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X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
X-Ray sources
Lenny Rivkin, PSI & EPFL
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Curved orbit of electrons in magnetic field
Accelerated charge Electromagnetic radiation
Wavelength continuously tunable !
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
60‘000 users world-wide
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
A larger view
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
The “brightness” of a light source:
Flux, F
FS x Ω
Brightness = constant x _________
Angular divergence, Ω
Source area, S
G. Margaritondo
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Steep rise in brightness
1021
1015
109
1900 1950 2000
Wigglers
Bending magnets
Undulators
Rotating anode
SPring8
ESRF
APS
Bertha Roentgen’s hand(exposure: 20 min)
Moore’s Law for semiconductors
SLSSOLEIL (F)DIAMOND (UK) …
the second waveXFEL
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Higher brightness: more photons on small sample or through a pinhole of ~ λ: coherence
measurements on very small probes (few μm crystals)
small divergence:compact mirrors, optics elementsminimized aberrations
short measurement times
high transverse coherencephase contrast imaging
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Microtomography
Brain blood vessels in a mousewith Alzheimer
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Overbooking of SLS beamlines
0
2
4
6
8
10
Lucia MS PX SIM SIS
2003 2004 2005 2006
Demand for beam time remains high
Industrial use is growing
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Undulators
( )β−= 1emitobs TT22γ
λλ ulight ≈
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Undulator radiation
⎟⎠
⎞⎜⎝
⎛++= 22
2
2 21
2θγ
γλλ Kn
u
Medi
um en
ergy
ring
s
( )un
Kλλ
21 2
21
* +=
λ∗ = 1.5 mm
λ∗ = 2‘500 mm
ESRF
, APS
K-e
dges
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Main R&D directions
o Short period (small gap) undulator developments
o Approaching diffraction limit: very small equilibrium emittance with large rings and damping wigglers
o Detector development complementing source improvements
o Linac based light sources development: ERLs
o Free electron lasers developments
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
In-vacuum undulators / s.c. undulators
Gapsdownto3 mm
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Cryo-cooled undulators
H. Kitamura, SPring-8
Zhentang Zhao PAC07, Albuquerque, New Mexico, June 25, 2007
Third Generation Light Sources in Operation
Zhentang Zhao PAC07, Albuquerque, New Mexico, June 25, 2007
Light SourceEnergy(GeV)
Circumference(m)
Emittance (nm.rad)
Current(mA) Straight Section Status
ESRF 6.0 844.4 3.7 200 32×6.3m Operational(1993)
APS 7.0 1104 3.0 100 40×6.7m Operational(1996)
SPring-8 8.0 1436 2.8 100 44×6.6m, 4×30m Operational(1997)
ALS 1.9 196.8 6.3 400 12×6.7m Operational(1993)
TLS 1.5 120 25 240 6×6m Operational(1993)
ELETTRA 2.0/2.4 259 7 300 12×6.1m Operational(1994)
PLS 2.5 280.56 10.3 200 12×6.8m Operational(1995)
LNLS 1.37 93.2 70 250 6×3m Operational(1997)
MAX-II 1.5 90 9.0 200 10×3.2m Operational(1997)
BESSY-II 1.7 240 6.1 200 8×5.7m, 8×4.9m Operational(1999)
Siberia-II 2.5 124 65 200 12×3m Operational(1999)
NewSUBARU 1.5 118.7 38 500 2×14m, 4×4m Operational(2000)
SLS 2.4-2.7 288 5 400 3×11.7m, 3×7m, 6×4m Operational(2001)
ANKA 2.5 110.4 50 200 4×5.6m, 4×2.2m Operational(2002)
CLS 2.9 170.88 18.1 500 12×5.2m Operational(2003)
SPEAR-3 3.0 234 12 500 2×7.6m,4×4.8m,12×3.1m Operational(2004)
SAGA-LS 1.4 75.6 7.5 300 8×2.93m Operational(2005)
Third Generation Light Sources in Operation
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Main R&D directions
o Short period (small gap) undulator developments
o Approaching diffraction limit: very small equilibrium emittance with large rings and damping wigglers
o Detector development complementing source improvements
o Linac based light sources development: ERLs
o Free electron lasers developments
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
The electron beam “emittance”:
Emittance = S x Ω
Angular divergence, Ω
Source area, S The brightness
depends on the geometry of the source, i.e., on the electron beam emittance
Ring equilibrium emittance
σ0
σ′0
to minimize the blow up due to multiple scattering in the absorber we can focus the beam
σ′ = σ′02 + σ′MS
2 σ′0 >> σ′MS
Theoretical Minimum Emittance lattice
Fmin = 112 15latt
32
0 Fθ ⋅⋅=x
qx J
ECε
Zhentang Zhao PAC07, Albuquerque, New Mexico, June 25, 2007
Third Generation Light Sources
1 2 3 4 5 6 7 8 9
1
10
100
MAX IISAGASAGA
Bessy IITSRF
ALS
CANDLE
PLSKazakhstan
TLS
NewSUBARU
LNLSSiberia II
ANKAIndus II
SESAME
CLS
ELETRRA
SLSSoleil
SPEAR3
ASP
ALBASSRF
DiamondNSLS IITPS
MAX IV
ESRF
PETRA III
