UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION III
. . . . . . . .CENTRAL REGIONAL LABORATORY83a.BESTGATE ROAD
ANNAPOLIS, MARYLAND 21401(301) 266-9180 [
I ; '
! j ' ! , - . . ,
DATE : December 8, :19S9 '} - '-". "7: '-"~-X_: •*_*" ; ".".:"L
SUBJECT: 9- Del JJuarries-. Site
FROM : Theresa A.Region III ESAT;DPQ (3ES23)
!
• Donna McCartneyRegional Project MaHager ( 3HW21 )
THRU : Patricia J. KrantzQuality Assurance Branch (
* Quarriescompleted by the Region III Environmental™
have any : questions: please
Attachment
cc: Andy Hop ton,, COM
TID File: 03890 15 !" Task 1126
flR3029!6
2S68A RIVA ROADSUITE 300ANNAPOUS, MD 21401
.M PHONE; 301-266-9887aesBBc&'CoriSLCJWTs
DATE: 7 DECEMBER 1989
SUBJECTS QmMI VALIDATION FOCASE 32544.,.. -fite: DELTA QUARRIES
EROM: DOUO HcXN gS v~" .. .. DON Q'BRI|lf.*-yORGANIC DATA REVIEWER ; *'_ 'ORGANIC £)AfA REVIEWER
IS AT DEPUTY PROJECT OFFICER;
THRU: DAN DRESSfiTEftMT tfSNApSR (acting)
Case 12544 consisted 9f ten'Vio °w evel water samples,submitted to IEAr Inc. / for volatile, semi-volatile^ andpesticide/PCB ahalyses. One (1) field duplicate _palr,_ one (1)trip blank/ and two (2) equipment blanks were included in thesesamples. The "trip blank wasT analyzed for volatiles only. Thesamples weife anaiyzed as a Contract Laboratory Program (CLP)Routine Analytical Service (RAS).
All samples were successfully analyzed for all target compounds,with the exception of 2-butanone. All instrument^and methodsensitivities were according to the Contract^Laboratory Program(CLP) Routine""Analytical Service (RAS) protocol.
MAJOR .jgQBLBM
o The response factor (RF) for 2-butanone was less than 0.05 inthe initial and/or continuing calibrations* The guantitationlimits for these compounds were qualified "R", and thepositive results were qualified "L". (See Table I in AppendixF for the affected samples).
HINDI :HBBl!BHffJ~ _ "". "• - - ".--" " . ' - . - . - . - .:,-;, ' '. -. _..._ TjS; :-~' --~-
O The^volatiies analyses of samples "CCHOO, 'CCH05_/ and CCH06 wereperformed eight (8) days from the date of sample collection.The technical holding time for volatile aromatics in watersamples of seven (7) days has been exceeded by~~one (1) day.The guantitation limits for aromatic volatiles were qualified
"the"affected samples.
302917
Page 2 of 3
o Several compounds failed precision criteria for initial and/orcontinuing calibrations. Quantitation limits for thesecompounds were qualified "UJ", and positive results warequalified "J" for the affected samples. (See Table I inAppendix F) . .........
BOTBS
o The MS/MSD analyses had compounds other than the spikingcompounds present. Following is a table of results andprecision estimates for these non-spiked ccsmpounds:
MS/MSD Non-Spiked Compounds
___Concentration fucr/L)___Compound . ,: CCH03 CCH03MS CCH03MSD %RSD
2-butanone 170 L 180 L 180 L 3.3%
phenol 72 NE NE IN
RSD - Relative Standard DeviationIN - IndeterminateNE - Mot Evaluated, a spiking compound found
during original sample analysis
o One (1) field duplicate pair was analyzed. Following is atable of results and precision estimates for these analyses:
Field Duplicate
: Concentration fgg/L)_____Compound . CCH05 _ CCH06 %RPD
1,1-dichloroethane 34 36 5.71,1,1-trichloroethane 29 31 6.7trichloroethene 3 J 3 J 0
o The reported Tentatively Identified Compounds (TIC's) inAppendix D have been reviewed and corrected during datavalidation. The semivolatile blanks contained several TIC's.These semivolatile TIC's were crossed out on the Form I's, andwere noted as blank contaminants.
fiR3Q2918
Page 3 of 3
The maximum concentrations of compounds found in the tripblank, equipment blanks, or method blanks are listed below.All samples with concentrations of common laboratorycontaminants less than ten times (<10X) the blankconcentration, and .uncommon laboratory contaminants less thanfive times (<5X) the blank concentration have been qualified"B11 in the data summary. (See Appendix F).
Compound Concentration
acetone * 12
* - Common Laboratory Contaminant
All data for Case 12544 were reviewed in accordance with theFunctional Guidelines for Evaluating Organic Analyses withModifications for use within Region III. The text of this reportaddresses only those problems affecting usability.
ATTACHMENTS
1) Appendix A - Glossary of Data Qualifiers2) Appendix B - Data Summary. These include:
(a) All positive results for target compounds withqualifier codes where applicable.(b) All unusable detection limits (qualified "R").
3) Appendix C - Results as Reported by the Laboratory for AllTarget Compounds
4) Appendix D - Reviewed and Corrected Tentatively IdentifiedCompounds
5) Appendix E - DPO Report for Contractual Compliance6) Appendix F - Support Documentation
DCN - DM911A10
GLOSSARY OF DATA QUALIFIER CODES (ORGANIC)
CODES RELATING TO(confidence concerning presence or absence of compounds):
U s Not detected. The associated number indicatesapproximate sample concentration necessary to bedetected*
(NO CODE) « Confirmed identification.
B - Not detected substantially above the level reportedin laboratory or field blanks.
R * Unreliable result. Analyte may or may not bepresent in the sample. Supporting data necessary toconfirm result.
N » Tentative identification. Consider present.Special methods may be needed to confirm itspresence or absence in future sampling efforts.
CODES RELATED IQ OUMTIT&TION(can'be used for both positive results and sample quantitatijlimits):
J « Analyte present. Reported value may not be accurateor precise.
K - Analyte present. Reported value may be biased high.Actual value is expected to be lower.
I, « Analyte present. Reported value may be biased low.Actual value is expected to be higher.
UJ « Not detected, quantitation limit may be inaccurateor imprecise.
TIL - Not detected, quantitation limit is probably higher.
CODES
Q - No analytical result.
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1 '1AVOLATILE ORGANICS ANALYSIS DATA SHEET
CCHOOLab Name: ISA ; ' Contract: 6S-W8-Q045 j
Lab Code: IEA Case po.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML Lab File ID: 0822306
Level: (low/med) LOW ; :: : Date Received: 8/16/89
% Moisture: not dec.100. , - .-: . ; ,. ^ ^Date Analyzed: 8/22/89
Column: (pack/cap) CAP . . \ Dilution Factor: 1.00
i • * • ' • ' -CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Qi r f. ..'..* -
i i——————j——f| 74-87-3—————Chlorornethane __________ I 10. U
74-83-9—————Brqmomethane_____.______75-01-4—————Vinyl Chloride_________75-00-3—————Chloroe thane___________75-09-2—————Methylene Chloride :.67-64-1—————Acetone ,________75-15-0—————Carbon Disulfide________75-35-4—————1,1-Dichloroethene_______75-34-3—————lrlrDichloroethane_______540-59-0—————1,2-Dichloroethene (total),67-66-3—————Chloroform_________\____"107-06-2 ————— 1,2-Dichloroethane „ ... .__78-93-3—————2-Butanone_________71-55-6—————1,1 > 1-Trichloroethane ___56-23-5—————Carbon Tetrachloride_____108-05-4—————Vinyl Acetate _________75-27-4—————Bromodichloromethane1-87-5—————1,2-Dichloropropane
10061-01-5——.-—-cis-1, 3-Dichloropropene79-01-6—————Trichloroethene124-48-1—————Dibromochloromethane_79-00-5—————1,1,2-Trichloroethane71-43-2—————Benzene
10061-02-6—————trans-1,3-Dichloropropene75-25-2—————Bromofonn108-10-1—————4-Methyl-2-Pentanone____591-78-6—————2-He?canone____________127-18-4—————Tetrachloroethene ..79-34-5—————1,1,5,2-Tetrachloroethane108-88-3—————Toluene ___________'108-90-7—————Chlorobenzene _________100-41-4—————Sthylbenzene__________100-42-5———— _____1330-20-7—————Xylene (total).
10. |U10. IU10. |U5. |U
13. IB.5. !U5. |U5. |U5. 1U5. IU5. IU10. |U5. |U5. IU10. |U5. |U5. [U5. |U5. IU5. IU5. IU5. [U5. [U5. |U10. |U10. ]U5. [U5. IU5. |U5. IU5. IU5. |U5. |U
IB EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ___
| CCHOOLab Name: IEA . Contract: 68-W8-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901403
Level: (low/med) LOW Date Received: 8/16/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/21/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2—————Phenol______________111-44-4—————bis (2-Chloroethyl) ether95-57-8—————2-Chlorophenol_______541-73-1—————1,3-Dichlorobenzene __106-46-7—————1,4-Dichlorobensene __100-51-6—————Benzyl alcohol_______95-50-1—————1,2-Dichlorobenzene __95-48-7—————2-Methylphenol108-60-1—————bis (2-Chloroisopropyl) ether106-44-5—————4-Methylphenol___________621-64-7—————N-Nitroso-di-n-propylamine_67-72-1—————Hexachloroethane_________98-95-3—————Nitrobenzene_____________78-59-1—————Isophorone______________88-75-5———--2-Nitrophenol ___________105-67-9—————2 , 4-Dimethylphenol________65-85-0—————Benzoic acid111-91-1—————bis(2-Chloroethoxy)methane_120-83-2—————2,4-Dichlorophenol________120-82-1—————1,2,4-Trichlorobenzene_____91-20-3—————Naphthalene _____________106-47-8—————4-Chloroaniline _________87-68-3—————Hexachlorobutadiene ______59-50-7—————4-Chloro-3-methylphenol ___91-57-6—————2-Methylnaphthalene ______77-47-4—————Hexachlorocyclopentadiene _88-06-2—————2,4,6-Trichlorophenol _____95-95-4—————2,4,5-Trichlorophenol _____91-58-7—————2-Chloronaphthalene ______88-74-4—————2-Nitroaniline___________131-11-3—————Dimethylphthalate ________208-96-8—————Acenap_hthylene___________606-20-2—————2,6-Dinitrotoluene________
10. |U10. |U10. |U10. |U10. IU10. (U10. JU10. [U10. (U10. |U10. |U10. IU10. |U10. |U10. JU10. IU50. |U10. |U10. |U10. |U10. |U10. |U10. |U10, IU10. IU10. IU10. |U50. |U10. |U50. IU10. IU10. "IU10. ]U
FORM I SV-1 o « 1/87 Re^
i 1C EPA SAMPLE NOSEMIVQLATILE ORGANICS ANALYSIS DATA SHEET - ______
; I CCHOOLab Name: IEA . i. Contract: 6S-W8-0045 I
Lab Code: IEA Case No.: 12544 "SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER| , „ : .„.,.„, j , Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML ^ Lab,File ID: 0901403
Q Level: (low/med) LOW ; -: Date Received: 8/16/89
% Moisture: not dec.100. dec. 0. , ,. Date Extracted: 8/21/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 " Dilution Factor: 1.00
1 ' '""" CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2—————3-Nitroaniline__83-32-9 ——— — -Aceiiaphthene____51-28-5 ————— 2,4-Dinitrophenol100-02-7 ————— 4-Nitrophenol __132-64-9—————Dibenzofuran121-14-2—————2,4-Dinitrotoluene______84-66-2—————Diet'hylPhthalate
7005-72-3—————4-Chlorophenyl-phenylether.86-73-7—————Fluorene______________"100-01-6—————4-Nitroaniline______534-52-1—————4,6-pinitro-2-methylphenol_86-30-6—————N-Nitrosodiphenylamine (1)~101-55-3 ————— 4-Bromophenyl-phenylether ~118-74-1—————Hexachlorobenzene ____"87-86-5—————Pentachlorophenol ______85-01-8—————Phenanthrene___________120-12-7—————Anthracene_____' ". ; . -84-74-2—————Di-n-butylphthalate _____206-44-0—————Fluoranthene_______-129-00-0—————Pyrene____s______i_______85-68-7—————Butylbenzylphthalate^^___91-94-1—————3,3 r-Dichlorgbenzidine___56-55-3—————Benzo(a) anthracene______218-01-9—————Chrysene ——117-81-7—————bis(2-Ethylhexyl)phthalate_117-84-0—————Di-n-octylphthalate ____"205-99-2—————Benzo(b)fluoranthene_____207-08-9—————3en2o(k)fluoranthene_____50-32-8—————Benzo(a)pyrene_________193-39-5—————Indeno( 1,2,3-cd)pyrene___53-70-3—————Dibenz(a,h)anthracene ___191-24-2—————3enzo(g,h,i)perylene_____
50. IU10. IU50. IU50. |U10. (U10. |U10. |U10. |U10. IU50. IU50. (U10. IU10. IU10. |U50. ]U10. |U10. IU10. JU10. IU10. |U10. |U20. |U10. IU10. 1U10. IU10. IU10. IU10. IU10. |U10. |U10. |U10. (U
(1) - Cannot be separated from diphenylaminei '•' •FORM I SV-2 1/87 Re
ID EPA SAMPLE NO,PESTICIDE ORGANICS ANALYSIS DATA SHEET _____
| " CCHOOLab Name: IEA Contract: 68-WS-0045 |______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No,: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL)ML * Lab File ID: DB5A4557
Level: (low/med) LOW Date Received: 8/16/89
% Moisture: not dec. 100. dec. 0. Date Extracted: 8/21/89
Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
O
319-84-6 ———— alpha-BHC319-85-7 ———— beta-BHC"51 Q_fi£*_3... _-.^c»T 4* =1 — Qtir*
58-89-9 ———— gamma-BHC76-44-8 ——— Heptachlor309-00-2 ———— Aldrin1024-57-3 ——— Heptachlor epoxide959-98-8 ———— Endosulfan I60-57-1 ——— Dieldrin72-55-9 ———— 4 4 ' -DDEf £• W ^ -3, f .U'J.U
72-20-8 ———— Endrin33213-65-9 ———— Endosulfan II
72-54-8 ———— 4 4 ' -DDDf & w / ~ Z W ~l f ±*U U
1031-07-8 ——— Endosulfan sulfate
72-43-5 ——— Methoxychlor53494-70-5 ——— Endrin ketone5103-71-9 ——— alpha-Chlordane5103-74-2 ——— gamma-Chlordane8001-35-2 ———— Toxaphene12674-11-2 ——— Aroclor-101611104-28-2 ——— Aroclor-122111141-16-5 ——— Aroclor-123253469-21-9 ——— -Aroclor-124212672-29-6 ——— Aroclor-124811097-69-1 ——— Aroclor-125411096-82-5 ———— Aroclor-1260
.050
.050
.050
.050
.050
.050
.050
.050.10.10.10.10.10.10.10.50.10.50.501.0.50.50.50.50.501.01.0
1IUiuIUiu|U iiu 1iu 1iuIUiuIUiuIUiuIUiuIUiuIUiuiuIUiuiuiuiuiuI
FORM I PEST ftR3Q2935 1/87 Rev
: 1A - ^ EPA SAMPLE NO,VOLATILE ORGANICS ANALYSIS DATA SHEET . .. . .
