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J o u r n a l o fM a t e r i a l sP r o c e s s i n gT e c h n o l o g yE L S E V IE R Journal of Materials Processing Technology49 (1995) 431-4 43
F r i c t i on w e l d i n g o f S t - A 1 an d A 1- C u m at e r i a l sB e k i r S . Y i l b a ~ a '* , A h m e t Z . $ a h i n a , N a f i z K a h r a m a n b , A h m e d Z . A 1 -G a r n i a
aKin g Fah d Universi ty o f Petro leum a nd Minerals, M echanica l Engineering Department ,Dhahran 31261 , Sa udi Arabia
b Erciy es University. E nginee ring Faculty, Kayseri, TurkeyReceived 26 M ay 1993; acce pted 19 A pril 1994
Industr ia l SummaryT he prese nt stud y investigates the m echa nical and m etallurgical pro pertie s of fr iction-weldedsteel-alum inium and alum inium -cop per bars, a f r ic t ion welder having been designed and buil tfor th is pu rpose. T he ef fects of the three m ain param eters : speed of ro tat ion; f r ic tion load; anddura t ion of welding; on the m etal lurgical and mec hanical proper t ies of the weld such as theyield, tensile and brea king strength s, are stud ied expe rim enta lly an d statistically. Th e metallu r-g ical proper t ies of the weld are examined using electron and optical microscopy.
1 . I n t r o d u c t i o nF r i c t i o n w e l d i n g i s c l a ss i fi e d a s a s o l i d - s t a t e w e l d i n g p r o c e s s , in w h i c h j o i n i n g
o c c u r s a t a t e m p e r a t u r e b e l o w t h e m e l t i n g p o i n t o f t h e w o r k m e t a l . W h e n m e l t in go c c u r s t h e r e is l i tt l e e v i d e n c e i n th e r e s u l t i n g w e l d e d e n d - p r o d u c t . H e a t is g e n e r a t e d b yd i r e c t c o n v e r s i o n o f m e c h a n i c a l e n e r g y i n t o t h e r m a l e n e r g y a t t h e i n t e r fa c e o f t h ew o r k p i e c e s d u r i n g t h e w e l d i n g p r o c e s s . F r i c t i o n w e l d s a r e m a d e b y h o l d i n g a n o n -r o t a t i n g w o r k p i e c e i n c o n t a c t w i t h a r o t a t i n g w o r k p i e c e u n d e r g r a d u a l l y i n c r e a s i n gp r e s s u r e u n t i l t h e i n te r f a c e r e a c h e s t h e w e l d i n g t e m p e r a t u r e , a n d t h e n s t o p p i n gr o t a t i o n t o c o m p l e t e t h e w e ld . T h e h e a t d e v e l o p e d a t t h e i n t e rf a c e r ai se s t h e t e m p e r -a t u r e o f t h e w o r k p i e c e s r a p i d l y o v e r a v e r y s h o r t a x i al d i st a n c e , to v a l u e s a p p r o a c h i n gt h e m e l t i n g r a n g e , w e l d i n g o c c u r r i n g u n d e r t h e i n f lu e n c e o f t h e p r e s s u r e t h a t is a p p l i e dw h e n t h e h e a t e d z o n e i s i n t h e p l a s t i c t e m p e r a t u r e r a n g e .
F r i c t i o n w e l d i n g c a n b e a c h i e v e d a t h i g h p r o d u c t i o n r a t e s a n d t h e r e f o r e is e c o n o m i -c a l in o p e r a t i o n , i n a p p l i c a t io n s w h e r e f r i c t io n w e l d i n g h a s r e p l a c e d o t h e r j o in i n gp r o c e s s e s , t h e p r o d u c t i o n r a t e h a v i n g b e e n i n c r e a s e d s u b s t a n t i a l l y [ 1 ] . S a v i n g s i nm a t e r i a l c a n b e r e a l i z e d a l s o b y t h e u s e o f f r i c t io n w e l d i n g , t h is b e i n g e s p e c i a l ly t r u e* Corresponding author.0924-0136/95/$09.50 ~(3 1995 Elsev ier Scien ce S.A. All righ ts reserved.S S D I 0 9 2 4 - 0 1 3 6 ( 9 4 ) 0 1 3 4 9 - 6
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432 B.S. Yi lba~ et al. / Journal o f Materials Processing Technology 49 (1995) 43 1-44 3w h e n j o i n i n g l a rg e -d i ame t e r ro t o r b o d i e s o r o t h e r ro t a t i n g me mb e r s , o r j o i n i n g t h eco m p o n en t s o f v a l v e sy s t ems I -2 ].
