W2014l3 0002%20 %20behchoko%20 %20snp%20field%20manual%20 %20jun%208 15

BEHCHOKǪ ̀ WATER LICENCE

Surveillance Network Program (SNP)

Field Manual Updated June 2015

The purpose of this field manual is to ensure safe and effective sampling for Licence W2014L3-0002

FIELD MANUAL

TABLE OF CONTENTS

Step 1. Safety

Step 2. Preparation

Step 3. Sampling Procedure – Part 1 - 4

Step 4. Sampling Locations & Requirements

Step 5. Sampling & Analysis

Step 6. Storing and Reporting Sampling Data

Additional Attachments:• Sampling Schedule• Sampling Checklist• Bottle / Cooler Order Form Example• Laboratory Order Form Example• Contacts

STEP 1. SAFETYBEFORE SAMPLING, MAKE SURE YOU ARE PREPARED WITH THE FOLLOWING:

VaccinationsIt is recommended that you get the

vaccinations for:

1. Hepatitis A & B2. Tetanus

Hand SanitizerUse hand sanitizer wipes

after each sample

Gloves + Field GearMake sure you wear proper field gear such as boots

Use gloves during sampling and discard afterwards inside cooler

STEP 2. PREPARATIONBEFORE SAMPLING, MAKE SURE THAT YOU PREPARE THE NECESSARY EQUIPMENT AND CONTACTS:

Pick a date! Select a date each month

to collect samples

Bottles and CoolerOrder bottles and a cooler from

Taiga Lab 3 days advance of sampling date

(use bottle order form, see Additional Attachments)

Ice packsCommunity should

have ice packs ready to keep samples

cold (but not frozen)

Taiga LabContact Taiga Lab and let

them know you are planning to send them

samples


Additional Bottles

TSS, Ammonia, Phosphate

Faecal Coliforms

Phenols Mercury & Total Metals

BOD/ CBOD

Oil & Grease pH/Conductivity

STERILE PHENOL

BTEX:(2 vials per sample; NO AIR IN BOTTLES)

TPH: Requires both the oil and grease and BTEX bottles


Label BottlesLabel each bottle with Licence # (Submission No.);

SNP # (Field Sample No.); the sample date and time; and ‘Name of the Community – SNP Program’ (Sample

Description)

STEP 3. SAMPLING PROCEDURE PART 11. Sample at the cleanest location first and as close to flight time as

possible (e.g. late morning if early afternoon flight, etc.)

2. AT EACH SNP LOCATION:

a) Wear gloves

b) Ensure bottles are labeled before collecting samples

c) Collect samples

d) Place used bottles in cooler and keep unused bottles in

separate bag

e) Discard used gloves in cooler

f) Use hand sanitizer wipes

STEP 3. SAMPLING PROCEDURE PART 3

Rinse Bottles 3 times and dump away from sampling area before taking actual sample filled to the top

“Fill and dump” x 3

FOR SAMPLING REQUIREMENTS:

pH/Conductivity

TSS, Ammonia, Phosphate

Mercury & Total Metals

BOD/ CBOD

STEP 3. SAMPLING PROCEDURE PART 4

DO NOT rinse bottle before taking actual sample. Instead, fill bottle to the top and record the time of day the sample was taken

FOR SAMPLING REQUIREMENTS:

Oil & Grease

STERILE

Faecal Coliforms

BTEX:(2 vials per sample; NO AIR IN BOTTLES)

TPH: Requires both the oil and grease and BTEX bottles

Phenols

PHENOL

SAMPLING SUMMARYSampling Parameters Bottles Needed Frequency of Sampling

Cubic metres n/a Daily: E1 & R1

BOD5 , CBOD, Faecal Coliforms, pH, Suspended Solids, Ammonia-Nitrogen, and

Total Phosphate

Monthly (June – October): E2, E3, E4, E5

10+ days prior to decant: R2

Weekly (see details): R3

Weekly (see details): R4

Sodium, Potassium, Magnesium, Sulphate, Total Phenols, Oil and Grease, Conductivity, Calcium, Total Lead, Total Chromium, Total

Nickel, Total Iron, Total Cadmium, Total Copper, Total Mercury, and Total Zinc

Once (June – October): E2, E3, E4, E5, R3, and R4

pH, Total Zinc, Sodium, Suspended Solids, Magnesium, Total Phosphate, Potassium, Sulphate, Total Phenols, Oil and Grease, Conductivity, Calcium, Total Lead, Total Chromium, Total Nickel, Total Iron, Total Cadmium, Total Copper, Total Mercury,

Faecal Coliforms, BTEX, and TPH

Twice per year during the months of June and September: R5, R6, R7, R8, R9, and R10

SNP 2014-E1 - Active

Where:

Raw water intake line at the Water Supply Facilities serving Edzo

Sampling Requirements:

Quantity and FrequencyMeasured & recorded in cubic metres (m3)

1 volume reading daily

STEP 4. SAMPLING LOCATIONS & REQUIREMENTS

SNP 2014-E2 – Active

Where:

In the Sewage Disposal Facilities serving Edzo, immediately prior to flowing towards the overflow ditches



1 sample monthly from June –October

1 sample between June –October

N62 46 16.1 W116 01 35.6

Sampling Requirements:SNP 2014-E3 – Active

Where:

Point of junction at the outflow ditches from the Sewage Disposal Facilities serving Edzo




P

N62 46 16.1 W116 01 30.0

SNP 2014-E4 – Active

Where:

In natural wetland system, immediately prior to entering Great Slave Lake

If unable to sample at this location, please see 2014-E5





P

Sampling Requirements:SNP 2014-E5 – Inactive

Where:

Great Slave Lake downstream from Sewage Disposal Facilities serving Edzo

ONLY SAMPLE HERE IF 2014-E4 IS UNABLE TO BE SAMPLED





P

SNP 2014-R1 - Active

Where:

Raw water intake line at the Water Supply Facilities serving Rae


Quantity and FrequencyMeasured & recorded in cubic metres (m3)

1 volume reading daily



Quantity and Frequency1 sample at least 10 days prior to decant

SNP 2014-R2 – Active

Where:

Sewage Disposal Facilities Serving Rae near decant structure

Send results to an Inspector prior to decant


N62 49 53.9 W116 00 33.9

Sampling Requirements:SNP 2014-R3 – Active

Where:

Point of outflow from the Sewage Disposal Facilities Serving Rae at the culvert crossing the Rae Access road



1. Weekly, beginning two weeks before decant2. every three days during decant flow

3. 1 sample one week after the end of decant flow


P

N62 49 43.9 W116 00 02.9

Sampling Requirements:SNP 2014-R4 – Active

Where:

At the end of Rae Wetland prior to entering Frank’s Channel

*During decant flow, this sample should becollected one day following collection of the sample at 2014-R3, or as determined by the retention time of the wetlands, to ensure that the effluent has reached this location



1. Weekly, beginning two weeks before decant2. every three days during decant flow*

3. 1 sample one week after the end of decant flow


P

N62 49 40.3 W117 13 50.2


Quantity and Frequency2 samples per year during the months of

June and September


Where:

Run-off from old Solid Waste Disposal Facilities (north-west of Landfarm)


P



June and September


Where:

New Solid Waste Disposal Facilities (north of waste footprint)


P



June and September


Where:

New Solid Waste Disposal Facilities (north-east of waste footprint, south-east of SNP station 2014-R6)


P



June and September


Where:

New Solid Waste Disposal Facilities (south of waste footprint, north of waterbody)


P



June and September


Where:

New Solid Waste Disposal Facilities (south of waste footprint, east of waterbody, south-east of SNP station 2014-R8)


P



June and September


Where:

New Solid Waste Disposal Facilities (south of waste footprint, west of waterbody, south-west of SNP station 2014-R9)


P

STEP 5. SAMPLING & ANALYSIS

Send samples to the Taiga Environmental Laboratory in Yellowknife for analysis along with the laboratory order form

Taiga will send you your results back in 14 days

When results come back from Taiga:

Record results and Fill out template for annual reporting (DUE MARCH 31 EACH YEAR), including reporting of all SNP results( ELECTRONIC TEMPLATE PROVIDED IN THE WLWB’s ONLINE REGISTRY AT WWW.WLWB.CA )

STEP 6. STORING AND REPORTING DATA

http://www.wlwb.ca/

Sample bottles (pre-labelled) and cooler

Heavy duty garbage bags (to carry bottles)

Rubber gloves - at least one clean pair per SNP site

(dispose of used gloves into garbage bag with the sample bottles)

Hand sanitizer

Rubber boots

Permanent markers

SAMPLING CHECKLIST

Sample bottles (pre-labelled) and cooler

Heavy duty garbage bags (to carry bottles)

Rubber gloves - at least one clean pair per SNP site

(dispose of used gloves into garbage bag with the sample bottles)

Hand sanitizer

Rubber boots

Permanent markers

SAMPLING CHECKLIST

SNP StationMonthly (between June and October = 5)

Once between June and October10 days before decant

Before decant (Once per week during the 2 weeks before)

