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1 L \ YIELDING OF A SENSITIVE CLAY AT LOW CONFINING PRESSURES

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L

\

YIELDING OF A SENSITIVE CLAY AT LOW

CONFINING PRESSURES

AUTHOR: Vincenzo Silves tri

TITLE OF THESIS: Yie1ding of a Sensitive Clay at Low Confining

Pressures

DEPARTMENT: Civil Engineering and App1ied Mechanics

DEGREE: Master of Engineering

SUMMARY

The aim of this study is the ana1ysis of comp1ex deformations in

a sensitive clay subjected to composite stress fields. The yie1ding

of this clay is investigated at 10w confining pressures, where it is

be1ieved that the soi1 response is marked1y inf1uenced by the nature

of the interpartic1e bonding forces. The physica1 mechanisms govern-

ing the behaviour of this clay are examined and discussed in view of

experimenta1 findings.

It is shown that this clay behaves as a britt1e mate rial in the

10w confining pressure range, not obeying a frictiona1 strength cri-

terion. Extrapolation of strength theories used for remou1ded c1ays

to the assessment of this undisturbed sensitive clay cannot be done.

It is a1so shown that the behaviour of this clay is dependent upon

the intermediate principal stress.

This study constitutes the first phase of a continuing investi-

1 \

1\ gation of bond effects on natura1 clay soi1 behaviour.

o

YIELDING OF A SENSITIVE CLAY AT LOW

CONFINING PRESSURES

by

Vincenzo Silvestri

A thesis submitted to the Faculty of Graduat.e Studies

and Researeh in partial fulfilment of the

requirements for the degree of

Master of Engineering

July, 1969

Department of Civil Engineering and Applied Mechanies

McGill University

Montreal, Canada

cv Vincenzo Silvestri 1970

- i -

ABSTRACT

The aim of this study is the analysis of complex deformations in

a sensitive clay subjected to composite stress fields. The yielding

of this clay is investigated at low confining pressures, where it is

believed that the soil respon5e i5 markedly influenced by the nature

of the interparticle bonding forces. The physical mechanisms govern-

ing the behaviour of this clay are examined and discussed in view of

experimental findings.

It is shown that this clay behaves as a brittle material in the

low confining pressure range, not obeying a frictional strength cri-

terion. Extrapolation of strength theories used for remoulded clays

to the assessment of this undisturbed sensitive clay cannot be done.

It is also shown that the behaviour of this clay is dependent upon the

intermediate principal stress.

This study constitutes the first phase of a continuing investiga-

tion of bond effects on natural clay soil behaviour.

Il

- 11 -

ACKNOWLEDGEMENTS

The author wishes to express his gratitude to Dr. R. N. Yong for

his guidance and encouragement during the course of the work. He is

indebted to Dr. E. McKyes for his advice and cooperation in the optical

study program, to Dr. R. L. Sloane for his aid in the X-ray diffraction

analysis, and to Mr. B. Cockayne for technical help. In addition,

thanks are due to Miss N. E. Boyce for the typing of this thesis.

The author wishes to acknowledge the financial assistance provided

by the National Research Council of Canada.

This study is part of the cooperative investigation on stability

of natural clays being undertaken between various Eastern Canadian

universities.

The samples of Leda clay were obtained through the cooperation of

Dr. P. LaRochelle, Professor of Civil Engineering, Laval University,

Quebec, to whom the author is most grateful.

- iii -

, TABLE OF CONTENTS

ABSTRACT i

ACKNOWLEDGEMENTS ii

TABLE OF CONTENTS iii

LIST OF FIGURES v

NOTATIONS viii

CHAPTER l INTRODUCTION 1

1.1 The General Problem............................ 1

1.2 Aim and Scope of the Present Study............. 2

CHAPTER II PRESENT STATE OF KNOWLEDGE 5

2.1 Mechanism of Shearing Resistance............... 5

2.2 Yie1ding of Sensitive C1ays.................... 8

2.3 Failure .. tt ••••• tt ••••••••••••••• tt tt. tt. tt •••• 15

2.4 Questions Arising in the Analysis of Leda Clay. 20

CHAPTER III LABORATORY INVESTIGATION 22

3.1 Experimentation................................ 22

3.2 Materia1 Characteristics................. .•. •.• 23

3.3 Testing ·Technique ...•.. tt ••• tt tt ••••• tt ••• tt tt. 26

3.3.a. Triaxia1 Test Programme................ 26

3.3.b. Optica1 Studies. .•••• •••.•.••• •••. .•••• 27

CHAPTER IV EXPERIMENTAL RESULTS 28

4.1 Faiiure........................................ 28

4.2 Stresses and S trains. . • • • • • • • . • • • • • • . . • . • . • • • • • 31

- iv -

4.3 Yield Surfaces................................. 33

4.4 Yielding Analysis.. .••... ••.•.••........• .•..•. 33

4.5 Results of Optical Studies..................... 41

CHAPTER V DISCUSSION OF RESULTS 49

5.1 Yield Behaviour................................ 49

5 • 2 Fa i 1 u re . . . . . . . • . . . . . . • . • • . . . . . . • • . . • . . . . • . . . . . • 52

5.3 Comparison and Analysis of Related Work........ 53

5.4 Field Correlation.............................. 59

CHAPTER VI CONCLUSIONS 61

6.1 Conclusions.................................... 61

6.2 Suggestions for Further Research............... 62

APPENDIX A TEST RESULTS 64

APPENDIX B PRINCIPAL STRESS SPACE METHOD 70

APPENDIX C GEOLOGICAL HISTORY OF LEDA CLAY 75

APPENDIX D OPTICAL METHOD 80

LIST OF REFERENCES 83

1

- v -

ill! QE. FIGURES

Title

Figure 2.1 Schematic Clay Structures (Yong and

Warkentin, 1966) 7

Figure 2.2 Influence of Structure on Stress-Strain

Relationships 11

Figure 2.3 Physical, Stress and Strain Spaces 13

Figure 2.4 Stress and Strain Increment Vectors on Octa-

hedral Planes (McKyes, 1969) 14

Figure 2.5 Mohr-Coulomb Envelopes and Experimental Test

Results 17

Figure 2.6 Mohr-Coulomb Failure Envelopes 18

Figure 2.7 The Influence of Structure on the Strength

Behaviour of Clays (Kenney, 1968) 19

Figure 3.1 Loading Apparatus 24

Figure 4.1 Mohr-Coulomb Plot for the Drained Triaxial Tests 29

Figure 4.2 Failure Stresses Plotted on a Reduced Octahedral

Plane 30

Figure 4.3 Typical Stress-Strain Diagram 32

Figure 4.4 Octahedral Shear Stress-Strain Relationship,

<Je = 2.5 psi 34

- vi -

Title

Figure 4.5 Octahedral Shear Stress-Strain Relationship,

Œe =5.0psi 35

Figure 4.6 Octahedral Shear Stress-Strain Relationship,

cre = 10.0 psi 36

Figure 4.7 Successive Yield Stresses Plotted on Reduced

OGtahedral Planes 37

Figure 4.8 Octahedral Shear Stresses at Equa1 Strains vs.

Octahedral Normal Stresses for Drained Tests 39

Figure 4.9 Octahedra1 Shear Stresses at Equal Strains vs.

Consolidation Pressures for Undrained Tests

(McKyes, 1969) 40

Figure 4.10 Reduced Stress-Strain Relationship 42

Figure 4.11 e - log P Curve 44

Figure 4.12 Microphotographs of Thin Sections Taken from

Natura1 Clay Samples 45

Figure 4.13 Microphotographs of Thin Sections Taken from

Consolidated Clay Samp1es 46

Figure 4.14 Microphotographs of Thin Sections Taken from

Failed Clay Samples 47

Figure 5.1 Mohr-Cou10mb Plot for the Consolidated Drained

Triaxia1 Tests (Con10n, 1966) 55

Figure 5.2 Failure Stresses and Stress Paths 57

- vii -

Title Page

Figure 5.3 Limiting Circles of von Mises Behaviour

(McKyes, 1969) 58

Figure B-l Geometry of Principal Stress Space 71

Figure B-2 Common Reduced Right Section 74

Figure C-l Clay Structures (Lambe, 1953) 78

Figure C-2 Schematic Picture of Clay Network 79

Figure D-l Interference Co1our Interpretation 82

b

c

c'

e

s

v

(1

(2 (3

(oct O'oct

° Oc

°1 CJ2 Œ3

Œoct Œ~ flJ ~'

_,.i .•

- viii -

NOTATIONS

cohesion intercept with respect to drained conditions

cohesion intercept with respect to effective conditions

void ratio

first stress invariant = 01 + 0"2 +Œ3 pressure

shear strength

volume

increment

strain in the major principal stress direction

strain in the intermediate principal stress direction

strain in the minor principal stress direction

normal octahedral strain

octahedral shearing strain

normal total stress

consolidation pressure

major principal stress

intermediate principal stress

minor principal stress

normal octahedral stress

effective normal stress

angle of internal friction under drained conditions

angle of internal friction with respect to effective

parameters

® ,)::i

(0" """1, ..

\::

"t'oct l:'*

psi

t/m2

t/ft2

TSF

- ix -

shear stress

octahedral shear stress

reduced octahedral shear stress

pounds per square inch

tons per square meter

tons per square foot

tons per square foot

- l -

INTRODUCTION

1.1 ~ General problem

In the study of sail mechanics it is evident that greater atten-

tian must be paid ta the problem of sail behaviour. One of the reasons

for this development is the increasing knowledge of the influence of

physico-chemical factors in governing the response of the sail.

Another reason is the need ta better understand the behaviour of clays

subjected ta external constraints.

When studying clay behaviour, it is necessary ta differentiate

between undisturbed and remoulded soils. Undisturbed clays generally

display greater structural influences than others because of the

arrangement of the sail particles and the nature of the interparticle

forces. Many undisturbed clays can be regarded as possessing strong

interparticle bonds arising from cementing agents, such as carbonates

and oxides, whereas completely remoulded clays lack these bonds and

exhibit different mechanical properties. The magnitude of structural

effects on the strength of an undisturbed clay is reflected in part by

its sensitivity, that is, the ratio of undisturbed ta remoulded

strength.

Leda clay of Eastern Canada has a strong, brittle structure which,

when disturbed, loses virtually aIl rigidity and the clay flows like a

- 2 -

viscous liquide The ability to lose strength on remoulding can be

partly explained by the open, bonded cardhouse structure of the clay,

and partly by its geological history (Crawford, 1963). More detailed

information regarding Leda clay is presented in Appendix C. The

unusual features displayed by the clay, namely, its compressibility

and high sensitivity, concern the engineer since they confront him

with specifie problems of slope stability, settlement predictions and

foundation design.

Slope failures in sensitive Leda clay are often catastrophic and

occur with sudden movemcnts (Eden, 1956; Bilodeau, 1956). Investiga-

tion of these slides has indicated that the clay is usually character-

ized by low friction angles, high cohesion, and low in-situ stresses.

These phenomena have suggested the inadequacy of the classical strength

theories in interpreting the behaviour of sensitive clays. Also, the

stage has not been reached when the shear strength of a soil can be

expressed in terms of physico-chemical properties of the soi1 parti-

cles and the pore fluide The c1assical strength theories of soil

mechanics cannot be used to estimate, with reasonab1e accuracy, the

minimum strength requirements. A1though they have been used, with

sorne success, for remoulded soi1s, the extent to which they can be

applied to undisturbed sensitive clays is in doubt (Crawford, 1963).

1.2 ~ ~ Scope of the Present Study

Recently, a program was begun by severa1 Eastern Canadian

universities to perform a detai1ed ana1ysis of tae response behaviour

& ..... ' ~

- 3 -

of Leda clay. The present study is part of this cooperative investi-

gation undertaken to assess fundamental properties of natural so1ls

and to interpret the soil response in view of the above properties.

The aim of this investigation is to study the behaviour of a

sensitive clay subjected to complex stress states and under low con-

fining pressure conditions. This study includes the influence of the

intermediate principal stress on the yielding of such a material, in

view of the scarcity of conclusive data on the behaviour of undisturbed

natural clays.

Investigation of the behaviour of Leda clay, under conditions

similar to those existing in the field, allows one to obtain rational

strength parameters. For example, in large slope failures, plane

strain conditions often prevail, whereas in small landslides, complex

stress states exist, and the ability to reproduce in-situ conditions

allows one to obtain meaningful results.

The apparat uS used to determine the strength parameters in this

study was designed to reproduce general field conditions, that is, it

provided three principal stresses that could be varied independently

of each other.

