591-78-625.0 1Iodomethane ND ug/L 04/14/15 19:17 74-88-410.0 1Isopropylbenzene (Cumene) ND ug/L 04/14/15 19:17 98-82-85.0 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 10 of 25
Reference 65 Page 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
501164031123 W 21st St 15-015
Sample: SB2-GW040915-T Lab ID: 50116403003 Collected: 04/09/15 11:55 Received: 04/10/15 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Indiana
p-Isopropyltoluene ND ug/L 04/14/15 19:17 99-87-65.0 1Methylene Chloride ND ug/L 04/14/15 19:17 75-09-25.0 11-Methylnaphthalene ND ug/L 04/14/15 19:17 90-12-0 N25.0 12-Methylnaphthalene ND ug/L 04/14/15 19:17 91-57-610.0 14-Methyl-2-pentanone (MIBK) ND ug/L 04/14/15 19:17 108-10-125.0 1Methyl-tert-butyl ether ND ug/L 04/14/15 19:17 1634-04-44.0 1Naphthalene ND ug/L 04/14/15 19:17 91-20-31.7 1n-Propylbenzene ND ug/L 04/14/15 19:17 103-65-15.0 1Styrene ND ug/L 04/14/15 19:17 100-42-55.0 11,1,1,2-Tetrachloroethane ND ug/L 04/14/15 19:17 630-20-65.0 11,1,2,2-Tetrachloroethane ND ug/L 04/14/15 19:17 79-34-55.0 1Tetrachloroethene 16.6 ug/L 04/14/15 19:17 127-18-45.0 1Toluene ND ug/L 04/14/15 19:17 108-88-35.0 11,2,3-Trichlorobenzene ND ug/L 04/14/15 19:17 87-61-65.0 11,2,4-Trichlorobenzene ND ug/L 04/14/15 19:17 120-82-15.0 11,1,1-Trichloroethane ND ug/L 04/14/15 19:17 71-55-65.0 11,1,2-Trichloroethane ND ug/L 04/14/15 19:17 79-00-55.0 1Trichloroethene 13.4 ug/L 04/14/15 19:17 79-01-65.0 1Trichlorofluoromethane ND ug/L 04/14/15 19:17 75-69-45.0 11,2,3-Trichloropropane ND ug/L 04/14/15 19:17 96-18-45.0 11,2,4-Trimethylbenzene ND ug/L 04/14/15 19:17 95-63-65.0 11,3,5-Trimethylbenzene ND ug/L 04/14/15 19:17 108-67-85.0 1Vinyl acetate ND ug/L 04/14/15 19:17 108-05-450.0 1Vinyl chloride ND ug/L 04/14/15 19:17 75-01-42.0 1Xylene (Total) ND ug/L 04/14/15 19:17 1330-20-710.0 1SurrogatesDibromofluoromethane (S) 108 %. 04/14/15 19:17 1868-53-779-116 14-Bromofluorobenzene (S) 95 %. 04/14/15 19:17 460-00-480-114 1Toluene-d8 (S) 94 %. 04/14/15 19:17 2037-26-581-110 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 11 of 25
Reference 65 Page 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
501164031123 W 21st St 15-015
Sample: SB3-GW040915-T Lab ID: 50116403004 Collected: 04/09/15 12:50 Received: 04/10/15 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Indiana
Acetone ND ug/L 04/14/15 20:25 67-64-1100 1Acrolein ND ug/L 04/14/15 20:25 107-02-850.0 1Acrylonitrile ND ug/L 04/14/15 20:25 107-13-1100 1Benzene ND ug/L 04/14/15 20:25 71-43-25.0 1Bromobenzene ND ug/L 04/14/15 20:25 108-86-15.0 1Bromochloromethane ND ug/L 04/14/15 20:25 74-97-55.0 1Bromodichloromethane ND ug/L 04/14/15 20:25 75-27-45.0 1Bromoform ND ug/L 04/14/15 20:25 75-25-25.0 1Bromomethane ND ug/L 04/14/15 20:25 74-83-95.0 12-Butanone (MEK) ND ug/L 04/14/15 20:25 78-93-325.0 1n-Butylbenzene ND ug/L 04/14/15 20:25 104-51-85.0 1sec-Butylbenzene ND ug/L 04/14/15 20:25 135-98-85.0 1tert-Butylbenzene ND ug/L 04/14/15 20:25 98-06-65.0 1Carbon disulfide ND ug/L 04/14/15 20:25 75-15-010.0 1Carbon tetrachloride ND ug/L 04/14/15 20:25 56-23-55.0 1Chlorobenzene ND ug/L 04/14/15 20:25 108-90-75.0 1Chloroethane ND ug/L 04/14/15 20:25 75-00-35.0 1Chloroform ND ug/L 04/14/15 20:25 67-66-35.0 1Chloromethane ND ug/L 04/14/15 20:25 74-87-35.0 12-Chlorotoluene ND ug/L 04/14/15 20:25 95-49-85.0 14-Chlorotoluene ND ug/L 04/14/15 20:25 106-43-45.0 1Dibromochloromethane ND ug/L 04/14/15 20:25 124-48-15.0 11,2-Dibromoethane (EDB) ND ug/L 04/14/15 20:25 106-93-45.0 1Dibromomethane ND ug/L 04/14/15 20:25 74-95-35.0 11,2-Dichlorobenzene ND ug/L 04/14/15 20:25 95-50-15.0 11,3-Dichlorobenzene ND ug/L 04/14/15 20:25 541-73-15.0 11,4-Dichlorobenzene ND ug/L 04/14/15 20:25 106-46-75.0 1trans-1,4-Dichloro-2-butene ND ug/L 04/14/15 20:25 110-57-6100 1Dichlorodifluoromethane ND ug/L 04/14/15 20:25 75-71-85.0 11,1-Dichloroethane ND ug/L 04/14/15 20:25 75-34-35.0 11,2-Dichloroethane ND ug/L 04/14/15 20:25 107-06-25.0 11,1-Dichloroethene ND ug/L 04/14/15 20:25 75-35-45.0 1cis-1,2-Dichloroethene ND ug/L 04/14/15 20:25 156-59-25.0 1trans-1,2-Dichloroethene ND ug/L 04/14/15 20:25 156-60-55.0 11,2-Dichloropropane ND ug/L 04/14/15 20:25 78-87-55.0 11,3-Dichloropropane ND ug/L 04/14/15 20:25 142-28-95.0 12,2-Dichloropropane ND ug/L 04/14/15 20:25 594-20-75.0 11,1-Dichloropropene ND ug/L 04/14/15 20:25 563-58-65.0 1cis-1,3-Dichloropropene ND ug/L 04/14/15 20:25 10061-01-55.0 1trans-1,3-Dichloropropene ND ug/L 04/14/15 20:25 10061-02-65.0 1Ethylbenzene ND ug/L 04/14/15 20:25 100-41-45.0 1Ethyl methacrylate ND ug/L 04/14/15 20:25 97-63-2100 1Hexachloro-1,3-butadiene ND ug/L 04/14/15 20:25 87-68-35.0 1n-Hexane ND ug/L 04/14/15 20:25 110-54-35.0 12-Hexanone ND ug/L 04/14/15 20:25 591-78-625.0 1Iodomethane ND ug/L 04/14/15 20:25 74-88-410.0 1Isopropylbenzene (Cumene) ND ug/L 04/14/15 20:25 98-82-85.0 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 12 of 25
Reference 65 Page 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
501164031123 W 21st St 15-015
Sample: SB3-GW040915-T Lab ID: 50116403004 Collected: 04/09/15 12:50 Received: 04/10/15 10:50 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 82608260 MSV Indiana