Every 3 days during decant flow (R4 is collected one day after R3)

After decant flow is done (R4 is collected one day after R3)

Twice per year between June and September

E2 Green, Black, Sterile, Purple

Red, Brown glass with yellow sticker (for Oil and Grease), and Brown glass with 'Phenol' on it





R2 Green, Black, Sterile, Purple

R3Red, Brown glass with yellow sticker (for Oil and Grease), Green, and Brown glass with 'Phenol' on it

Green, Black, Sterile, Purple

Green, Black, Sterile, Purple Green, Black, Sterile, Purple

R4Red, Brown glass with yellow sticker (for Oil and Grease), Green, and Brown glass with 'Phenol' on it

Green, Black, Sterile, Purple

Green, Black, Sterile, Purple Green, Black, Sterile, Purple

R5Green, Black, Red, Sterile, Brown glass with yellow sticker (for Oil and Grease), Brown glass with 'Phenol' on it , Brown glass (aka 'extractable hydrocarbons on the bottle form' for TPH), BTEX Vial (3)





R10Green, Black, Red, Sterile, Brown glass with yellow sticker (for Oil and Grease),Brown glass with 'Phenol' on it , Brown glass (aka 'extractable hydrocarbons on the bottle form' for TPH), BTEX Vial (3)

Subtotals

minimum

15

15 15 5

54

4 4

15 42

2 2

2

12 12 12 12

1212 36

122

2 2

25

Note: Sampling Schedule does not include daily sampling at SNP Stations 2014-E1 & 2014-R1

SAMPLING SCHEDULE

TAIGA ENVIRONMENTAL LABORATORY Bottle &/or Preservative Order Form

Date Ordered: 201 - Date Required: 201 -Name: Company: Project name or Location

Address :

Phone : Fax·

Pick up: Ship by Air: Pack as TOG: Cooler required:

DYes DYes DYes DYes

ONo ONo DNo ONo

Date Filled. 201 - Filled By:

NOTE: Bottles and preservatives are provided free of charge for analysis earned out at Taiga Bottles, preservatives and laboratory supplies for other use, may be subject to additional charges Unused bottles and preservatl\·C cannot be returned to the laboratory for reuse

Parameter Type No. of No. of No. of QC Batch# Numherof QC Batch#of Field Travel Bottles for of Bottles Preservatives Pres. Sent

Blanks Blanks Samples Sent -

• Routine (Green) Not Required

• Nutrients (Black) NotReqwred

0 Bacti (Sterile sealed) Not Required Not Required NotReqwred

• BOD (Purple) Not'Requ1red NotReqwred Not Required

Total Metals (Red)

0 Dissolved Metals (Red) see no1e I

Arsenic Speciation Bottle Net Required 8 ot Requtred Not Requtred

• Cyanide (Blue)

Thiocyanate (Orange)

0 Hexane Extractable Material (Oil & Grease ) (Brown glass. wide or narrow-mouth)

CD Phenol (Brown glass. narro~-mouth)

Sulphide

• Radionuclide

Chlorophyll A Not Requtred Not Required Not Requtred

Extractable Hydrocarbons (Brown glass) NotReqwred see note 1

BTEX/Purgeable HC see 1w1es 2 and 3 Not Required

THM (Glass vial 40mL) see nole 3 NotReqwred

Metals or Hydrocarbons in sediment Not Required Not Requtred Not Required (500mLjar)

Metals or Hydrocarbons in sediment NotReqwred Not Reqwred Not Required (2SOmLJar)

Metals or Hydrocarbons in sediment Not Required Not Required NotReqwred (12SmLjar) --Metals or Hydrocarbons in sediment 'Not Required Not Required NotReqwred (60mLjar or Whirl Pak Bag)

Other:

Other Field Supplies: (e.g. Type I uv• water)

Notes: I- D1ssofred me/als bot1les will be presenY!d al 1he labora/Dry if !he sample 1s no1jil1ered m lhe field 77ie jillermg and addmon of presenu/lve 1s 520.00 sample. 2· For TPH reques/s, bolh lhe ex/rac/able hydrocarbons (bro11 n glass boll le) and /he BTEX P11rgeable HC (40ml wal) have lo be s11bm111ed. J . For BTEX Purgeable HC and THM, please submil /lt o vials for each sample (m lhe e>•enl air b11bbles occur in /he vials, a back-up sample can be analJ:ed)

Shaded areas are for laboratory use only.

Taiga Enwronmenta/ Labora/Ory Bottle.. Presen·atn•e Orrler Fom1 Reviswn 4 Ejfecm•e Da1e /8-No1•-09

Page __ of __ Fom1 ID: FOR QOOI File ID: 55/A.4./

FOR QOOl -Bo11le_Presen·a1i1•e Order Form

W2014L3-0002 (1 decant)

3636482417

3612

17

17

31

Jess

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TAIGA ENVIRONMENTAL LABORATORY Bottle &/or Preservative Order Form

Date Ordered: 201 - Date Required: 201 -Name: Company: Project name or Location

Address :

Phone : Fax·

Pick up: Ship by Air: Pack as TOG: Cooler required:

DYes DYes DYes DYes

ONo ONo DNo ONo

Date Filled. 201 - Filled By:

NOTE: Bottles and preservatives are provided free of charge for analysis earned out at Taiga Bottles, preservatives and laboratory supplies for other use, may be subject to additional charges Unused bottles and preservatl\·C cannot be returned to the laboratory for reuse

Parameter Type No. of No. of No. of QC Batch# Numherof QC Batch#of Field Travel Bottles for of Bottles Preservatives Pres. Sent

Blanks Blanks Samples Sent -

• Routine (Green) Not Required

• Nutrients (Black) NotReqwred

0 Bacti (Sterile sealed) Not Required Not Required NotReqwred

• BOD (Purple) Not'Requ1red NotReqwred Not Required

Total Metals (Red)

0 Dissolved Metals (Red) see no1e I

Arsenic Speciation Bottle Net Required 8 ot Requtred Not Requtred

• Cyanide (Blue)

Thiocyanate (Orange)

0 Hexane Extractable Material (Oil & Grease ) (Brown glass. wide or narrow-mouth)

CD Phenol (Brown glass. narro~-mouth)

Sulphide

• Radionuclide

Chlorophyll A Not Requtred Not Required Not Requtred

Extractable Hydrocarbons (Brown glass) NotReqwred see note 1

BTEX/Purgeable HC see 1w1es 2 and 3 Not Required

THM (Glass vial 40mL) see nole 3 NotReqwred

Metals or Hydrocarbons in sediment Not Required Not Requtred Not Required (500mLjar)

Metals or Hydrocarbons in sediment NotReqwred Not Reqwred Not Required (2SOmLJar)

Metals or Hydrocarbons in sediment Not Required Not Required NotReqwred (12SmLjar) --Metals or Hydrocarbons in sediment 'Not Required Not Required NotReqwred (60mLjar or Whirl Pak Bag)

Other:

Other Field Supplies: (e.g. Type I uv• water)

Notes: I- D1ssofred me/als bot1les will be presenY!d al 1he labora/Dry if !he sample 1s no1jil1ered m lhe field 77ie jillermg and addmon of presenu/lve 1s 520.00 sample. 2· For TPH reques/s, bolh lhe ex/rac/able hydrocarbons (bro11 n glass boll le) and /he BTEX P11rgeable HC (40ml wal) have lo be s11bm111ed. J . For BTEX Purgeable HC and THM, please submil /lt o vials for each sample (m lhe e>•enl air b11bbles occur in /he vials, a back-up sample can be analJ:ed)

Shaded areas are for laboratory use only.

Taiga Enwronmenta/ Labora/Ory Bottle.. Presen·atn•e Orrler Fom1 Reviswn 4 Ejfecm•e Da1e /8-No1•-09

Page __ of __ Fom1 ID: FOR QOOI File ID: 55/A.4./

FOR QOOl -Bo11le_Presen·a1i1•e Order Form

W2014L3-0002 (2 decants)

4545453317

36

12

17

17

32

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- .-.-. --TAIGA ENVIRONMENTAL LABORATORY

LABORATOIRE ENVIRONNEMENT AL TAIGA 4601 - 52 Avenue, P.O. Box 1500, Yellowknife, NT, XIA 2R3

Tel : (867) 669-2788 • Fax: (867) 669-2718 www.taiga.gc.ca Batch No

Send Results & Invoice to:

FIELD SHEET

(Please notify if results or invoice are to be sent to different locations)

Company/Agency:-------------

Address:

City ff own: ______ Provincefferritory: __ _

Client Project No:--------------

Date collected:---- ----------

Time collected: -------------

Sampler:-----------------

Location: -----------------Postal Code: Rush Required: CIYes CINo

Note: Analysis may he suhc01uroc1ed willwllf prior notice. Fax:--------Phone:--------

E-mail :-----------------

Signature :------------------

See rererse fi>r /row lo complete form and sampling protocols.