In this study, confining pressures ranging from 2.5 to 10 psi are

used. Since these pressures are well below the preconsolidation pres-

sure of the tested soil, it is possible ta study the influence of the

interparticle bonds on the yielding of the ciay and to simulate low

confining pressure conditions of landslide situations. Undisturbed

clay samples were obtained from a site where a slope failure had

- 4 -

occurred, through the cooperation of Dr. P. LaRochelle, Professor of

Civil Engineering, Laval University, Quebec.

The data are presented on principal stress space where a direct

comparison may be made between the experimental results and sorne of

the classical strength theories.

A complementary research program performed in this investigation

involves the study of clay fabric by means of a polarizing microscope

and subsequent interpretation of interference colours obtained.

Undisturbed, consolidated and failed clay specimens are used, and

changes in clay fabric are related to changes in mechanical proper-

ties.

The intent of this study is to increase the present knowledge of

the properties of sensitive clays and provide further insight into

the contribution of natural bonds to the behaviour of sensitive clays.

- 5 -

CHAPTERll

PRESENT ~ OF KNOWLEDGE

Unlike otber materials, tbe strengtb and deformation of cohesive

soils cannot be defined in terms of simple properties such as yield

strengtb and elastic modulus. The nature of tbe clay-water system

renders it difficult to estahlish a unique strengtb criterion. Since

clay soils are not ideal materials and their bebaviour is neitber

elastic nor plastic, it is difficult to apply conventional theories

of mechanics to analyze the sbear strength of a soil.

2.1 Mechanism of Shearing Resistance

In spite of tbe advancement in tbe knowledge of soil physics, it

is impossible to exactly describe tbe mechanisms that resist shear in

an undisturbed clay specimen.

An understanding of the shearing bebaviour of natural clays

requires: ·(a) knowledge of the way in which clay particles interact,

(b) information about the role of water and diffused ions in governing

the nature and distribution of interparticle forces, and (c) knowledge

of possible cementation (or natural) bonds.

A fundamental appreciation of the physico-cbemical properties is

of utmost importance for a better understanding of the deformation and

strength characteristics of clay soils.

®'" ",f.:.:.,' .'

- 6 -

Investigations of this problem by Lambe (1953, 1958) and Rosenquist

(1959, 1962) have clarified the influence of physico-chemical factors

upon the mechanical behaviour of clays. Canadian clays in particular

have been studied by Crawford (1960, 1963), Penner (1963), and Quigley

and Thompson (1966). These authors agree on the fact that the sensi-

tivity of Leda clay de pends upon the brittle, bonded cardhouse struc-

ture of the clay. However, no one has yet subjected this clay to

complex stress states; therefore, it has been impossible to obtain the

complete yield response under varying intermediate principai stress.

The arrangement of clay particles and the interactions among the

solid and liquid phases determine the response behaviour of a clay

soil, that is, the response of the soil to an external set of con-

straints. This geometrical arrangement of mineral particles, called

fabric, together with the associated interparticle forces is generally

defined as the structure of the soil (Yong and Warkentin, 1966). The

concept that clay platelets are surrounded by double water and ion

layers has been accepted by most researchers in the field of soil

mechanics. These adsorbed and partially bound layers primarily serve

to transfer and distribute the electrical forces between the clay

particles, and the nature of the interstitial fluid is of primary

importance to this role.

During shear, interparticle bonds are broken, and particles become

semi-oriented and any force resisting this movement contributes to the

shear strength of remoulded clay (Figure ?l).

The physical mechanisms governing the behaviour of clay soils are:

Structural Bonding \

- 7 -

(0) Undisturbed

Clay Particle

Potential Failure

Plane

Q) c o

~ ~ ~j ----o~-~r__\ --- ~---__ ~CEl~~c=:.? ____ c:::;s. ___ _

o c:::::::::::r "' c ;;) ~ ~ c - c:::::::J ::) ~

Developed Failure

(b) After Sheoring Plane

Figure 2-1. Schematic Clay structures (Yong and WorkentinJ 1966)

- 8 -

1. sliding resistance between particles, and

2. interlocking between particles

However, in a clay-water system, the interaction of clay particles is

such that there is a minimum of actual physical contact between par-

ticles (Yong and Warkentin, 1966). It is believed that the water film

surrounding the clay plate lets yields plastically when the particles

are pushed together with Little or no deformation of the actual par-

ticles. In the light of these concepts, sliding resistance can no ~'

;,1' "

>~

longer be accepted as resulting from particle contact; rather, a more

satisfactory concept of shearing resistance must be developed in such

a way as to take into account the phenomena Just described.

In addition, under low pressures, the shear strength of sensitive

clays is almost totally composed of cohesion. Cohesion may be regarded

as the integral adhesion, because it represents the attraction between

particles in "contact".

The above phenomena govern the response of undisturbed clays. That

is, they determine the yielding and failure behaviour of sensitive

clays subjected to applied external constraints.

2.2 Yielding of Sensitive elays

When investigating yielding and failure of sensitive clays, it is

necessary to differentiate between these two terms. For example, the

failure of brittle mate rials occurs as a fracture with resulting dis-

continuous areas of deformation. Thus "fracture" can be identified

- 9 -

with "failure", while yield is used to describe the onset of irrecover-

able, uniform deformations.

When a'material is subjected to increasing loads, the resulting

stress will eventually become high enough to cause the solid to yield

and, finally, to fail. In most metals, if the state of stress is

uniaxial, it is often easy to specify a unique yield point. However,

if a complex stress field is acting, what combination of .these stresses

will cause yield? It is known, for example, that in most metals a

hydrostatic stress, that is, equal stresses in all directions, will not

cause yie1ding, even for very large values of the confining pressure.

The criteria for deciding which combinat ion of multiaxial stress will

cause yie1ding are called yie1d criteria.

For most metals, a stress-strain re1ationship is characterized by

an initial e1astic stage, followed by irrecoverable plastic deforma-

tions at higher stresses. On1y when there is a sharp "break" in the

stress-strain curve can yie1d be easi1y defined.

On the other hand, cohesive soils are characterized by nonlinear

stress-strain curves. C1ays undergo irrecoverable deformations at

very low stress 1eve1s, and thus their stress-strain re1ationships may

be regarded to represent a succession of yie1d points. Further, in

clay soi1s, where interparticle forces control the soil response, the

stress-strain curves are genera1ly time-dependent. Thus an analytical

description of yie1d or failure of a cohesive soil must take al1 these

factors into account.

Considering the deformation characteristics of sensitive c1ays,

it has been proposed by Go1dstein and Ter-Stepanian (1957) that

~ ~

- 10 -

interparticle forces be divided into two groups, one producing brittle

bonds which permit elastic deformations and then fail, and the other

forming viscous bonds, which break under stress, and reform as the

shearing process continues.

As was previously noted, there are indications that at the con-

tacts between particles of certain c1ays there are strong cemented bonds

(Lambe, 1960; Quig1ey and Thompson, 1966). These bonds act as if they

were britt1e materials, perhaps crysta11ine in nature, and cause sensi-

tive clays to be characterized by high shear strengths at 10w strains.

The maximum shear strength occurs when the bond strength is fully mobi-

1ized and this develops at 10w strains because of the brittle nature of

the cementing agents. Beyond the maximum strength further breakdown of

the cementation bonds occurs with increasing strains. Figure 2.2 illu-

strates the stress-strain response of a sensitive clay and of a

remou1ded or unbonded clay.

A mechanistic understanding of the reasons for the behaviour of a

sensitive clay can be deve10ped by inspection of the nature of the clay-

water interaction. The bonded clay is re1atively stiffer up to point A,

where a structural breakdown occurs and large deformation starts to

develop. As the stress leve1 is increased, partial or total breakdown

of the bonds occur because of the internal complexities of the soil

structure, causing bending, tension, and shear stress. When the soil

structure is subjected to a shear stress, failure of the cementation

bonds is most likely to occur due to the tensile stress resulting

from: (a) bending at the contact points, (b) diagonal tension due to

shear stress, and (c) direct tension due to local dilatations (Conlon,

- 11 -

Sensitive Clay

\ Remoulded Clay

Strain

Figure 2-2. Influence of Structure on Stress-Strain

Relationships

- 12 -

1966). Thus the shear strength of a soi1 structure deve10ped in this

way may not be adequate1y defined by c1assical frictiona1 shear

fai1ure theories.

Remou1ded c1ays, on the other hand, behave different1y. There is

no concentrated breakdown of bonds, rather a progressive breaking

occurs, and these bonds can be identified as the viscous bonds that

break under stress and reform continuous1y as partic1es more relative

to each other.

As discussed in Chapter l, it is desirab1e to investigate the

influence of the intermediate principal stress on the yie1d behaviour

of Leda clay. lt was mentioned that the c1earest way of summarizing

the resu1ts was to show yie1d and fai1ure surfaces in principal stress

spaces. To i11ustrate these spaces, schematic diagrams showing the

re1ationships between stresses and strains in physica1 and stress-

strain spaces are shown in Figure 2.3.

Little is known about tbe behaviour of sensitive c1ays at 10w

stress 1eve1s. McKyes (1969) has shown that, for remou1ded kao1inite,

the von Mises criterion cou1d we11 represent the yie1d behaviour of

the materia1, at 1east up to a certain octahedra1 shearing strain. The

experimenta1 resu1ts obtained by McKyes (1969) are shown in Figure 2.4.

At tbe present time the comp1ex deformation characteristics of

natura1 c1ays subjected to 10w stress 1eve1s are not weIl understood.

In sensitive c1ays interpartic1e bonds may al10w the shear strength

in tension to be equa1 to that in compression, at 1east for 10w

strains and, perhaps, at 10w confining pressures (Con10n, 1966;

Townsend, 1966). lt is weLl known that most sensitive c1ays are

y - 13-

4&---q,e" x (0) Physical space

z

(b) Stress space

Space diagonal ( €'.-=E:1= e, )

€o,t =~ ( ~+ e,+ e, ) ~

t.. =~~e;-E:.l'+k;t;)~(E:;€) J • jIt:-----------..€1

(c) Strain space

Figure 2-3. Physical J Stress and Strain Spaces

@,.{': . ' .•. ' . ..

q-::30 psi

1" = 5 psi

0(=5pSi, 1": 2.67psi

O"c-::60 psi 1" = 10 psi

- 14 -

Q1'€1

cre.:: 45 psi

1" = 10 psi

Legend

+ I~ "t d Ooct oct

~

Limiting Circles of Levy-Mises

Behaviour

Figure 2-4. Stress and Strain Increment Vectors on Octahedrol Planes(McKyes,1969)

- 15 -

relatively stiff and are characterized by brittle behaviour (Crawford,

1963).

2.3 Failure

The Coulomb equation,

l = c+utan% (1)

where

~= shear strength,

C = cohesion,

(j= normal stress, and

r6= friction angle

has been applied with sorne success to remoulded soils (Bishop, 1966).

However, the extent to which it can be used to represent the state of

failure of undisturbed, sensitive clays is in question. Recently, doubt

has arisen about the adequacy of this classical theory in the prediction

of the shear strength of both undisturbed and remoulded clays. For

instance, Shibata and Karube (1965), and Henkel and Wade (1966) have

reported deviations from the Mohr-Coulomb predictions, for remoulded

clays under complex stress states, due to the influence of varying

intermediate principal stress. But Wu, Loh and Malvern (1963), Bishop

(1966), and McKyes (1969) have shown that the Mohr-Coulomb criterion

could quite closely represent the failure condition of remoulded clays.

- 16 -

Sorne of these experimental results, plotted on deviatoric planes in

principal stress space, are shown in Figure 2.5.

In general, most researchers agree that the Mohr-Coulornb criterion

has been reasonably well supported by experiments in the case of re-

moulded clays, with small deviations sometirnes developing when an

intermediate principal stress is acting.

However, the Mohr-Coulomb criterion has not been found valid for

many natural clays. Conlon (1966) and Kenney (1968), for example,

have reported failure envelopes of the forro illustrated in Figure 2.6.

Their study included both Scandinavian and Canadian sensitive clays.

These authors believe that the deviations from the Mohr-Coulomb cri-

terion, occurring at low pressures, are due to natural bonds. In

fact, at confining stresses below the soil preconsolidation pressures,

it would seem that the soil response is greatly affected by the

brittle nature of the bonds. As the confining pressure is increased,

partial or total breakdown of the structural bonds occurs, and the

behaviour of the clay approaches that of a remoulded (or unbonded)

clay, characterized by a straight failure envelope (Kenney, 1968), as

shown in Figure 2.7.