p-Isopropyltoluene ND ug/L 04/14/15 20:25 99-87-65.0 1Methylene Chloride ND ug/L 04/14/15 20:25 75-09-25.0 11-Methylnaphthalene ND ug/L 04/14/15 20:25 90-12-0 N25.0 12-Methylnaphthalene ND ug/L 04/14/15 20:25 91-57-610.0 14-Methyl-2-pentanone (MIBK) ND ug/L 04/14/15 20:25 108-10-125.0 1Methyl-tert-butyl ether ND ug/L 04/14/15 20:25 1634-04-44.0 1Naphthalene ND ug/L 04/14/15 20:25 91-20-31.7 1n-Propylbenzene ND ug/L 04/14/15 20:25 103-65-15.0 1Styrene ND ug/L 04/14/15 20:25 100-42-55.0 11,1,1,2-Tetrachloroethane ND ug/L 04/14/15 20:25 630-20-65.0 11,1,2,2-Tetrachloroethane ND ug/L 04/14/15 20:25 79-34-55.0 1Tetrachloroethene 12.4 ug/L 04/14/15 20:25 127-18-45.0 1Toluene ND ug/L 04/14/15 20:25 108-88-35.0 11,2,3-Trichlorobenzene ND ug/L 04/14/15 20:25 87-61-65.0 11,2,4-Trichlorobenzene ND ug/L 04/14/15 20:25 120-82-15.0 11,1,1-Trichloroethane ND ug/L 04/14/15 20:25 71-55-65.0 11,1,2-Trichloroethane ND ug/L 04/14/15 20:25 79-00-55.0 1Trichloroethene 18.2 ug/L 04/14/15 20:25 79-01-65.0 1Trichlorofluoromethane ND ug/L 04/14/15 20:25 75-69-45.0 11,2,3-Trichloropropane ND ug/L 04/14/15 20:25 96-18-45.0 11,2,4-Trimethylbenzene ND ug/L 04/14/15 20:25 95-63-65.0 11,3,5-Trimethylbenzene ND ug/L 04/14/15 20:25 108-67-85.0 1Vinyl acetate ND ug/L 04/14/15 20:25 108-05-450.0 1Vinyl chloride ND ug/L 04/14/15 20:25 75-01-42.0 1Xylene (Total) ND ug/L 04/14/15 20:25 1330-20-710.0 1SurrogatesDibromofluoromethane (S) 108 %. 04/14/15 20:25 1868-53-779-116 14-Bromofluorobenzene (S) 100 %. 04/14/15 20:25 460-00-480-114 1Toluene-d8 (S) 96 %. 04/14/15 20:25 2037-26-581-110 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 13 of 25
Reference 65 Page 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
501164031123 W 21st St 15-015
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:QC Batch Method:
Analysis Method:Analysis Description:
MSV/75600EPA 8260
EPA 82608260 MSV
Associated Lab Samples: 50116403001, 50116403002, 50116403003, 50116403004
Parameter UnitsBlankResult
ReportingLimit Qualifiers
METHOD BLANK: 1275064Associated Lab Samples: 50116403001, 50116403002, 50116403003, 50116403004
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 5.0 04/14/15 15:531,1,1-Trichloroethane ug/L ND 5.0 04/14/15 15:531,1,2,2-Tetrachloroethane ug/L ND 5.0 04/14/15 15:531,1,2-Trichloroethane ug/L ND 5.0 04/14/15 15:531,1-Dichloroethane ug/L ND 5.0 04/14/15 15:531,1-Dichloroethene ug/L ND 5.0 04/14/15 15:531,1-Dichloropropene ug/L ND 5.0 04/14/15 15:531,2,3-Trichlorobenzene ug/L ND 5.0 04/14/15 15:531,2,3-Trichloropropane ug/L ND 5.0 04/14/15 15:531,2,4-Trichlorobenzene ug/L ND 5.0 04/14/15 15:531,2,4-Trimethylbenzene ug/L ND 5.0 04/14/15 15:531,2-Dibromoethane (EDB) ug/L ND 5.0 04/14/15 15:531,2-Dichlorobenzene ug/L ND 5.0 04/14/15 15:531,2-Dichloroethane ug/L ND 5.0 04/14/15 15:531,2-Dichloropropane ug/L ND 5.0 04/14/15 15:531,3,5-Trimethylbenzene ug/L ND 5.0 04/14/15 15:531,3-Dichlorobenzene ug/L ND 5.0 04/14/15 15:531,3-Dichloropropane ug/L ND 5.0 04/14/15 15:531,4-Dichlorobenzene ug/L ND 5.0 04/14/15 15:531-Methylnaphthalene ug/L ND 5.0 N204/14/15 15:532,2-Dichloropropane ug/L ND 5.0 04/14/15 15:532-Butanone (MEK) ug/L