Date Received _____ Received By -----

Commen~----------------(Laboratory use only)

Sample Type (fr<shwotcr, sewage, wostc:wotcr, notable. 2T0undwater. salt water. etc)

Client Sample ID (As it should aooear on final rcoortl

Taiga Sample ID (Laboratory use only)

-WATER SAMPLES -

20\4- E:1 ZfJ\4-€3

Boule Typo and Parametor I I PLEASE CHECK PARAMETERS REQUESTED BELOW: _p..!:!, Conductivi!)'., Alkalini!)'. ~ I Cond I Alk lllA"" I Cond I Alk WI" I Cond Alk Individual Anions Suite D Cl Tio, 1

F 1NO,-N ]~ Cl lso, IF INO,-N INO,-N Cl lso, ii IN0 2-N INO,-N

Total Nitrite iliQ,) +Nitrate C.fiQV- NO ~ NO,-N -~~N~(),-,~+...,N~C~)-,_-N~~-i·-'-~N~()-,~+"""N.,..C~) ,...,-N~~-i

Individual Cations Suite D -------· --~--L~)g J Na I K Ca Mg l Na j K Ca ' Mg I Na ~ Hardness (Calculated) 1 lardnc~s I lardness I lardness Reactive Silica ----·-· ------·---·- SfO, S10, StO·

Laboratorv use only Rec'd Y N Rce'd Y N Rce 'd Y N

Chlorine: Total , Residual T Cl I R Cl T. Cl R Cl T. CI I R. CI Chemical Oxygen Demand COD COD COD Color ______ -~flrarc_r_!! J True Apparent j True Apparent j True Turbidity ________ _l~_!!"~dity Turh1dity Turb1d1tv Total Suspended Solids, Dissolved Solids ~ l __ ·r_'D_S __ , ·1 W I TDS ·~ • TDS

~ll::IEA:i-m'-"m""?on"'i:::.a --;;:;-:--;--c;::7"--;---,~,-:;--·I-~ ~ ~---- ~-N

I Phosphorus· Total , Dissolved, Ortl}Q___ ~DP --0-,-, - • ~ I DP ] OP ~T DP J OP Carbon. Total, Dissolved . ____ ,.-_-_-_1_'c_X:_' -~l_l_J<_)_C __ , __ -_r_o_c _ _,.l __ D_O_C __ , __ T_O_C_' _ _,jf---D_O_C_' __ , Nitrogen · Total ,~D~i=ss~o~lv~e~d~----i---·r_N~'-,-,_,,~! -~D_N_' ___ 1 __ -_rN_..,..,.,-,"-',.----D-N ___ 1 ___ 1_.N_.,.,.....,,~---D~N---I Visible Oil and Grease Visible Visible

~~-1~~ ~~~~ Visible ,_

Laboratory use only Received Y N

.!! Fecal Coliforrns (FC)

·5 Total Cohforrns (TC), E. Colt (EC) ·1c l l IS oo Fecal Stre(ltococcus (FS)

Laboratory use only - Received Y N T __ •c

Stcnle contnmcr Y N

Biological Oxygen Demand arbonaceous BOD Laboratorv use only lease indicate if sample is reserved and/or filtered

ICP-MS(I) : Cd, Cr, Cu. Co, Mn, N1. Pb, Zn, Fe __

IMO

Received Y N T

ltll Pres I

lotal

ICP-MS(2): 25 clement scan includes As I otal Dis~oh cd (not included B ,_fu,!lg~--•------- __ _

ndividual Metals by ICP-MS plcnsc cuclc each metal) Ag, Al , As, B, Ba,, Be, 1, Cd, Co, Cr, Cs, Cu, Fe, Hg, L1, Mn, Mo, 1, Pb, Rb Sb, Se, Sn, Sr, T1, Tl, U, V, Zn

lo ta I

Recetved y N Received y N

v \J;k"" ·1c IC re I l·C

IS IS Received Y N T •c Received Y N T •c Sterile cantwncr Y N-- Stenlc contamer Y N--

lu,KJ

Rcec1vcd Y N T •c Received Y N T

Pre~ Pre-; '

lotJI lotJI

lot.ti rota(

·rotal Dt~~olvcd lotal

Laboratorv use only TMrce'd Y N DMrcc'd Y N TM rec'd Y N DMrce'd Y N ITM rce'd Y N JDMrec'd YN

Hexane Extractable Material (O&Gl 11 Hv\ Ill· Iv\ HEM Rec'd Y N Laboratory use onlv Rec'd Y N Pr.. Y N R..:'d Y N Pres Y N Pres Y N

BTEX, Purgeable HC (40mL x 2 vials) BTEX Purg llC B'ITX J Purg llC 13TEX I Purg llC Extractable HC (IL amber g,_las_s_b_o_tt_le~)_, ____ E_xt_l_IC_' ____ ,, ____ E_x_t l_·l_C ____

11 ____ l_:Ox_·t_l-_IC_' ____

1

Trihalomethanes (40 mL x 2 vials) T l IM THM Tl IM Laboratory use only Vial rec'd Y N Ext rec'd Y N Vial rce 'd Y N Ext rce'd Y N Vial rec'd Y N Ext rec 'd Y N

I Other: see special rea11est form For safety purposes, please disclose any contaminants (e g heavy metals, cyamde. etc) that may be present at !ugh levels and pose a risk to human health

Taiga Enwronmental Laboratory Taiga Field Sheet Rews10n 4 Effec//l•e Date 18.Jan-IO

Page __ of __ Form ID: FOR Q005 File /D; 551.4 4 5

FOR Q005 Taiga Field Sheet Rews1011 4

33

(

TAIGA ENVIRONMENTAL LABO RA TORY LABORATOIRE ENVIRONNEMENT AL TAIGA

4601 - 52 Avenue, P.O. Box 1500, Yellowknife, NT, XIA 2R3 Tel : (867) 669-2788 • Fax: (867) 669-2718

FIELD SHEET

www.taiga.gc.ca Batch No

Send Results & Invoice to: (Please notify if results or invoice are to be sent to different locations) Client Project No:--------------

Date collected:--------------

Time collected: ---------------


Address:

Sampler: _________________ _

City ff own: ______ Provincefferritory: __ _ Location:-----------------

Postal Code: Rush Required: CJYes CJNo

Fax: _______ _ Phone:-------

E-mail:-----------------

Signature :------------------

Note: Analysis may he .mhcomrac1ed wilhoul prior notice. See rei-erse for how to complele fimn and sampling prolc>eo/s.

Date Received ______ Received By _ _ __ _

Commen~ ----------------(Lnboratory use only)

Sample Type (fn:shwntcr, sewage, wnstcwotcr, ootilblc. groundwater. salt water. etc)

Client Sample ID (As it should aooear on final reoort)


Color Turbidity Total Suspended Solids, Dissolved Solids

Ammonia Phosphorus· Total, Dissolved, Ortho Carbon Total, Dissolved Nitrogen: Total , Dissolved V1s1ble Oil and Grease Laboratory use only

.!!I Fecal Coliforrns (FC) ·5 Total Coliforrns (TC), E Coli (EC) ii5 Fecal Stre tococcus FS

Laboratory use only

enDemand

-WATER SAMPLES -

2.0\4-&1- '2....0\L{- E:.3 Zo\4-€.lt

..J PLEASE CHECK PARAMETERS REQUESTED BELOW:

T. Cl R Cl COD

Apparenl True Turb1d1ty

TSS I TDS NII,

R Cl

Apparent J Tru~-----·---Turb1d1ty

TSS I TI)S __ _

NH,

Rec'd Y N

T. Cl I R. Cl COD

Apparent J True Turb1d1ty

TSS I TDS Nl!,-N

Tl' [ TOC

DP 1-or- ---n>J DOC TOC

DP I _9E _____ TJ> I DOC TOC

DP

I , OP

DOC TN DN TN DN TN DN

Visible Received Y N

IC -re

IS

Received

IC IC:

Visible y N

IC

l IS

IC

Visible Rcce1v.d Y N

re ll \ I C

IS Received Y N T Stenle contnmer Y N

•c Received Y N T •c Received Y N T __ •c Stenle contamer Y N-- Stenle container Y N

BOD BOD BOD CBOD CBOD lBOD

Received Y N T •c Received y N T •c Received Y N T ·c --

Pres f F tit Pre'> Pres I 1111t Pre~ !'re' 111! !'re<;

Total D1 ~'ol ved TotJI Dl'mihed lotJI D1'sohcd

Total D1ssoh cd ·rot..tl D1~~olved Iota! D1~~ohed

-,~ I --

I~ D1s~oh ed Dl'>'>Ohcd T~ [)1<;soh cd

TM rec'd Y N DM rec'd Y N

I -Rec'd Y N Pres Y N

B n X Purg llC B I I X I Purg llC Brr X Purg llC r ... 1 llC htllC l "t llC lllM lllM lllM

For safety purposes, please disclose any contaminants (e g heavy metals, cyanide, etc) that may be present at high levels and pose a risk to human health

Taiga Enwronmenta/ Laboratory1

Taiga Field Sheet Rev1S1on 4 Ejfecm•e Date 18-.lan-10

Page __ of __ Form JD: FOR Q005 Ftle JD. 5514.45

FOR Q005 - Taiga Field Sheet Rel'ISion 4

34

O"'c...~ (~~ dwvv 3 OJ-ob0 TAIGA ENVIRONMENTAL LABORATORY

LABO RA TOIRE ENVIRONNEMENT AL TAIGA 4601 - 52 Avenue, P.O. Box 1500, Yellowknife, NT, XIA 2R3

Tel : (867) 669-2788 •Fax: (867) 669-2718

FIELD SHEET


Send Results & Invoice to: (Please notify if results or invoice ore to be sent to different locat1ons)

Company/Agency:-------- -----

Address

City ff own

Postal Code.