Sorne investigators have reported fracture-type of failure in

natural clay slopes. For instance, Collins (1956) advocates the Tresca

1 criterion or a modified forro could represent the yi.elding and failure

behaviour of sorne natural elays sinee the physical considerations

agree with the mathematical requirements.

Consider the physical aspects. At very low stress levels, the

® .. ........ '.

behaviour of sensitive clays is governed by the cementation bonds, and

(/)' = 320 •

c'=o •

- 17 -

r:/J '= 33.70

0

c'=0.3psi

0""3

WU,Loh and Malvern(1963) Shibataand Karube(1965)

1J'=25.BO

c': 0

Henkel and Wade (1966)

Figure 2-5. Mohr-Coulomb Envelopes and Experimental

Test Results

- 18 -

5 LOdalen

4 Minimum strength ~ N 5/0'-0.6 E 3 " -t-J ~

l-'2

1

°0

tI) a.

1

160

~ 80 l-'

n

_Seines ~G"t ~Dra~~en .,;t Ulle nsake r X Vormsund

Naddum

2. 3 4 5 (3 1 2 an) t/m

1 •

an) PSI

Conlon(19GG)

Kenney(19GS)

ç6:: 36°

Figure 2-6. Mohr- Coulomb Failure Envelopes

- 19 -

Figure 2-7. The Influence of Structure on the

Strength Behaviour of Clays

( Kenney ,1968 )

- 20 -

the clay behaves as a brittle material. Also, at confining pressures

below the soil preconsolidation pressure, the frictional resistance of the

clay is very small, and the shearing resistance is almost exclusively com-

posed of cohesion. According to Schmertmann and Hall (1961), the cohesion

component of peak strength in clays develops to its maximum value at very

low compressive strains, while the friction component requires a much

greater strain to reach its maximum value. Since sensitive clays fail at

very low strains, usually of the order of one to two percent, and if the

shear strength reaches a value close to the cohesion value, the clay will

suddenly fail. In addition, as cohesion arises mainly from brittle bonds

in the case of undisturbed Leda clays, the strength of these soils may be

the same both in compression and "extension" tests. However, once the bonds

are broken, the behaviour of these soils may be different and the failure

stresses may or may not correspond to the Mohr-Coulomb requirements.

Knowledge of the strength and deformation characteristics of

undisturbed clays is of utmost importance at low stress and strain

levels because these are the conditions which prevail in field problems

for which limited strains are allowed.

2.4 Questions Arising in ~ Analysis of Leda Clay Behaviour

Leda clay confronts the engineer with specifie, important prob-

lems of soil mechanics. Slope stability analyses, for example, are

among the most difficult problems occurring in this clay. In order

to apply any strength theory, one must first know if a specifie the ory

will provide accurate field predictions, and secondly, if the the ory

- 21 -

is va1id for the most genera1 conditions. Since genera1 stress condi-

tions require three unequa1 principal stresses acting at a point in the

materia1, then one shou1d use an experimenta1 device that wou1d satisfy

genera1 stress conditions, i.e. three principal stresses shou1d be

app1ied to clay specimens.

Then, experimenta1 yie1d and fai1ure surfaces cou1d be represented

in principal stress space and compared to c1assica1 strength theories.

A1so, by investigating the behaviour of Leda clay unàer conditions

of low confining pressures, yie1d and fai1ure surfaces are determined

for this range of pressures, where the influence of the original bonds

has the most effect upon the response of the soi1.

Other important factors that affect the behaviour of Leda clay

are its original structure and its changes in structure due to applied

stresses. A direct observation of the fabric of Leda clay a1lows the

assessment of mechanica1 properties. A1so, fai1ure planes may be

investigated, and the appearance of the fai1ure zone renders it

possible to determine the mode of fai1ure and the distribution of

stresses prior to and during fai1ure. In fact, a clay samp1e with a

single thin straight failure zone is characterized by a re1ative1y

uniform stress state (Yong and Warkentin, 1966).

Further, since the deformations in the three principal strain

directions cou1d be derived, the effect of the various stress combina-

tionson the generation of these strains cou1d be determined and corre-

1ated with the physica1 mechanisms invo1ved in the shear resistance of

Leda clay.

- 22 -

CHAPTER ru

LABORATORY INVESTIGATION

A series of triaxia1 tests invo1ving the application of three

variable principal stresses was performed on a sensitive Leda clay.

The object was to relate the response behaviour of the clay under a

comp1ex stress field to its physica1 characteristics, such as struc-

tura1 bonding and sensitivity. The presence of the intermediate

principal stress al10ws fai1ure and yie1d surfaces to be determined

for complex stress states. In addition, since a11 tests were performed

at 10w confining pressures, the shape of these surfaces cou1d be asso-

ciated with the physico-chemica1 properties of the soi1 in this impor-

tant range of stresses.

3.1 Experimentation

In most soil mechanics prob1ems, rea1istic solutions in terms of

stress and deformation characteristics have been difficu1t if not

impossible to obtain, even when idea1 behaviour was assumed. To improve

solutions, experimenta1 techniques must be deve10ped in such a way as

to obtain realistic prf!dictions of the response properties of the soil

and of the stress distribution within the materia1.

The triaxia1 10ading apparatus used in this study a110wed the

intermediate principal stress to be app1ied to a prismatic clay speci-

men in a manner simi1ar to that of Shibata and Karube (1965). Figure

- 23 -

3.1 presents a detailed view of the characteristics of the triaxial

cell assembly. The device included dial gauges to measure deforma-

tions in the major and minor principal stress directions. This cell

was used by McKyes (1969) to investigate the behaviour of remoulded

kaolinite under states of complex stresses.

The major principal stress was applied by means of a loading

frame, piston and top and bottom lucite caps. The intermediate prin-

cipal stress was applied by a pair of rubber membranes covered by thin

polyethylene sheets and encased in brass boxes. The membranes were

filled up with water and the polyethylene sheets were lubricated to

avoid any friction between the specimen and the membranes. Both the

cell pressure (or minor principal stress) and the intermediate prin-

cipal stress were maintained by self-compensating mercury pressure

systems (Bishop and Henkel, 1962).

It is necessary to mention that aIl tests were performed under

drained conditions, and that volume changes were recorded in order to

derive the strains in the intermediate principal stress direction.

By inspecting the clay samples after failure, it was found that

the sides, on which the intermediate principal stress was acting,

remained plane, indicating a uniform stress distribution throughout

the specimen.

3.2 Material Characteristics

The soil used in this study was a gray Leda clay from a deposit

near Quebec City, Quebec. Soil samples were taken in a recently

;...~

A- Semple B- Loading Platens C - Intermediate Pressure Boxes D- Sample Membrane E - Polyethylene Membrane F - Porous Stone G - Ceii H - Lateral Deflection Gauge

- 24 -

J - Intermediate Pressure Chamber

Figure 3 .. 1. L oading Apparatus

~L_ '""0_- "_0 ...... ....... ... ... . .............. " ..... , ..... • __ ... '''' .'o ... A • . =,."...~'-' ._ ... "'0 ........ lI. .• ~ ........... 0 .00 ..... ..5 ......... __ .. ....... _ ........... C1'3 .,1. ... _ ... 0 •...• .'._ ....... , ... oC _:.', ... j>, •. ~~." ...... c ... o: '.C .. ,> ....... !

- 25 -

failed embankment at a depth of 10 feet, 5 feet below the failure zone.

Undisturbed sampl~s of the clay were obtained through the cooperation

of Dr. P. LaRochelle, Professor of Civil Engineering, Laval University,

Quebec.

Presented in this section are the results of mineralogical and

standard engineering tests performed on this soil.

An X-ray diffraction study of the mineralogical content of this

clay revealed the presence of illite, chlorite and kaolinite, and of

lesser amounts of interstratified mica-like clays and vermiculite.

Non-clay mineraIs identified in the 2-micron fraction included feld-

spar (plagioclase) and quartz, and smaller amounts of amphibole.

The results of standard soil mechanies tests are summarized

below:

Natural water content

Apparent preconsolidation

pressure

Liquid limit

Plastic limit

Specifie gravit y

Gradation (~ finer by weight)

Silt size

- 0.06 mm

Clay size

- 2 micron

- 1 micron

64'f, .:!: 0.5'f,

1.6 TSF

2.80

100'f,

79'f,

60'f,

€;J,":.,:. ,-: .'&

'.

- 26 -

Sensitivity 80

Liquidity index 1.8

This clay is a good example of the type outlined in Chapter l,

which occurs widely across Canada, and confronts the engineer with

specifie problems in the Interpretation of slope stability and in

foundation design.

3.3 Testing Technique

3.3.a Triaxial ~ Programme

From 12 in. x 12 in. x 12 in. undisturbed clay blocks, specimens

measuring 4 in. x 2 in. x 1 1/2 in. were tri~~ed and installed in the

triaxial cell described in Section 3.1.

After installation in the apparatus, each specimen was consoli-

dated at a chosen confining pressure of either 2.5, 5.0 or 10.0 pounds

per square inch. At the end of the consolidation period, small loading

Increments were applied to the sample until failure occurred. The

ratio b ~cri~~-~)was constant for each test, and varied between

zero and one in the study. That is, cr~ varied between cr) and ~ ~

where a;:).. 0; ~ 0; This allowed the complete range of the inter-

mediate principal stress to be covered. Also, when observed on a prin-

cipal stress space, each lcading pa th appeared as a straight line

radiating from the hydrostatic axis.

The applied stresses chosen were such as to determine the yield

and failure envelopes of the soil over the entire l:ange of the inter-

- 27 -

mediate principal stresses. These stress surfaces could then be com-

pared to those obeying ideal behaviours, such as Mohr-Coulomb, von

Mises and Tresca criteria.

l.l.b Optical Studies

In order to investigate the fabric of undisturbed, conso1idated

end feiled cley semples, an optical method for the direct observation

of interference colours from clay thin sections was employed in this

study. This method was applied by Yong and Japp (1968) to study clay

fabric changes in relation to known app1ied pressures and by McKyes

(1969) to investi.gate the shape and thickness of fai1ure zones in

samples of remoulded kao1inite.

This technique, which is detailed in Appendix D, has the advan-

tages that it is possible to distinguish co10urs a litt1e easier than

1ight intensities without the use of a photometer. Lafeber (1968) has

pointed out that the photometrie method cou1d only be app1ied to an

elementary particle configuration, such as parallel orientation.

Thin sections of Leda clay were obtained from samp1es in which the

soil moisture had been exchanged with Carbowax 1000 in the manner des-

cribed by Mitchell (1956), and Yong and Leitch (1967). Microphoto-

graphs of these sections were then taken and interpreted in view of

the interference colour technique, as described in Appendix D.

- 28 -

CHAPTER IV

a EXPERIMENTAL RESULTS

Appendix A presents the test data obtained in this study.

4.1 Failure

The object in this section is to determine whether the Mohr-

Coulomb failure criterion adequately describes the rupture behaviour

of the sensitive bonded clay used in this study.

The results of standard triaxial tests performed on prismatic

clay samples are shown in Figure 4.1 on a Mohr diagram. In aIl cases,

including those of varying intermediate principal stress, failure was

characterized by the appearance of distinct slip zones in the samples

and sudden 1055 of bearing capacity. The inclination angle of the

failure lines was observed to vary between 45 0 and 550 • The Mohr-

Coulomb requires the slip lines to be inclined at an angle:

o 0 0 0 0

9 = 45 + "2 ~ 45 + 5 = 50

The failure stresses, including those of varying intermediate

principal stress, are presented on a reduced deviatoric plane in prin-

cipal stress space and are shown in Figure 4.2, according to the method

described in Appendix B. It should be emphasized that such a plot of

experimental results does not presuppose the validity of the Mohr-

~tr~~~~r~~1i\~ti{c~~1!}:~J'\~{;;·~'·}1;:;:~it";"'~~I;;J! '''.' .. ~i·<·t i"k"" , .... ~'.:r ... :o\ " ""~l' •• -., -ia ~~,..~. -. ~~~~~ •. ; .. :U~·_·~"1."'_'''''~' ___ '~''A __ ' __ ~ ___ ._,_.

@)"" .... ,.},,-~ .~.

(/) 0..