ND 25.0 04/14/15 15:532-Chlorotoluene ug/L ND 5.0 04/14/15 15:532-Hexanone ug/L ND 25.0 04/14/15 15:532-Methylnaphthalene ug/L ND 10.0 04/14/15 15:534-Chlorotoluene ug/L ND 5.0 04/14/15 15:534-Methyl-2-pentanone (MIBK) ug/L ND 25.0 04/14/15 15:53Acetone ug/L ND 100 04/14/15 15:53Acrolein ug/L ND 50.0 04/14/15 15:53Acrylonitrile ug/L ND 100 04/14/15 15:53Benzene ug/L ND 5.0 04/14/15 15:53Bromobenzene ug/L ND 5.0 04/14/15 15:53Bromochloromethane ug/L ND 5.0 04/14/15 15:53Bromodichloromethane ug/L ND 5.0 04/14/15 15:53Bromoform ug/L ND 5.0 04/14/15 15:53Bromomethane ug/L ND 5.0 04/14/15 15:53Carbon disulfide ug/L ND 10.0 04/14/15 15:53Carbon tetrachloride ug/L ND 5.0 04/14/15 15:53Chlorobenzene ug/L ND 5.0 04/14/15 15:53Chloroethane ug/L ND 5.0 04/14/15 15:53Chloroform ug/L ND 5.0 04/14/15 15:53
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 14 of 25
Reference 65 Page 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
501164031123 W 21st St 15-015
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter UnitsBlankResult
ReportingLimit Qualifiers
METHOD BLANK: 1275064Associated Lab Samples: 50116403001, 50116403002, 50116403003, 50116403004
Matrix: Water
Analyzed
Chloromethane ug/L ND 5.0 04/14/15 15:53cis-1,2-Dichloroethene ug/L ND 5.0 04/14/15 15:53cis-1,3-Dichloropropene ug/L ND 5.0 04/14/15 15:53Dibromochloromethane ug/L ND 5.0 04/14/15 15:53Dibromomethane ug/L ND 5.0 04/14/15 15:53Dichlorodifluoromethane ug/L ND 5.0 04/14/15 15:53Ethyl methacrylate ug/L ND 100 04/14/15 15:53Ethylbenzene ug/L ND 5.0 04/14/15 15:53Hexachloro-1,3-butadiene ug/L ND 5.0 04/14/15 15:53Iodomethane ug/L ND 10.0 04/14/15 15:53Isopropylbenzene (Cumene) ug/L ND 5.0 04/14/15 15:53Methyl-tert-butyl ether ug/L ND 4.0 04/14/15 15:53Methylene Chloride ug/L ND 5.0 04/14/15 15:53n-Butylbenzene ug/L ND 5.0 04/14/15 15:53n-Hexane ug/L ND 5.0 04/14/15 15:53n-Propylbenzene ug/L ND 5.0 04/14/15 15:53Naphthalene ug/L ND 1.7 04/14/15 15:53p-Isopropyltoluene ug/L ND 5.0 04/14/15 15:53sec-Butylbenzene ug/L ND 5.0 04/14/15 15:53Styrene ug/L ND 5.0 04/14/15 15:53tert-Butylbenzene ug/L ND 5.0 04/14/15 15:53Tetrachloroethene ug/L ND 5.0 04/14/15 15:53Toluene ug/L ND 5.0 04/14/15 15:53trans-1,2-Dichloroethene ug/L ND 5.0 04/14/15 15:53trans-1,3-Dichloropropene ug/L ND 5.0 04/14/15 15:53trans-1,4-Dichloro-2-butene ug/L ND 100 04/14/15 15:53Trichloroethene ug/L ND 5.0 04/14/15 15:53Trichlorofluoromethane ug/L ND 5.0 04/14/15 15:53Vinyl acetate ug/L ND 50.0 04/14/15 15:53Vinyl chloride ug/L ND 2.0 04/14/15 15:53Xylene (Total) ug/L ND 10.0 04/14/15 15:534-Bromofluorobenzene (S) %. 98 80-114 04/14/15 15:53Dibromofluoromethane (S) %. 109 79-116 04/14/15 15:53Toluene-d8 (S) %. 97 81-110 04/14/15 15:53
Parameter UnitsLCS
Result% RecLimits Qualifiers% RecConc.