______ Provinceffemtory __ _

Phone: _______ _ Fax --------

Client Project No:-------------

Date collected:---------- - ---


Sampler: - ---------------

Location:---------------Rush Required: [JYes [JNo Note: Aualpi,· may he s11hc01r1roc11..'d 11'il/ww prwr uouce.

See ll!rersc for /wll' to complete form am/ sampling proux:ol~.

E-mail ------------- ---- - Date Received _____ Received By -----Signature : ________________ _ Comments --,-,-------------

(Lnboratory use only)

-WATER SAMPLES -Sample Type {freshwater, sewage, wnstcwatcr,

notable . 21'oundwater. salt water. e1c)

Client Sample ID 2.0\L\- {2.. ~ 'l.n\4-~4 (As it should oooeor on finol reoonl


Boule Tvoe and Parameter I.../ I PLEASE CHECK PARAMETE.RS REQUESTED BELOW: pH, Conductivi!)', Alkalini!)' _pl I I C"6J AI J.. fill lW I Alk pl! I Cum! I Alk Individual Anions Suite 0 ('I ~I · INO,-N I KOi-N ~illNO,-N lr-.o,-'1 c1 lso, 'r INO,-N INo,-N Total Nitrite lliQ~) + Nitrate (N01) NO, +NO,-N

c~~~~--V--NO, +NO,-N

Individual Cations Suite 0 CaVj Mgv NaY'f ('V l a I Mg J Na l "' Hardness (Calculated) 1-Iardnes\ 1 Iardness I lardne>> Reactive Silica S101

S1(1;' ______________ S10 , -

Laboratory use only Rec'd y N Ret:'d y N Rec·d y N

Chlorine: Total, Residual T Cl I R Cl T. Cl R. CI ·1. Cl I R Cl Chemical Oxygen Demand COD COD COD Color i\pp.ircnt ·1 rue Apparent J__J.I_~.£, ____ Apparent l True Turbidity Turb1d1t) Turbid1tv Turb1d1ty Total Suspended Solids, Dissolved Solids TSS 'IDS TSS -,.-·--To-;- -- TSS I 'IDS

r: Ammonia NII, Nll:i_ Nil,-N Phosphorus: Total . Dissolved. Ortho ·1 p DI' [ OP f'P DP OP Tl' l DP I OP . ---· -L----·--·· Carbon: Total Dissolved TOC DOC roe I DOC TOC DOC Nitrogen· Total Dissolved ·1N DN TN UN TN DN Visible 01! and Grease V1s1 ble V1stble V1s1ble -Laboratory use only Received y N Received y N Received y N

uf Fecal Cohforms (FC) I·C re IC

t Total Coltforms (TC), E Coli (EC) IC IC IC IC ll 1-C iii Fecal Streotococcus CFS) I!:> IS fS

Laboratory use only Received y N T __ •c Received y N T ·c Rccc1ved y N T •c Stcnle contnmer Y N Stenlc contamcr Y N Stcnle contamcr Y N

Biolo11.ical Oxv11.en Demand UOD BOD BOD arbonaceous BOD CBOD CllOD CBOD Laboratory use onlv - Received y N T •c Received y N T ·c Ret:e1ved Y N T ·c lease indicate 1f sample is

!'res n I Filt f l'rcs l-1 Pre~ Fil1n Presn Pres l'l Fih n l'rcsn reserved and/or fil tered I ICP-MS( I)· Cd. Cr. Cu. Co, Mn, N1. Pb, I

--

Total Dissolved Total D1ssohed Total Dissolved Zn, Fe -ICP-MS(2). 25 element scan mcludes As Total I D1ssohcd fol.ti D1>>ohed Total Dissolved lnot tncluded B ..!!.!.J:!s~) _[

ndividual Metals by ICP-MS v · 7 pie 1rcle~h "'Iii!_) Ag.~I , As, B, Ba, Be, Total D1ssohcd f ulal D1»olved Total Dissolved I, Co, r c. L~ Li, Mn~

b Rb1 1 Se, S"n, Sr, T1, Tl, U, V ..!! Laboratory use only TM rec'd Y N DMrec'd Y N TM rec'd Y N DMrec'd Y N TMrec'd Y N DMrec'd YN

I Hexane Extractable Material (O&GI llUt'f llEM llEM Laboratorv use onlv Rec'd y N Pres y N Rec·d Y N Pres y N Rec'd Y N Pres y N

BTEX, Purgeable HC (40mL x 2 vials) Bl! X Purg llC BTIX I Purg llC !HEX I Purg IIC Extractable HC ( IL amber glass bottle) E:-.1 IIC hlHC E:-.1 IIC

:Trihalomethanes (40 ml x 2 vials) TllM rnrvt TllM Laboratory use only Vial rec'd Y N Extrec'd Y N Vial rec'd Y N Ext rec 'd Y N Vial rec'd YN Ext rec 'd Y N I Other: see special rea11es1 form 'T-oho.l t"'~" ·-- • c. --r Nhl l n.01 .... ..t <.

For safety purposes, please dtsclose any contaminants (e g heavy metals, cyanide etc) 1hat may be present at high levels and pose a nsk to human health

Taiga Em7ronmenta/ Laboratory Tmga Field Sheel Rernwn 4 Ejfe<1i1•e Dale /8.Jan-10

Page of Fonn JD. FOR Q005 File JD · 551.4.4.5

FOR Q005 Taiga Field Slree/ Rei7swn 4

35

En"'1fallmontlJ/ l.Abonltot>t..abor11to1ro EntnrannomontAI

Special Request Form

(to be attached/s11b111itted with origi11a/ field sheet)

Date Received: _____ Received By: ____ _ 'J.aboratory Use 011/y

Sample Type (freshwater, sewage, potable, wastewater, groundwater)

Client Sample ID l:. (As it should appear on final report) ,20\4... l,. Taiga Sample ID Laboratory Use On~v

Description of Analysis Required: (Including method, subcontractor, special instructions , etc.)

~~ Ph~ls CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

LABORATOIRE ENVIRONNEMENTAL TA"iGA 4601 52nd Avenue, C.P. 1500, Yellowknife, NT X1A 2R3

Telephone: 867-669-2788 • Telecopieur: 867-669-2718 www.enr.aov.ca

) ) PLEASE CHECK PARAMETERS REQUESTED BELOW:

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

CJ

36

EnvtronmontJJJ ~tot>Lllbonltolro EnW'ronnomontaJ


(to be attaclred/submitted wit Ir origi11al field slreet)

[Date Received· tLaboratory• Use Only

Sample Type

Received By _ _

(freshwater, sewage, potable, wastewater, groundwater)

LABORATOIRE ENVIRONNEMENTAL TA'iGA 4601 52nd Avenue, C.P. 1500, Yellowknife, NT X1A 2R3

Telephone : 867-669-2788 • Telecopieur: 867-669-2718 www.enr.gov.ca

Client Sample ID ·z.:Pl4-£.3 (As it should appear on final report)

Ta iga Sample ID Laboratory Use 011(1•

Description of Analysis Required: (Including method, subcontractor, special instructions, etc.) ( .J ) PLEASE CHECK PARAMETERS REQUESTED BELOW:

r;¥'" "f ~Al ~lr a a a a a a a a a a a a a a a a a a a a a a a a a a a a a

(

37

LABORATOIRE ENVIRONNEMENTAL TA"iGA 4601 52"d Avenue, C.P. 1500, Yellowknife, NT X1A 2R3

Telephone : 867-669-2788 • Telecopieur : 867-669-2718 www.enr.gov.ca

Envlronmont41 UOOl'afOt>Lllboratolm EnWronnomonta.1

Special Request Form Onu.. cg~ ~ 3 a .. t.i1oe.-) (to be a1tac/1edlsub111i1ted wit Ii origi11a/ field s/ieet)

ioate Received Laboralo!J' U.>e Only

Sample Type

Received By ____ _


Client Sample ID 2.0 l4 -G.'-1 (As it should appear on final report)

Taiga Sample ID Laboratory C \<e Only

Description of Analysis Required: (Including method, subcontractor, special instructions, etc.)