(/) (/) (l) L

-+-' lf)

L 0 ID .c lf)

20

10

0 0

ccot(t> = 26.3 psi

20

@',i h

-;-:'~'\.:-~ ~,,":;l'

Preconsolidation pressure

line

-=10 0

40 Effective Normal Stress ~ psi

Figure 4-1. Mohr- Coulomb Plot for the Drained Triaxial Tests N \0

- 30 -

von Mises 01

\

\ \

c=5 psi \ ~ , \

JZf=10.8° , \ \ ~ \ \ , , \ , ,

\ \ , Stress path ,

\ \

0;= °2 ,

\ \ , , '\ ~ ~ \ \ , , \ ,

',,\

Legend symbol Oë

• 2.5psi + 5.0 )( 10.0

Figure 4-2. Failure Stresses Plotted on a

Reduced Octahedral Plane

- 31 -

Coulomb criterion for various stress combinat ions but is merely a

convenient metbod for comparing test results witb classical tbeories

(McKyes, 1969).

Figure 4.2 sbows all tbe failure stress combinations on a common

deviatoric plane in principal stress space, togetber witb tbe Mobr-

Coulomb, Tresca, and von Mises failure surfaces. It is clear tbat tbe

Mobr-Coulomb p~edictions based on axially symmetrical strengtb tests

do not comprise a valid failure criterion. The test results sbow

deviations from tbe Mobr-Coulomb criterion similar to tbose obtained

by Sbibata and Karube (1965) for a remoulded clay.

4.2 Stresses ~ Strains

Typical principal stress difference-axial strain curves will be

sbown to illustrate tbe possible influence of tbe intermediate princi-

pal stress on tbe bebaviour of tbe clay. Sucb curves are presented in

Figure 4.3 for the test data of tbis investigation. It is clear from

tbis figure tbat for stress ratios, b, less tban one balf, tbe clay

response is to sorne extent influenced by tbe intermediate principal

stress. However, for higber values of tbe stress ratio, tbe clay

bebaves as a very stiff mate rial and is less affected by variations in

intermediate principal stress. Also, Figure 4.3 presents volumetric

strains as a function of the major principal strain. It is clear tbat

no conclusive evidence may be obtained since no significélnt pattern is

sbown. Tbis lack of conclusive data on tbe generation of volumetric

strains was observed tbrougbout ·tbe study.

16

12

(/) Q.

B ..

~ f

0 4

o

~ 0.4

......... c o CI)

~ 0.8 L Cl.

E o u -

- 32 -

Legend

symbol b=(a-Π)/(0 - q) ~ 3 1

• 0 + 1/4 t:l 1/2 x 3/4 0 1

1.0 2.0

o-c=2.5 psi

Figure4-3. Typical Stress-Strain Diagram

- 33 -

The relationships between octahedral shearing stresses and

strains, for all stress combinations, will be presented because:

(a) yield surfaces are directly derived from these curves, and (b) they

show the influence of the intermediate principal stress upon the yield

loci. These diagrams are shown in Figures 4.4, 4.5 and 4.6. Each dia-

gram shows that there is not a unique relationship for each respective

consolidation pressure; rather, considerable difference betwe~n the

curves occurs, depending on the stress ratio, b. In general, for higher

stress ratios, the clay shows a larger stiffness.

4.3 Yield Surfaces

The purpose of this section ia to de termine whether the yield

behaviour of Leda clay can be easily described by one of the existing

theories, such as the Mohr-Coulomb concept, tbe Tresca condition, or

the von Mises criterion.

Figure 4.7 shows successive yield stress surfaces on a common

reduced octahedral plane in principal str~ss space based on equal

octahedral strains, together with the Mohr-Coulomb, extended von Mises,

and extended Tresca theoretical surfaces, as described in Appendix B.

It is clear from this figure that no classical theory can adequately

describe the behaviour of Leda clay.

4.4 Yielding Analysis

Since it 18 well established that consolidation pressures

® @

8 1

b=3/4

r b, =1 b=O __ L

"'" rY / 6

(/) Legend Q.

-+-' 4 symbol b=(o; -~)/(a: -0;)

u • w 0 0 .p-

l-' + 1/4

2 [!J 1/2 )<. 3/4 0 1

O_Y~~~~~ 1

V- 01 3.0 tJ oct 1 10 4.0

Figure4-4. ()ctahedral Shear Stress-Strain Relationship J OC = 2.5psi

®;.~., ;, .. ;t~

-;;~ ; ,

(/) a. .. ~

u 0

~

10

8 b=3/4 b=1/4 b=O

6 Legend

symbol 4 ft

• -1-

0

)<

0

A '<[9

b=(Œ1.- ~)/(a:. - ~)

0 1/4 1/2 3/4

1

0' , , , , o 1.0 2.0 3.0 4.0

~/ .. oct) 0/0

Figure4-5. Octahedral Shear Stress-Strain Relationship)0(;=5.0psi

w V1

~i~1~~~~~~~~~3~:I~~i~~!· ... ~f;fi~;:;;J1l~~~it'li~tiliJ';~i,~;~~.~~·~~"'~"Jré·-{fflf.'?~Ew)({rr;~,.?; ... :,",tf!j?1;~(·~~i'Ç·\~1F!1~:::ir."'1i-\~~:~H':_\1i.r::~~w='1

~ l~)' ~

li) 0..

+-' u 0

t-Y

10

8

b =1/2 1

G

l b :1 Drfj

2~ ///;/ "-..., - \.;1

B~ ~

Legend

symbol b::(cr~ - ~)/(a,-o;)

• 0 + 1/4 t:l 1/2 )( 3/4 0 1

~.'.> ~

00 1.0 2.0 y; 01 3.0 4.0 o oct, 0

Figure 4 - G. Octahedral Shear Stress-Strain Relationship J CYc" =10.0psi

w 0-

- 37 -

(0) q= 2.5 psi (b) Œc=5.0pSi

(c) Oè -=10.0 psi Legend

-Tresca

-.-- von Mises ----- Mohr-Coulomb

• 0: =0.25 010 ott 0 ooç-t=O.50

03 x Oc,tt=O.75

Figure 4-7. Successive Yield Stresses Plotted on

Reduced Octahedral Planes

- 38 -

influence the relative stiffness of a clay material, then a plot of

'1: 0"1" Vs. 6'01.1" would show whether ~oc.'t has a consistent stiffening

effect on the material. McKyes (1969) has shown that initial confining

pressures have a linear stiffening effect upon the strength of a

remoulded clay tested in undrained shear. The difference between octa­

hedral and initial confining pressures in drained tests is that the

latter is an isotropic normal stress state, while the octahedral normal

stress is generally a result of an anisotropic consolidation stress

state. Nevertheless, it is probable that changes in clay stiffeness

may be related to the octahedral normal stress, ~O~~, acting in the

material. Figure 4.8 shows the procedure for obtaining such a relation­

ship. The experimental points lie approximately on straight lines ori­

ginating from a single point on the negative part of the abscissa. The

negative intercept is -26 pounds per squarp. inch, which coincides with

the value of - c cot tif (Figure 4.1). The straight Hnes indicate

that the stress-strain diagrams of Figures 4.4, 4.5 and 4.6 are similar

in shape and indicate that the octahedral shear strength (or stiffness)

of the clay increases linearly with octahedral normal stress. In order

to compare the above methods of presenting test results, that is, ~O'~

Vs. 601."'(; and "l.oc.-t Vs. bG ,the data obtained by McKyes (1969)

in undrained tests on a remoulded clay are shown in Figure 4.9.

With the results of Figure 4.9, an apprmcimation to the octahedral

stress-strain relationships for a11 consolidation pressures investigated

is obtained by using a new stress variable. This new stress variable

is defined as:

~l'",~~p.x~t:'!;r~~~l'::'·i1h"'.;r ,'!'-......... '.' -, ,.. '{ "':~~:.lt:_~L...:.:_,: .... ::>::~~.")·1m .... _t:.~."'"'7~~",-'_~·<~~"':.l.''''' ......... _ .... _____ _

e·· -t .. l'.s· •• <

Le~;Jend

• Yoct=·25%

x 0' oct = 1 %

0 ooct =4 0/0

-10

8

tIl a. .. "06 0

P

o

~)(

• • _ ... 10

Œoct J psi

_. ~ )( )f~

.tm\ ~

20

Figure 4-8. Octahedral Shear Stresses at Equal Strains vs. Octahedral Norma 1

Str'esses for Drained Tests

c...> \0

,~i1-t·-f:i~W{t;:f~!4;~~Î:~;~'!.t:~,~~·::~"..r)t~';O;·\f:'··~'·Y:"'1~ç:'<"." ·~"·If'·;'O<'~)';t5' .. · ... • " ... ,,' f ~." ••• ~ ... :, "," " ~.''" ......

t.?\ t~ @

40

30 -(oct ft~ psi

20r ~._. ~ ~ ooct ... _n. 0

1 10

1 1 O~~ n-0.1 010 -~

0 0 ~

0 -20 -10 0 10 20 30 40 50 GO

OC., psi

Figure 4-9. Octahedral Shear Stresses at Equal Strains vs. Consolidation

Pressures for Undrained Tests (McKyes J 1969)

- 41 -

(2)

where '"'G~ is the new stress variable, and 6ôc..~ is the octahedral

normal stress. This method is similar to that used by McKyes (1969)

to obtain a unique relationship bet\-1een r-t.,.:J#: and lo,--t:'. . Figure 4.10 shows the stress-strain relationship about which the

test results fall in a band of scatter. The reduction to a single

relationship implies that the behaviour of this clay may be approxi-

mately described by a von Mises criterion, at least for the higher

confining pressures. When observed on a common octahedral plane, this

yield surface is a circle, and Figure 4.7 (a, b, c) shows that, while

the observed experimental yield surfaces do not compare well with

circles at ~, = 2.5 pounds per square inch, circles become a more

reasonable approximation to the results at higher confining pressures.

4.5 Results of Optical Studies

As previously mentioned, this study involves the use of optical

means in order to investigate clay fabric. Clay fabric is defined as

the arrangement of soil particles, without including the associated

interparticle forces.

In this section, clay fabric will be presented and related to the

stress state of the soil. This relies on the interpretation of the

soil structure, based upon intuitive physical reasoning and in view of

Ff~~?'1j~;f!t~i~$a~~;st~~·p:;~'~'~>~\~~it~::t';~'."':"(7i~lI'·'·'. "tl*lb; '., ",. l' ' " « "3" "7- -

eD'··· t..- ;!' ~:.-,\.,

o + • o o

+ o + + _______ 0 +

~g

"0 ~ 0,08 o ~ ~ u

00

~ . o

Legend

symbol

o

+

oc 2.5 psi

5.0

• 10.0

©

o •

, , 00- 1 2 3 4

Yoct ) 0/0

Figure 4-10. Reduced Stress-Strain Relationship

.po­N

ft

- 43 -

previous studies on the structure of Leda clay.

The microscopie views which are of interest are those regarding

sections of undisturbed, consolidated, and failed clay samples. The

microphotographs of undisturbed and consolidated clay specimens should

be studied by taking into consideration the e-log p curve shown in

Figure 4.11. Pertinent views are presented in Figures 4.12 and 4.13.

Figure 4.12 shows a horizontal and vertical section of an undisturbed

clay sample, whereas Figure 4.13 presents similar views of a Leda clay

specimen consolidated to a pressure of 40 tons per square foot. A

direct comparison in clay fabric is achieved by considering both

figures.

lt has been shown that under high pressures, clay particles

become oriented (Quigley and Thompson, 1966). When viewed under pola-

rized light, these particles would optically act as one large particle

and, according to the method outlined in Appendix D, the field of

view appears uniformly red through a gypsurn interference plate. This

is clearly satisfied by Figure 4.13 for the consolidated Leda clay.

On the other hand, undisturbed clay samples, because of their

flocculated structure, would show mixtures of different colours.

Figure 4.12 presents such a case. The presence of darker and lighter

areas indicates the flocculated, open structure of Leda clay. This

finding agrees with the work of Mitchell (1956), Crawford (1963) and

Quig1ey and Thompson (1966).

In addition, sections of failed samples are shown in Figure 4.14.

These views present failure planes as single straight zones 15 microns

thick, and confirm the intuitive concept of Yong and Warkentin (1966)

i

1

l i

1 1 l ,

@, ... ~~ :.-: .,-.'

1.8

1.6 ....

1.4 r-

1.2 r-(!)

0 -t-J ----=

-0 rY 1.0

-0

0 >

0.8 r-

~ 0.6 .61

---:---r--

1-

1\ 1 -

r-t-~- - t---t---- r--r-- ~ ---- r----

--

:1 2 p) t/ft 1

\ ~ ~

1\ ~

i-- .............

r--- r-..... ....... 1\

'\.