I CCH01Lab Name: IEA _ .Contract: 68-W8-0045 |______
Lab Code: IEA Case No.: 12544. SAS No,, t. SDG No.: CCHOO
Matrix: (soil/water) WATER ; Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML Lab rFile ID: 0822307
Level: (low/med) LOW Date Received: 8/16/89
% Moisture: not dec.100. \ .. :. Date Analyzed: 8/22/89
Column: (pack/cap) CAP ! ! Dilution Factor: 1.00
'-.- CONCENTRATION UNITS;CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
1| 74-87-3-i *?.£ — a ** — Q_j / 4 — 00 — ;? —| 75-01-4-| 75-00-3-| 75-09-2-
67-64-1-75-15-0-
; 75-35-4-ITT e ""i jf *s75-34-3-I 540-59-0-
67-66-3-107-06-2-7Q_QT_'l_/ O J J — J —
71-55-6-56-23-5-108-05-4-75-27-4-"7Q_Q*T_C_./o— o /— D—
10061-01-5-"7Q m _£C_/ y-Ul — O —124-48-1-J» £• T U ^
79-00-5-71-43-2-
10061-02-6-75-25-2-108-10-1-COT —"70— £ .
127-18-4-79-34-5-.i -• j
i na-sa— "3-.1 flQ — QH— 7— -
100-41-4-100-42-5-1330-20-7-
———— Chlpromethane ; - .———— Bromomethane———— vinyl Chloride———— Chloroe thane———— Methylene Chloride———— Acetone———— Carbon Disulf ide
^ f ±, ^ . S A U ^ " *—— '••*i4—— *A"»—
———— 1 , 1-Dichloroethane———— 1,2-Dichloroethene (total) _———— Chloroform———— 1 f 2-Dichloroethane———— 2-Butanone———— 1,1,1-Trichloroethane———— Carbon Tetrachloride
vinyi Aceuaue———— Brombdichloromethane———— 1,2-Dichloropropane———— cis-1 , 3 -Dichloroprqpene _^ _ (
^ •>* S«*A-i* V * "*«• '•**!«•**'••
———— Dibromochloromethane———— 1,1,2-Trichloroethane— — — — — uenzeiie———— trans-1 , 3 -Dichloropropene _———— Bromoform———— 4-Methyl-2-Pentanone
———— Toluene———— Chlofobenzene
———— Styrene- ——— Xvlene (total)
' !
10.10.10.10.5.10.5.5.5.5.5.5.10.5.5.10.5.5.5.5.5.5.5.5.5.10.10.5.5.5.5.5.5.5.
1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUiuIUIUIUIUIUIUIU1
FORM I VGA fl R 3 0 2 9 3 6
IB EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ' ______
II CCH01
Lab Name: IEA Contract: 68-W8-0045 1
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901404
Level: (low/med) LOW Date Received: 8/16/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/21/89
Extraction: (SepF/Cont/Sonc) CCNT Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/NJ N pH: 6.0 Dilution Factor: : 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
J
108-95-2—————Phenol_______________111-44-4—————bis (2-Chloroethyl) ether95-57-8—————2-Chlorophenol_______541-73-1—————1,3-Dichlorobenzene __
46-7—————1,4-Dichlorobenzene ______100-51-6 ——— —Benzyl alcohol___________95-50-1—————1,2-Dichlorobenzene ______95-48-7—————2-Methylphenol___________108-60-1—————bis (2-Chloroisopropyl) ether106-44-5—————4-Methylphenol___________621-64-7—————N-Nitroso-di-n-propylamine67-72-1————QQ — Q ?_•)_ __ -.__yo—yO JS-59-1—————Isophorone
•2-Nitrophenol-67-9—————2,4-Dimethylphenol_
65-85-0—————Benzoic acid111-91-1—————bis (2-Chloroethoxy) methane_120-83-2—————2,4-Dichlorophenol_______120-82-1—————1,2,4-Trichlorobenzene_____91-20-3—————Naphthalene '___________106-47-8—————4-Chloroaniline
•Hexachlorobutadiene59-50-7—————4-Chloro-3-methylphenol
•2-Methylnaphthalene77-47-4—————Hexachlorocyclopentadiene88-06-2—————2,4,6-Trichlorophenol __95-95-4—————2,4,5-Trichlorophenol __
•2-Chloronaphthalene88-74-4—————2-Nitroaniline____131-11-3—————Dimethylphthalate _208-96-8—————Acenaphthylene____606-20-2—————2,6-Dinitrotoluene
10. |U10. |U10. |U10. |U10. IU10. IU10. IU10. |U10. |U10. IU10. IU10. |U10. |U10. |U10. |U10. (U50. |U10. IU10. IU10. |U10. |U10. |U10. |U10. |U10. (U10. IU10. IU50. |U10. IU50. |U10. |U10. 'IU10. IU
FORM I SV-1 ^ rt ™ ~ -T i/87 R£SR302937
"" " "1C " " . . . -^_ ....... • EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET . ___________ -_
' -^ • | CCH01
Lab Name: IEA ,' t Contract: 68-W8-0045 |
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER _ , Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901404
Level: (low/med) LOW * Date Received: 8/16/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/21/89
Extraction: (SepF/Cont/Sonc) CCNT ___ Date Analyzed: 9/ 1/89[ '• , -- - " .t: -:._?T" pi ~~ ." -
GPC Cleanup: (Y/N) N pH: 6.0 " Dilution Factor: 1.00
:C"6NCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2 ——8*5 — T3 -Q__-c 1 i Q cDl-2o-3 —— -•100-02-7 ——132 64-9- — -.!» J A* W i-"
121 14-2- — •^ Af - j» *•84-66-2 —— •W W v A*
7005-72-3 —— -O d "7T "7oo— / J — / — — — •100-01-6 —— -534-52-1 —— •86-30-6 —— •101-55-3 —— •118-74-1 —— -D*7 QC_C_ _.__.o / — ob— O— — — •85-01-8 —— -
1 A 1 1 "7120-12-7----84-74 2 — --U X 1 ^>
206-44-0 —— -129-00-0 —— •O C CO "7O3-OO-7-- —QI -QA-1 ....
56-55-3 —— •*5i fl-.ni — Q— — --1 1 "7 O1 "T11 /-81-7 — —
on^— QQ O-__.207-08-9 —— -^n-77-fl __ -
1 Q7_'IQ_ «;_ — — .C *5 "7 f\ OD 3" /0-3----
TOT ^ Jl ^191-24-2 —— -
—— 3-Nitroaniline—— Acenaphthene—— 2 , 4-Dinitrophenol—— 4-Nitrophenol—— Dibenzofuran—— 2 , 4-Dinitrotoluene—— Diethylphthalate—— 4-Chlorophenyl-phenylether _—— Fluorene :—— 4-Nitroaniline—— 4 , 6-Dinitro-2-methylphenol _—— N-Nitrosodiphenylamine ( 1 )"__—— 4-Bromophenyl-phenylether ~_ _
—— Pentachlorophenol
—— Anthracene ...—— Di-n-butylphthalate—— Fluoranthene—— Pyrene- —— Butylbenzylphthalate—— 3 , 3 r:-Dichlorobenzidine—— Benzo ( a ) anthracene
Vr** * J »JWiA*—
. —— bis(2-Ethylhexyl)phthalate _- —— Di-n-octylphthalate ~- —— Benzo ( b ) f luoranthene. —— Benzo ( k) f luoranthene
. —— Indeno (1,2 , 3-cd)pyrene
• —— Benzo ( a , h , i ) perylene
50.10.50.50.10.10.10.10.10.50.50.10.10.10.50.10.10.10.10.10.10.20.10.10.10.10.10.10.10.10.10.10.