~rotru f1tP..V\Ol~ a a a a a a a a a

( I PLEASE CHECK PARAMETERS REQUESTED BELOW:

a a a a a a a a a a a a a a a a a a a a

(

38

linvironm.nroJ L.llborero,,. '-*boniitolro l!nWronnontontAI


(to be attac/1edlsub111itted wit It origi11al field slteet)

Date Received __ Received By -----,aboratory Use Only


LABORATOIRE ENVIRONNEMENTAL TA"iGA 4601 52"d Avenue, C.P. 1500, Yellowknife, NT X1A 2R3

Telephone : 867-669-2788 • Telecopieur : 867-669-2718 www.enr.gov.ca

Client Sample ID 'Z.Dl4-P (As it should appear on final report)

Taiga Sample ID I aboratory Use Only

Description of Analysis Required: (Including method, subcontractor, special instructions, etc ) I I PLEASE CHECK PARAMETERS REQUESTED BELOW:

V"~attll P~ll CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

( ....

39


Telephone: 867-669-2788 • Telecopieur: 867-669-2718 www.enr.gov.ca

EnvlronmontAI L.ataOlatotY Lllboratoko EntnronnomantaJ

Special Request Form o"~c~J~ !()c.~) (to be a11acl1edlsubmi11ed with origi11aljield sheet)

Date Received: _____ Received By _ 'laboratory U1e Only


Client Sample ID '2-0l l{ -£.l1 (As it should appear on final report)

Taiga Sample ID Laboratory Use Only

Description of Analysis Required: (lncludmg method, subcontractor, special instructions, etc) (VI PLEASE CHECK PARAMETERS REQUESTED BEWW:

o/1"ol-a.l ~ls 0 0

0 0 0

0 0 0

0 0 0

0 0 0

0 0 0

0 0 0

0 0 0

0 0 0

0 0 0

c

40

(

I w\ce ~v cllAv-t~ JVV\e_. TAIGA ENVIRONMENTAL LAB~TORY

LABO RA TOIRE ENVIRONNEMENT ALT AIGA 4601 - 52 Avenue, P.O. Box 1500, Yellowknife, NT, XIA 2R3

Tel : (867) 669-2788 • Fax: (867) 669-27 I 8 ----.. --Send Results & Invoice to:


FIELD SHEET

(Please notify if results or invoice are to be sent to different locations) Client Project No:-------------

Date collected·--------------

Time collected: --------------

Sampler·----------------

Location -----------------


Address:

CityfT'own: ______ Provincefferritory: __ _

Postal Code: Rush Required. CJYes CJNo

Fax:--------Phone:-------

E-mail:------------------

Signature :------------------

Note: Anal; \'IS ma; he .mhconlmctc.·d 1111/10111prwr1w 11ce

Sample Type (freshwater, sewage, wastewater. ootablc . m>undwntcr. salt water. etc)

Client Sample ID (As it should aooear on final reoort)

Taiga Sample ID (Laboratory""' only)

Color Turbidity

en Demand

Tolal Suspended Sohds, 01Ssolved Solids

Ammonia Phosphorus: Total , Dissolved, Ortho Carbon: Total, Dissolved Nitrogen. Total , Dissolved Visible 011 and Grease Laboratory use only

.!!I Fecal Coliforrns (FC)

·5 Total Col iforrns (TC), E. Coli (EC) ii5 Fecal Stre[>tococcus (FS)

Laboratory use only

See rel·er.se for hou to complete fomJ and samplmg protocol\

Date Received -----Received By -----

Commen~ ---,...,~-------------(Laboratmy use only)

-WATER SAMPLES -

W\4-~S

SiO, Rec'd y N

T. Cl R CJ COD

App~rcnt True Turb1d1ty ~

fi( TOC TN

NU, DP

V1sihlc Received Y N

·re IS

·ros

I m' DOC

IC

ro~lf-~'

Rec"d y N

T.Cl R Cl COD

A pparcnt True J>1rbidity

_·_MI'S'" ] TDS

·w/j TOC TN

Rcc.e1ved

IC

NIJ, DP

I Visible y N

I IS

I OP DOC DN

IC

Received Y N T __ •c Received Y N T •c Stcnlc contnmcr Y N Stcnle container Y N--

BOD BOD CBOD CflOD

Received Y N T __ •c Received y N T __ •c

!'res l 1lt Pre-, Pre; 111! Pre;

I otJI Dt'>'>Oll ed lotJI Dl'i'ioll ed

Total D1ssoh cd lot.ii D1;;ohcd - v ·rot.ii D1;;ohcd

Thi rec·d Y N DM rec'd Y N

·Wt~-fl..~

Rec'd Y N

T. CI R CJ COD

Apparent j True ] urb1ditv ~ I . TDS

Nll ,-N jj;i"l DP I Of' TOC [ r.loc

---'·1"'·N __ _, __ DN Visible

Received Y N

·l

IC l·C IS

Received y N T ·c Sterile container Y N

BOD CBOD

Received Y N T __ •c

l lit Prcs l

lotJl D1ssol\cd

Iota! [)1;-,01\ ed

V',-Iota! D1-,.,oh ed

'd YN

Rec'd Y N Pres Y N Rec'd Y N Pres Y N Rec·d Y N Pres Y N

Purg JI(' h.t HC

I JIM

[} l'urg !IC h.tllC

IHM

BTE · I Purg I re ___ 1 .... ~

IHM

For safely purposes, please disclose any contaminants ( e g heavy meta s, cyanide elc ) that may be present at high levels and pose a risk Io human heallh

Taiga Enwronmenlal Laboratory Taiga Field Sheet Revision 4 Ejfectn•e Date /8.Jan-10

Page __ of __ Form ID FOR Q005 File JD. 551.4.4 5

FOR Q005 Taiga Field Sheet Rews1on 4

41

C.

"lwlcR_ Tr.:::N~~.::NTA~~~:i-RY~ 1 ~ riil!illiiiilliiiliil'[iii LABORATOIRE ENVIRONNEMENT AL TAIGA SHEET

4601 - 52 Avenue, P.O. Box 1500, Yellowknife, NT, XIA 2R3 Tel : (867) 669-2788 • Fax: (867) 669-2718


Send Results & Invoice to: (Please notify if results or mvo1ce are to be sent to different locations)


Address:

Cityrrown: ______ Provincerrerritory: __ _

Postal Code:

Phone: -------- Fax: _ ______ _

E -ma i I:--- ---------------

Signature :------------------

Client Project No --------------


Time collected

Sampler: _________________ _

Location·----------------Rush Required CJYes CJNo Note: Anal) tti\ ma; he s11hcon1roc1ed 11 iJlumt pnor nollcc.:

Sec rt:\'Cfj·cfor Jwu lo complete form and .romp/mg proloco/\

_____ Received By ____ _ Date Received Comments ----------------(Laboratory use only)

-WATER SAMPLES-Sample Type (freshwater, scwngc, wastewater,

at.able . oundwntcr. SD.It water. ere)

Client Sample ID (As it should 11 car on final re art)


Rec'd Y N

T Cl R Cl COD

Color i\pparcnl J. __ I rue Turbidity )"ur~1d11y Total Suspended Sohds, Dissolved Sohds --~ TDS

•iil·A-:-.::.:m=m:...:o::n:::;ica==========--I NI h

Phosphorus· Total , Dissolved, Ortho V l DP . L .. 2.1' Carbon- Total, Dissolved TOC DOC Nitrogen: Total , Dissolved "IN DN Visible Oil and Grease Laboratory use only

~ Fecal Cohforrns (FC)

·5 Total Col iforrns (TC). E Coli (EC) ii5 . Fecal S tre tococcus F S

Laboratory use only

V1s1hlc Received Y N

r ,

IC IC IS

Received Y N T __ •c Stenlc container Y N

BOD CllOD


Pre' fl It r I Pres I l

I I Dissolved

-1--

i D1s\.nlvcd I

Recd Y N Rec'd Y N

T. Cl R. CI ·1c1 I R c1 COD COD

Apparent j True i\ppilrent j ·r rue _L Turh1d1ty J urh1d1t)

aorss I TDs ~ I ·1Ds Nlh Nlh-N W']'or I 01-, - -ki"'~J-1~)1-, __ o_P_ ,

·roe DOC IOC [ DOC TN D 11 DN

____ V_1s_il_1le V1sihlc Rece1 ved Y N Received Y N

r ..

IC IC LC rs IS

Re..,ved Y N T _•c Received Y N T •c Stcnle container Y N Stenle container Y N -

BOD BOD CllOD CBOD

Received Y N T _ _ •c Received Y N T---.-C-

Pre~ fl ~ ' il1n Pres l

T~· DIN>hcd ·rota!

ki{-Dissolved

Pre~ Filt Pre~

Iota!