'" -~

10

~ 1\

~ ~

100

~ ~

Figure 4-11_ e-logP Curve

~-~ .. _~~~_-_IL~ .. _ .«-"'.·,.o.:t<Ilu.i''''-.... a:x;&; ... 4~~'.j,<Q.a~~~~x~ll.$;i~?i'Jf..~:1<~1'<~t~~-1ii~~:(t.~7!~j~Dnl

- 45 -

.-1 • •

-------~-----------~------~-------------------------

- . . I! -. ,

. - . ., .. _~ .. ~ ......... ---.-.. _'.-"'_ ..... _.~-----_.-_ ... -._~ .. _~_." .....• ' ~~-_ .. ,.~ ~ ..... "-, .. ~_. ,

(a) Hari zontal section(Undisturbed sample)

(b) Vertical section (Undisturbed sample)

Figure4-12. Microphotographs of Thin Sections Taken from Natural Clay Samples

J X40

F 1 (j Ll r~ e 4 - Î 2 i\1ll r~ 0 p hot 0 g r 0 ::J h S of T n 1 n Sec t 1 ons

foken from NJturol (::Joy Somples) X~+O

- ,," -

(a) Horizontal section

( b) Vertical section

Figure4-13 Mlcr~ophotogrcphs of Thin Sections

Taken from Consolidated Clay Samples, X.150

\0) HOrizontal section X":+O

(i)) Vertical sectlOrl J Xl50

FI~ure 4-1·4 f\! icrO:Jnotogrophs of Thin Sections

T 0 f\ c n t r 0 ni F 0 Il e dei a y Som pie s

- 48 -

that, under uniform stress field conditions, the failure zone of a

cohesive soil sample can be of the type illustrated in Figure 4.14.

- 49 -

DISCUSSION ~ RESULTS

As stated in Chapter II, the analysis of soil response must

involve a study of the physical properties of the clay-water system.

Thus this chapter will relate observed behaviour to physical mechanisms

that govern the clay response.

5.1 ~ Behaviour

The strength of cohesive soils may be described by using analy­

tical concepts whenever possible and by considering the physical

mechanisms that determine the soil response behaviour.

When the application of the Mohr-Coulomb theory is in doubt, th1s

is unfortunate because it is very desirable for practical purposes to

have a satisfactory the ory for the determination of strength parameters

from standard triaxial tests.

It is shown on a reduced deviatoric plane in Figure 4.7 that at

10w equivalent strains, the reduced yie1d surfaces in principal stress

space are close to regu1ar hexagons. Such yield loci define a mate­

rial in which shear strains are a unique function of the maximum shear

stress and overal1 confining pressure, and it is known as the extended

Tresca criterion. From the soi1 response the indication is that the

shear resistance of Leda clay is of a pure shear type, rather than

frictions1. In other words, at stresses below the preconsolidation

e - 50 -

pressure in this undisturbed clay, the influence of the intrinsic

stresses controls the shearing resistance. Under these pressures, the

soil response behaviour is governed by the brittle nature of the inter­

particle bonds. Failure occurs at low strains (Figures 4.4, 4.5 and

4.6), and the consolidation pressure has only a small effect upon the

strength of Leda clay (Figure 4.1). At very high confining pressures,

structural brea~~own cccurs because of the stresses applied to the

clay and failure of the brittle interparticle bonds follows the genera­

tion of shear stresses and tensile stresses acting on the individual

clay particles (Con Ion, 1966).

Evidence of the natural bonds upon the yield characteristics of

Leda clay has been achieved because, as shown in Figure 4.7, approxi­

mate model relationships between the equivalent shear stresses and

strains were obtained at different consolidation pressures. These

findings imply the validity of the extended Tresca at lower confining

pressures and of the von Mises criterion at higher octahedral normal

stresses. It was shown in Chapter IV, Figures 4.7 and 4.10, that

circles in stress space become a better approximation to the yield

behaviour of Leda clay at higher confining pressures. This is so

because, under these high stresses, breakdown of the clay bonded

structure occurs and the clay behaves more as a remoulded soil. This

fact agrees with the findings of Conlon (1966) and Kenney (1967, 1968).

Also, McKyes (1969) has shown that the behaviour of remoulded kaolinite

is weIl represented by the von Mises criterion in the initial portion

of the stress-strain curve. In this investigation, considerable experi­

mental scatter is present (Figure 4.10), and further study has to be

- 51 -

carried out in both the physico-chemica1 aspect and the yie1d behaviour

of Leda clay.

From the experimenta1 resu1ts it is c1ear that the concepts of

shearing resistance assumed at the yie1d and fai1ure conditions, by the

Mohr-Cou10mb criterion, cannot be app1ied.

When the behaviour of the clay response ls analyzed at 10w strains,

1t 18 apparent that the physical mechanisrn5 that govern the shear

resistance are very different from those acting after large straining

occurs. In fact, when fai1ure is reached, macroscopica11y observable

shearing planes develop, and the clay partic1es in the slip zone have

a1igned themse1ves para11e1 to the fai1ure plane (Figure 4.14). That

is, preferred partic1e orientation occurs, and when investigating the

deformation characteristics at 10w and high strain 1eve1s, account must

be taken of the changes in soi1 structure as a resu1t of the shearing

process.

In genera1, it is c1ear that this clay behaves as a stiffer mate­

rial under the influence of higher intermediate principal stress ratios.

At the present time, it is not known whether the increase in stiffness

is due to (a) a corresponding increase in the octahedra1 normal stress,

(b) the soi1 response behaviour under the various stress ratios, or

(c) a combination of (a) and (b). A1so, it is be1ieved that the undis­

turbed clay structure and in particu1ar the brittle bonds are a major

factor in governing the response of Leda clay, according to the state

of stresses existing in the material.

- 52 -

5.2 Failure

In aIl samples tested, failure was observed to occur by means of

two symmetrical shearing planes. However, the angle of inclination of

the sli~ lines was not constant, but it varied with the intermediate

principal stress difference. No failure was observed to have occurred

by uniform yielding (or bulg1ng); th1s fact may have resulted from the

experimental constraints, that is, top and bottom loading caps.

Figure 4.2 presents the failure stresses on a common deviatoric

plane. It is evident that, when an intermediate principal stress acts,

deviations from the Mohr-Coulomb predictions are obtained. stnce the

amounts of shear and volumetrie strains in the mate rial differ when

the intermediate principal stress is or is not present, the indication

1s that fabric changes from the undisturbed state must be distinct in

the two conditions. As Figure 4.3 shows, the strain at failure i5

much less, when the intermediate principal stress acts, than that of

the axially symmetrical case of ~~ = ~3 • That is, tbe elay struc­

ture reacts differently to the various stress combinations. This

could account for the increased strength and deviations from the Mohr­

Coulomb criterion in the intermediate stress range.

The question about the application of the Mohr-Coulomb eriterion

in the case of Leda clay or sensitive clays in general was brought up

in Chapter Il, in view of the complexities of the undisturbed clay­

water system. This study has shown that the Mohr-Coulomb failure

criterion does not accurately describe the behaviour of Leda clay in

this important range of stresses.

- 53 -

A1so, this investigation has shown that the octahedra1 shear

strength of Leda clay in drained tests varies 1inear1y with the octa­

hedra1 normal stress, plus a constant equal to " ecot si ". Similar

evidence has been shown from uniaxia1 tests (Henke1, 1968) and for

remou1ded kao1inite under comp1ex stress states (McKyes, 1969).

Another problem mentioned previously was that of determining

whether a uniform stress field was acting on the clay samp1es in this

study. Yong and Warkentin (1966) suggest that under uniform stress

conditions, failure zones are characterized by single rupture planes.

In this study, the direct observation of the Interference colours

was chosen as the most usefu1 method of giving meaningful soil fabric

characteristics. Appendix D exp1ains in detail the Interpretation of

the interference co10urs obtained in this study.

Evidence of thin fai1ure zones is shown in Figure 4.14. The

fai1ure planes observed in this study are seen to be single, straight

thin fai1ure zones of very high degree of partic1e para1le1ism, as

indicated by the soUd blue line in Figure 4 .. 14. The thickness of the

fai1ure zone is seen to be approximate1y fifteen microns. Further, the

clay structure in the surroundings of the fai1ure plane is apparently

similar to that of undisturbed clay (Figure 4.12). The presence of

single failur~ planes supports the assumption that the stresses were

re1ative1y uniform over the entire clay specimen.

5.3 Comparison ~ Analysis of Related Work

Recent studies on the yield and fai1ure behaviour of undisturbed,

- 54 -

sensitive c1ays have shown interesting resu1ts. Bonded natura1 c1ays,

when subjected to standard triaxia1 tests, exhibit the fai1ure behaviour

presented in Figure 5.1 (Con10n, 1966). Simi1ar fai1ure enve10pes have

been reported by Kenney (1967, 1968) and a1so are shown in this study

(Figure 4.1). The re1ationship shown in Figure 5.1 presents three

distinct behaviours.

Section (a) represents the case of undisturbed specimens sheared

under extreme1y 10w confining pressures. The behaviour of the clay

is governed by the nature of the cementing bonds and by the stresses

experienced by the pore water. The failure plane is usual1y vertical,

indicating a sp1itting or tension fai1ure.

Section (b) shows the case of samp1es sheared under 10w consolida­

tion pressures. The slope of the failure envelope is close to the

horizontal, indicating that confining pressures have litt1e effect

upon the shear strength of the materia1. That is, under such all­

around pressures, the undisturbed clay structure is preserved, and the

fai1ure stresses will be determined by the relative strength of the

interparticle bonds, in particu1ar, the cementation bonds. Therefore,

it is c1ear that, in the case of a strong1y bonded clay, a very 10w

friction angle is obtained, so long as the confining pressures are

be10w the preconso1idation pressure of the undisturbed soi1. The tests

in this study were performed under the ab ove conditions, and the results

are shawn in Figure 4.1. ln this case, a value of ~ = 10.80 was

obtained; this, in fact, is a 10w friction angle.

Section (c) represents the case of specimens sheared under high

confining pressures. From this it is noted that there is essential1y

1 1 1 1 1 1 1

- 55 -

'a b

Effective Norm al Stress" psi

Figure 5-1. Mohr- Coulom b Plot for the

Consolidated Drained Triaxi al Tests

(Conlon 1 1966)

- 56 -

no cohesion intercept and therefore, when sheared, this soi1 behaves

essentia11y as a norma11y conso1idated and unbonded clay and is able

to fu11y mobi1ize its friction angle. Thus, at sufficient1y high a11-

around pressures, even without the application of a stress difference,

the original bonds break down because of the overa11 volume change and

the interna1 comp1exities of the soi1-water system, causing bending,

tension and shear stresses.

Based on experimental eviàence, several modiÏications to the

classical failure criteria have been suggested. Shibata and Karube

(1965), working with remou1ded c1ays, suggest a slight1y rounded shape

for the failure surface in principal stress space, fo110wing c10sely

the out1ine of the Mohr-Coulomb criterion (Figure 5.2).

Composite stresses in a clay sample May be established by using

hollow cylindrical specimens which would allow for pressures to be

app1ied both internally and externa1ly, in addition to axial stresses.

The resu1ting stresses May be computed by using thick-walled tube

theory. Simi1ar experiments were reported by Wu, Loh and Malvern (1963),

and the test results are shown in Figure 5.2

McKyes (1969) reports failure stresses obeying Mohr-Coulomb predic­

tions in the range of intermediate principal stress. The experiments

were performed on remoulded samples of kaolinite. These results are

shown in Figure 5.2

In addition, McKyes (1969) was able to represent the initial yie1d

behaviour of remou1ded kao1inite by means of p1asticity concepts

derived for the von Mises requirements. The resu1ts are shown in

Figure 5.3 and May be direct1y compareà with those obtained in this

, cp=32 c'= 0

- 57 -

01

~'= 33.7 c'= 0.3 psi

Stress paths

1 f J f 1

Wu Loh & Malvern ( 1963) O"c=41-58 psi

1

P,= 19 c'= 5psi ,

\ \ \ \

\ \ \

~ " \ \ " " \ \ \ " , ,\,

" ", \' \ '" , \ \ '" \ \ \ '~\.' \\

McKyes ( 19(9) Oë = 30-60 psi

Shibata & Karube(1965) 0ë=30psi

1>=10.8 , c:5psi

This Study ~ =2.5-10 psi

Figure 5-2. Failure Stresses and Stress Paths

- 58 -

~= 30psi 1" = 5 psi

0ë=60psi 1"= 10psi

,

\ \ \. , \ ' \ ' , \ ' \ ' , \ , , .