1275065LABORATORY CONTROL SAMPLE:LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.850 106 61-1351,1,1-Trichloroethane ug/L 52.550 105 71-1291,1,2,2-Tetrachloroethane ug/L 47.950 96 66-1261,1,2-Trichloroethane ug/L 46.750 93 77-1301,1-Dichloroethane ug/L 51.950 104 75-1301,1-Dichloroethene ug/L 45.450 91 68-127
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 15 of 25
Reference 65 Page 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
501164031123 W 21st St 15-015
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter UnitsLCS
Result% RecLimits Qualifiers% RecConc.
1275065LABORATORY CONTROL SAMPLE:LCSSpike
1,1-Dichloropropene ug/L 56.550 113 78-1301,2,3-Trichlorobenzene ug/L 52.650 105 70-1301,2,3-Trichloropropane ug/L 49.450 99 58-1421,2,4-Trichlorobenzene ug/L 52.950 106 68-1311,2,4-Trimethylbenzene ug/L 52.350 105 69-1271,2-Dibromoethane (EDB) ug/L 50.850 102 76-1251,2-Dichlorobenzene ug/L 51.250 102 75-1231,2-Dichloroethane ug/L 50.950 102 75-1281,2-Dichloropropane ug/L 51.750 103 74-1211,3,5-Trimethylbenzene ug/L 51.650 103 70-1261,3-Dichlorobenzene ug/L 50.650 101 74-1221,3-Dichloropropane ug/L 50.050 100 74-1231,4-Dichlorobenzene ug/L 48.350 97 76-1201-Methylnaphthalene ug/L 45.3 N250 91 39-1412,2-Dichloropropane ug/L 60.950 122 50-1372-Butanone (MEK) ug/L 249250 100 58-1392-Chlorotoluene ug/L 50.250 100 74-1222-Hexanone ug/L 254250 101 54-1402-Methylnaphthalene ug/L 49.550 99 54-1514-Chlorotoluene ug/L 48.750 97 77-1234-Methyl-2-pentanone (MIBK) ug/L 245250 98 58-138Acetone ug/L 186250 74 49-150Acrolein ug/L 10801000 108 41-200Acrylonitrile ug/L 203200 101 63-137Benzene ug/L 50.550 101 74-122Bromobenzene ug/L 46.350 93 72-127Bromochloromethane ug/L 54.450 109 63-132Bromodichloromethane ug/L 49.850 100 62-136Bromoform ug/L 47.450 95 44-134Bromomethane ug/L 79.450 159 22-181Carbon disulfide ug/L 48.650 97 59-132Carbon tetrachloride ug/L 57.750 115 56-137Chlorobenzene ug/L 49.450 99 78-123Chloroethane ug/L 48.150 96 60-144Chloroform ug/L 48.150 96 78-126Chloromethane ug/L 44.950 90 42-134cis-1,2-Dichloroethene ug/L 54.650 109 75-122cis-1,3-Dichloropropene ug/L 53.350 107 64-126Dibromochloromethane ug/L 48.950 98 58-128Dibromomethane ug/L 50.250 100 73-125Dichlorodifluoromethane ug/L 48.750 97 35-181Ethyl methacrylate ug/L 220200 110 69-133Ethylbenzene ug/L 51.650 103 66-133Hexachloro-1,3-butadiene ug/L 51.050 102 59-145Iodomethane ug/L 119100 119 21-170Isopropylbenzene (Cumene) ug/L 54.250 108 69-124Methyl-tert-butyl ether ug/L 46.550 93 69-122
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 16 of 25
Reference 65 Page 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
501164031123 W 21st St 15-015
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter UnitsLCS
Result% RecLimits Qualifiers% RecConc.