W h en w e l d i n g d is s imi l a r m e t a ls b y f r ic t io n w e l d i ng , p ro b l em s a r i se n o t o n l y f ro mt h e d i ff e r en t h a rd n es s e s an d me l t in g p o i n t s o f th e m a t e r ia l s , b u t a l s o fro m t h eposs ib i l i ty o f in te rac t ion p ro du cing e i ther b r i tt l e in te rm eta l l ic ph ases o r low mel t ing-p o i n t eu t ec t i c s [3 ] . I n t h e a l u mi n i u m/ s t ee l s y s t em, i n t e rme t a l l i c co mp o u n d s a r ea ma j o r p ro b l em, i n g en e ra l t h e fo rm a t i o n o f i n te rme t a l li c p h as es b e i n g co n s i d e redu n d es i r ab le . D aw es [4 ] h a s i n t ro d u ce d a r e l a t i o n s h i p b e t w een th e p ro p e r t i e s o f j o i n t san d d i s s i mi l a r ma t e r i a l s w h i ch fo rm b r i t t l e i n t e rme t a l l i c co mp o u n d s , an d t h e t i meav a i l ab l e fo r th e fo rm a t i o n o f t h e co m p o u n d s , co n c l u d i n g t h a t s a t i sf ac t o ry w e l d sco u l d b e m ad e i f t h e w e l d i n g co n d i t i o n s w ere s u ch t h a t t h e i n cu b a t i o n p e r i o d w asl o n g e r t h an t h e w e l d ti me . H o w ev e r , th e ex i s ten ce o f an i n cu b a t i o n p e r i o d fo ri n t e rme t a l l i c f o rma t i o n i s q u es t i o n ab l e an d co n t ro l s h o u l d b e b as ed o n l i mi t i n g t h ei n t e rme t a l l i c t h i ck n es s r a t h e r t h an o n u s i n g an i n cu b a t i o n p e r i o d .T h e p re s en t s t u d y i n v es ti g a te s t h e p ro p e r t i e s o f f ri c ti o n w e l d s fo r s t ee l - a l u mi n i u man d co p p e r - a l u mi n i u m b a r s , a f r i c t i o n w e l d e r h av i n g b een d es i g n ed an d man u fac -t u r ed fo r th i s p u rp o s e . A t emp e ra t u re s en s o r is em p l o y ed i n th e s y s t em t o mo n i t o r t h eh ea t i n g t i me an d p ro v i d e f eed -b ack t o t h e e l ec t ro n i c co n t ro l l e r .
T h e n u m b er o f p a r am e t e r s i n v o l v ed in f r ic t io n w e l d in g is q u i te l a rge , s o t h a ta s t a t i s t i c a l ap p ro ach b as ed o n o n e - f ac t o r - a t - a - t i me i s t ed i o u s an d u n s a t i s f ac t o ry .The refo re , s t a ti s t ica l des ign o f the expe r ime nt b ased on fac to r i a l ana lys i s i s necessary .In t h e l i g h t o f p r ev i o u s s t u d i e s [5 ,6 ] , t h e p r e s en t w o rk is ex t en d ed t o i n c l u d e t h es ta t i st i ca l an a lys i s o f the fac to rs a f fec t ing the f r i c tion-weld ing p rocess , these fac to rsi n c lu d i n g s p eed o f ro t a t i o n , f o rg in g l o ad a n d w e l d i n g ti me . T o ach i ev e a co mp l e t eb loc k ana lys i s, t h ree l eve ls o f each fac to r have been se lec ted .