\ \ \ , \ \, , \ \' , \ \' ',\ , , \ \, ~\'

\ \ \ , \ , \ , , , ,

" \ \ , \ \ , \ , \ , .. \ \ \

',\\

~

ct =45psi 1" = 10psi

Legend

-.p- -- .. -

Stress path

Figure5-3. Limiting Circles of vonMises Behaviour (McKyes ~ 1969)

- 59 -

study and which are presented in Figure 4.7. The nature of the soi1

structure is seen to govern the response behaviour of these two c1ays

in view of the phenamena described in this section. Because undis­

turbed sensitive c1ays disp1ay greater structural influences at 10w

ce11 pressures than remou1ded soi1s, the effect of these phenomena has

been manifested in the dissimi1arity of yie1d behaviour of the two

c1ays. At higher consolidation pressures the behaviour of Leda clay

is seen to more c10se1y match that of remou1ded clay.

Further, this study has shown that the fai1ure surfaces of Leda

clay differ in shape fram the yie1d surfaces because when failure is

reached, the behaviour ~f the clay is governed by the appearance of

distinct surfaces of separation, that is, fai1ure planes. At low

strains, the material response is governed by the nature of the inter­

partic1e forces and the initial soil partic1e arrangement.

5.4 ~ Correlation

This study has shown that the Mohr-Cou10mb criterion cannot be

used to accurate1y estimate the fai1ure stresses of sensitive c1ays

subjected to comp1ex stress fields. This stress condition prevai1s in

sma11 and medium lands1ides and renders it difficu1t to ana1yze slope

stabi1ity prob1ems.

lt has been shown that under 10w stress conditions Leda clay has

a large strength in "extension". This condition often OCf::urs in the

progressive fai1ure of slopes. In fact, just prior to fai1ure, part of

the slope may sustain considerable tensile stresses.

- 60 -

When a slope fails, usually a liquid clay failure zone exists on

which the slide moves. Also, when each sampl~ had failed, the failure

plane was clearly a liquidified clay zone.

Generally, slope failures in sensitive clays are characterized by

very small movements. In fact, failure usually occurred with strains

less th an two or three percent (Bilodeau, 1956; Con Ion, 1966).

Finally, slope failures in Leda clay are characterized by sudden

movements. When testing each clay sample, it was found that failure

occurred suddenly; in fact, the last applied load could stay on the

sample for a few days without causing large strains, and then the

sample could fail suddenly with little or no warning.

- 61 -

CONCLUSIONS

6.1 Conclusions

The results of this study have shown the following conclusions:

1. The triaxial apparatus, used by Yong and McKyes (1967), and

McKyes (1969) for remoulded clays, has shown to provide

stress deformation characteristics of an undisturbed sensi­

tive clay subjected to complex stress fields.

2. It has been shown that under very low confining pressures and

under complex stress conditions, Leda clay appears to yield

according to a maximum shear stress criterion. The reason

for such a behaviour is that the strength of the natural

bonds does not de pend to a great extent upon the value of the

normal stress.

3. As confining pressures increased, partial breakdown of the

structural bonds occurred, and the behaviour of Leda clay

approached that of a remoulded clay. In other words, the

clay appeared to yield more according to a von Mises criterion.

4. Tne appiication oÏ the Mour-Coulomb Ïailure criter10n 18 fiot

valid for this clay under the stress conditions described above.

This is because the requirement of this criterion, tbat the

- 62 -

intermediate principal stress is without influence on the

failure of a material, is clearly not satisfied for this clay.

The observed failure surface in principal stress space shows

a rounded envelope. The maximum deviation occurs when the

intermediate principal stress is close to half-way between the

major and minor principal stresses and is approximately 10

percent of the Mohr-Coulomb prediction.

5. For high applied intermediate principal stresses, Leda clay

behaves as a more brittle material than under uniaxia1 condi­

tions. This is demonstrated by the increased stiffness and

by the very small strains occurring at failure in the former

instance.

6. By using interference colour techniques, it was found that

failure zones in Leda clay were single thin rupture planes.

These planes were seen to be thin, straight zones having a

high1y oriented clay fabric.

7. Also, by using the method of (5), Leda clay was found to have

an open, flocculated structure and the clay fabric was corre­

lated with the mechanical properties displayed by the clay,

such as sensitivity and yield behaviour.

6.2 Suggestions for Further Research

In order to better understand yield and failure of sensitive

clays, several important aspects of these problems require further

research.

- 63 -

Yielding of undisturbed clays must be investigated at confining

pressures above the preconsolidation pressure. It is believed that,

in this range of stresses, natural bonds no longer govern the soil

response, since these bonds may undergo a complete breakdown and the

soil will then behave as a normally consolidated clay.

Further microscopic studies should be conducted in conjunction

with more advanced physico-chemical investigations in order to arrive

at a better understanding of the detailed fabric and the basic

mechanisms contributing to the shear resistance of undisturbed sensi­

tive clays.

- 64 -

APPENDIX ê.

!![!. RESULTS

,.. C'i. t::, AV E., ~2. E.) V

psi psi psi 'f, 'f, 'f, 'f,

b=O

4.17 2.50 2.50 - 0.039 + 0.050 - 0.045 - 0.045

5.83 2.50 2.50 - 0.039 + 0.125 - 0.082 - 0.082

7.49 2.50 2.50 - 0.039 + 0.225 - 0.132 - 0.132

9.15 2.50 2.50 - 0.039 + 0.375 - 0.207 - 0.207

12.43 2.50 2.50 - 0.037 + 0.750 - 0.393 - 0.393

15.68 2.50 2.50 - 0.035 + 1.180 - 0.608 - 0.608

b::O

4.17 2.50 2.50 + 0.037 + 0.063 - 0.013 - 0.013

5.83 2.50 2.50 + 0.045 + 0.163 - 0.059 - 0.059

7.48 2.50 2.50 + 0.129 + 0.313 - 0.092 - 0.092

9.15 2.50 2.50 + 0.211 + 0.413 - 0.107 - 0.107

10.77 2.50 2.50 + 0.251 + 0.685 - 0.217 - 0.217

12.42 2.50 2.50 + 0.394 + 0.838 - 0.222 - 0.222

14.04 Il c::n ".JV

Il c:n '.JV

• n J.l\n ,. U.'+'U

• 11 ", .... T l..uo.;) - û.322 - û.322

15.75 2.50 2.50 + 0.633 + 1.462 - 0.415 - 0.415

e

- 65 -

Gl 6'"1. e!r3 AV

6, ez v e.3

psi psi psi ~ ~ ~ ~

b=1/4

5.82 3.33 2.50 + 0.161 + 0.275 + 0.058 - 0.163

9.14 4.17 2.50 + 0.302 + 0.600 + 0.189 - 0.488

12.40 5.00 2.50 + 0.399 + 1.000 + 0.011 - 0.613

15.60 5.83 2.50 + 0.918 + 1. 750 + 0.081 - 0.913

17.20 6.25 2.50 + 0.922 + 1.900 - 0.031 - 0.948

b=1/2

5.82 4.17 2.50 + 0.354 + 0.275 + 0.092 - 0.013

9.15 5.83 2.50 + 0.612 + 0.675 - 0.033 - 0.030

12.40 7.50 2.50 + 0.926 + 1.150 - 0.137 - 0.088

15.53 9.17 2.50 + 1.715 + 2.325 + 1.828 - 2.438

16.94 10.00 2.50 + 1. 786 + 3.875 + 2.024 - 4.113

b=3/4

5.83 5.00 2.50 + 0.044 + 0.125 - 0.019 - 0.063

9.15 7.50 2.50 - 0.139 + 0.250 - 0.189 - 0.200

12.45 10.00 2.50 - 0.179 + 0.450 - 0.367 - 0.263

15.76 12.50 2.50 - 0.035 + 0.675 - 0.285 - 0.425

17.34 13.75 2.50 + 0.238 + 1.200 + 1.825 - 2.789

18.90 15.00 2.50 + 0.298 + 1.500 + 1. 936 - 3.138

b=1.0

5.83 5.83 2.50 + 0.164 + 0.150 + 0.139 - 0.125

9.15 9.17 2.50 + 0.237 + 0.300 + 0.170 - 0.233

- 66 -

Gj AV ~. ~a C;-3 - é. ... E3 " psi psi psi ~ ~ ~ ~

!?=!.:.Q. (ccnt inued)

12.45 12.50 2.50 + 0.455 + 0.475 + 0.338 - 0.358

15.75 15.83 2.50 + 0.477 + 0.625 + 0.317 - 0.465

~

8.33 5.00 5.00 + 0.040 + 0.100 - 0.059 0.0

11.65 5.00 5.00 + 0.163 + 0.300 - 0.037 - 0.100

14.94 5.00 5.00 + 0.260 + 0.650 - 0.193 - 0.198

18.17 5.00 5.00 + 0.689 + 1.350 - 0.461 - 0.300

19.36 5.00 5.00 + 0.895 + 4.47 - 2.485 - 1.090

b=1/4

8.33 5.83 5.00 - 0.016 + 0.200 - 0.151 - 0.065

11.66 6.67 5.00 - 0.033 + 0.375 - 0.313 - 0.098

14.95 7.50 5.00 - 0.032 + 0.575 - 0.469 - 0.138

18.24 8.33 5.00 - 0.023 + 0.750 - 0.558 - 0.170

21.45 9.17 5.00 + 0.079 + 1.500 - 1.199 - 0.223

b=1/2

8.33 6.67 5.00 + 0.264 + 0.200 + 0.112 - 0.048

11.65 8.33 5.00 + 0.424 + 0.350 + 0.139 - 0.065

14.92 10.00 5.00 + 0.704 + 0.812 + 0.062 - 0.170

18.10 11.67 5.00 + 0.742 + 1.700 - 0.751 - 0.208

19.60 12.50 5.00 + 1.104 + 2.750 - 1.239 - 0.408

21.00 13.33 5.00 + 1. 790 + 4.200 + 0.073 - 2.483

- 67 -

Gï c;;-~ 6"'3 4!1V é, E'Z, 63 -V

psi psi psi cf, cf, cf, cf,

b=3/4

8.33 7.50 5.00 + 0.0 + 0.250 - 0.213 - 0.038

Il.66 10.00 5.00 + 0.086 + 0.400 - 0.226 - 0.088

14.95 12.50 5.00 + 0.211 + 0.625 - 0.277 - 0.137

18.24 15.00 5.00 + 0.480 + 0.850 - 0.083 - 0.288

21.50 17 .50 5.00 + 0.522 + 1.075 - 0.078 - 0.475

~

8.33 8.33 5.00 + 0.382 + 0.200 + 0.182 0.0

11.66 11.67 5.00 + 0.776 + 0.400 + 0.376 0.0

14.95 15.00 5.00 + 0.964 + 0.600 + 0.452 - 0.088

18.21 18.33 5.00 + 0.945 + 0.850 + 0.350 - 0.255

È.=2.