APS
Operational Commissioning Construction Planned
Emitt
ance
(nm
.rad)
Energy (GeV)
SPring8
PEP-X
Zhentang Zhao PAC07, Albuquerque, New Mexico, June 25, 2007
New Synchrotron Radiation Facilities
Zhentang Zhao PAC07, Albuquerque, New Mexico, June 25, 2007
New Synchrotron Radiation Facilities
Zhentang Zhao PAC07, Albuquerque, New Mexico, June 25, 2007
New Synchrotron Radiation Facilities
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
FromPEP-II
toPEP-X
Use of damping wigglers as in PETRA III to reach 0.1 nm.rad
Zhentang Zhao PAC07, Albuquerque, New Mexico, June 25, 2007
1 2 3 4 5 6 7 8 9
100
200
300
400
500
600
Operational Commissioning Construction Planned
ELETTRA
SLSPLS
Bessy IITSRF
ALS
CLSIndus II
Kazakhstan
SPEAR3ASP,CANDLE
MAX IV
TPS
Soleil
ANKA
TLS Siberia IINewSUBARU
ALBA
SESAME
SAGA LS
LNLS MAX II
Diamond
SSRF
Circ
umfe
renc
e (m
)
Energy (GeV)
3 4 5 6 7 8 9
1000
1500
2000
25003000
PETRA III
SPring8
APS
ESRFNSLS II
Third Generation Light Sources
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
CERN’s 27 km ‘tunnel with a future’
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Top-up injection: key to stability
TOP-UP INJECTION
TIME
ELEC
TRO
N IN
TEN
SITY
also Trickle Charge cont. Injection at PEP-II, KEKB
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Top-up is key to the source stabilityConstant thermal load on:
• Beam line optics• Accelerator components (BPMs, vacuum chamber…)
Tunnel Temperature [0C] 25 ± 0.03
average Temperatures of the 5 Sectors
25.4
25.3
25.2
25.1
25.0
24.9
24.8
24.7
1 day
0.050average Temperatures of the 5 Sectors
σx
Beamsizes σx σy [µm]
σx
σy
1 day
Vertical emittance εy → 4 pm-rad; coupling εy/εx ~ 0.08%
Beam lifetime ~7h, not relevant! Injection every 1.5 min
1 μm
Diffraction limit @ 1 Å
Damping Rings beam emittances
30
ATFachieved
ILC
ATFDesign
SLC
CLIC DRdesign
CLIC 500 GeVCLIC
3 TeV SLS
NSLS IIscaled
0.001
0.010
0.100
1.000
10.0000.1 1 10 100
Horizontal Emittance (μrad-m)
Vert
ical
Em
ittan
ce (
μra
d-m
)
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
H. Ohkuma, JASRI/SPring-8, EPAC08
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Top up vs. top offWhich definition?
top off vb.
(tr., adv,) to finish or complete, esp. with some decisive action: he topped off the affair by committing suicide.
top up vb. (tr.,adv. ) Brit.
1. to raise the level of (a liquid, powder, etc.) in (a container), usually bringing it to the brim of the container: top up the sugar in those bowls.
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Protein structure
N. Ban et. al.
Part of a Ribosome
Diffraction pattern
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Spectacular growth of structural biology
35’000
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Nobel Prizes in Chemistry to Synchrotron Radiation Work in Protein Crystallography
1997 John E. WalkerStructure of F1-ATPase
2003 Roderick McKinnonStructure of Cellular Ion Channels
2006 Roger D. KronbergStructure of RNA polimerase
Transverse coherence
• High brightness gives coherence
• Wave optics methods for X-rays(all chapters in Born & Wolf)
• Holography
phase contrast imaging
The knee of a spider
J. Gobrecht, SLS-SAC Meeting,11 July 07
Lithographic Performance
MNE 06, Ekinci et al
20 nmHSQ
CALIXARENE
12.5 nm
EIPBN 06, Solak et al
period=35.3 nm (516 Gbit/in2 )
• Worldwide highest resolution in photon-based lithography
• Field size: up to 2x2 mm2 (Achromatic Talbot)
• High throughput: ~10’000x e-beam
• Quality, reproducibility: enabling industrial operation
EIPBN 07, Solak et al
CALIXARENE
Fundamentals:Stable, coherent sourceShort wavelength (13.5 nm)No proximity effect (electron mean free path <1 nm)
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Main R&D directions
o Approaching diffraction limit: very small equilibrium emittance with large rings and damping wigglers
o Short period (small gap) undulator developments
o Detector development complementing source improvements
o Linac based light sources development: ERLs
o Free electron lasers developments
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
X-ray phase contrast imagingusing a shearing interferometer based on microfabricated silicon diffraction gratings
Phase-object example:100µm and 200µm styrene beads
Tomographic phase reconstruction of a spider
Advantages:significantly enhanced contrast compared to conventional "absorption-mode" for light materials
High potential in medical diagnosis and research
C. David, T. Weitkamp
F. Pfeiffer et al., PRL 94, April 2005
User OfficeX-ray Radiography of a fish
conventional Absorption a(+ details c , e, g)
Phase contrast Microscopy b(+ details d, f, h)
(F.Pfeiffer)
User Office
Franz Pfeiffer Coherent X ray
phase contrastabsorption
17.5 keV,synchrotron results
Into the hospital ?