1IUiuIUIUIUIUIUIUIUIU!UIUIUIUIUIUIUIUIUIUiuIUIUIUIUIU .IUIUIUIUIUIUI
(1) - Cannot be separated from diphenylamine
' : FORM I SV-2 " 1/87 Re
I " ^ 1M302938
ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET
I CCH01Lab Name: IEA . Contract: 63-W3-Q045 j______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO '
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000, (g/mL)ML * Lab File ID: DB5A4555
Level: (low/med) LOW . Date Received: 8/16/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/17/89
Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
319-84-6————alpha-BHC319-85-7————beta-BHC319-86-8————delta-BHC58-89-9———gamma-BHC76-44-8————Heptachlor309-00-2————Aldrin1024-57-3———Heptachlor epoxide959-98-8————Endosulfan I60-57-1———Dieldrin72-55-9————4,4! -DDE72-20-8———Endrin
33213-65-9———Endosulfan II72-54-8————4 ,4 ' -DDD
1031-07-8———Sndosulfan sulfate50-29-3————4, 4 ' -DDT72-43-5———Methoxychlor
53494-70-5————Endrin ketone5103-71-9———alpha-Chlordane5103-74-2———gamma-Chlordane8001-35-2————Toxaphene12674-11-2————Aroclor-101611104-28-2———Aroclor-122111141-16-5———Aroclor-123253469-21-9———Aroclor-124212672-29-6————Aroclor-124811097-69-1———Aroclor-125411096-82-5————Aroclor-1260
I.050 |U.050 |U.050 |U.050 IU.050 IU.050 IU.050 [U.050 (U.10 IU.10 IU,10 |U.10 IU.10 |U.10 IU.10 IU,50 IU.10 |U.50 |U.50 |U1.0 |U.50 |U.50 [U,50 [U,50 [U,50 [U1.0 [U1.0 IU
FORM I PEST 1/87 RevAR302939
r1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET ____________; I
I CCH02Lab Name: IEA m Contract: 68-W8-0045 (___________
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
O Sample wt/vol: 5. (g/rnL) ML Lab File ID: 0822308
Level": (low/med) LOW Date Received: 8/18/89
% Moisture: not dec.100. -: ;. Date Analyzed: 8/22/89
O Column: (pack/cap) CAP '. . . r . Dilution Factor: 1.00
' ' :: '••-- CONCENTRATION UNITS:CAS NO. COMPOUND , (ug/L or ug/Kg) UG/L Q
C|
3
74-87-3—————Chloromethane _____._____| 10. |U74-83-9—————Bromomethane :______| 10. JU75-01-4—————Vinyl Chloride,75-00-3—————Chloroethanei-09-2—————Methylene Chloride_
67-64-1- , ________75-15-0—————Carbon Disulfide_75-35-4—————1,1-Dichloroethene75-34-3—————1,1-Dichloroethane^_______540-59-0—————1,2-Dichloroethene (total)_67-66-3—————Chloroform_________107-06-2—————1,2-Dichloroe thane__78-93-3—————2-Butanone. .___. ...,,..„ .71-55-6—————1,1,1-Trichloroethane56-23-5—————Carbon Tetrachloride__108-05-4—————Vinyl Acetate _____75-27-4—————Bromodichlorqrnethane
•1,2-Dichloropropane10061-01-5—————cis-1,3-Dichloropropene
79-01-6—————Trichloroethene124-48-1—————Dibromochlorome thane_79-00-5—————l,lf 2-Trichloroethane71-43-2————
10061-02-6—————trans-1,3-Dichloropropene __75-25-2—————Bromoform108-10-1—————4-Methyl-2-Pentanone_591-78-6—————2-Hexanone________"127-18-4—————Tetrachloroethene .....79-34-5—————1,1,2,2-Tetrachloroethane _
88-3—————Toluene __-• :108-90-7—————Chlorobensene100-41-4——:——Ethylbenzene_\100-42-5—————Styrene _____1330-20-7—————Xylene (total)
10. IU10. |U5. [U10. |U5. |U5. IU5. |U5. IU5. [U5. |U10. |U5. |U5. |U
10. IU5. |U5. [U5. [U5. IU5. IU5. [U5. |U5. |U5. |U10. |U10. [U5. [U5. [U5. IU5. IU5. |U5. [U5. |U
FORM I VOA flR3029^0 ' 1/87 Rev
rIB EPA SAMPLE NO
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET '________
1 CCH02Lab Name: IEA Contract: 68-W8-0045 |_______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No,: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828409O Level: (low/med) LOW Date Received: 8/18/89
% Moisture: not dec.100. dec. 0. . Date Extracted: 8/18/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 8/28/89O
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2—————Phenol______________111-44-4—————bis (2-Chloroethyl) ether95-57-8—————2-Chlorophenol_______541-73-1—————1,3-106-46-7—————1,4-100-51-6—————Benzyl alcohol
i-50-1—————1,2-Dichlorobenzene ______95-48-7—————2-Methylphenol____________108-60-1—————bis (2-Chloroisopropyl) ether106-44-5—————4-Methylphenol___________621-64-7—————N-Nitroso-di-n-propylamine_67-72-1—————Hexachloroethane
•Nitrobenzene73-59-1—————Isophorone______________88-75-5—————2-Nitrophenol ___________105-67-9—————2,4-Dimethylphenol________65-85-0———-——Bensoic acid_____________111-91-1—————bis (2-Chloroethoxy)me thane_120-83-2—————2,4-Dichlorophenol________120-82-1—————1,2,4-91-20-3—————Naphthalene __106-47-8 ————— 4-Chloroaniline
•Hexachlorobutadiene59-50-7—————4-Chloro-3-methylphenol ___91-57-6—————2-Methylnaphthalene ______77-47-4—————Hexachlorocyclopentadiene _
•2,4,6-Trichlorophenol ____•2,4,5-Trichlorophenol ____
91-58-7—————2-Chloronaphthalene88-74-4 ————— 2-Nitroaniline____131-11-3————Dimethylphthalate _208-96-8—————Acenaphthylene____606-20-2—————2,6-Dinitrotoluene_
10. |U10. IU10. [U10. [U10. IU10. IU10. IU10. |U10. |U10. |U10. |U10. |U10. |U10. IU10. IU10. IU50. |U10. IU10. |U10. |U10. |U10. |U10. |U10. |U10. IU10. IU10. IU50. IU10. |U50. ]U10. |U10. '|U10. IU
FORM I SV-1 a n o r» rt f , 1/87 -Ri
: 1C . . . . . _ ' EPA SAMPLE NCSEMIVOIATILS ORGANXCS ANALYSIS DATA SHEET
.... I CCH02
Lab Name: IEA Contract: 68-WS-Q045 |
Lab Code: IEA Case No.: 12544 SAS No.: . - SDG No.: CCHOO
Matrix: (soil/water) WATER " Lab iSample ID:
Sample wt/vol: 1000. - (g/mL) ML - Lab File ID: 0828409
Level: (low/med) LOW "ii' Date Received: 8/18/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/18/89
Extraction: (SepF/Cont/Sonc) CONT • '...Date Analyzed: 8/28/89
GPC Cleanup: (Y/N) N pH: 6.0 ^Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2—————3-Nitroaniline_____[_____83-32-9—————Acenaphthene____ :_____51-28-5 ————— 2,4-Dini'trophenol _______100-02-7 ————— 4-Nitrophenol ___________132-64-9—————Dibenzofuran_____ . ____121-14-2—————2,4-Dinitrotoluene________84-66-2—————Diethylphthalate_________
7005-72-3 ————— 4-Chlorqphenyl-phenylether _86-73-7—————Fluorene_______... ____"__100-01-6—————4-Nitroaniline___________534-52-1—————4,6-Dinitro-2-methylphenol_86-30-6—————N-Nitrosodiphenylamine (1)I_101-55-3 ————— 4-Bromophenyl-phenylether ~__118-74-1—————Hexachlorobenzene :____~__87-86-5—————Pentachlorophenol ..______85-01-8—————Phenanthrene - -----____120-12-7—————Anthracene_______________84-74-2—————Di-n-butylphthalate ______206-44-0—————Fluoranthene_____________129-00-0—————Pyrehe______ .. . . .______85-68-7—————Butylbenzylphthalate______91-94-1—————3 ,3 T -Dichlorobenzidine_____56-55-3—————Benzo (a) anthracene________218-01-9—————Chrysene_________._______117-81-7—————bis(2-Ethylhexyl)phthalate_117-84-0—————Di-n-octylphthalate ______205-99-2—————Benzo (b)f luoranthene______207-08-9—————Benzo (kjf luoranthene______50-32-8—————Benzo(a)pyrene___________193-39-5—————Indeno(l,2,3-cd)pyrene_____53-70-3—————Dibenz( a, h) anthracene191-24-2—————Benzo (g,h,i)perylene
50. IU I10. IU I50. [U I50, |U |10. IU I10. |U 110. |U |10. IU |10. |U I50. |U I50. |U I10. |U I10. |U |10. |U I50. ]U T10. IU I10. IU I10. IU I10. IU I10. |U I10. |U I20. IU I10. IU I10. IU I10. |U I10. |U 110. |U 110. [U I10. IU I10. IU I10. |U I10. .|U I
(1) - Cannot be seoarated from diphenylamine* i - , j - - - - -i FORM I SV-2 1/87 Re
ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET
| CCH02Lab Name: IEA Contract: 68-W8-0045 I
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
O Sample wt/vol: 1000. (g/mL)ML Lab File ID: DB5A4558
Level: (low/med) LOW Date Received: 8/18/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/21/89
O Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
O
O
319-84-6————alpha-BHC319-85-7————beta-BHC319-86-8————delta-BHC58-89-9————gamma-76-44-8———Heptachlor309-00-2————Aldrin1024-57-3————Heptachlor epoxide959-98-8———Endosulfan I60-57-1———Dieldrin72-55-9————4,4'-DDE72-20-8———Endrin
33213-65-9————Endosulfan II72-54-8————4,4'-DDD
1031-07-8———Endosulfan sulfate:,4f-DDT
72-43-5———Methoxychlor53494-70-5—-—Endrin ketone5103-71-9———alpha-Chlordane5103-74-2———gamma-Chlordane8001-35-2————Toxaphene12674-11-2————Aroclor-101611104-28-2———Aroclor-122111141-16-5———Aroclor-123253469-21-9————Aroclor-124212672-29-6———Aroclor-124811097-69-1———Aroclor-125411096-82-5———Aroclor-1260
.050 |U
.050 |U
.050 |U
.050 |U
.050 |U
.050 ]U
.050 IU
.050 |U.10 ]U.10 IU.10 IU.10 IU.10 |U.10 IU.10 |U.50 |U.10 |U.50 |U.50 |U1.0 |U.50 |U.50 |U.50 |U.50 |U.50 IU1.0 IU1.0 IU
FOKM I PEST 1/87flR3029U3
1A EPA SAMPLE NO.VOLATILE ORSANICS ANALYSIS DATA SHEET m___________
; |
I CCH03Lab Name: IEA . . .. Contract: 68-W8-OQ45 j___________
Lab Code: IEA Case No.: 12544 SAS Np.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.' (g/mL) ML_ Lab File ID: 0822309
Level: (low/med) LOW Date Received: 8/18/89
% Moisture: not dec.100. ', "'„ .', . , :,i .Date Analyzed: 8/22/89
Column: (pack/cap) CAP __ j : DilutionTFactor: 1.00
..-CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3 ————— Chlorornethane74-83-9 ————— Bromomethane . _75-01-4 ————— Vinyl Chloride - - - -75-00-3 ————— Chloroethane75_Q9_2- — ------Methylene Chloride67-64-1 ————— Acetone :. -75-15-0 ————— Carbon Disulfide.75-35-4 ————— 1,1-Dichloroethene75-34-3 ————— 1,1-Dichloroethane540-59-0 ————— 1,2-Dichloroethene (total)67-66-3 ————— Chloroform107-06-2 ————— 1 , 2-Dichloroethane
71-55-6 ————— 1,1,1-Trichloroethane56-23-5 ————— Carbon Tetrachloride108-05-4 ————— Vinyl Acetate75-27-4 ————— Bromodichloromethane78-87-5 ————— 1,2-Dichloropropane
10061-01-5 ————— cis-1, 3-Dichloropropene ___
124-48-1 ————— Dibromqqhlqrome thane79-00-5 ————— 1,1,2-Trichloroe thane71-43-2 ————— Benzene
10061-02-6 ————— trans-1, 3-Dichloropropene _T t "1C *1 ~» - - - — _g — - - —75-25-2 — • ——— Bromororm108-10-1 ————— 4-Methyl-2-Pentanone591-78-6 ————— 2-Hexanone
108-90-7 ————— Chlorcbenzene100-41-4 ————— Ethylbenzene,4. W W 1 4_ _^ _^W.T-«B S_>AA^^
1330-20-7 ————— Xylene (total)
10.10.10.10.5.19.5.5.5.5.5.5.
170.5.5.10.5.5.5.5.5.5.5.5.5.10.10.5.5.5.5.5.5.5.
1IUIUIUIUinIBiuiu
. iuiuiu[U1iuiuITTITJiuiuiu!U|U|UiuiuiuiuiuIUiuIUIUiuIU1
VOA
IB EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET •_________
I CCH03Lab Name: IEA • Contract: 68-W8-0045 ______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828410
Level: (low/med) LOW Date Received: 8/18/89
% Moisture: not dec. 100. dec. 0. Date Extracted: 8/22/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 8/28/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
-Phenol111-44-4—————bis (2-Chloroethyl) ether95-57-8—————2-Chlorophenol_______541-73-1—————1,3-Dichlorobenzene __106-46-7—————1,4-100-51-6—————Benzyl alcohol____95-50-1—————1,2-Dichlorobenzenej-48-7—————2-Methylphenol
108-60-1————bis (2"Chloroisopropyl) ether106-44-5 ————— 4-Methylphenol___________621-64-7—————N-Nitroso-di-n-propylamine_67-72-1—————Hexachloroethane
-Nitrobenzenet-59-1—————Isophorone
88-75-5—————2-Nitrophenol ___105-67-9—————2,4-Dimethylphenol_65-85-0—————Benzoic acid111-91-1—————bis (2-Chloroethoxy) methane_120-83-2—————2,4-Dichlorophenol________120-82-1—————1,2,4-Trichlorobenzene____91-20-3—————Naphthalene
•4-Chloroaniline87-68-3—————Hexachlorobutadiene59-50-7—————4-Chloro-3-methylphenol91-57-6—————2-Methylnaphthalene __77.47-4—————Hexachlorocyclopentadiei88-06-2—————2,4,6-Trichlorophenol __95-95-4—————2,4,5-Trichlorophenol __91-58-7—————2-Chloronaphthalene __88-74-4—————2-Nitroaniline_______131-11-3—————Dimethylphthalate ____
606-20-2—————2,6-Dinitrotoluene
72. |10. |U10. IU10. IU10. IU10. |U10. |U10. |U10. ]U10. |U10. |U10. IU10. |U10. IU10. IU10. |U50. IU10. IU10. |U10. IU10. |U10. |U10. |U10. IU10. IU10. IU10. IU50. |U10. IU50. |U10. |U10. IU10. |U •
SR30291t5 l'j
.: 1C ... ' EPA SAMPLE NCSEMIVOLATILE ORGANICS ANALYSIS DATA.SHEET ____________
.- , - ., - • . - " : • | CCH03Lab Name: IEA Contract: 68-W8-0045 |
Lab Code: IEA . Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML '.__ Lab File ID: 0828410
Level: (low/med) LOW - "Date Received: 8/18/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/22/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 8/28/89
GPC Cleanup: (Y/N) N , pH: 6.0 Dilution Factor: 1.00
' " - - CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or -ug/Kg) UG/L Q
i : : i——————i——i1 99-09-2 ————— 3-Nitroaniline .:. . ... I 50. |U I
S3-3 2-9—————Acenaohthene __________| 10. JU I51-28-5—————2,4-Dinitrophenol ___,____| 50. |U I100-02-7 ————— 4-Nitrophenol ___________I 50. |U |132-64-9—————Dibenzofuran_______;______\ 10. |U I
_ 121-14-2—————2,4-DinitrQto_luene____ .__.. I 10. 1U |" "84-66-2—————Diethylphthalate_________I 10. |U I7005-72-3 ————— 4-Chlorophenyl-phenylether_| 10. JU |86-73-7—————Flubrene . ... ' I 10. IU I100-01-6—————4-Nitroaniline___________| 50. [U 1534-52-1 ————— 4,6-Dinitro-2-methylphenol_| 50. IU I86-30-6—————N-Nitrosodiphenylamine (1)"_| 10. IU I101-55-3—————4-Bromophenyl-phenylether "_1 10. |U j118-74-1—————Hexachlorobenzene I 10. |U |87-86-5—————Pentachlorophenol .____| 50. |U I85-01-8—————Phenanthrene_______ I 10. | U |120-12-7—————Anthracene______________| 10. |U |84-74-2—————Di-n-butylphthalate ______| 10. IU j206-44-0—————Fluoranthene]_____________| 10. JU |129-00-0—————Pyrene_________________| 10. JU I85-68-7—————Butylbenzylphthalate______| 10. |U I91-94-1—————3 ,3 ' -Dichlorobenzidine____| 20. |U I56-55-3—————Benzo (a) anthracene________j 10. |U j218-01-9—————Chrysene__________:_____| 10. [U I117-81-7—————bis(2-Ethylhexyl)phthalate _J 10. |U I117-84-0—————Di-n-octylphthalate | 10. |U |205-99-2—————Benzo (b)f luoranthene______I 10. |U 1207-08-9—————Benzo(k)f luoranthene______| 10. |U |50-32-8—————Benzo (a)pyrene___________j 10. JU [193-39-5—————Indeno(l,2,3-cd)pyrene____| 10. |U |53-70-3—————Dibenz(a,h)anthracene _____j 10. |U j191-24-2—————Benzo (g,h,i)perylene_____ | 10. JU j
(1) - Cannot be separated from diphenylamine
FORM I SV-2 1/87 Re
: ^ ^ "^ flR3029U6 '
rID EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET ____
| - CCH03Lab Name: IEA Contract: 68-W3-0045 |______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (sail/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL)ML • Lab File ID: DB5A4560
Level: (low/med) LOW Date Received: 8/18/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/21/89
Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
O
O
319-84-6————alpha-BHC319-85-7————beta-BHC319-86-8————delta-BHC58-89-9————gamma-BHC76-44-8———Heptachlor309-00-2————Aldrin1024-57-3———Heptachlor epoxide959-98-8———Endosulfan I60-57-1———Dieldrin72-55-9————4,4'-DDE72-20-8———Endrin
33213-65-9————Endosulfan II72-54-8————4,41-DDD
1031-07-8———Endosulfan sulfate50-29-3————4,4f -DDT72-43-5———Methoxychlor
53494-70-5———Endrin ketone5103-71-9———alpha-Chlordane5103-74-2———gamma-Chlordane8001-35-2————Toxaphene12674-11-2————Aroclor-101611104-28-2————Aroclor-122111141-16-5———Aroclor-123253469-21-9———Aroclor-124212672-29-6———Aroclor-124811097-69-1————Aroclor-125411096-82-5————Aroclor-1260
.050 |U
.050 |U
.050 |U
.050 )U
.050 IU
.050 ]U
.050 IU
.050 IU.10 |U.10 IU.10 IU.10 |U.10 |U.10 |U.10 |U.50 IU.10 |U.50 |U.50 )U1.0 |U.50 IU.50 IU.50 |U.50 |U.50 |U1.0 |U1.0 |U
FORM i PEST flR3029U7 1>f87 Rev
r. .:... • . - - i - - •. -1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET ______________I
• - - — - - - - * • ' | CCH04Lab Name: IEA Contract: 6S-W8-OQ45 I
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML \ Lab File ID: 0822313
Level: (low/med) LOW Date Received: 8/18/89
% Moisture: not dec.100. ; _^Date Analyzed: 8/22/89
Column: (pack/cap) CAP \ . Dilution Factor: 1.00
! ~ ", ' ... CONCENTRATION UNITS:CAS NO. COMPOUND , (ug/L or ug/Kg) UG/L Q
74-87-3 ——74-83-9 ——75-01-4 ——75-00-3 ——75-09-2 ——67-64-1 ——75-15-0 ——75-35-4- —1 W —4 _/ j»
~7 e "5 A n75-34-3 ——540-59-0 ——£ 7 — A £ _ "5 _ — _
107-06-2 ——78-93-3 —— -71-55-6 ——C f ™l "5 !?56-23-5 —— •108-05-4 —— •"T C ^ A75-27-4- — •7fl — Q7 — R — — _.