1275065LABORATORY CONTROL SAMPLE:LCSSpike
Methylene Chloride ug/L 50.850 102 68-132n-Butylbenzene ug/L 54.350 109 70-126n-Hexane ug/L 53.250 106 51-125n-Propylbenzene ug/L 52.950 106 71-122Naphthalene ug/L 45.250 90 68-127p-Isopropyltoluene ug/L 52.250 104 72-132sec-Butylbenzene ug/L 54.350 109 70-128Styrene ug/L 51.650 103 74-126tert-Butylbenzene ug/L 44.150 88 51-118Tetrachloroethene ug/L 49.150 98 69-130Toluene ug/L 49.150 98 72-122trans-1,2-Dichloroethene ug/L 50.250 100 72-124trans-1,3-Dichloropropene ug/L 57.350 115 64-121trans-1,4-Dichloro-2-butene ug/L 198200 99 56-133Trichloroethene ug/L 51.250 102 76-126Trichlorofluoromethane ug/L 49.350 99 76-149Vinyl acetate ug/L 231200 115 45-151Vinyl chloride ug/L 49.250 98 59-126Xylene (Total) ug/L 153150 102 70-1244-Bromofluorobenzene (S) %. 103 80-114Dibromofluoromethane (S) %. 105 79-116Toluene-d8 (S) %. 98 81-110
Parameter UnitsMS
Result% RecLimits Qualifiers% RecConc.
1275066MATRIX SPIKE SAMPLE:MSSpike
Result50116403002
1,1,1,2-Tetrachloroethane ug/L 43.850 88 50-132ND1,1,1-Trichloroethane ug/L 47.650 95 60-138ND1,1,2,2-Tetrachloroethane ug/L 38.750 77 55-128ND1,1,2-Trichloroethane ug/L 41.950 84 61-139ND1,1-Dichloroethane ug/L 46.550 93 57-147ND1,1-Dichloroethene ug/L 43.050 86 55-145ND1,1-Dichloropropene ug/L 51.650 103 55-147ND1,2,3-Trichlorobenzene ug/L 41.750 83 31-141ND1,2,3-Trichloropropane ug/L 40.950 82 58-133ND1,2,4-Trichlorobenzene ug/L 41.350 83 25-143ND1,2,4-Trimethylbenzene ug/L 43.050 86 18-149ND1,2-Dibromoethane (EDB) ug/L 43.850 88 63-129ND1,2-Dichlorobenzene ug/L 41.250 82 38-136ND1,2-Dichloroethane ug/L 46.750 93 62-138ND1,2-Dichloropropane ug/L 45.050 90 59-130ND1,3,5-Trimethylbenzene ug/L 42.450 85 20-147ND1,3-Dichlorobenzene ug/L 40.750 81 28-141ND1,3-Dichloropropane ug/L 44.250 88 62-127ND1,4-Dichlorobenzene ug/L 39.350 79 30-139ND
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 17 of 25
Reference 65 Page 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
501164031123 W 21st St 15-015
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter UnitsMS
Result% RecLimits Qualifiers% RecConc.