I otal Dissolved

Dissolved

TM rec'd Y N DM rec'd Y N TM rec'd Y N

Ill Rec'd Y N Pres Y N Rec 'd Y N

I .. ' Puig l!C I \.tllC l llM

For safety purposes, please disclose any contaminants (e g heavy metals, cyanide, etc) that may be present at high levels and pose a risk 10 human health

Taiga Em•ironmental Laboratnry Taiga Field Sheet Re\'/Sion 4 Ejfecllw! Datt /8.Jan-10

ff · : I Purg llC o, Purg llC htHC lllM

E'>LllC 111~1

Page of_ Form ID· FOR QOOS File ID· S5U 4 S

FOR QOOS Taiga Field Sheel Re\'iswn 4

42

LABORATOIRE ENVIRONNEMENTAL TA'iGA 4601 52nd Avenue, C.P. 1500, Yellowknife NT X1A 2R3

Telephone : 867-669-2788 • Telecopieur: B67-669-2718

""""""m""'""·-"'"wry -~~~~~~~-~~-~-~~~-~~~~~~~~_..lwww~~- 2ean~r.992o~v.~ca~ L.aboratolro EnW.l'DnlKl!n'HlntaJ


(to be attaclredlsubmitted wit Ir origi11al field slreet)

Date Received .aboratory Use Only

Received By -~~~~~~~-------------------------


Client Sample ID 2..z>l4-{LS (As it should appear on final report)

Taiga Sample ID laboratory l /.rn Only

Description of Analysis Required: (Including method subcontractor special instructions etc )

( ) PLEASE CHECK PARAMETERS REQUESTED BELOW·

~o\n\~lc CJ CJ

~...::~ · ' -~, t n CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

43

LABORATOIRE ENVIRONNEMENTAL TA'iGA 4601 52nd Avenue, C.P. 1500, Yellowknife, NT X1A 2R3

Telephone : 867-669-2788 • Telecopieur: 867-669-2718

~m~""Labonl""" -------~~-~~~---~~----~~--__:www~~·~e~nlr.~g~o~v~.c:a.a ~tolro.l!n~tl&I

Special Request Form '\" v.--'-<..e.- c-<r J-cp...r (to be a11ached/s11b111it1ed with origi11a/ field sheet)

Date Received Received By .aboral<!!)' u,eo 11-l;-, -- ----------------------


Client Sample ID

7nll-i-R~ (As it should appear on final report)

Ta iga Sample ID I aboratory Urn 011/y

Description of Analysis Required: (Including method, subcontractor special instructions etc ) ( (PLEASE CHECK PARAMETERS REQUESTED BELOW·

ti1'"nhl.\ ~ u "h. CJ CJ

~~ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

c

C~.·

44

~monrm~ro,,.

t..bort:ltoho l!nvlronnDtnontm


(to be al/acltedls11b111i1ted wit It origi11al field sheet)

Date Received: _____ Received By Laboratory Use 011ly


LABORATOIRE ENVIRONNEMENTAL TAi"GA 4601 52"d Avenue, C.P. 1500, Yellowknife, NT X1A 2R3

Telephone: 867-669-2788 • Telecopieur: 867-669-2718 www.enr.gov.ca

Client Sample ID 12.0\\{- R1-(As it should appear on final report)

Taiga Sample ID /.aboratory U•e Only

Description of Analysis Required: (Includmg method, subcontractor, special instructions etc )

( ] PLEASE CHECK PARAMETERS REQUESTED BELOW:

V1N\-a \ ~~.,. l/\o\ S CJ CJ

~' \\?~ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

45

Envlt'OnmontDI L.aoontrory LllbonltokD ~nrironnomotttAI


(to be attached/s11b111itted with origi11aljield sheet)

Date Received Laboratory l ~'e Onfy

Sample Type

__ Received By·----


LABORATOIRE ENVIRONNEMENTAL TAi"GA 4601 52"d Avenue, C.P. 1500, Yellowknife, NT X1A 2R3


Client Sample ID 2-0\4 -(lg (As it should appear on final repon)

Taiga Sample ID Laboratory l 'se Only


) ) PLEASE CHECK PARAMETERS REQUESTED BELOW:

~rl-nl ~\<; Cl Cl

o/.-cpl:+ Cl Cl

Cl Cl Cl

Cl Cl Cl

Cl Cl Cl

Cl Cl Cl

Cl Cl Cl

Cl Cl Cl

Cl Cl Cl

Cl Cl Cl

C ..

46



Special Request Form .......r-

\ C,.....l c..c... r-c.r (to be a11ached/s11b111i11ed with origi11al field sheet)

Date Received: _____ Received By -----aboratory U.re 011/y


Client Sample ID 2.D \ 4- '2..0\ (As it should appear on final report)

Taiga Sample ID Laboratory Use Only


( ../ ( PLEASE CHECK PARAMETERS REQUESTED BELOW:

~/ "lo-\-0. \ ~(,V\.c)\S CJ CJ

cV'""'f\?\t CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

CJ CJ CJ

47

Envlnmmontlll LMbonlitot)" Ubon:ltalnl ~~llU

LABORATOIRE ENVIRONNEMENTAL TAi°GA 4601 52°d Avenue, C.P. 1500, Yellowknife, NT X1A 2R3


Special Request Form --r:t~ \ ..u-(to be attacltedlsubmitted witlt origi11a/jie/d slteet)

!Date Received: Received By __ _ Laboratory { !rn 011/y


Client Sample ID Z.0\4- e\t> (As it should appear on final report)

Taiga Sample ID I ahoratory l se Only


) -./ ) PLEASE CHECK PARAMETERS REQUESTED BELOW:

~rr\-,,. \ Ph~ \s Q Q

CV'f'P\\_ Q Q

Q Q Q

Q Q Q

Q Q Q

Q Q Q

Q Q Q

Q Q Q

Q Q Q

Q Q Q

48

10 D~\.f s be~e- De.cad TAIGA ENVIRONMENTAL LABORATORY

LABO RA TOIRE ENVIRONNEMENT AL TAIGA 4601 - 52 Avenue, P.O. Box 1500, Yellowknife, NT, XIA 2R3

Tel : (867) 669-2788 •Fax: (867) 669-2718

FIELD SHEET


Send Results & Invoice to : (Please notify if results or invoice are to be sent to different locations)


Address:

City ff own: ______ Provincefferritory: __ _

Postal Code:

Phone: _______ _ Fax: _ _____ _

E-mail:------------------

Signature :------------------



Time collected: ---------------Sam p 1 er:------------------

Location:----------------Rush Required: DYes DNo Note: Aualpiis may he .mhc01rtroc1ed withow prior 1101tcc.

See rewr.n~ fur Jwu to complete form and sampling protocol.\·

Date Received _____ Received By ____ _

Comments -----------------(Laboratory use only)

-WATER SAMPLES -Sample Type (freshwater. ' '"'"•&•. wastewater,

ootablc . "°oundw11tcr. s.1lt water. etc)

Client Sample ID ·2..0 \4 - ~ "2-(As it should aoocor on final rcoort)


...J PLEASE CHECK PARAMETERS RE UESTED BELOW: Alk 11 . Cond Alk fll I Cond Alk

Cl l!>o, lt:JNo,-N~-N ~ I [NOJf[NO!-N

Rec 'd Y N

T Cl R. CI en Demand COD

Color Ap11arent J!_~_e __ _ Turbidity rurh1d1t) Total Suspended Sohds, Dissolved Solids ·ij.< - [ [)~ Ammonia - ~.,/

-,;-,/ I~ -Phosphorus· Total, Dissolved, Ortho ~--• __ D~ Ol' Carbon: Total, Dissolved ____ ·1 OC · DOC Nitrogen· Total Dissolved TN '--_QN Visible 011 and Grease V1 1hlc Laboratory use only

., 1 Fecal Coli forms (FC)

~ ! Total Coliforrns (TC), E Col i (EC) Ci5 Fecal Stre tococcus FS

Laboratory use only

en Demand

lease indicate if sample is reserved and/or filtered

Received Y N

rr 1 <. IS

Received Y N T __ •c Stcnlc container Y N

D l D


lilt

ICP-MS( I): Cd, Cr. Cu, Co, Mn. N1. Pb, Total D"'ioh ed ----~z=n~ ___ ___ _

1 ___ _

ICP-MS(2). 25 clement scan includes As rotal I Dissol,ed __ (not included B ,.!&!:!J! ,~--•-----~ ndividual Metals by lCP-MS please circle each metal) Ag, Al, As, B, Ba, Be,

1, Cd, Co, Cr, Cs, Cu, Fe, Hg, L1 , Mn, Mo, Total D1,solvcd

Cu NO, +N01-N [ Mg Na~

Hurdne~s

S10: Rec'd Y N

T. Cl R Cl

NO +NO-N CuMg~a 1 "

llardne~\

S102

Rec'd Y N

T. Cl I R Cl O~l COD

Apparent j True Apparent ·r rue Turbiditv Turh1d1t\

1 __ ·~1 ~~s~--,-,'-1,_·-T_Ds~· __ ·_1 ss I · rns

Nll,-N Nlh II' l DJ> ·roe

l"N Visible

Received y N

re IC I

J OP DOC ON

IC

II' IOC IN

DI'