To inves t iga te the me chan ica l p rope r t i es o f the d i s s imi la r f r ic t ion welds , t ens il e andm i c ro -h a rd n es s t e st in g o f t h e r e s u l t an t w e l d s a r e ca r r ied o u t , me t a l l u rg i ca l ch an g es i nt h e w e l d i n g zo n e b e i n g s t u d i ed a l s o u s i n g SE M an d o p t i ca l mi c ro s co p y .
2. ExperimentalT h e ro t a t i n g w o rk p i ece is d r i v en b y a 1 0 k W e l ect ri c mo t o r w i t h a v a r i ab l e
ro t a t i o n a l s p eed o f u p t o 3 5 0 0 rp m max i mu m . In a l l te s t s th e f r i c ti o n p e r i o d isd e t e rm i n ed b y a t em p era t u re r is e i n t h e w e l d i n g zo n e , a co n t ro l l in g d ev i ce ac t i v a ti n gt h e fo rg i n g l o ad an d s e t ti n g t h e d u ra t i o n w h en t h e t emp era t u re o f t h e w e l d i n g zo n ereach es t h e r eq u i r ed v a lu e . F i g . 1 s h o w s t h e ex p e r i men t a l s e t -u p em p l o y i n g t h ep u rp o s e -b u i l t f r i c ti o n w e l d e r [7 ] .
In in i ti a l tr i al s , a wide range o f m ach ine se t t ings wa s exp lo red , whi l e main ta in ingm an y o t h e r p a ram e t e r s , i .e t h e c lean l in e s s o f th e s u r f aces o f t h e s am p l e s an d t h ed u ra t i o n o f t h e w e l d in g . It s h o u l d b e n o t ed t h a t e ach s am p l e w as c l ean ed b e fo rew e l d i n g u s i n g ace t o n e w h i ch en s u re g r ea s e - an d d i r t - f r ee s u r f aces . T h e a i m w as t oex p l o re t h e e f fec ts o f d if f er en t co m b i n a t i o n s o f ro t a t i o n a l s p eed , fr i c ti o n a l l o ad an dt em p era t u re r is e in t h e w e l d zo n e . A co m b i n a t i o n o f t h e mach i n e s e tt in g s r e s u lt in g i nr ep ro d u c i b l e mech an i ca l p ro p e r t i e s w as s el ec ted fo r t h e r em a i n i n g p a r t o f t h e s t u d y .
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434 B.S. Y ilba~ et al. / Journal o f Materials Processing Technology 49 (1995) 43 1-44 3Table 1Welding parameters and their levels
Level 1 Level 2 Level 3Speed of rotation (rpm) 2000 2500 2800Applied load (kg) 5-12.74 6.37 17.83 7.64-22.93Welding duration (s) 4 7 10
3 . F a c t o r i a l a n a l y s i sTo investigate the effects of factors governing the friction welding process on the
resultant weld properties, it was necessary to employ factorial analysis based ona statistical approach. In this case, the influence of each factor could be examinedindividually, together with that of their interactions. This required a complete fac-torial design, in which the selected factors were varied at appropriately selected levels.A mathematical model relevant to the present analysis is given in Appendix A.The responses considered in the factorial analysis included yield strength, tensilestrength and breaking strength.