1275066MATRIX SPIKE SAMPLE:MSSpike
Result50116403002
1-Methylnaphthalene ug/L 39.1 N250 78 23-143ND2,2-Dichloropropane ug/L 48.350 97 37-139ND2-Butanone (MEK) ug/L 219250 87 37-156ND2-Chlorotoluene ug/L 41.450 83 27-142ND2-Hexanone ug/L 224250 90 44-143ND2-Methylnaphthalene ug/L 39.350 79 24-151ND4-Chlorotoluene ug/L 40.350 81 27-144ND4-Methyl-2-pentanone (MIBK) ug/L 215250 86 46-144NDAcetone ug/L 158250 63 39-156NDAcrolein ug/L 9291000 93 33-200NDAcrylonitrile ug/L 170200 85 48-149NDBenzene ug/L 45.750 91 62-129NDBromobenzene ug/L 41.150 82 39-140NDBromochloromethane ug/L 50.050 100 49-142NDBromodichloromethane ug/L 43.850 88 50-142NDBromoform ug/L 38.050 76 36-125NDBromomethane ug/L 74.650 149 13-179NDCarbon disulfide ug/L 44.450 89 45-142NDCarbon tetrachloride ug/L 52.650 105 46-142NDChlorobenzene ug/L 43.750 87 49-136NDChloroethane ug/L 42.050 84 47-160NDChloroform ug/L 44.050 86 54-150NDChloromethane ug/L 39.650 79 30-148NDcis-1,2-Dichloroethene ug/L 46.650 93 60-135NDcis-1,3-Dichloropropene ug/L 46.050 92 52-123NDDibromochloromethane ug/L 41.750 83 48-125NDDibromomethane ug/L 45.150 90 59-134NDDichlorodifluoromethane ug/L 46.750 93 24-197NDEthyl methacrylate ug/L 191200 96 55-139NDEthylbenzene ug/L 46.050 92 28-153NDHexachloro-1,3-butadiene ug/L 41.750 83 10-176NDIodomethane ug/L 99.8100 100 17-157NDIsopropylbenzene (Cumene) ug/L 48.350 97 18-152NDMethyl-tert-butyl ether ug/L 39.450 79 63-130NDMethylene Chloride ug/L 41.550 83 45-156NDn-Butylbenzene ug/L 44.050 88 10-161NDn-Hexane ug/L 47.050 94 33-144NDn-Propylbenzene ug/L 44.250 88 16-150NDNaphthalene ug/L 36.450 73 39-140NDp-Isopropyltoluene ug/L 43.150 86 10-163NDsec-Butylbenzene ug/L 45.850 92 10-160NDStyrene ug/L 44.850 90 36-139NDtert-Butylbenzene ug/L 36.950 74 12-134NDTetrachloroethene ug/L 54.050 88 33-15110.2Toluene ug/L 44.150 88 50-132NDtrans-1,2-Dichloroethene ug/L 45.450 91 40-153NDtrans-1,3-Dichloropropene ug/L 46.650 93 48-122ND
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 18 of 25
Reference 65 Page 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
501164031123 W 21st St 15-015
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter UnitsMS
Result% RecLimits Qualifiers% RecConc.
1275066MATRIX SPIKE SAMPLE:MSSpike
Result50116403002
trans-1,4-Dichloro-2-butene ug/L 172200 86 32-139NDTrichloroethene ug/L 56.150 90 50-14311.1Trichlorofluoromethane ug/L 46.850 94 60-175NDVinyl acetate ug/L 184200 92 17-142NDVinyl chloride ug/L 45.350 91 44-145NDXylene (Total) ug/L 135150 90 29-145ND4-Bromofluorobenzene (S) %. 102 80-114Dibromofluoromethane (S) %. 105 79-116Toluene-d8 (S) %. 100 81-110
Parameter UnitsDup
ResultMaxRPD QualifiersRPDResult
501164030031275067SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 20ND1,1,1-Trichloroethane ug/L ND 20ND1,1,2,2-Tetrachloroethane ug/L ND 20ND1,1,2-Trichloroethane ug/L ND 20ND1,1-Dichloroethane ug/L ND 20ND1,1-Dichloroethene ug/L ND 20ND1,1-Dichloropropene ug/L ND 20ND1,2,3-Trichlorobenzene ug/L ND 20ND1,2,3-Trichloropropane ug/L ND 20ND1,2,4-Trichlorobenzene ug/L ND 20ND1,2,4-Trimethylbenzene ug/L ND 20ND1,2-Dibromoethane (EDB) ug/L ND 20ND1,2-Dichlorobenzene ug/L ND 20ND1,2-Dichloroethane ug/L ND 20ND1,2-Dichloropropane ug/L ND 20ND1,3,5-Trimethylbenzene ug/L ND 20ND1,3-Dichlorobenzene ug/L ND 20ND1,3-Dichloropropane ug/L ND 20ND1,4-Dichlorobenzene ug/L ND 20ND1-Methylnaphthalene ug/L ND N220ND2,2-Dichloropropane ug/L ND 20ND2-Butanone (MEK) ug/L ND 20ND2-Chlorotoluene ug/L ND 20ND2-Hexanone ug/L ND 20ND2-Methylnaphthalene ug/L ND 20ND4-Chlorotoluene ug/L ND 20ND4-Methyl-2-pentanone (MIBK) ug/L ND 20NDAcetone ug/L ND 20NDAcrolein ug/L ND 20NDAcrylonitrile ug/L ND 20NDBenzene ug/L ND 20NDBromobenzene ug/L ND 20ND