10061-01-5 —— -79-01-6 —— -124-48-1 —— -79-00-5 —— -71-43-2 ———
10061-02-6 —— -7K_^ C — T —/ 3™ -i3*"Z— — — -108-10-1 —— -5Q1 — 7fl — £-.— . -1 ?7 — 1 Q — A — — — .79-34-5 ———1 — ' V * "• «J
1 OS-Sfl — "5— — — -1 053 — 00 — 7 — — — -100-41-4 —— r100-42-5 ———1330-20-7 ———
—— Chloromethane—— Bromomethane—— Vinyl Chloride—— Chloroethane
fc*W 1— >i*_J __%__'! A S_ «a* t A. V_V<V ____ . _ .. __
——— Acetone—— Carbon Disulfide—— 1 , 1-Dichloroethene—— 1 , 1-Dichloroethane—— 1,2-pichloraethene . (total) _—— Chloroform—— 1 , 2-Dichloroethane—— 2-Butanone—— 1,1,1-Trichloroethane—— Carbon Tetrachloride
r 11 J. JAW— > W*i WC
—— Bromodichlororne thane—— 1 , 2-Dichloropropane—— cis-1, 3 -Dichloropropeiie ___—— Trichloroethene—— Dibromochloromethane—— 1 , 1 , 2-Trichloroethane
—— trans-l/3-Dichloropropene _. —— Bromofonn
*_w «>*A_2 _• _• *—*— -i-k***rf**1—>
- —— 2-Hexanone_> <u • «— . i— fc«irf»_rf. ^ A. *rf ••_ <B*_<H>4<A^v
• —— 1,1,2,2-Tetrachloroethahe _
s*iiJ,W_. WA-"i.ll<.*CiliV—
•— — — Ft~Hvl fo 'n 7*e*ne*ij*— iijr ^ w«x*4 iAw.-. — -. c v VT n Afcj> W^ — • WllW
—— Xylene (total)i
10.10.10.10.5.10.5.5.5.5.5.5.10.5.5.10.5.5.5.5.5.5.5.5.S.10.10.5.5.5.5.5.5.5.
1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU -IUIUIUIUiuIU
• iuIUiuIUIU .IU1
flfi30291(8 i/87 K«M31
r
1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
I CCH05Lab Name: IEA Contract: 68-W8-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML Lab File ID: 0831303
Level: (low/med) LOW Date Received: 8/25/89
%.Moisture: not dec.100. Date Analyzed: 8/31/89
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
C
O
iI 74-87-3 ——
1 75-01-4 ——| 1 — * v> _> X
1 75-00-3 ——
| 75-15-0 —— •1~r i™ « i r* * 475-35-4 —— •1*7 C — 1 jl • 175-34-3 —— •I 540-59-0 —— •| 67-66-3 —— -| 107-06-2 —— •
I 71-55-6 —— -I 56-23-5 —— -I 108-05-4 —— •IT C. *• t *T A75-27-4 —— •1 7Q..Q7 — c: _ .,.
[10061*01-5 —— •
I 124-48-1 —— -
I 71-43-2 —— •i * _• A •—« _•110061-02-6 —— -i 7 c; _•?=;.. •?— — *..| 108-10-1 —— -
1 127-18-4 —— -| UV — • V «W W "X
| 79-34-5 —— -
i 108-90-7 —— •
i 1QQ-42-5 ———| U* U U "1 _» ~JIt — t *^ rt O rt ~T1330-20-7 ———
—— Chloromethane—— Bromomethane—— Vinvl Chloride——— Chloroethane—— Methvlene Chloride
—— Carbon Disulfide—— 1 , 1-Dichloroethene—— 1 f 1-Dichloroethane—— 1 f 2-Dichloroethene ( total ) _—— Chloroform—— 1,2-Dichloroethane—— 2-Butanone
—— Carbon TetrachlorideV J«t_j[ Jv «-% rt v *•<•_. '—.'w.
—— Bromodichloromethane—— 1 , 2-Dichloropropane—— cis-1, 3-Dichloropropene ___- —— Trichloroethene—— Dibromochloromethane—— 1 , 1 f 2-Trichloroethane
—— trans-1, 3-Dichloropropene _——— Bromof orm—— 4-Methyl-2-Pentanone——— 2 -Hexano ne
—— 1,1,2,2-Tetrachloroethane _
- —— Chlorobenzene
b> v*^ — > <- ** -*• —— Xvlene "(total)
10.10.10.10.5.10.5.5.34.5.5.5.10.29.5.10.5.5.5.3.5.5.5.5.5.10.10.5.5.5.5.5.5.5.
1
IUiuIUIU[Uiu|U1IUiuIUiuIiuiuiuIUIU1 JIUIU -iuIUiuiuiuiuiu!Uiuiuiu |IU |1
FORM i VOA AR3G29^9 -/"
rIB EPA SAMPLE NO
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET '________m
I ' - - - - | CCH05Lab Name: IEA ' t ~ . Contract: 63-W8-0045 I____________
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901409
Level: (low/med) LOW Date Received: 8/25/89
% Moisture: not dec.100. dec. 0. : Date. Extracted: 8/25/89
Extraction: (SepF/Cont/Sonc) CONT . . Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N | pH: 6.0 _ ' ; Dilution Factor: 1.00
i . : • CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2—————Phenol ____________111-44-4—————bis(2-Chloroethyl)ether95-57-8 ————— 2-Chlorophenol_____.541-73-1—————1,3-Dichlorobenzene106-46-7—————1,4-Dichlorobenzene
Cjfc 1 100-51-6—————Benzyl alcohol95-50-1—————1,2-Dichlorobenzene _____95-48-7—————2-Methylphenol_____108-60-1—————bis (2-Chloroisopropyl) ether"106-44-5—————4-Methylphenol_________621-64-7—————N-Nitroso-di-n-propylamine^"67-72-1—————Hexachloroethane _____"_98-95-3—————Nitrobenzene _ ________"78-59-1—————Isophorone_______________88-75-5—————2-Nxtrophenol ___________105-67-9—————2,4-Dimethylphenol______"65-85-0—————Benzoic acid _____111-91-1—————bis (2-Chloroethoxy)methane120-83-2—————2,4-Dichlorophenol______"120-82-1—————I,2r4-Trichlorobenzene____"91-20-3—————Naphthalene '_______ "106-47-8 ————— 4-Chloroaniline - -87-68-3—————Hexachlorobutadiene . .59-50-7—————4-Chloro-3-methylphenol __"91-57-6—————2-Methylnaphthalene _____"77-47-4—————Hexachlorocyclopentadiene _88-06-2—————2,4,6-Trichlorophenol ____~95-95-4—————2t 4,5-Trichlorophenol _____91-58-7—————2-Chloronaphthalene ______88-74-4 ————— 2-Nitroaniline______;____"131-11-3—————Dimethylphthalate _______)208-96-8—————Acenaphthylene______;_____606-20-2 ————— 2,6-Dinitrotoluene_______[
10. |U10. |U10. |U10. |U10. [U10. |U10. |U10. |U10. |U10. |U10. IU10. |U10. IU10. (U10. |U10. |U50. IU10. IU10. [U10. ]U10. IU10. |U10. |U10. |U10. |U10. |U10. [U50. (U10. |U50. |U10. |U10. |U10. |U
EPA SAMPLE NO
| CCH05Lab Name: IEA Contract: 68-W8-0045 I______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901409
Level: (low/med) LOW ' Date Received: 8/25/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/25/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2—————3-Nitroaniline___83-32-9—————Acenaphthene______51-28-5—————2,4-Dinitrophenol100-02-7—————4-Nitrophenol "132-64-9—————Dibenzofuran_____121-14-2—————2,4-Dinitrotoluene84-66-2—————Diethylphthalate-72-3—————4-Chlorophenyl-phenylether_
86-73-7—————Fluorene_______________100-01-6—————4-Nitroaniline__________534-52-1—————4,6-Dinitro-2-methylphenol_86-30-6—————N-Nitrosodiphenylamine (1)~101-55-3 ————— 4-Bromophenyl-phenylether _118-74-1—————Hexachlorobenzene
•Pentachlorophenol85-01-8——— ___________120-12-7—————Anthracene_____________84-74-2—————Di-n-butylphthalate _____206-44-0—————Fluoranthene____________129-00-0—————Pyrene________________85-68-7—————Butylbenzylphthalate_____91-94-1—————3,3' -Dichlorobenzidine56-55-3—————Benzo (a) anthracene______218-01-9—————Chrysene_______________117-81-7—————bis(2-Ethylhexyl)phthalate_117-84-0—————Di-n-octylphthalate
-Benzo (b) f luoranthene^207-08-9—————Benzo (k)f luoranthene"
32-s—————Benzo (a) pyrene______39-5—————Indeno (1,2,3-cd)pyrene_
53-70-3—————Dibenz(a,h)anthracene191-24-2—————Benzo (g ,h, i) perylene
50. [U10. |U50. IU50. |U10. |U10. IU10. |U10. |U10. IU50. [U50. |U10. IU10. |U10. [U50. IU10. IU10. |U10. |U10. |U10. IU10. IU20. ]U10. IU10. |U10. |U10. |U10. |U10. IU10. IU10. IU10. IU10. IU
(1) - Cannot be separated from diphenylamine
FORM I SV-2 1/87 ReSR30295I
r
ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET ______________
- - •- - - 1 I| CCH05 I
Lab Name: IEA Contract: 68-W8-0045 I____________1
Lab Code: IEA Case No.: 12544 SAS No.: ' SDG No.: CCHOO
Matrix: (soil/water) WATER , Lab Sample ID:
> Sample wt/yol: 1000. (g/mL)ML • Lab File ID: DB5A4564
Level: (low/med) LCW . -T Date Received: 8/25/89
% Moisture: not dec.100. '., dec. 0. ^ Date Extracted: 8/29/89
r> Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 ..._._. Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
319-84-6 ——— alpha-BHC319-85-7 ——— beta-BHC31 Q — Q £_Q____..,-3i-» 1 +-a— tatir1
58-89-9 ——— gamma-BHC76-44-8 ———— Heptachlor
I 309-00-2 ———— AldrinI 1024-57-3 ——— Heptachlor epoxide
959-98-8 ——— Endosulfan I60-57-1 ——— Dieldrin
72-20-8 ——— Endrin33213-65-9 ———— Endosulfan II
72-54-8 ———— 4 4 ' -DDD1 — • «J * w f , "4 _^ l. ._
1031-07-8 ——— Endosulfan sulfate50-29-3- — — -4 4 ' -T)DT•— ' W *• — / — ' 1,1 i»/XS_.