4 . D i s c u s s i o nThe welding parameters of applied load for developing friction, speed of rotation
and welding duration determine the thermal phenomenon occurring during the weld-ing process. The cleanliness of the samples may be considered as secondary import-ance. Increased friction load secures a slight reduction of weld-zone temperature, withthe consequent production of less intermetallic compound at the interface, whilst theforging load becomes important only when considering consolidation at the interface.When examining the effect of parameters on the resulting weld properties, it isobserved that increasing the speed of rotation and the level of friction load during theheating period, gives deformation conditions that activate the contacting surfaceswhilst also limiting the temperature/time conditions for joint heating, and conse-quently minimize the formation of intermetallics. There is no significant effect ob-served on the recorded parameters by changing the surface finish. Reduced surfacecleanliness in terms of contaminants, especially grease, reduces the quality of thewelded joint, consistent with the findings of earlier-reported work [8].Discussions based on the resultant weld properties will be presented under twosub-headings, as follows.4 .1 . S t e e l - a l u m i n i u m w e l d s
Tensile test results are shown in Fig. 3. Some of the welds show poor strength,which may occur due to some accumulation of alloying elements at the interface as
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B.S. Yilba~ et al. / Jou rna l of Materials Process ing Technology 4 9 (1995) 4 31 ~ 43 4 3 5
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11001 8 0 0
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9001 8 0 0
I I I I2 0 0 0 2 2 0 0 2 4 0 0 2 6 0 0
Load ap plied5-12.74 kg6.37-1783 kg7.64-22.93 kg
I2 8 0 0 3 0 0 0S p e e d ( r p m )
2 0 0 0 2 2 0 0 2 4 0 0 2 6 0 0 2 8 0 0S p e e d ( r p m )
Load Appl ied5-12.74 kg6.37-1783 kg7.64-22.93 kg
I3 0 0 0
Load Appl ied/ J ~ 5-12.74kgd J ~ 6 .37-1783 kg
d 7.64-22.93 kgI! I I I2 0 0 0 2 2 0 0 2 4 0 0 2 6 0 0 2 8 0 0 3 0 0 0
S p e e d ( r p m )Fig . 3 . Tensi le-test results (S t -A1) .
a resu l t o f t emp erature r i se an d th e ex is t ence o f in term eta l l ic layers such as FeA1 . Anin t e r me t a l li c t h ic k n e s s o f 0 . 1 - 1 ktm i s a c c e p t a b le f or t h e s o u n d w e ld s , a b o v e t h i s v a lu ew e ld s w i t h l o w s t r e n g t h b e in g p r o d u c e d . I n t h e l a t t e r c a s e , i t i s n o t e d t h a t t h ein t e r me t a l li c l a y er i s t h i c k in t h e m id - r a d iu s o f t h e w e ld , a n d t h in a t t h e c e n t e r a n d
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436 B.S. Y ilba~ et al. / Journal o f Materials Processino T echnolooy 49 (1995) 431 -44 3
A>"r -
4 0 0
3 0 0
Ww 2 0 0G )r =
l Uz 1 O0
II n t e r f a c e
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] g ~ A I
I I1 2
D i s t a n c e ( m m )Fig. 4. Microhardness-test results (St-AI).
p e r i p h e r y o f t h e w e l d , t h e r e l a t i v e a b s e n c e o f i n t e r m e t a l l i c l a y e r a t t h e c e n t e r b e i n gc o n s i s t e n t w i t h t h e l o w r e l a t iv e v e l o c i t y i n t h is r e g i o n .
M i c r o h a r d n e s s t e st r e su l ts a r e s h o w n i n F i g . 4 , d e c r e a s e in m i c r o h a r d n e s s b e i n gn o t e d i n t h e s te e l z o n e . T h e w i d t h o f t h e h e a t - a f fe c t e d z o n e is v e r y sm a l l a s c o m p a r e dt o t h a t f o r o t h e r t h e r m a l - w e l d i n g p r o c e ss e s .
M i c r o p h o t o g r a p h s o f t h e i n t e rf a c e z o n e a r e s h o w n i n F i g. 5 , i n w h i c h i t is o b s e r v e dt h a t h e a v y d e f o r m a t i o n o c c u r s a t th e i n t e r fa c e . I n t h is c a se , i t is m o s t p r o b a b l e t h a t t h ea l u m i n i u m o x i d e f ilm i s b r o k e n u p , a l l o w i n g t h e e x p o s u r e o f u n af f e c te d s u rf a ce . A sa l u m i n i u m is r e l a t iv e l y s o f t, t h is r e s u l ts i n a l a r g e a m o u n t o f d e f o r m a t i o n , s o t h a ts u r fa c e c o n t a c t a t t h e i n te r f a c e s h o u l d n o t b e a s ig n i fi c a nt p r o b le m . H o w e v e r , t h es t a b le a l u m i n i u m o x i d e p r e s e n ts a b a r r i e r to b o n d f o r m a t i o n , a n d c o n s e q u e n t l y t h et i m e s a n d t e m p e r a t u r e s r e q u i r e d i n d i f f u s i o n i s c o n d u c t i v e t o t h e f o r m a t i o n a n dg r o w t h o f i n t e r m e t a l li c s .