[ Vis1lilc

RctclVcd Y N

IC

Ol' DOl DN

IC IC ls IS

Received Y N T •c Received Y N T Stenle contamcr Y N-- Stenle container Y N

BOD BOD CBOD CBOD

Received Y N T •c Received Y N T __ •c

Pres Filt Pre~ Pre> l111t n l're,n

"lotal lotal

"[otal lotal -----~-----1

Total lotal

1, Pb, Rb. Sb Se Sn. Sr, Tt , Tl,,_, U~,,_V'"'.~Z""n--ll-----------•---~~---~~~i--~~~--~=~-I Laborato use onl TM rec' d Y N DM rec'd Y N TM rec'd Y N DM rec'd Y N I rec'd Y N DM rec'd Y N

For safety purposes, please disclose any contaminants (e g heavy metals. cyanide, etc) that may be present at lugh levels and pose a nsl. to human health

Taiga Enwronmemal Laboratory Taiga Field Sheet Rewswn ./ Effecti\'e Date 18..Jan-I 0

Page _ _ of __ Form ID. FOR Q005 File ID. 551 . ./../.5

FOR Q005 Taiga Field Sheet Rewswn ./

49

TAIGA ENVIRONMENTAL LABORATORY LABORATOIRE ENVIRONNEMENT AL TAIGA

4601 - 52 Avenue, P.O. Box 1500, Yellowknife , NT, XIA 2R3 Tel : (867) 669-2788 •Fax: (867) 669-2718

FIELD SHEET

www.taigagc.ca Batch No

Send Results & Invoice to: (Please notify if results or invoice are to be sent to different locations) Client Project No:-------------

Date collected:---------------

Time collected:


Address:

Sampler: _________________ _

Cityrfown: _ _____ Provincerrerritory: __ _ Location:----------------

Rush Required: DYes ONo Postal Code:

Phone: _______ _ Fax:--------Note: Ana/yJi.r may he jUhconlracted withow prior notice.

See rewrse for how 10 comple!te form a11J sampling prolocul'i.

E-mail:----- -------------

Signature :------------------

Date Received _____ Received By

Comments ----------------(Loboratoiy use only)

Sample Type (frosh\\'nl<:r, sewose. wastewater, table. oundwotcr. salt water. c1c)

Client Sample ID (As it should• ear on final re ort)

Taiga Sample ID (Loboratoiy use only)

Color Turbidity

en Demand

Total Suspended Solids, Dissolved Soltds Ammonia Phosphorus: Total , Dissolved, Ortho Carbon. Total, Dissolved Nitrogen: Total. Dissolved Visible Oil and Grease Laboratory use only

~ \ Fecal Coliforrns (FC)

·5 Total Coliforrns (TC), E. Coli (EC) ii5 Fecal Stre(ltococcus FS

Laboratory use only

en Demand

[BTEX, Purgeable HC (40mL x 2 vials) [Extractable HC ( IL amber glass bottle) Tnhaiomethanes (40 mL x 2 vials Laborato use onl · !Other: sees ecial re uest orm

-WATER SAMPLES -

_r. 11 Cund I Alk Cl SO, I NO,-N NO.-N

NO,+NO,-N K Ca I tvlg ] Na [ K

I lnrdne% S10,

Reo'd Y N Rec 'd Y N Rec'd Y N

T Cl R Cl T Cl R Cl T. Cl I R. Cl COD COD COD

Apparent True Turbidity

-~~ 'IDS

'lY - DI' OP ~Jf)!' OP ~ DP OP l--'-T~O~C-~-~D~O~C __ 11 __ 'f~{)~C'-' l~)O~C~'--• --'-l~O~C---+------'-D~C~)C~'--1 ___:!:.!':!__ l DN IN UN IN DN

Visibl e V1s1blc Received Y N Received Y N

TC IC IC l IC IS IS

Received y N T __ ·c y N Stcnle contnmcr Y N

ll c

Recctved y N T •c Received y

Pres n I r·i1 t11 Prcsr1 Pres Pre~

Total I Dissolved Total D1s·mhed

Total Dissolved 'Iota! D1~~ol ved ---- .l

I

Total

I Dissolved Total D1~~olved

TM rec'd Y N DM rec'd Y N TM rec'd Y N DM rec·d Y N

Ill 1'1 llEM Rec'd Y N Pres Y N

B II \'. Purg llC E\.tllC Tl!M

Vial rec'd Y N Ext rec 'd Y N

Rec 0 d Y N Pres Y N

B IEX j Purg IIC r: .. t 11c Tilt-.!

Vtal rec'd Y N Ext rec'd Y N

V1s1hlc Received Y N

IC

re I IS

RC(:c1vcd y N

1-C

T •c Stcnlc container Y N

BOD CBOD

N T "C --Pre~ l111t Pres

lotJI D1ssoh ed

Total U1~'>ohed

I otal Dl'>~oh ed

rec 'd Y N DM rec 'd Y N

HEM Rec'd Y N Pres Y N

Irl EX I Purg I JC fat HC rlIM

Vtal rec 'd Y N Ext rec'd Y N

For safety purposes, please disclose any contaminants (e g heavy metals, cyanide, etc) that may be present at !ugh levels and pose a nsk to human heahh

Taiga Em·ironmemal Laboratory Taiga Field Sheet Revision./ Ejfecf/l·e Date 18.Jan-JO

Page of __ Form ID: FOR Q005 File ID: 55/../../_5

FOR Q005 Taiga Field Sheet Re»iswn ./

50

c.

TAIGA ENVIRONMENTAL LABORATORY LABO RA TOI RE ENVIRONNEMENT AL TAIGA

4601 - 52 Avenue, P.O. Box 1500, Yellowknife, NT, XIA 2R3

~ f.O\l-\-RL\ \s So.Mr I~ FIELD Dnt. ~ ~~ SHEET ~

----- Tel : (867) 669-2788 •Fax: (867) 669-2718 www.taiga.gc.ca Batch No

Send Results & Invoice to: (Please notify if results or invoice are to be sent to different locations)


Address:

Cityffown: ______ Province/Territory: __ _

Postal Code:




Sampler:----------------

Location: ----------------Rush Required: CJYes CJNo

Fax: _______ _ Phone:-------

E-mail:-----------------

Signature :-----------------

Note: A11alp;i.r may he suhco111rac1ed u·i1hu111 prior nurice. See ren!r.\·e for /toll' lo complclc fon11 and sampling pro1ocol.1t.

Date Received _____ Received By -----Comments _...,...,. _____________ _ (Loboratory use only)

-WATER SAMPLES -Sample Type (fn:shw•t<r, sew•se. wostcwatcr,

notable . tttoundwiltcr. Slllt water. etc )

Client Sample ID 2Dl4-12-~ L.0\4-f-4 (As it should aooear on final reoort)


Boule Tvoe and Parameter • I../ I PLEASE CHECK Pt\JtAMETERS REQUESTED BELOW: _IJH Conductivity Alkalinit)' I~ I C'ond AH .. __eTI I Cond I Alk r.11 I Cond Alk Ind ividual Anions Suite D C'l I so, I I· I NO,-N I N0,-'1 Cl ~O, .JF NO,-N I NO_;-N c1 lso, Jr INO,-N INO,-N Total Nitrite~)+ Nitrate lliQi)_ NO,+ N01-N NO, +NO,-N N02 + NO,-N Indiv idual Cations Suite D Ca I Mg Na K Ca _[ _~g ___ Na l~ Ca l Mg J Na l K Hardness (Calculate~f=~---=:- I lardness Hardness - 1 lan.lness Reactive S iltca S1CJ , ------- Si() S1CJ , -Laboratorv use only Rec'd y N Rec'd y N Rec'd y N

Chlorine: Total, Residual T Cl I R Cl T Cl R Cl T. Cl I R.CI Chemical Oxygen Demand COD COD COD Color Apparent ·1 rue Apparent I True Apparent j True Turbid tty Turb1d1tv Turb1d1tv Turb1d1ty Total Suspended Solids, Dissolved Solids -~ r - ·r DS ~· ·ms ·1ss I "IDS

m"'!ll Ammonia ~ \)lK, Nlh-N Phosphorus Total, Dissolved, Ortho W--~----1T I 01' wrr)~' I OP Tl' I DI' I 01'

[ I

Carbon Total, Dissolved TOC DOC ·roe I

DOC TOC DOC Nitrogen Total , Dissolved 'IN I DN "IN DN rr-. DN Visible Oil and Grease V1 ihle Visible V1s1hlc -Laboratory use only Received y N Received y N Received y N

.!!I Fecal Col iforrns (FC) l\V" ~ I('

·5 Total Cohforrns (TC), E Colt (ECJ re I l re ll IC I IC ~ Fecal Streotococcus (FS) rs IS IS

~

Received __ ·c Laboratory use only Received y N T _·c y N T •c Received y N T

Stenlc conuuner Y_, N Sterile container )'. N-- Stenle container Y N

Biolol!l ical Oxviten Demand !¥'}[) # IM'l'D, BOD arbonaceous BOD .....£~ Cf.u.11') CBOD Laboratorv use onlv Received y N T ·c Received y N T __ •c Received Y N T "C

lease ind icate if sample is Pres r11t f l'rcsl l Pres fl l1·I1t n Pres 1'1cs !-tit Pres reserved and/or filtered - -I--