72-43-5 ——— Methoxychlor53494-70-5 ——— Endrin ketone5103-71-9 ——— alpha-Chlordane5103-74-2 ——— gamma-Chlordane8001-35-2 ——— Toxaphene12674-11-2 ——— Aroclor-101611104-28-2 ——— r-Aroclor-122111141-16-5 ———— Aroclor-123253469-21-9 ———— Aroclor-124212672-29-6 ———— Aroclor-124811097-69-1 ——— Aroclor-125411096-82-5 ——— Aroclor-1260
.050
.050
.050
.050
.050
.050
.050
.050.10.10.10.10.10,10.10.50.10.50.501.0.50.50.50.50.501.01.0
iiuiuiuiuiuiuiuIUiuIUIUIUIUIUIUIUIUiuIUiuiuiuIUiuiuiuiu1
FORM I PEST ^R302952 . 1/87
1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______________
i .I CCH06
Lab Name: IEA Contract: 63-W8-0045 j________
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML Lab File ID: 0831304
Level: (low/med) LOW Date Received: 8/25/89
% Moisture: not dec.100. Date Analyzed: 8/31/89
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3 ————— Chloromethane/ ** — o j **;? —— ———— n-7OuiOiiieuiia.iis75-01-4 ————— Vinyl Chloride75-00-3 ————— Chloroethane75-09-2 ————— Methylene Chloride
75-15-0 ————— Carbon Disulfide
75-34-3 ————— 1,1-Dichloroethane540-59-0 ————— 1,2-Dichloroethene (total) _67-66-3 ————— Chloroform107-06-2 ————— 1 , 2-Dichloroethane78-93-3 ————— 2-Butanone
108-05-4 ————— Vinyl Acetate75-27-4 ————— Bromodichlorome thane78-87-5 ————— 1 , 2-Dichloropropane
10061-01-5 ————— cis-1, 3-Dichloropropene79-01-6 ————— Trichloroethene124-48-1 ————— Dibromochloromethane79-00-5 ————— 1 , 1 , 2-Trichloroethane
10061-02-6 ————— trans-1, 3-Dichloropropene _75-25-2 ————— Bromoform .108-10-1 ————— 4-Methyl-2-Pentanone591-78-6 ————— 2-Hexanone127-18-4 ————— Tetrachloroethene79-34-5 ————— 1 ,1,2, 2-Tetrachloroethane _
108-90-7 ————— Chlorobenzene100-41-4 ————— Ethylbenzene
1330-20-7 ———— Xylene (total)
10.10.10.10.5.10.5.5.36.5.5.5.10.31.5.10.5.5.5.3.5.5.5.5.5.10.10.5.5.5.5.5.5.5.
tIU!UIUIUIU IIU|U 1iu 11IUIUIUIU1IUIUIUIUIU1 Jiu|UiuIUIUIUIUiuiuIUiuIUiuIU.1
3R3G2953FORM I VOA 1/87 Rev
/ — • ' ' ' --.- _ . _ _ — — - " - : . - - - - . - - — - - - - -
IB : SPASEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
.
^ * • .:: _,*•''* r • . - | CCH06Lab Name: IEA -' ' Contract: 68-W8-0045 |
Lab Code: IEA Case No.: 12544 SAS No,: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901410
Level: (low/med) LOW ; Date Received: 8/25/89
% Moisture: not dec.100. dec. 0. T Date Extracted: 8/25/89
Extraction: (SepF/Cont/Sonc) CONT, ._ ... _.Date. Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 .,. 1 Dilution Factor: 1.00
; ^ -XON-ENTRATION UNITS:CAS.NO. COMPOUND (ug/L or ug/Kg) UG/L Q
111-44-4—————bis;(2-Chloroethyl) ether95-57-8 ————— 2-Chlorophenol_______541-73-1—————l,3|-Dichlorobenzene __106-46-7—————1,4-Dichlorobenzene __100-51-6—————Benzyl alcohol_______95-50-1—————1,2-Dichlorobenzene __
•2-Methylphenol108-60-1—————bis (2-Chloroisopropyl) ether106-44-5 ————— 4-Methyiphenol_________621-64-7—————N-Nitroso-di-n-propylaminea_67-72-1—————Hexachloroethane
108-95-2—————Phenol _" _ _ - _ - - - - \ 10, |U10. |U10. |U10. |U10. |U10. [U10. |U10. |U10. |U10. |U10. |U10. |U10. JU10. [U10. |U10. |U50. |U10. |U10. |U10. IU10. [U10. IU10. IU10. |U
78-59-1—————Isophorone______________88-75-5 ————— 2-Nitrophenol _________105-67-9—————2,4-Dimethylphenol________65—85—0———•"———Benzoic acid_____________111-91-1—————bis (2 -Chloroe thoxy) methane^
"-83-2 ————— 2,4-Dichlorophenol120-82-1—————1,2,4-Trichlorobenzene____91-20-3—————Naphthalene ____ . .106-47-8—————4-Chloroaniline ________"87-68-3—————Hexachlorqbutadiene _____59-50-7—————4-Chloro-3-methylphenol __"91-57-6—————2-Methylnaphthalene _____"77-47-4—————Hexachlorocyclopentadiene J88-06-2—————2,4,6-T.richlorophenol ___™95-95-4—————2,4,5-Trichlorophenol ___"91-58-7—————2-Chloronaphthalene .______"88-74-4—————2-Nitroaniline_____ -131-11-3—————Dimethylphthalate ______"
-96-8—————Acenaphthylene606-20-2—————2,6-Dinitrotoluene
10. |U10. |U10. |U50. |U10. |U50. IU-10. |U10. '|U10. IU
FORM I SV-1
1C EPA SAMPLE NOr SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ___
I CCH06Lab Name: IEA Contract: 68-W8-0045 j______
Lab Code: IEA Case No-: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901410
Level: (low/med) LOW 4 Date Received: 8/25/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/25/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2 ————— 3-Nitroaniline __________83-32-9 ————— Acenaphthene ___________51-28-5 ————— 2, 4-Dinitrophenol ______100-02-7 ————— 4-Nitrophenol- __________132-64-9 ————— Dibenzofuran ____121-14-2 ————— 2 , 4-Dinitrotoluene ______84-66-2 ————— Diethylphthalate ________
7005-72-3 ————— 4-Chlorophenyl-phenylether_86-73-7 ————— Fluorene ______________ "100-01-6 ————— 4-Nitroaniline __________534-52-1 ————— 4,6-Dinitro-2-methylphenol_86-30-6 ————— N-Nitrosodiphenylamine (1)~101-55-3 ————— 4-Bromophenyl-phenylether ~118-74-1 ————— Hexachlorobenzene ______ "87-86-5 ————— Pentachlorophenol ______85-01-8 ————— Phenanthrene ___________120-12-7 ————— Anthracene _____________84-74-2 ————— Di-n-butylphthalate _____206-44-0 ————— Fluoranthene ____129-00-0^- ———— Pyrene ________________85-68-7 ————— Butylbenzylphthalate _____91-94-1 ————— 3 , 3 ! -Dichlorobenzidine ___56-55-3 ————— Benzo (a) anthracene ______218-01-9 ————— Chrysene117-81-7 ————— bis(2-Ethylhexyl)phthalate.117-84-0 ————— Di-n-octylphthalate ____ ]205-99-2 ————— Benzo (b)f luoranthene _____207-08-9 ————— Benzo (k)f luoranthene _____50-32-8 ————— Benzo(a)pyrene _________193-39-5 ————— Indeno(l,2,3-cd)pyrene ___53-70-3 ————— Dibenz ( a ,h) anthracene ___191-24-2 ————— Benzo (g,h,i)perylene _____
(1) - Carihot'be separated from diphenylamine
50. |U10. |U50. |U50. IU10. |U10. |U10. |U10. |U10. |U50. |U50. |U10. |U10. IU10. IU50. |U10. |U10. |U10. |U10. |U10. IU10. |U20. IU10. IU10. IU10. IU10. |U10. |U10. IU10. |U10. |U10. |U10. |U
FORM I SV-2 1/87 ReflR302955
ID EPA SAMPLE NO,PESTICIDE ORGANICS ANALYSIS DATA SHEET
I CCH06Lab Name: IEA Contract: 68-W8-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER ; Lab Sample ID:
Sample wt/vol: 1000. (g/mL)ML • Lab File ID: DB5A4566
Level: (low/med) LOW Date Received: 8/25/89
% Moisture: not dec.100, dec. 0. Date Extracted: 8/29/89
Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
; CONCENTRATION UNITS:CAS NO. COMPOUND _ (ug/L or ug/Kg) UG/L Q
319-84-6————alpha-BHC319-85-7————beta-BHC319-86-8————delta-BHC58-89-9————ganuna-BHC76-44-8————Heptachlor309-00-2————Aldrin1024-57-3———Heptachlor epoxide959-98-8———Endosulfan I60-57-1———Dieldrin72-55-9————4,4'-DDE72-20-8———Endrin
33213-65-9———Endosulfan II72-54-8————4,4'-DDD
1031-07-8———Endosulfan sulfate50-29-3 ———— 4,4!-DDT72-43-5———Methoxychlor
53494-70-5———Endrin ketone5103-71-9———alpha-Chlordane5103-74-2———gamma-Chlqrdane8001-35-2———Toxaphene12674-11-2————Aroclor-101611104-28-2———Aroclor-122111141-16-5————Aroclor-123253469-21-9————Aroclor-124212672-29-6———Aroclor-124811097-69-1———Aroclor-125411096-82-5———Aroclor-1260
I.050 |U.050 |U.050 IU.050 (U.050 IU.050 |U.050 |U.050 IU.10 |U.10 ]U.10 IU.10 IU.10 IU.10 |U.10 IU• 50 IU.10 IU.50 |U.50 [U1.0 |U.50 |U.50 |U.50 |U.50 |U.50 |U1.0 |U1.0 |U
FORM I PEST ' 1/87 Rev
1A EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET
I CCH07Lab Name: IEA Contract: 63-W8-0045 I
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML Lab File ID: 0831305
Level: (low/med) LOW Date Received: 8/26/89
% Moisture: not dec.100* Date Analyzed: 8/31/89
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
o
o
74-87-3—————Chloromethane74-83-9 —— —— -Bromome thane__75-01-4—————Vinyl Chloride75-00-3—————Chloroethane
•Methylene Chloride67-64-1—————Acetonei-15-0—————Carbon Disulfide
-1,1-Dichloroethene______•1,1-Dichloroethane______-1,2-Dichloroethene (total)
r-66-3—————Chloroform107-06-2—————1,2-Dichloroethane__78-93-3—————2-Butanone_________71-55-6—————1,1,1-Trichloroethane56-23-5—————Carbon Tetrachloride_108-05-4—————Vinyl Acetate _____75-27-4—————Bromodichloromethane_78-87-5—————1,2-Dichloropropane
10061-01-5—————cis-1,3-Dichloropropene79-01-6—————Trichloroethene ____124-48-1—————Dibromochloromethane_79-00-5—————1,1,2-Trichloroethane71-43-2————
10061-02-6—————trans-1,3-Dichloropropene75-25-2—————Bromoform108-10-1—————4-Methyl-2-Pentanone,
78-6—————2-Hexanone-18-4—————Tetrachloroethene
79-34-5—————1 f 1,2,2-Tetrachloroethane•Toluene
108-90-7—————Chlorobenzene100-41-4——-——Ethylbenzene100-42-5—————Styrene _____1330-20-7—————Xylene (total).