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 19 of 25
Reference 65 Page 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
501164031123 W 21st St 15-015
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter UnitsDup
ResultMaxRPD QualifiersRPDResult
501164030031275067SAMPLE DUPLICATE:
Bromochloromethane ug/L ND 20NDBromodichloromethane ug/L ND 20NDBromoform ug/L ND 20NDBromomethane ug/L ND 20NDCarbon disulfide ug/L ND 20NDCarbon tetrachloride ug/L ND 20NDChlorobenzene ug/L ND 20NDChloroethane ug/L ND 20NDChloroform ug/L ND 20NDChloromethane ug/L ND 20NDcis-1,2-Dichloroethene ug/L ND 20NDcis-1,3-Dichloropropene ug/L ND 20NDDibromochloromethane ug/L ND 20NDDibromomethane ug/L ND 20NDDichlorodifluoromethane ug/L ND 20NDEthyl methacrylate ug/L ND 20NDEthylbenzene ug/L ND 20NDHexachloro-1,3-butadiene ug/L ND 20NDIodomethane ug/L ND 20NDIsopropylbenzene (Cumene) ug/L ND 20NDMethyl-tert-butyl ether ug/L ND 20NDMethylene Chloride ug/L ND 20NDn-Butylbenzene ug/L ND 20NDn-Hexane ug/L ND 20NDn-Propylbenzene ug/L ND 20NDNaphthalene ug/L ND 20NDp-Isopropyltoluene ug/L ND 20NDsec-Butylbenzene ug/L ND 20NDStyrene ug/L ND 20NDtert-Butylbenzene ug/L ND 20NDTetrachloroethene ug/L 17.9 7 2016.6Toluene ug/L ND 20NDtrans-1,2-Dichloroethene ug/L ND 20NDtrans-1,3-Dichloropropene ug/L ND 20NDtrans-1,4-Dichloro-2-butene ug/L ND 20NDTrichloroethene ug/L 14.8 10 2013.4Trichlorofluoromethane ug/L ND 20NDVinyl acetate ug/L ND 20NDVinyl chloride ug/L ND 20NDXylene (Total) ug/L ND 20ND4-Bromofluorobenzene (S) %. 99 495Dibromofluoromethane (S) %. 109 1108Toluene-d8 (S) %. 97 494
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 20 of 25
Reference 65 Page 46
#=QL#
QUALIFIERS
Pace Project No.:Project:
501164031123 W 21st St 15-015
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.ND - Not Detected at or above adjusted reporting limit.J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.PQL - Practical Quantitation Limit.RL - Reporting Limit.S - Surrogate1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.SG - Silica Gel - Clean-UpU - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The lab does not hold TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 21 of 25
Reference 65 Page 47
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:Project:
501164031123 W 21st St 15-015
Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch
50116403001 MSV/75600TRIP EPA 826050116403002 MSV/75600SB1-GW040915-T EPA 826050116403003 MSV/75600SB2-GW040915-T EPA 826050116403004 MSV/75600SB3-GW040915-T EPA 8260
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 04/15/2015 02:52 PM
Pace Analytical Services, Inc.7726 Moller Road
Indianapolis, IN 46268(317)228-3100
Pace Analytical Services, Inc.Not NELAP Accredited
4860 Blazer ParkwayDublin, OH 43017
(614)486-5421
Page 22 of 25
Reference 65 Page 48
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Reference 65 Page 49
Page 24 of 25
Reference 65 Page 50
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Reference 65 Page 51