(C.David, F.Pfeiffer)
Franz Pfeiffer – Super-Resolution STXM
Lensless coherent Scanning Microscopy with hard X-rays
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Ultrafast X-ray science
X-ray Free Electron Lasers extend the ultrafast laser techniques to the X-ray domain
„Seeing“ structures evolving with time as phenomena take place
FEMTO: Slicing technique at synchrotrons
Similar technique to reach < 1 fs with XFELs
„If you want to understand function,study structure“
Francis Crick
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
harpo10-27
yocto10-24
milli10-3
micro10-6
nano10-9
pico10-12
femto10-15
atto10-18
zepto10-21
Ultrafast lasers
SynchrotronsLaser plasmas
XFEL’s
Current lasers:
X-ray sources:
Science:Acoustic phonons
Vibrations (Optical phonons) Chemistry and BiochemStrings,
CosmologyParticle Collisions Electron dynamics
Ultrafast Sources and Science
J. Hastings
Laser slicingPioneering ideas and experiments at ALS
Facilities at ALS, BESSYII, SLS
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Dynamics on atomic scale visible with ultra-short X-ray pulses
Phys. Rev. Lett. 99, 174801 (2007)
First optical experiment with atomic resolution:
Amplification and dampingof lattice vibrations
FEMTO
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Main R&D directions
o Approaching diffraction limit: very small equilibrium emittance with large rings and damping wigglers
o Short period (small gap) undulator developments
o Detector development complementing source improvements
o Linac based light sources development: ERLs
o Free electron lasers developments
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Energy Recovery Linac SchematicSingle pass: emittance and energy spread are determined by injector, can be much smaller than in storage ring
Ch. Sinclair, Cornell
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Main R&D directions
o Approaching diffraction limit: very small equilibrium emittance with large rings and damping wigglers
o Short period (small gap) undulator developments
o Detector development complementing source improvements
o Linac based light sources development: ERLs
o Free electron lasers developments
COHERENT EMISSION BY THE ELECTRONS
INCOHERENT EMISSION COHERENT EMISSION
Intensity ∝ N Intensity ∝ N 2
WAVELENGTH
MUCH HIGHER BRIGHTNESS CAN BE REACHED WHEN THE ELECTRONS COOPERATE
INCOHERENT EMISSION COHERENT EMISSION
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
From rings to linear accelerators
o The number of beamlines served simultaneously
o The stability of the rings based sources
o High average brightness
- Fewer beamlines
- Very short pulses, single shot measurements
- High peak brightness
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
European XFELDESY 2013
1 km
JapanSCSS – SPring8 2010
X-FEL facilities
USALCLS – SLAC 2009
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
1035
1025
1015
10 ps 100 fs 1fs
Slicing
ERLs
X-ray FELs atto…
2G rings
3G rings
Peak
Bri
ghtn
ess
Pulse duration
FELs and ERLs COMPLEMENT the Ring sources
H.-D. Nuhn, H. Winick After H.-D. Nuhn, H. Winick
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Structure determination of single molecules before the Coulomb explosion
H. Chapman(2007)
Peak brightness of the FELs
courtesy T. Shintake
X-Ray
~109 103 by e− quality, long undulators
106 by FEL gain
1 Å
photons per phase-space volume per band-width
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Main R&D directions
o Approaching diffraction limit: very small equilibrium emittance with large rings and damping wigglers
o Short period (small gap) undulator developments
o Detector development complementing source improvements
o Linac based light sources development: ERLs
o Free electron lasers developments
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Hybrid-Pixel Technology
Indium bump-bonding technology18um bumps
Si-sensor with pixelated pn-diode structure
CMOS chip technology,
Direct Detection of X-rays
Single Photon Counting
Frame rate ~ 1 kHz
X-rays
Spin-off company from PSIC. Brönnimann, et al
Cutting-edge 2D pixel detectors
Advanced detectors: collaboration with HEP detector groups
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Further reading
X-ray sources, ICFA Seminar, SNAL, October 2008, L. Rivkin, PSI & EPFL
Summary
Strong growth in ring based supply continues
Complementary laser-like X-ray sources for atomic
resolution studies: lots of learning to do
Linac based sources for ultra-fast X-ray science
Detector development is crucial
Sample damage: a problem looking for a solution