10. IU10. |U10. |U10. IU5. IU
170. IB5. |U5. [U5. |U48. |5. |U12. |10. |U12. |5. |U10. |U5. |U5. |U5. |U53. |5. |U5. |U5. |U5. |U5. IU
11. I10. |U4. | J5. [U5. |U5. |U5. |U5. |U5. IU
an o n o Q c "7_™. _ ._. HO Uel 3 3 / 1/87 Rev
r
IB , EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ____ ___
1 * = - • - " * • : ' • • • . I CCH07Lab Name: IEA Contract: 68-W8-0045 |______
Lab Code: IEA Case No.: 12544 SAS No.: . SDG No.: CCHOO
Matrix: (soil/water) WATER __ . Lab Sample ID:
Sample wt/vol: 1000. ' (g/mL) ML Lab File ID: 0911407
Level: (low/med) LOW Date Received: 8/26/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/30/89
Extraction: (SepF/Cont/Sonc) SEPF ^ Date Analyzed: 9/11/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2—————Phenol______111-44-4————-bis(2-Chloroethyl)ether __95-57-8 ————— 2-Chlorophenol__________541-73-1—————1,3 -Dichlorobenzene .106-46-7—————1,4-Dichlorobenzene _____"100-51-6—————Benzyl alcohol__________95-50-1—————1,2-Dichlorobenzene _____"95-48-7—————2-Methylphenol .. .____"108-60-1—————bis (2-Chloroisopropyl) ether"106-44-5 ————— 4-Methylphenol .. /' "621-64-7—————N-Nitroso-di-n-propylamine_"67-72-1—————Hexachloroethane ___~98-95-3—————Nitrobenzene____.._._. ._____78-59-1—————Isophorone_____________"88-75-5—————2-Nitrophenol ____________105-67-9—————2,4-Dimethylphenol _____65-85-0—————Benzoic acid ____"111-91-1—————bis(2-Chloroethoxy)methane_"120-83-2—————2,4-Dichlorophenol________120-82-1—————1,2,4-Trichlorobenzene____91-20-3—————Naphthalene _____________"106-47-8—————4-Chloroaniline _________"87-68-3—————Hexaqhlorobutadiene __,____59-50-7—————4-Chioro-3-methylphenol __"91-57-6—————2-Methylnaphthalene _______"77-47-4—————Hexachlorocyclopentadiene_88-06-2—————2,4,6-Trichlorophenol ___"95-95-4—————2,4,5-Trichlorophenol [____~m91-58-7—————2-Chloranaphthalene ______88-74-4—————2-Nitroaniline__________]131-11-3—————Dimethylphthalate _______]208-96-8—————Acenaphthylene___________606-20-2—————2,6-Dinitrotoluene________
10. IU10. (U10. |U10. IU10. |U10. |U10. |U10. [U10. |U10. |U10. IU10. (U10. |U10. |U10. |U10. IU50. |U10. |U10. IU10. |U10. IU10. ]U10. IU10. |U10. |U10. |U10. |U50. |U10. IU50. (U10. .|U10. IU10. |U
FORM i sv-i4R302958 1/87
1C EPA SAMPLE NCSEMI VOLATILE ORGANICS ANALYSIS DATA SHEET ____________
| CCH07Lab Name: IEA Contract: 68-W8-0045 [_____
Lab Code: IEA Case No,: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER . _. Lab 'Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0911407
Level: (low/med) LOW • Date Received: 8/26/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/30/89
Extraction: (SepF/Cont/Sonc) *SEPF Date Analyzed: 9/11/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
J
ft? ?7 QSI 9ft S
inn n7 7132-64-9 ———•if -J *• W X ->
1 71 —1 A-.7 — — —Q A _£ C n _.O4— too— Z— — — —
7005-72-3 ———O tf ~T "5 ~T
100-01-6 ———E? ™t >* C •"* •*534-52-1 ——— •
101-55-3 ——— -1 1 fl-7-l-1 —— — -.Q7 — QK t£ — _.
1 7H-1 '7—7 — - -,8 A — 7 A — 7— — — — .
206-44-0 ——— -129-00-0 ——— -85-68-7 ——— -
Sfi cc t01 a_ni -Q— — -.1 1 7— QI — 7 — __-..1 17 — QA — 0 — - — --205-99-2 ————****** _f _< _*C A 0*5 Q50-j.i-S — - —
1 QT — Q_c;— ___-
191-24-2 ————_W — ' U. _• '4 _r
—— 3-Nitroaniline^ ^ _/\csno.pri wiiGns—— 2 , 4-Dinitrophenol—— 4-Nitrophenol—— Dibenzofuran- — 2 , 4-Dinitrotoluene—— Diethylphthalate—— 4-Chlorophenyl-phenylether _—— Fluorene— 4-Nitroaniline—— 4 1 6-Dinitro-2-methylphenol _—— N-Nitrosodiphenylamine (1) _—— 4-Bromophenyl-phenylether _
nts -ddiiui tjiJGii-* ciit-—— Pentachlorophenol—— Phenanthrene
Ar^+*Viv-a r*^n&jHwlltil— T^lCGnC
—— Di-n-butylphthalate- — Fluoranthene- — Pyrene• — Butylbenzylphthalate- — 3,3 ' -Dichlorobenzidine- — Benzo ( a ) anthracene
.-tt. — .- f c-c^r^dt—iiir _r *— <cnc—bis ( 2-Ethylhexyl)phthalate _- — Di-n-octylphthalate• — Benzo ( b ) f luoranthene- — Benzo ( k ) f luoranthene• — Benzo ( a ) pyrene• — Indeno (1,2, 3-cd ) pyrene. — Dibenz ( a ,h) anthracene
T 2 _ _ / y« £ \ — .rt >— *»1 Ar\^Ds.iiio , ti , j- j yttijf icnc
50.10.50.50.10.10.10.10.10.50.50.10.10.10.50.10.10.10.10.10.10.20.10.10.10.10.10.10.10.10.10.10.
iiuIUiutuiuIU Iiu !IUIUiuIUiuIUiuiutuiuiuiuiuiuiuiuIUiuiuiuIUiuiu
•!° ((1) - Cannot be separated from diphenylamine
FORM I SV-2 1/87 ReSR302959 •
PESTICIDE ORGANICS ANALYSIS DATA SHEET _______ LE
~_ == ~? ^ ! CCH07Lab Name: IEA ,. _"" ' Contract": 68-W8-0045 1______
Lab Code: IEA Case No.: 12544 SAS No.: ' SDG No.: CCHQQ
Matrix: (soil/water) WATER . I ab Sample ID:
> Sample wt/vol: 1000. (g/mL)ML * Lab File ID: DB5A4568
Level: (low/med) LOW Date Received: 8/26/89
% Moisture: not dec.100. dec. 0. Pate Extracted: 8/28/89
r> Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
1 - CONCENTRATION UNITS: "CAS NO. COMPOUND . (ug/L or ug/Kg) UG/L Q
j 319-84-6————alpha-BHC| 319-85-7————beta-BHC| 319-86-8————delta-BHC1 58-89-9———gamma-BHC| 76-44-8———Heptachlor[ 309-00-2———AldrinI 1024-57-3———Heptachlor epoxide| 959-98-8———Endpsulfan II 60-57-1———DieldrinI 72-55-9————4,4'-DDE1 72-20-8———Endrin| 33213-65-9————Endpsulfan III 72-54-8————4,4!-DDDj 1031-07-8———Endpsulfan sulfate[ 50-29-3————4, 4' -DOT| 72-43-5———Methoxychlor| 53494-70-5———Endrin ketpne| 5103-71-9———alpha-Chlordanej 5103-74-2———gamma-Chlordanej 8001-35-2———Toxaphenet 12674-11-2————Aroclor-1016| 11104-28-2————Aroclor-1221| 11141-16-5———Aroclor-1232| 53469-21-9————Aroclor-1242| 12672-29-6———Aroclor-1248I 11097-69-1———Aroclor-1254
.050 IU
.050 |U
.050 |U
.050 |U
.050 IU
.050 |U
.050 |U
.050 [U.10 IU.10 [U.10 |U.10 IU.10 |U.10 [U.10 |U.50 |U.10 IU.50 |U.50 |U1-0 |U.50 |U.50 |U.50 [U,50 |U.50 |U1.0 |U
11096-82-5————Aroclor-1260 | 1.0 [U
FORM I PEST 1/87 Re\
, : i:; SR302960
1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
I ccHoaLab Name: IEA Contract: 63-W8-OQ45 ____
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCEOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML Lab File ID: 0831306
Level: (low/med) LOW Date Received: 8/26/89
% Moisture: not dec.100. Date Analyzed: 8/31/89
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3 ————— Chlorome thane7 4 - 8 3 - 9 ————— Bromome thane75-01-4 ————— Vinyl Chloride75-00-3 ————— Chloroethane
O / 0*41, — — — — — rtCSuOllS75-15-0 ————— Carbon Disulfide75-35-4 ————— 1,1-Dichloroethene75-34-3 ————— 1,1-Dichloroe thane540-59-0 ————— 1,2-Dichloroethene (total) _67-66-3 ————— Chloroform107-06-2 ————— 1,2-Dichloroethane
/ o — jj — j— — — — £.~~ ouucmoiis71-55-6 ————— 1 „ 1 . 1-Trichloroethane
108-05-4 ————— Vinyl Acetate75-27-4 ————— Bromodichlorome thane78-87-5 ————— 1,2-Dichloropropane
10061-01-5 ————— cis-1, 3-Dichloropropene ___79-01-6 ————— Trichloroethene124-48-1 ————— Dibromochloromethane79-00-5 ————— 1,1,2-Trichloroethane
10061-02-6 ————— trans-1, 3-Dichloropropene _75-25-2 ————— Bromoform108-10-1 ————— 4-Methyl-2-Pentanone591-78-6 ————— 2-Hexanone127-18-4 ————— Tetrachloroethene
/ - 7 J r t 3 _-,,_. f £, f £• J.S Ui cLWii-Lwiwe; UIIcLilc108-88-3 ————— Toluene108-90-7 ————— Chlorobenzene100-41-4 ————— Ethylbenzene
10.10.10.10.5.10.5.5.5.5.5.5.10.5.5.10.5.5.5.5.5.5.5.5.5.10.10.5.5.5.5.5.5.5.
1|UIU|U!UIUIUiu iIU 'IUIUIUiuiuIUIUIUIUIUIUIUiuIUIUIUIUiuIUIUIUIUIUIUIU jIU1
FORM I VOA fl R 3 0 2 9 6 1 1/87 Rev
rI B , „ ; . , . - E P A SAMPLE N O .
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
"••""' : I CCH08Lab Name: IEA ^ .& Contract: 63-W8-0045 |______
Lab Code: IEA Case No.:.12544 SAS No.: . SDG No.: CCHOO
Matrix: (soil/water) WATER, . i., ..Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0911409
Level: (low/med) LOW " :. Date Received: 8/26/89
% Moisture: not dec.lQQ, dec. 0. Date Extracted: 8/28/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/11/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
: ' CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2—————Phenol_________________111-44-4—————bis (2-Chloroethyl)ether __"m95-57-8 ————— 2-Chlorophenol___________541-73-1—————1,3-Dichlorobenzene _____]106-46-7—————1,4-Dichlorobenzene _____]100-51-6—————Benzyl alcohol___________95-50-1—————1,2-Dichlorobenzene _____"95-48-7—————2-Methylphenol__________"108-60-1—————bis (2-Chloroisopropyl) ether"106-44-5—————4-Methylphenol___________621-64-7—————N-Nitroso-di-n-propylamine_67-72-1—————Hexachloroethane________"98-95-3—————Nitrobenzene_______ "78-59-1—————Isophorone_____________88-75-5—————2-Nitrophenol __________105-67-9—————2,4-Dimethylphenol_______65-85-0—————Benzoic acid111-91-1—————bis (2-Chloroethoxy)me thane_120-83-2—————2,4-Dichlorophenol________120-82-1—————1,2,4-Trichlorobenzene____91-20-3—————Naphthalene ____________"106-47-8—————4-Chloroaniline _________~87-68-3—————Hexachlorobutadiene : -59-50-7—————4-Chioro-3-methylphenol __91-57-6—————2-Methylnaphthalene ______"77-47-4—————Hexachlorocyclopentadiene _"88-06-2—————2,4,6-Trichlorophenol ____"95-95-4—————2,4,5-Trichlorophenol ____"91-58-7 ————— 2-Chloronaphthalene -____"88-74-4 ————— 2-Nitroa.niline___________*131-11-3—————Dime thy Iphthalate _______"208-96-8—————Acenaphthylene___________"606-20-2 ————— 2,6-Dinitrotoluene________
10. [U10. |U10. |U10. |U10. |U10. |U10. |U10. IU10. [U10. |U10. ]U10. IU10. [U10. |U10. |U10. |U50. IU10. |U10. IU10. |U10. |U10. |U10. |U10. IU10. IU10. IU10. |U50. |U10. |U50. JU10. .|U10. |U10. |U
FORM I SV-1 fiDOfionro ' 1/87 Re
1C " EPA SAMPLE NCSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ________ _____
I CCH08Lab Name: IEA Contract: 68-W8-0045 1______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0911409
Level: (low/med) LOW ' Date Received: 8/26/89% Moisture: not dec.100. dec. 0. Date Extracted: 8/28/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/11/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
.? i? — U j ** £. — — — 3 fi -L V.J. UculX.L J.ilt;83-32-9 ————— Acenaphthene51-28-5 ————— 2,4-Dinitrophenol100-02-7 ————— 4-Nitrophenol132-64-9 ————— Dibenzofuran121-14-2 ————— 2 , 4-Dinitrotoluene84-66-2 ————— Diethylphthalate
7005-72-3 ————— 4-Chlorophenyl-phenylether86-73-7 ————— Fluorene100-01-6 ————— 4-Nitroaniline534-52-1 ——— - — 4,6-Dinitro-2-methylphenol _86-30-6 ————— N-Nitrosodiphenylamine (1) _101-55-3 ————— 4-Bromophenyl-phenylether _118-74-1 ————— Hexachlorobenzene87-86-5 ————— Pentachlorophenol85-01-8 ————— Phenanthrene
84-74-2 ————— Di-n-butylphthalate206-44-0 ————— Fluoranthene129-00-0 ————— Pyrene85-68-7 ————— Butylbenzylphthalate91-94-1 ————— 3 , 3 ' "Dichlorobenzidine
117-81-7 ————— bis(2-Ethylhexyl)phthalate _117-84-0 ————— Di-n-octylphthalate205-99-2- ————— Benzo (b)f luoranthene207-08-9 ————— Benzo (k)f luoranthene
193-39-5 ————— Indeno(l,2,3-cd)pYrene53-70-3 ————— DibenzC a, h) anthracene191-24-2 ————— Benzo (g,h,i)perylene
-
50.10.50.50.10.10.10.10.10.50.50.10.10.10.50.10.10.10.10.10.10.20.10.10.10.10.10.10.10.10.10.10.