I t is f o u n d f r o m T a b l e 2 t h a t t h e m a i n e f fe c t s o f a ll th e p a r a m e t e r s o n y i e ld , t e n s il ea n d b r e a k i n g s t r e n g t h s a r e n o t s i g n if ic a n t . O n t h e o t h e r h a n d , f i r s t - o r d e r i n t e r a c -t i o n s o f t h e s e p a r a m e t e r s h a v e a s i g n i f ic a n t e ff e c t o n t h e t e n s i le p r o p e r t i e s o f t h er e s u l t i n g w e ld s . T h i s m a y i n d i c a t e t h a t e a c h f a c t o r h a s l i t tl e i n d i v i d u a l e f f e ct o n t h et e n s il e p r o p e r t i e s , b u t t h e c o u p l i n g o f f r ic t i o n lo a d , s p e e d o f r o t a t i o n a n d w e l d i n g t i m eh as s i g n i f i can t e f f ec t o n t h e s e p r o p e r t i e s . I n t h i s c a s e , i t is d if f icu l t t o m ak e ana s s e s m e n t a s t o w h i c h p a r a m e t e r h a s a g r e a t e r e f fe c t t h a n t h e o t h e r s o n t h e s ep r o p e r t i e s .4 .2 . A l u m i n i u m -co p p er we l d s
T e n s i l e te s t r e s u lt s a r e s h o w n i n F i g . 6 . S o m e j o i n t s f a il e d d u e t o t h e l a c k o f b o n d i n g(i.e . v e r y l it tl e b o n d i n g o f a l u m i n i u m o n t o t h e f r a c t u r e f a c es o f t h e c o p p e r ) a n d t h ec o p p e r f r a c t u r e f ac e s s h o w a p a l e g r e y a l u m i n i u m l a y er , w h i c h m a y c o n t a i n a c o n -s i d e ra b l e a m o u n t o f i n t e rm e t a l l ic c o m p o u n d a t t h e in t e rf a c e. W h e n t h e s p e ed o f
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B.S. Y ilba~ et al. / Journal of Materials Processing T echnology 4 9 (1995) 431 -44 3 437
Fig . 5 . M i c roph ot ogra phy of t he we l d i ng zone (S t-A1).
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438 B.S. Y i lba~ et al . / Journal o f Materials Processing Technology 49 (1995) 43 1-44 3Table 2Statistical effects of w eld parameters on mec hanical proper-ties for steel-alum inium weldsParameters Stee l -a luminium
Yield Tensile Breakings t re n g t h s t r e n g t h s t re n g t hn 0.1 > 0.1 > 0.1 >P 0.1 > 0.1 > 0.1 >t 0.1 > 0.1 > 0.1 >n x P 0.01 < 0.01 < 0.1 >n x t 0.01 < 0.01 < 0.1 >P x t 0.01 < 0.01 < 0.1 >
r o t a t i o n i n c r e a s e s , m i c r o p o r e s a t t h e i n t e r f a c e d e c r e a s e , r e s u l t i n g i n a h o m o g e n e o u sb o n d .