13.33 10.00 10.00 + 0.001 + 0.125 - 0.0399 - 0.085

16.65 10.00 10.00 + 0.033 + 0.375 - 0.229 - 0.113

19.92 10.00 10.00 + 0.174 + 0.775 - 0.439 - 0.163

22.96 10.00 10.00 + 0.686 + 2.750 - 1.532 - 0.533

25.15 10.00 10.00 + 1.900 + 9.960 - 7.147 - 0.913

26.60 10.00 10.00 +10.420

b=1/4

13.33 10.83 10.00 + 0.001 + 0.025 + 0.013 - 0.038

16.66 11.67 10.00 + 0.037 + 0.200 - 0.063 - 0.100

ct 19.94 12.50 10.00 + 0.101 + 0.600 - 0.349 - 0.150

- 68 -

Gj c;"1, C;" AV é, E:.~ E:.3 'T

psi psi psi cf; cf; cf; cf;

b=1/4 (continued)

23.20 13.33 10.00 + 0.256 + 1.125 - 0.569 - 0.200

26.32 14.17 10.00 + 0.732 + 1.900 - 0.856 - 0.312

21.90 14.58 10.00 + 0.854 + 2.300 - 1.046 - 0.400

28.46 15.00 10.00 + 2.590 + 8.350 - 1.735 - 4.025

29.63 15.42 10.00 + 3.110 +10.425 - 1.715 - 5.600

b=1/2

13.33 11.67 10.00 + 0.003 + 0.075 - 0.039 - 0.033

16.66 13.33 10.00 + 0.028 + 0.225 - 0.147 - 0.050

19.95 15.00 10.00 + 0.067 + 0.500 - 0.378 - 0.055

23.20 16.67 10.00 + 0.151 + 0.913 - 0.649 - 0.113

26.38 18.33 10.00 + 1.146 + 1.850 - 0.279 - 0.425

27.87 19.17 10.00 + 1.234 + 2.550 - 0.741 - 0.575

29.27 20.00 10.00 + 1.522 + 3.775 - 1.103 - 1.150

b=3/4

13.33 12.50 10.00 + 0.001 + 0.075 - 0.049 - 0.025

16.66 15.00 10.00 + 0.033 + 0.250 - 0.142 - 0.075

19.95 17.50 10.00 + 0.295 + 0.500 - 0.079 - 0.125

23.15 20.00 10.00 + 1.310 + 1.300 + 0.523 - 0.513

25.91 22.50 11 n nn • 1') 1,n -} J. Lc:.n ..L n S1?n - 3.300 .LV.vv T &..L/V ""'.VJV . v. "' .. ""

27.37 23.75 10.00 + 2 .372 + 5 .425 + 0.897 - 3.950

28.50 25.00 10.00 + 2.810 + 8.000 + 0.110 - 5 .300

30.00 26.25 10.00 + 2 .850 + 8.150 + 0.113 - 5 .413

- 69 -

6. 6""z. G""~ AV

6, E:z. E:..3 ~ psi psi psi ~ ~ ~ ~

b=3/4 (continued)

31.30 27.50 10.00 + 3.244 + 9.500 + 0.744 - 6.700

~

13.33 13.30 10.00 + 0.035 + 0.075 0.0 - 0.040

16.66 16.67 10.00 + 0.149 + 0.200 + 0.335 - 0.085

19.97 20.00 10.00 + 1.603 + 0.450 + 1.476 - 0.323

23.20 23.33 10.00 + 1.940 + 0.800 + 1.800 - 0.660

26.45 26.67 10.00 + 2.870 + 1.250 + 3.394 - 1.773

27.65 28.33 10.00 + 2.900 + 3.900 - 3.723

- 70 -

APPENDIX!

PRINCIPAL STRESS SPACE METHOD

The following method follows closely that reported by McKyes

(1969) •

a) Octahedral Functions

In the stress space shawn in Figure B-l, the vector ~ represents

the state of stresses (0; ,~,o;) acting on a clay specimen. The

stress vector!S may be divided into two parts, one which is along

the hydrostatic line (cr. = a", = as) and one which i8 perpendicular

to it. It is clear from thi8 figure that:

where: QQI~(OI+ (it+ 0;)( ï+ J+k) = J1 ( ï+ j+k ) 3 3"

and:

_ J" -'/3

Th h is Q'P d i li h d 1 1 e ot er component ,an t es on an octa e ra pane

perpendicular to the hydrostatic axis.

- 71 -

(0)

( b)

x

1],1<. =unit vectors

0"3

01( Oblique view)

Figure 8-1. Geometry of Principal Stress

- 72 -

OP =5- 00'

411-and :1- t fJ J 2. J j J] OP =~q- :3 ) +{O,- 34 +(q- 3" t

=~Loct

where "'Coc.t = shear stress on octahedral plane.

Similarly in principal strain space:

=~ foct

where ~Lt = shear strain on octahedral plane.

f3Tô(~ may be plotted either in cartesian coordinates as

(x, y) OL' in polar coordinates as ( f3' t oc.t. ,e), where:

- 73 -

b) The Common Right Section

To examine the adequacy of any yield criterion, it is convenient

to represent experimental data and theoretical predictions in such a

way as the degree of agreement between the two may be immediately seen.

New reduced stress coordinates may be used when yield surfaces, gene-

rated by straight lines, are compared. In Figure B-2, the Mohr-Coulomb

failure surface i8 used as an illustration.

The reduced stress points can be easily described as follows:

X= X

~(o:-o;) J. = ~H J. +3(H) {3

y:. y ~( 2 cr. -cr. - cr.)

~i +(3H =

J1 +3(H) (3

't/2-

~L~t~= I3Toct = ~ q-o;)\(01.- o,j+(a; - 0 4 r ]

~ +/3H J., + 3 (H) f3

e'= e

- 74 -

()3

Reduced right section

Figure 8-2. Common Reduced Right Section

- 75 -

APPENDlX ~

GEOLOGICAL HISTORY ~~~

In nature, clay deposits are frequently stratified. The strata

may be composed of soils of similar properties, or of soil types having

different characteristics. The clay is considered anisotropic because

of these physical characteristics.

Leda clay of Eastern Canada belongs to the type described above.

The most important feature of this clay is its sensitivity, that is,

the ratio of undisturbed strength to remoulded strength.

In view of the obvious importance of soil structure to sensitivity

and shear strength, it is worth reviewing the geologic history of Leda

clay.

During the Pleistocene, when the recession of the continental iee

sheets was going on, conditions were highly favourable to the develop­

ment of widespread marginal lakes. At the time of maximum extension of

the ice the less mountainous parts of the underlying floors were

depressed into shallow regions by the isostatic effect of the load of

ice. In the late Pleistocene time, the crust was gradually unloaded

and isostatic recovery worked in from the margins of these depressions

(Karrow7 1960). Consequently, for thousands of years there were large

aëeas, abaüdônned by ice, that slopeà towaràs anà beneath the receding

ice fronts. Many of these became giant lakes, while others were

invaded by the sea. As the ice sheets were retreating and because of

the isostatic balance, lands, that were once depressed by several

- 76 -

hundred feet, started to rebound and today these sediments are often

found above cea level (Karrow, 1960; Allen and Johns, 1960).

elays with properties similar to those of Leda clay are the well­

known Scandinavian quick clays. These soils have been investigated by

Rosenquist as early as 1946, Osterman (1960), Bjerrum (1961) and others.

The sensitivity of Norwegian marine clays is strictly related to

the salt concentration of the pore fluide This is explained by the

"leacbing effect" on sensitivity which 1a based Oil the fact that sedi­

mentation took place in sea water or brackish water (Rosenquist, 1946;

Skempton and Northey, 1952; Bjerrum and Rosenquist, 1956).

When the sedimentation of these clays had ceased and if the depo­

sits were subsequently invaded by fresh waters, considerable leaching

occurred. The general configuration of the minerals in clay, from

which the salts are leached out, may remain unalteredj and if the ori­

ginal structure is not disturbed, the clay will exhibit a considerable

shear strength. When leaching occurs, the thickness of the adsorbed

water layers decreases; hence more free water is available in the

interstitial pores. Then, on remoulding, this clay will exhibit a

shear strength lower than that of the original clay. This hypothesis

to explain t~e sensitivity of Norwegian clays was confirmed by Skempton

and Northey (1952).

Leda clay is thought to have been formed in the same way, but

erosion by fresh waters and subsequent redeposition are responsible for

its flocculated structure. This open structure is attributed to resi­

dual cations from the original marine deposit (Eden and Crawford, 1957).

Also, it is believed that factors other than leaching have contributed

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to the sensitivity aince there appears to be no correlation between

salt concentration and sensitivity with depth (Crawford, 1960).

Eden and Crawford (1965) report pore water salt concentrations

of the order of one to two grams per liter, while a wide range of

salt concentrations has been reported for Norwegian marine clays

(Bjerrum, 1954). However, more conclusive data about existing salt

concentrations are needed since it has been reported that in areas

where majo~ slides occurreâ, Îor example, Nicolet, Quebec, in 1956

where a high salt concentration was found (Crawford, 1960).

In 1953, Lambe presented schematic diagrams of the structure of

clays. For undisturbed marine clays, an open structure similar to

the cardhouse model postulated by Goldschmidt (1926) was shown, whereas

in fresh water sediments, the structure was thought somewhat denser and,

in remoulded clays, was supposed to have a high degree of parallelism

(Figure C-l).

In 1957, Tan presented a schematic picture of a clay mineraI

arrangement dominated by edge-to-face contacts (Figure C-2). Today,

by means of electron microscopy, it is possible to prove that the

mineraI arrangement of undisturbed marine clays corresponds to the

cardhouse structure of Goldschmidt and Lambe and, in fact, exactly

agrees with the theoretical work of Tan, (Lambe, 1960).

Legend

(a) (b) (c)

Figure C-1.

- 78 -

(c)

Undisturbed salt water deposit U ndi sturbed fresh water deposit Remoulded clay

- 79 -

FigureC-2. Schematic Picture of Clay

Network ( Tan J 1Q57)

- 80 -

APPENDIX !!

OPTICAL METHOD

In order to investigate the fabric of undisturbed, consolidated

and failed clay samples, an optical method for the direct observation

of the clay surface was developed.

To apply standard optical procedures to the study of clay fabric,

it was necessary to replace the soil moisture with a high molecular

weight polyethylene glycol compound (Carbowax 1000). This mate rial is

hard at room temperature, melts at 450C and is soluble in water in all

proportions. Small samples oj~ the clay were placed in the melted

material in the manner described by Mitchell (1956) and Leitch (1967).

Since at the end of six days the water in the clay was replaced by

the melted Carbowax, the samples were removed from the bath and allowed

to cool. Thin clay sections of 25-micron thickness were then cut by

me ans of a medical microtome knife (teitch, 1967) and were viewed in a

polarizing microscope. With such a microscope there are various means

of analyzing the orientation of clay particles owing to the difference

in refractive indices between tbe optical axes of the individual clay

platelets. This property, known as birefringence, causes various inter­

ference colours to be observed, depending upon the nature, thickness and

relative orientation of clay particles (Kerr, 1959).

The absence of past work using interference colour technique in

clay fabric studies renders it difficult to be exact in the evaluation

of the results; however, single crystal theories may be applied

- 81 -

(Mitchell, 1956; Leitch, 1967; Yong and Japp, 1968).

The crossed-nico1s method is used and the gypsum red plate is

introduced between the thin section and the ana1yzer. The procedure

is out1ined be10w and fo110ws c10se1y that of Yong and Japp (1968).

If the clay partic1es are oriented in the manner shown in Figure

D-1(a), then the field of view will have a uniform red co10ur. If the

clay partic1es are inc1ined with respect to the incoming 1ight, then

the field of view will appear as shades of green and orange.

If the clay partic1es are oriented as shown in Figure D-1(b),

the field of view will have a greenish co1our; and if the clay parti­

c1es are oriented at about 900 c10ckwise from the position in Figure

D-1(b), the observer will see shades of orange and ye11ow. This condi­

tion is shown in Figure D-1(c).

F10ccu1ated and random1y oriented clay fabrics will show co1our

mixtures ranging between green and ye110w. For undisturbed clay speci­

mens, the co10urs wou1d not be as uniform1y distributed as in the case

of oriented samp1es. Darker and 1ighter regions are characteristics

of these c1ays, indicating a f10ccu1ated structure.

- 82 -

Polari zed light

ClelY particle

Edge of clay pcrticle

/ (a)

Light into paper ( b)

1 1 1

1 1 1

Edge of clay particle

Figure D-1. Interference Colour Interpretation

- 83 -

1!§! QE. ~ERENCES

Allen, V. T. and Johns, w. D., "C1ays and clay mineraIs of New Eng1and and Eastern Canada", l!!:!!!.. ~. ~. ~., 71:75-86, 1960.

Bilodeau, P. M., ''The N:ico1et Lands1ide", Proceedings ~ Canadian §2!l Mechanics Conference, TM46:11-13, 1956.

Bishop, A. W., "The strength of soils as engineering materia1s", Geotechnique, 6th Rankine Lecture, 16:91-128, 1966.

Bishop, A. W. and Henke1, D. J., I!!.! Measurement 2t Soil Properties !!!. ~ Triaxia1 Test, 2nd ed., Arnold, London, 1962, 190 pp.

Bjerrum, L., "Geotechnica1 properties of Norwegian marine c1ays", Geotechnique, 4:2:49-69, 1954.

Bjerrum, L., '1he effective shear strength parameters of sensitive c1ays", Proceedings ~ M. ~. !2!l~. ~. Eng., Paris, France, 1;23-28, 1961.

Bjerrum, L. and Rosenquist, 1. Th., "Sorne experiments with artificia1 sedimented c1ays," Geotechnique, 6 :3: 124-136, 1956.

Brydon, J. E. and Patry, L. M., '~inera10gy of Champlain Sea Sediments and a Rideau Clay Soil Profile", Canadian l. ~ ~., 41:169-181, 1961.

Collins, A., Lands1ides !!!. C1ays, (tr.ans1ated by W. R. Schriever), University of Texas Press, Austin, Texas, U. S. A., 1956.

Con10n, R. J., ''Landslide on the To1nustouc River, Quebec", Canadian Geotechnica1 Journal, 3:3:113-144, 1966.