1IUIUIUIUIUIUIU .iu 1iuIUIUIUiuIUIUIUIUIUiuIUtuiuIUIU|UiuIUIUIUiuiu•1" (
•
ft(1) - Cannot be separated from diphenylamine
FORM I SV-2 1/87 Re
&R3Q2963
r . - . .
EPA SAMPLE NO,
| CCH08Lab Name: IEA i; Contract: 68-W8-0045 |_ _
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER _, . . , Lab Sample ID:
Sample wt/vol: 1000. (g/mL)ML - Lab File ID: DB5A4569
Level: (low/med) LOW \ ... Date Received: 8/26/89
% Moisture: not dec. 100. dec. 0. Date Extracted: 8/28/89
Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 T :__. Dilution Factor: 1.00
UNITS :CAS NO. COMPOUND _ (ug/L or ug/Kg) UG/L
1 : . • , •I 319-84-6 ———— alpha-BHC
"71 Q — sm — "7 — — — — _T-t«+-3 —rsErr*JJ.-7 03 / — — se&a, ariw
58-89-9 ———— gamma-BHC76-44-8 ———— Heptachlor309-00-2 ——— Aldrin1024-57-3 ——— Heptachlor epoxide959-98-8 ——— Endosulfan I60-57-1 ——— Dieldrin77 — =;=;-Q— -_-.- A _it -.nnp72-20-8 ——— Endrin
33213-65-9 ——— Endosulfan II72-54-8- —— --4 4 ' DDDI f* -J ~* <ij ~X f ±J±S±J
1031-07-8 ——— Endosulfan sulfate
72-43-5 ——— Methoxychlor53494-70-5 ——— Endrin ketone5103-71-9 — — — alpha-Chlordane _ . . . . . .5103-74-2 ——— gamma-Chlordane8001-35-2 ——— Toxaphene12674-11-2 ———— Aroclor-101611104-28-2 ——— Aroclor-122111141-16-5 ——— Aroclor-123253469-21-9 ———— Aroclor-124212672-29-6 ——— Aroclor-124811097-69-1 ——— Aroclor-125411096-82-5 ——— Aroclor-1260
,050.050.050.050.050.050.050.050.10.10.10.10.10.10.10.50.10.50.501.0.50.50.50.50.501.01.0
1IUIUIUIUIUIUIUIUiuiuiuIUIUIUIUiuIUIUIUIUiuiuIUIU[UIUIU1
FORM I PEST . 1/87
1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______________
1 CCH09Lab Name: IEA Contract: 68-W3-0045 j______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML Lab File ID: 0831307
Level: (low/med) LOW Date Received: 8/26/89
% Moisture: not dec.100. Date Analyzed: 8/31/89
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3 ————— Chloromethane74-83-9 ————— Bromome thane75-01-4 ————— Vinyl Chloride75-00-3 ————— Chloroethane75-09-2 ————— Methylene Chloride\J * W X _» C >h*iM *•*•****-»
75-15-0 ————— Carbon Disulfide75-35-4 ————— 1,1-Dichloroethene75-34-3 ————— 1,1-Dichloroe thane540-59-0 ————— 1,2-Dichloroethene (total)67-66-3 ————— Chloroform107-06-2 ————— 1,2-Dichloroethane78-93-3 ————— 2-Butanone71-55-6 ————— 1,1, 1-Trichloroe thane
108-05-4 ————— Vinyl Acetate75-27-4 ————— Bromodichloromethane78-87-5 ————— 1 , 2-Dichloropropane
10061-01-5 ————— cis-1, 3-Dichloropropene ___i J \JJrn W ^L_> U.'wll.L WX. Ww U. i'— 11<_>
124-48-1 ————— Dibromochlorome thane79-00-5 ————— 1,1,2-Trichloroethane
10061-02-6 ————— trans-lf 3-Dichloropropene _»t •• ^ ™* ~» »* _ - _ — _ _ff _ _ ___75-25-2 —— —--Bromoform108-10-1 ————— 4-Methyl-2-Pentanone591-78-6 ————— 2-Hexanone
108-88-3 ————— Toluene108-90-7 ————— Chlorobenzene100-41-4 ————— Ethvlbenzene100-42-5 ————— Stvrene1330-20-7 ————— Xvlene (total)
10.10.10.10.5.8.5.5.5.5.5.5.10.5.5.10.5.5.5.5.5.5.5.5.5.10.10.5.5.5.5.5.5.5.
1IUIU
iuIUIBJiuiuiu[UiuIUIUiuIUIUiuiuiuiuiuiuiuIU
IU
iuIUiuIUiuiu ;|U II I
FORM I VOA " 1/87 RevflR302965
; IB EPA SAMPLE NO.SEMIVOLATILE CRGANICS ANALYSIS DATA SHEET
. . : - , . -- _ I CCH09Lab Name: IEA r Contract: 68-W8-0045 |______
Lab Code: IEA Case No.: 12544 _ SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. , (g/mL) ML Lab File ID: 0911410
Level: (low/med) LOW ; Date Received: 8/26/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/28/89
Extraction: (SepF/Cont/Scnc) CONT Date Analyzed: 9/11/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
: CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2—————Phenol______________111-44-4—————bis (2-Chloroethyl)ether ___95-57-8 ————— 2-Chlorophenol___________541-73-1—————1,3-Dichlorobenzene ^______106-46-7—————1,4-Dichlorobenzene . ____100-51-6—————Benzyl alcohol___________95-50-1—————1,2-Dichlorobensene ______95-48-7 ————— 2-Methylphenol___________108-60-1—————bis (,2-Chloroisopropyl) ether106-44-5 ————— 4-Methylphenol___________621-64-7—————N-Nitroso-di-n-propylamine_67-72-1—————Hexachloroethane____98-95-3—————Nitrobenzene______i_______78-59-1—————Isophorone ____\_____88-75-5 ————— 2-Nitrophenol ___________105-67-9 ————— 2,4-Dimethylphenol________65-85-0—————Benzoic acid111-91-1—————bis (2-Chloroethoxy)me thane_120-83-2 ————— 2,4-Dichlorophenol______120-82-1—————1,2,4-Trichlorobenzene____91-20-3—————Naphthalene ... _____106-47-8—————4-Chloroaniline ________~87-68-3—————Hexachlorobutadiene _^____~59-50-7—————4-Chloro-3-methylphenol _._91-57-6—————2-Methylnaphthalene ______77-47-4—————Hexachlorocyclopentadiene _88-06-2—————2,4,6-Trichlorophenol ____~95-95-4—————2,4,5-Trichlorophenol____"91 58-7 ————— 2-Chloronaphthalene _____388-74-4—————2-Nitroaniline.____~131-11-3—————Dimethylphthalate ________208-96-8—————Acenaphthylene___________606-20-2—————2,6-Dinitrotoluene_______~
10. |U10. |U10. |U10. |U10. IU10. IU10. IU10. |U10. |U10. |U10. |U10. |U10. |U10. |U10. |U10. |U50. |U10. |U10. [U10. |U10. |U10. |U10. |U10. |U10. |U10. IU10. |U50. |U10. |U50. |U10. |U10. '|U10. |U__I
Fc^Misv-1- UR3Q2966
r- EPA SAMPLE NC
I CCH09Lab Name: IEA Contract: 68-W8-0045 I______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHQO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0911410
Level: (low/med) LOW ' Date Received: 8/26/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/28/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/11/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
C 99-09-2 ————— 3-Nitroaniline ___________83-32-9 ————— Acenaphthene _____________51-28-5 ————— 2 , 4-Dinitrophenol ________100-02-7 ————— 4-Nitrophenol ___________132-64-9 ————— Dibenzofuran _____________121-14-2 ————— 2 , 4-Dinitrotoluene _______84-66-2 ————— Diethylphthalate _________
7005-72-3 ————— 4-Chlorophenyl-phenylether _86-73-7 ————— Fluorene ________________100-01-6 ————— 4-Nitroaniline ___________534-52-1 ————— 4f 6-Dinitro-2-methylphenol _86-30-6 ————— N-Nitrosodiphenylamine (1) _101-55-3 ——— — 4-Bromophenyl-phenylether _118-74-1 ————— Hexachlorobenzene ________87-86-5 ————— Pentachlorophenol ________85-01-8 ————— Phenanthrene _____________120-12-7 ————— Anthracene ______________84-74-2 ————— Di-n-butylphthalate ______206-44-0 ————— Fluoranthene _____________129-00-0 ————— Pyrene _________ - _______85-68-7 ————— Butylbenzylphthalate ______91-94-1 ————— 3 , 3 f -Dichlorobenzidine _____56-55-3 ————— Benzo (a) anthracene ________218-01-9 ————— Chrysene
O I 117-81-7—————bis (2-Ethylhexyl) phthalate_117-84-0—————Di-n-octylphthalate205-99-2 ————— Benzo (b)f luoranthene207-08-9 ————— Benzo (k)f luoranthene50-32-8 ————— Benzo(a)pyrene193-39-5 ————— Indeno( 1,2, 3 -cd) pyrene53-70-3 ————— Dibenz( a ,h) anthracene191-24-2 ————— Benzo (g,h,i)perylene
50. )U10. IU50. IU50. |U10. |U10. |U10. [U10. IU10. |U50. IU50. IU10. |U10. |U10. |U50. |U10. |U10. |U10. IU10. |U10. IU10. |U20. IU10. IU10. |U10. |U10. |U10. |U10. |U10. |U10. IU10. |U10. .IU
(1) - Cannot be separated from diphenylamine
FORM I SV-2 1/87 Re88302967
ID EPA SAMPLE NO,PESTICIDE ORGANICS ANALYSIS DATA SHEET
<. - " . " - • • ? - . - | CCH09Lab Name: IEA Contract: 68-W8-0045 |
Lab Code: ISA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/raL)ML ^ Lab File ID: DB5A4570
Level: (low/med) LOW _ Date Received: 8/26/89
% Moisture: not dec. 100. dec. 0. _ Da?e Extracted: 8/28/89
Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1,00
"CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
319-84-6————alpha-BHC 1 .050 |U319-85-7————beta-BHC319-86-8————delta-BHC58-89-9————gamma-BHC76-44-8———Heptachlor309-00-2———Aldrin1024-57-3———Heptachlor epoxide959-98-8———Endosulfan I60-57-1———Dieldrin72-55-9————4,4'-DDE72-20-8———Endrin
33213-65-9———Endosulfan II72-54-8————4,4 '-DDD
1031-07-8———Endosulfan sulfate50-29-3————4,4'-DOT72-43-5———Methoxychlor
53494-70-5———Endrin ketone5103-71-9———alpha-Chlordane5103-74-2———gamma-Chlordane8001-35-2———Toxaphene12674-11-2————Aroclor-101611104-28-2———Aroc-lor-122111141-16-5———Aroclor-123253469-21-9————Aroclor-124212672-29-6———Aroclor-124811097-69-1———Aroclor-125411096-82-5———Aroclor-1260
.050 IU
.050 |U
.050 [U
.050 IU
.050 |U
.050 |U
.050 |U.10 |U.10 |U.10 IU.10 ]U.10 IU.10 |U.10 IU.50 |U.10 |U.50 [U.50 |U1.0 IU.50 IU.50 [U.50 IU.50 |U.50 |U1.0 |U1.0 |U
FORM I PEST • 1/87 Re\
flR302968
IS EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ____________TENTATIVELY IDENTIFIED COMPOUNDS I ————————————
: I CCHOOLab Name: IEA . Contract: 63-W8-0045
Lab Code: ISA Case No-: 12544 SAS No.: • SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML , Lab File ID: 0822306
Level: (low/med) LOW Date Received: 8/16/89
% Moisture: not dec.100. Date Analyzed: 8/22/89
Column: (pack/cap) CAP - - -- ; Dilution Factor: ... 1..00
- CONCENTRATION UNITS:Number TICs found: 0 .-,:.. (ug/L or ug/Kg) UG/L
CAS NUMBER
1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25,26.27.28.29.30.
.
; COMPOUND NAME
r . i
,
I
I
t
RT | EST. CONC.r . . . . . . , | — . -, . i . ._
111111111111111I1111111I1!11111
Q
FORM I VOA-TJCT 1/87 Re
- - f IF . -- ... -. . -- - EPA SAMPLE NCSEMIVOLATILE ORGANICS ANALYSIS DATA S2EET ____________
TENTATIVELY IDENTIFIED COMPOUNDS II CCHOO
Lab Name: IEA Contract: 68-W8-0045 I
Lab Code: IEA Case No.: 12544 .SAS No.: SDG No..: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901403
Level: (low/med) LOW ' Date Received: 8/16/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/21/89
Extraction: (SepF/Cont/Sohc) CONT . . . . Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 12 (ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME
_. . . 3. 4 _____ ---• — --— I TJN^MCWNT _ „ i TrvrryvTOT,rvr
—— 3-, ——————— - —— —4. - -5. - -6. - -7. - -8. - -9. - -10. - -11. - -12. - -13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
-WKNGWN ——————————————UNKNOWN
I UNKNOWNUNKNOWN AROMATIC[UNKNOWN — - 'UNKNOWNUNKNOWNUNKNOWNUNKNOWNUNKNOWN
i 1| RT
—— i —— i ——— 8.62—— i ——— 3—43 —
1 10 081 10.671 14.721 18.70
- : - i 18.971 19.051 20.73I 22.101 22.631 23.031111
: 111111111
- 1111
: I1
EST. CONC. Q!_...___ —— .. ..-_Q — f-3-T— -————— «-= — S-BT? —
20 I"077>vi 20./// /jrf 10.
&*<"£ ?2*s • .20.to~Tfi'~>.-*7i+r-
10!50.10.40.