ICP-MS( I) ' Cd, Cr, Cu, Co, Mn, N1, Pb, Total D1ssolled Total Dissol\ ed lntal D1ssoh ed Zn Fe i --!CP-MS(2) 25 element soon includes As I Total D1ssolvcd Tola! D1ssol\cd Iola! Dissolved

(not included B,J!!...!:!~- I ---nd1vidual Metals by ICP-MS I pleosc e1n:le each metal) Ag, Al. As, B, Ba, Be, I

rota I Dissolved Total D1s~lvcd fatal Dissolved 1, Cd, Co, Cr, Cs, Cu, Fe, Hg, L1, Mn, Mo,

I 1, Pb Rb, Sb Se Sn, Sr T1 Tl, U, V, Zn -Laboratorv use only TM rec'd Y N DMree'd Y N TMrec'd Y N DMrec'd Y N lrMrec'd Y N DMrec'd YN !Hexane Extractable Material (O&G) Ill 1\1 HEM HEM

Laboratorv use onlv Rec'd Y N Pres y N Rec'd Y N Pres y N Rec'd Y N Pres y N

BTEX, Purgeable HC (40mL x 2 vials) Bl EX Purg !IC BTEX I Purg !IC IHEX I Purg IIC Extractable HC (IL amber glass bottle) E:--t llC Ext I-IC htl-IC

ITnhalomethanes 140 mL x 2 vials) TllM TllM Tiil\! Laboratory use only Vial rec'd Y N Ext rec 'd Y N Vial rec'd Y N fat rec'd Y N Vial rec'd Y N Ext rec 'd Y N

!Other: see special reques/ form For safety purposes, please disclose any contaminants (e g heavy mecals. cyanide, etc) that may be present at high levels and pose a risk to human health

Taiga Enwronmental Laboralory• Taiga Field Sheet Rewsio114 Effecl/l'e Date 18.Jan-JO

Page __ of __

Fann ID. FOR Q005 File ID. 55/A 4 5 FOR Q005 - Taiga Field Sheet Rel'IS1on 4

Zl>l4-~}

51

A\W \)terA~ (o~~SO\~~ TAIGA ENVIRONMENTAL LABORATORY

LABO RA TOIRE ENVIRONNEMENT ALT AIGA 4601 - 52 Avenue, P.O. Box 1500, Yellowknife, NT, XIA 2R3

Tel : (867) 669-2788 •Fax: (867) 669-2718

FIELD SHEET

------ www.taiga.gc.ca Batch No

Send Results & Invoice to: (Please notify if results or invoice ore to be sent to different locations)


Address:

City ff own: ______ Provincefferritory : __ _

Postal Code:

Cl ient Project No:--------- ----

Date collected: - - ------------

Time collected: --- ----------

Sampler:----------------

Location:---------------

Rush Required: ClYes ClNo

Fax:--------Note: Analysis may he suhc0111roc1ed wi1Jwu1 priur notice.

See ll!\'f!rsefur Jtoir to complele fom1 and sampling protocol.\· Phone:----- --

E-mail:-----------------

Signature :-------------- ---

Date Received -----Received By ____ _

Comments _ _,--------------(Lnbora1ory use only)

Sample Type (fn:shwall:r, sewasc, wnstcwatcr, pot:iblc . _(troundwoatcr. 54Jt water. etc)

Client Sample ID (As ii should appear on final reoort)


Bollie Type and Parameler

-WATER SAMPLES -

I-./ I PLEASE CHECK PARAMETERS REOUESTED BELOW:

nH Conductivi!)I_, Alkal inity ____ 1 , c\lo('!'-'--+l_C..o,'<i-'H~1d'---'""'A~lk-'--- l --'1cr-cli"r-r--iCro"'°'nd"'-~l.-'-A"'lk~· _ 1___r.1 l I Cond All-. Individual Anions Suite D C'I ISO, I· IN<J,·1' INO,-N Cl l!>O" II INOi-N IN0.1-N Cl ISO, ;r INO,-N INO,-N Total Nitrite~) + Nitrate (N03) NO, + N01-N , ___ N_ O . + NO,-N NO, + N_<~),_-N ___ , Individual Cations Suite D Ca J Mg Na ] K Ca I Mg Na I I\. Ca ' l'vtil ~a [ I\. Hardness (Calculate-~) __ -=--~- I lardne;~ I lardne;s l lardness Reactive Sil ica ~ ____ s_' 1_C_.i,____ S10: S10, _ Laboratory use onlv Ree'd Y N Rec'd Y N Rec'd Y N

Chlorine: Total, Residual T Cl I R. Cl T. Cl R Cl T. Cl I R Cl Chemical Oxv<>en Demand COD COD COD

Color -~P.Pi!~~nt I rrue Apparcnl j True Apparent J ·r rue Turbidity --· _ ]:_t_1~b1dtt) rurh1d1ty rurb1dil) Total Suspended Solids, Dissolved Solids ·~ - I ·r DS " ...e _l_ TDS "I SS J ·1 DS _A_m_m-on..,i'a----~------•----·~c-,~-----·~-- ~,----ii-~~-N~I~i-, . .,..N,--~--i

IPhosphorus Total, Dissolved, Ortho --~ ___ DP I OP --v l DP I np ll'l_n_P ___ O_l'_ ,

Carbon Total, Dissolved TOC DOC lOC DOC 11~C [ f~~C

"I Fecal Coliforrns (FC) ~ Total Coliforrns (TC). E. Col i (EC) ool Fecal Streptococcus (FS)

·-Received

"IC

V1s1hlc y N Received -v

l l IC IS

Visible y N Recc1\'ed y N

W" I I l

IC

re r IC rs I~

Laboratory use only Received Y N T •c Received Y N T __ •c Sterile contnmcr Y N Stenle contamcr Y N

Received Y N T __ •c Stenle container Y N

Biolog1cal Oxv11.en Demand I1'if) llf.lrl BOD

lease indicate if sample is reserved and/or fil tered

ICP-MS(I ). Cd, Cr, Cu, Co, Mn, N1, Pb, Zn Fo

ICP-MS(2): 25 element scan includes As

Pre~ n Total

•c

lilt Presl l

i Dl','>Ohed

I

Received Y N T •c Received y N T •c

Pres n Pres I ilt Pres

total lotal

Total I D1ssohcd ----(not mcludod B, !!!...!:!gd!)) __

1 _____ -"-

ndividual Metals by ICP-MS

lotal D1;;olvcd -----t-- --

plensc ctn:lc eoch me .. I) Ag, Al, As, B, Ba, Be, 1, Cd, Co, Cr, Cs, Cu, Fo, Hg, Lt, Mn, Mo, 1, Pb, Rb, Sb, Se, Sn, Sr, Tt Tl, U, V, Zn Laboratorv use onlv

]Hexane Extractable Material (O&G)

Total D1s~ohcd Total 1 D1;;olved I otal D1s-.ohed

TM rec 'd Y N DM rec"d Y N TM rec'd Y N I DM rec 'd Y N tn.1 rec'd Y N 1DM rec 'd Y N Ill 1\1 Ill · 1\1 11 EM

Laboratory use only Rec'd Y N Pres Y N Rec'd Y N Pres Y N Rec'd Y N Pres Y N

fBTEX, Purgeable HC (40mL x 2 vials) B !TX Purg I IC BTEX J Purg I IC B"I EX I Purg I IC

Extractable HC (IL amber gclas=s'-b"-'o'-"11"-'le"-)-l·-----'-'l:"'-.t'-l~l=l---- •-----"['-x"'"t "-H'-"C'-----•-----'-'E"'.\.'-t l~l=C ____ 1

[~=~:~h=e~~~ mL x 2

v_ia_ls,l ___ ,_V_ial~r-ec'_d _Y~-~-1 -1~-.~-,-ec-·-d ~Y~N,--11v'"-,a~I r-oc~'d,,..,..,-Y~·~,_· l_l~-=~-re-c'"'·d~Y-N~1V1al rec 'd Y ·~ll~ rec'd YN !Other: see special reauestform

For safety purposes, please disclose any contaminants (e g heaV)' metals, cyanide . etc) that may be present al high levels and pose a risk to human health

Taiga Enl'lronmenta/ LahoralOry Taiga Field Sheet Revmon 4 Effecm•e Date I 8.Jun. I 0

Page _ _ of __ Form JD. FOR Q005 File ID. 551.4.4 5

FOR Q005 Taiga Field Sheet Re1'ls1on 4

52

4601 - 52nd AvenueYellowknife, NT X1A 3Z4Phone: (867) 765-6645Lab Analysis (After hours): (867) 444-8378Fax: (867) 920-8740Email: [email protected]*To order Bottles and Cooler: Fax or email the form to Taiga Lab

David WilsonBehchokǫ ̀ Courier(867) 445-92222(867) 392-6347

Wek’eezhii Land and Water Board#1-4905 48th StYellowknife, NT X1A 3S3Telephone: 867-765-4592Fax: 867-765-4593

CONTACTS

53

mailto:[email protected]

Documents

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