Corforth, D. H., "Sorne experiments on the influence of strain condi­tions on the strength of sand", GeotechniQue. 17:2:143-167, 1964.

Crawford, C. B., Discussion to ''Canadian Pleistocene Marine Clays" by P. F. Karrow, proceedings ~ Can~dian ~ Mechanics Conference, TM69:103-105, 1960.

- 84 -

Crawford, C. B., "The influence of strain on shearing resistance of sensitive clay", Proceedings ASTM. 61: 1250-76, 1961.

Crawford, C. B., "Cohesion in an undisturbed sensitive clay", ~­technique. 13:2:132-145, 1963.

Crawford, C. B., "The resistance of soil structure to consolidation", Canadian Geotechnica1 Journal. 2:2:90-97, 1965.

Crawford, C. B. and Eden, W. J., "A comparison of 1aboratory resu1ts with in-situ properties of Leda clay", Proceedings !!!.E!!!!!l. ~. ~~. ~. Eng., Montreal, Canada, 1:31-35, 1965.

Crawford, C. B. and Eden, W. J., "Stability 'of natura1 slopes in sensitive c1ays", Proceedings ~ 93, SM4:419-436, 1967.

Eden, W. J., ''The Bawkesbury Lands1ide", Proceedings ~ Canadian §2!! Mechanics Conference. TM46:14-22, 1956.

Eden, W. J. and Brydon, J. E., "Some observations on the measurement of sensitive claya", Proceedings ASDf, 61:1239-1249, 1961.

Eden, W. J. and Crawford, C. B., '~eotecbnica1 properties of Leda clay in the ottawa region", Proceedings Fourth !!!l. ~. !2.!! Mech. ~. Eng., London, 1:22-27, 1957.

Gadd, N. R., "Geo10gica1 aspects of Eastern Canada flow slides", ~oceedings ~ Canadian !2!l Mechanics Conference, TM46:2-8, 1956.

Go1dschmidt, V. M., ''Unders8ke1ser over 1ersedimenter" (Investigations of sedimentary c1ays), Nordisk Jordbrugsforskning, proceedings Third Conference, Oslo, Norway, 434-445, 1926.

Go1dstein, M. and Ter-Stepanian, G., "The 10ng-term strength of c1ays and depth creep of slopes", Proceedings Fourth !!!!. ~. ~ ~. ~. Eng., London, 2:311-314, 1957.

Grim, R. E., "Physico-chemica1 properties of so11s: clay mineraIs", proceedings ~.§2., SM2:1-18, 1959.

Benke1, D. J., Oral presentation. Symposium on Advances in Soi1 Mechanics, Waterloo, Ontario, Canada, 1968.

Benke1, D. J. and Wade, N. B., "Plane strain tests on a saturated remoulded clay", Proceedings ~ 92, SM6:67-80, 1966.

- 85 -

Hvors1ev, M. J., "Conditions of faUure for remou1ded cohesive soUs", Proceedings llE!!~. Q2.!:![. §.2!!.~. ~. Eng., cambridge, 3:48-51, 1936.

Hvors1ev, M. J., "Physica1 components of thf: shear strength of satu­rated c1ays", ASCE Reaearch Conference on Shear Strength of Cohesive Soi1s, Boulder, Colorado, U. S. A., 169-273-3, 1960.

Karrow, P. F., ''Canadian Pleistocene Marine C1ays", Proceedings 14th Canadian !2!h Mechanics Conference, TM69:94-l02, 1960.

Kenney, T. C., Discussion to "Geotechnical properties of glacial lake clays" by T. H. Wu, proceedings ~ §.!, SM):67-79, 1959.

Kenney, T. C., ''Field measurements of in-situ stresses in quick clays", Proceedings Geotechnica1 Conference. Oslo, Norway, 1:49-56, 1967.

Kenney, T. C., "Slide behaviour and shear resistance of a quick clay determined from a study of the landslide at SeInes, Norway", Proceedings Geotechnical Conference, oslo, Norway, 1:57-64, 1967.

Kenney, T. C., ''The influence of mineraI composition on the residual strength of natura1 soUs", Proceedings Geotechnica1 Conference, Oslo, Norway, 1:123-130, 1967.

Kenney, T. C., "A review of recent research on strength and consolida­tion of soft, sensitive c1ays", Canadian Geotechnica1 Journal, 5:2:97-119, 1968.

Kenney, T. C., Moum, J •. and Berre, T., "An experimenta1 study of bonds in a natura1 clay", Proceedings Geotechnica1 Conference, oslo, Norway, 1:65-70, 1967.

Kerr, P. F., Optica1 Minera10gy, McGraw-Hi11 Book Company, New York, 1959, 442 pp.

Kirkpatrick, W. M., "The condition of failure for sands", proceedings Fourth ~. Conf. 22!l~. ~. Eng., London, 1:172-178, 1957.

Kjellman, W., "Report on an apparatus for consummate investigation of the mechantca1 properties of soUs ", proceedings ~!!!l. Q2.!:![. ~~. ~. Eng., Cambridge, 1:16-20, 1936.

Ladanyi, B., Morin, J. P. and Pelchat, C., "Post-peak behaviour of sensitive c1ays in undrained shear", Q!nadian Geotechnica1 Journal, 5:2:59-68, 1968.

- 86 -

Lafeber, D., Discussion ta 'Microscopic structures in kaolin subjected ta direct shear", by N. R. Morgenstern and J. S. Tchalenko, Geotechnique. 18:379-382, 1968.

Lambe, T. W., ''The structure of inorganic soUs", Proceedings ~ J.!, 1953.

Lambe, T. W., "The structure of compacted clay", Proceedings ~ ~ SM2:l654:l-34, 1958.

Lambe, T. W., "Physico-chemical pl'operties of soUs: ro1e of sail technology", proceedings ~ §2., SM2:55-70, 1959.

Lambe, T. W., "A mechanistic picture of shear strength in clay", ASCE Research Conference on Shear Strength of Cohesive Soi1s, Boulder, Colorado, U. S. A., 555-580, 1960.

Lambe, T. W. and Martin, R. T., "Composition and engineering properties of sail (III) ", Proceedings HRB 34:566-582, 1955.

Lambe, T. W. and Martin, R. T., "Composition and engineering properties of soU (IV)", Proceedings HRB35:661-677, 1956.

Leitch, H. C., "The rate dependent mechanism of shear failure in è1ay soils;' McGi11 University, Montreal, Canada, Ph.D. Thesis, 1967.

Leitch, H. C. and Yong, R. N., 'The r~t~ dependent mechanism of shear failure in clay soUs", SoU Mechanics Series !2.. ll, Report to Defence Research Board of Canada, Report No. D. Phys. R. (G), Misc. 28, 1967.

Lo, K. Y. and Milligan, V., "Shear strength properties of two strati­fied clays", Proceedings ASCE ll., SMl:l-lS, 1967.

McKyes, E., "Intermediate principal stress effects on the yielding of a clay", McGill University, Montreal, canada, Master of Engineering Thesis, 1967.

McKyes, E., ''Yielding of a remoulded clay under comp1ex stress states", MeGill University, Montreal, Canada; Ph.D. Thesis; 1969.

Meyerhof, G. G., SUIl1IIary of "The mechanism of flow slides in coheslve soUs", Proceedings !Q!!!. Canadian SoU Mechanics Conference, TM46:9-l0, 1956.

- 87 -

Mitchell, J. K., "The fabric of natural clays and its relation to engineering properties", Proceedings HRB 35:693-713, 1956.

Morgenstern, N. R. and Tchalenko, J. S., '~icroscopic structures in kaolin subjected to direct shear", Geotechnique, 17:4:309-329, 1967.

Morgenstern, N. R. and Tchalenko, J. S., '~icrostructural observations on shear zones from slips in natural clays", Proceedings Geotech­~ Conference, Oslo, Norway, 153-158, 1967.

Osterman, J., "Notes on the shearing resistance of soft clays", ~ Polytechnica Scandinavica, 263/1959, Stockholm, Sweden, 22 pp., 1960.

Parry, R. H. G., '~atent interparticle forces in clays", Nature, 183: 538-539, 1959.

Penner, E., "Sensitivity in Leda clay", Nature, 197:347-348, 1963.

Quigley, R. M., "The engineering properties of iUite related to fabric and pore water composition", Proceedings ~ Canadian !2!l Mechanics Conference, TM82:2l-42, 1962.

Quigley, R. M. and Thompson, C. D., ''The fabric of anisotropically consolidated sensitive marine clay", Canadian Geotechnical Journal, 13:2:61-73, 1966.

Rendulic, L., "Relation between void ratio and effective principal stresses for a remoulded silty clay", Proceedings ~~. ~. Soil ~. ~. Eng., Cambridge, 3:48-51, 1936.

Rochette, P. A., "Experimental and theoretical investigation on the engineering properties of Canadian natural clay deposits", Proceedings ~ Canadian ~ Mechanics Conference, TM46:27-34, 1956.

Roscoe, K. H., Schofield, A. N. and Wroth, C. P., "On the yielding of so11s", Geotechnique, 8:1:22-53, 1958.

Rosenquist,!. Th., "Am le ires kvikkaktighet" (The sensitivity of clays), Statens Vegvesen, Veglaboratoriet, Meddelelse, No. 4:5, 1946.

Rosenquist,!. Th., "Considerations on the sensitivity of Norwegian quick clays", Geotechnique, 3:5:~95-200, 1953.

- 88 -

Rosenquist, 1. Th., "Investigations in the clay~electrolyte water system", Norwegian Geotechnical Institute, Pub. No. 9, Oslo, Norway, P. 125, 1955.

Rosenquist, 1. Th., "Phys ico-chemical properties of so11&: so11-water systems", Proceedings ~.§2., SM2 :31-53, 1959.

Rosenquist, 1. Th., '1he influence of physico-chernical factors upon the mechanical properties of clays", Proceedings ~ Natl onal Conference ~ Clays ~ Clay MineraIs, Lafayette, Indiana, U. S. A., pergamon Press, New York, 9:12-27, 1962.

Schmertmann, J. H. and Osterberg, J. O., "An experimental study of the development of cobesion and friction with axial strain in satu­rated cohesive so11s", ASCE Research Conference on Shear Strength of Cohesive Soils, Boulder, Colorado, U. s. A. 643-694, 1960.

Schmertmann, J. H. and BaIl, J. R., '~ohesion after non-hydrostatic consolidation", proceedings ~ §L, SM4:39-60, 1961.

Shibata, R. N. and Karube, D., "Influence of the variation of the inter­mediate principal stress on mechanical properties of normally consolidated clays", Proceedings §.!!!!!.!!!!. Q2!!!.. !2!!.~ ~. ~. Eng., 1:359-363, 1965.

Skempton, A. W. and Northey, R. D., ''The sensitivity of claya", Q!2.­technique, 3:1:30-53, 1952.

Soderman, L. G., Kenney, T. C. and Loh, A. K., "Geotechnical properties of glacial clays in Lake St. Clair region of Ontario", Proceedings ~ Canadian ~ Mechanics Conference, TM69:55-87, 1960.

Soderman, L. G. and Quigley, R. M., "Geotechnical properties of three Ontario clays", Canadian Geotechnical Journal, 11:2:167-189, 1965.

Spence, R. A. and Glynn, T. E., "Shear characteristics of a marine clay", Proceedings ~ ~ SM4: 85-107, 1962.

Tan, T. K., "Structure Mechanics of Clays", Academia Sinica. Soil Mechantes Laboratory, !nstitute Civ. Eng. end Arch. Harbin, China, 1957.

Terzaghi, K., "Undisturbed clay samples and undisturbed clays", Journal Boston ~. Civ. Engrs., 28:211-231, 1941.

- 89 -

Townsend, D. L., Discussion to '~andslide on the Tolnustouc River, Quebec", by R. J. Conlon, Canadian Geotechnical Journal, 4:3: 351-352.

Wu, T. H., Loh, A. K. and Malvern, L. E., "Study of faUure envelope of soUs", proceedings ~.§2., SM1:145-l82, 1963.

Yong, R. N. and Warkentin, B. P., Introduction12!2!l behaviour, Macmillan, New York, 1966, 451 pp.

Yong, R. N. and McKyes, E., 'Yielding of a clay in a complex stress field", Third panameriean Conf. Soil. Mech. FOUild. Eng., 1:131-148, 1967.

Yong, R. N. and Japp, R. D., "Soil water relationships and their engineering applications", Report to Cornell Aeronautical Labora­tory Inc. on Contract S-68-5, 1968.