I n F i g . 7 m i c r o h a r d n e s s t e s t r e s u lt s a r e s h o w n . S m a l l c h a n g e s o c c u r in m i c r o h a r d -n e s s i n t h e c o p p e r z o n e , w h i c h m a y b e d u e t o th e c o m p a r a t i v e l y h ig h h e a t - t r a n s f e rc o e ff i ci e nt o f c o p p e r . I n F i g. 8, t h e m i c r o p h o t o g r a p h y o f t h e A l - c o p p e r z o n e i s s h o w n ,i n w h i c h a r e s o l v ed l a y e r o f i n t e r m e t a l li c c o m p o u n d is s e en t o o c c u r a l o n g t h ei n te r fa c e . A c o m p o u n d l a y e r d e v e l o p s a t t h e i n te r fa c e , t h e d e p t h o f w h i c h l a y e ri n c r e a s e s w h e n t h e r o t a t i o n a l s p e e d i n c r e a s e s a n d t h e f r i c t i o n l o a d r e d u c e s . A ni n c re a se i n t h e c o m p o u n d l a y e r r e su lt s in p o o r m e c h a n i c a l p r o p e r ti e s. T h e s m o o t h -n e s s o f t h e c o p p e r f a c e g i v e s a g o o d i n d i c a t i o n o n b o n d i n t e g r it y , si n c e t h e b u l kd e f o r m a t i o n i s c o n f i n e d t o t h e a l u m i n i u m . S o m e d e f e c t s o c c u r a t t h e i n t e r f a c e a n dl a r g e p a r t ic l e s o f c o p p e r a r e e m b e d d e d i n t h e a l u m i n i u m , s h o w i n g t h e e v id e n c e o fs w i r l f l o w i n t h e a l u m i n i u m .
S t a ti s ti c a l a n a l y s is s h o w s i m i l a r r es u l ts t o t h o s e o b t a i n e d f o r s t e e l - a l u m i n i u mw e l d s . A g a i n , i t i s d i ff i cu l t to d i s t i n g u i s h t h e e f f e ct o f e a c h i n d i v i d u a l p a r a m e t e r i n t h ep r o c e s s. C o u p l i n g e ff ec ts o f f r ic t io n l o a d , s p e e d o f r o t a t i o n a n d w e l d i n g t i m e o n t h et e n s i le p r o p e r t i e s a r e s i g n i f ic a n t . T a b l e 3 s h o w s t h e r e s u l t s o f t h e s t a t is t i c a l a n a l y s is .
5 . C o n c l u s i o n s
T h e c o n c l u s i o n s d e r i v e d f r o m t h e p r e s e n t w o r k m a y b e l i s t e d a s f o l l o w .5 . 1 . S t e e l - a l u m i n i u m w e l d s
1. T e n s i le p r o p e r t i e s i m p r o v e f o r s t e e l - a l u m i n i u m w e l d s w h e n t h e i n t er m e t a l l ict h i c k n e s s e x t e n d s o n l y t o 0 . 2 - 1 la m, a b o v e th i s v a l u e w e l d s w i t h p o o r s t r e n g t h s b e i n gp r o d u c e d . T h e i n t e r m e t a l l ic l a y e r t h i c k e n s a t th e m i d - r a d i u s a n d b e c o m e s t h i n a t t hec e n t e r a n d p e r i p h e r y o f t h e w e ld .
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Fig . 8 . M ic r o p h o to g r ap h y o f t h e we ld in g zo n e ( A1- Cu) .
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4 4 2 B . S . Y i l b a ~ e t a l. / J o u r n a l o f M a t e r i a l s P r o c e s s i n g T e c h n o l o g y 4 9 ( 1 9 9 5 ) 4 3 1 - 4 4 3
T a b l e 3S t a t is t ic a l e ff e ct s o f w e l d p a r a m e t e r s o n m e c h a n i c a lp r o p e r ti e s fo r a l u m i n i u m - c o p p e r w e ld s
P a r a m e t e r s A l u m i n i u m - c o p p e rY i e ld T e n s i l e B r e a k i n gs t r e n g t h s t r e n g t h s t r e n g t h
n 0.1 > 0.1 > 0.1 >P 0.1 > 0.1 > 0.1 >t 0.1 > 0.1 > 0.1 >n x P 0 .1 < 0 .01 < 0 .1