JJJJJJJJJ
FORM I SV-TIC 1/87 R
: " I" flR30297l '
r
C
O
IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ___________TENTATIVELY IDENTIFIED COMPOUNDS |
I CCH01Lab Name: IEA Contract: 68-W8-0045 I
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHQO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML . Lab File ID: 0822307
Level: (low/med) LOW Date Received: 8/16/89
% Moisture: not dec.100. Date Analyzed: 8/22/89
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/L
CAS NUMBER | COMPOUND NAME^ __ -__« ——————— s ——— -:.,,...,.. J ---< —————— -i—— - —————————————————————————————————————— : ——————— * ————
1. 1' 2. !
3. 14. 15. 16. 17. I8. 19. !
10. 111. 112. 113. 114. 115. I16. I17. I18. I19. I20. !21. |'22. |~ 23. I24. I2 5 . |26. 127. I28. |29. I30. 1
1
RT EST. CONC. Q
A-W^
-_h —
FORM I VOA-TIC 1/87 Re
flR302372
-" IF EPA SAMPLE NCSSM1VOLATILE ORGANICS ANALYSIS DATA SHSST .____________
TENTATIVELY IDENTIFIED COMPOUNDS I-LT-.K.*- . i . • I CCH01Lab Name: I2A ... _ .Contract: 68-W8-0045 I
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901404
Level: (low/med) LOW -; Date Received: 8/16/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/21/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 4 Jug/L or ug/Kg) UG/L
CAS NUTXSER 1 COMPOUND NAME
— In ————————T _
3. - -—— 4-, ——————— - —— ___
5.6.7.8.9.10.11.12.13.14.15.16. !17. 118. I19. I20, 121. I22. i
1 23. I24. I25. I26. I27. I28. I29. 130. 1
i
t TTKlT'xTrrWltT ', lJ*<*>-»i w VV.t - -
-UN-KNCWN ————UNKNOWNU N WN
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9.6710 08
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FORM I SV-TIC " 1/87 R
:; " . : - ' ",::Mft"R'302973 '
IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ____________TENTATIVELY IDENTIFIED COMPOUNDS [
I CCH02Lab Name: IEA Contract: 63-W8-0045 |
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER. Lab Sample ID:
Sample wt/vol: 5.' (g/mL) ML . Lab File ID: 0822303
Level: (low/med) LOW Date Received: 8/18/89
% Moisture: not dec.100. Date Analysed: 8/22/39iColumn: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/L
1CAS NUMBER | COMPOUND NAME
1. 1-2. i3. !4. i5. i6. i7. 18. i9. 1
10. 111. 112. i13. 114. i15. i16. I17. 118. !19. i20. I'21. - IJ22. i23. I24. 125. 126. 127. 128. 129. 130. [
1
RT EST. CONC.
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FORM I VOA-TIC 1/87 Re
v«A/
r . : IF EPA SAMPLE NCSSMIVOLATILE ORGANICS ANALYSIS DATA SHEET ____________
TENTATIVELY IDENTIFIED COMPOUNDS |~~——————————I CCH02
Lab Name: IEA Contract: 63-W8-0045 j
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828409
Level: (low/med) LOW - Date Received: 8/18/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/13/89
Extraction: (SepF/Cont/Sonc) CONT Date Analysed: 8/28/89
GPC Cleanup: (Y/N) N ' pH: 6.0 Dilution Factor: 1.00
.CONCENTRATION UNITS:Number TICs found: 4 (ug/L or ug/Kg) UG/L
CAS NUMBER i COMPOUND NAME1 — -J J.i — t, ——————1 -»1 —— a-* ——————— " —— "" —13. - -1 —— 4, ——————— - —— —1 5.1 6.! 7.! 8.1 9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
f^JNKNGWN —————— : ————————— : — « ——[-UNKM WNUNKNOWN , — - .. , ;- -UNKNOWN ——————— - ————— -- - • : ——
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FORM I SV-TIC 1/87 R
• flR302975
IE EPA SAMPLE NO-VOLATILE ORGANICS ANALYSIS DATA SHEET ____________TENTATIVELY IDEOTIFIED COMPOUNDS I
1. CCH03Lab Name: ISA. Contract: 68-W8-0045 I__
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML . Lab File ID: 0822309
Level: (low/med) LCW Date Received: 8/18/89
%_ Moisture: not dec.100. • Date Analyzed: 8/22/89
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 1 • (ug/L or ug/Kg) UG/L
i i i i———————j| CAS NUMBER 1 COMPOUND NAME | RT 1 EST. CONC. 1 Q
1. 109-99-92.3.4.5.6.7.a.9.10.11.12.13.14.15.16.17.18.19.20.21.'22.23.24.25.26.27.28.29.30.
Furan, tetrahydro- 11.63 100. J
A*r
— * —
FORM I VOA-TIC 1/87 Re
flR30Z976
IF : EPA SAMPLESSMIVOLATILS CRGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS. . I- - - - - | CCH03
Lab Name: IEA : , . Contract: 68-W8-0045 I
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER _ Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828410
Level: (low/med) LOW . _: :: Date Received: 8/18/89
% Moisture: not dec. 100. dec. 0* . . Date Extracted: 8/22/89
Extraction: (SepF/Cont/Sonc) CONT ^ ..„_,« Date Analyzed: 8/28/89
-GPC Cleanup: (Y/N) N pH: 6.0 _ Dilution Factor: 1.00
• ""' CONCENTRATION UNITS:Number TICs found: 6 ; , (ug/L or ug/Kg) UG/L
CAS NUMBER
1. - --j _3. - -4. 104-76-75. 872-50-46. 149-57-57.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30. 1
1
,: 1.COMPOUND NAME | RT
UNKNOWN I 8.62•UNKNOWN- ———————— - ————————— 1 ——— 9.43UNKNOWN ' I 9.671-Hexanol, 2-ethyl- I 11.682-Pyrrolidinone, 1 -methyl- _ j 11.88Hexanoic acid, 2-ethyl- I 13.33
i1iiI11i1111Iii1!111111
^ 11
EST. CONC.
20.— ^0D3>~1 q"""" 40?}"~* 1000.r*"' 100.
QJ
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FORM I SV-TIC 1/87 EifiR302977 '
IE EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET _____________TENTATIVELY IDENTIFIED COMPOUNDS [
[ CCHQ4Lab Name: IEA Contract: 63-WS-QQ45 |_______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML ' Lab File ID: 0822313
Level: (low/med) LOW Date Received: 8/18/89
% Moisture: not dec.100. Date Analyzed: 8/22/89
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/L
1GAS NUMBER | COMPOUND NAME
1. I2. 13. 14. 15. 16. 17. 18. 19. 1
10. I11. !12. 113. i14. 115. 116. 117. 118. 119. 120. i21. 122. I23. 124. 125. 126. 127. 128. 129. I30. I
1
RT EST. CONC.— ———— . ———— Q
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-A.
FORM I VOA-TIC 1/87 Re
fiR3Q?378
IS EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _____________TENTATIVELY IDENTIFIED COMPOUNDS [
| CCH05Lab Name: IEA -..- - Contract: 63-W8-0045 I______
Lab Code: IEA Case No.: 12544 SAS No.: • SDG No.: CCHOO
Matrix: (soil/watsr) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML , Lab File ID: 0831303
Level: (low/med) LOW Dates Received: 8/25/89
% Moisture: not dec. 100. : Date Analyzed: 8/31/89
Column: (pack/cap) CAP : Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/L
1 ' 1CAS NUMBER | COMPOUND NAME ( RT
i. i • • i2. 1 . ' |3. I '- : 1 '4. 1 15. 1 16. 1 17. 1 ^-18. 1 19. 1 1
10. 1 I11. 1 '112. 1 I13. 1 114. 1 I15. I 116. I I1 7 . I ' 118. I I19. 1 I20. 1 I21. 1 I22. I I23. 1 I24. I I25. I I26. I I27. | I28. 1 I29. 1 130. 1 1
1 1
EST. CONC.=====
Q
FORM I VOA-TIC 1/87 Rev
- 1 flR30297"9
IF EPA SAMPLESEMIVOLATILE ORGANICS ANALYSIS DATA SHEET __
TENTATIVELY IDENTIFIED COMPOUNDS II CCH05
Lab Name: IEA Contract: 68-W8-0045 I______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: .CCHOQ
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901409
Level: (low/med) LOW Date Received: 8/25/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/25/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 2 (ug/L or ug/Kg) UG/L
iCAS NUMBER \ COMPOUND NAME
» 1 w.t. .l'w ti *,i
2. - - I UNKNOWN3. 14. I5. 16. 17. 18. 19. I
10. I11. 112. 113. 114. 115. !16. I17. 118. 119. I20. I21. 122. I23. ]24. I25. I26. 127. I28. I29. I30. 1
1
1RT 1 EST. CONC.B A -i j r> 3 f*i -i -.10 7 j'""/" lo!
i Zf& k.\ f o-r- 7 ** s»~~-<+'7~dst'
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ftFORM I SV-TIC , 1/87 R
rIE EPA SAMPLE NO.
VOLATILE CRGANICS ANALYSIS DATA SHEET ____________TENTATIVELY IDENTIFIED COMPOUNDS 1———————————
| CCH06Lab Name: IEA - Contract: 68-W8-0045 |______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML > Lab File ID: 0831304
Level: (low/med) LOW : Date Received: 8/25/89
% Moisture: not dec.100. , .. . >- Date Analyzed: 8/31/89
Column: (pack/cap) CAP . : Dilution Factoi::. . 1.00
; CONCENTRATION UNITS:Number TICs found: 1 - (ug/L or ug/Kg) UG/L
1 1I CAS NUMBER [ COMPOUND NAME
|1. - - [UNKNOWN1 2 . 11 3. 1! 4. II 5. 1! 6. |17. I1 8. !1 9 . 11 10. 11 11. 11 12. 11 13. I1 14. I! 15. 11 16. 11 17. !1 18. 11 19. 11 20. 1I 21. II 22. 11 23. 11 24. 11 25. 1I 25. I1 27. 11 28. 11 29. II 30. i1 I
RT
5.20
EST. CONC.
5.
Q
J
FORM:I VOA-TIC .. 1/87 Re
"-AR302981 ' -""'
-____ IF EPA SAMPLE N<.SEMIVOLATILE ORGANICS" ANALYSIS DATA SHEET ___________
TENTATIVELY IDENTIFIED COMPOUNDS I "I CCH06
Lab Name: IEA Contract: 68-W8-0045 j
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.:
Matrix: (soil/water) WATER Lab 'Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901410
Level: (low/med) LOW * Date Received: 8/25/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/25/89
Extraction: (SepF/Cont/Sonc) COOT " Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 4 (ug/L or ug/Kg) UG/L
iCAS NUMBER i COMPOUND NAME
————— ————— | .HTT ,_ .^___^. ^ ^____. ————— .Tr
i — ± ——— . , -4.tT>nc rcwN — ~- • • -2. - - [UNKNOWN
__ 3...J ——————— . —— - — (-UNXNCWN"- •-•••' • — '•»- "--— i- ...«4. - - [UNKNOWN5. I6. 17. Ia. .]9. I10. i
11. i12. 113. !14, 115. I16. I17. i18. I19. I20. [21. 122. 123. 124. 125. 126. !27. I28. I29. 130. 1
I
RT
9 42>^ • £ J~
9.67....... 10-tlO •J. U • .*. w
10.68„
EST. CONC.
...-) Q •Sk --•-.. -j y *£>„/•» 10lt/2J?/&4 "it/ t~3 fa** - f\
J. U I
20.£/ /4r{ot iTrf j*£*s*& T &AS
•
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4_v—*_FORM I SV-TIC 1/87 E^
: • IE EPA SAMPLEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED. COMPOUNDS I
| CCH07Lab Name: IEA . ;s .Contract: 63-WS-Q045 j
Lab Code: IEA Case No".: 12544 SAS No.: • SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML Lab File ID: 0831305
Level: (low/med) LOW Date Received: 8/26/89
% Moisture: not dec.100. . ' "" ., ; Date Analysed: 8/31/89
Column: (pack/cap) CAP Dilution Factor: 1-00
; CONCENTRATION UNITS:Number TICs found: 1 (ug/L or ug/Kg) UG/L
1| CAS NUMBER— ™— ~"~" ~* ~"11. - -
1 2.\ 3.1 4.I 5.1 6.1 7.i a.I 9.! 10.1 11.1 12.1 13.1 14.1 15.1 16.1 17.1 18.! 19.1 20.1 21.I 22.i 23.I 24.1 25.1 26.i 27.! 23.1 29.i 30.I
ICOMPOUND NAME | RT
UNKNOWN "-" | 7.65|111
' 1' 1
11111111111.-.. ,1
- - 111
- 11111111
EST. CONC.
20.
QJ
FORM I VOA-TIC 1/87 Re-
_ ,-Vr-fiR3Q2983
IF . EPA SAMPLE NSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ____________
TENTATIVELY IDENTIFIED COMPOUNDS II CCE07
Lab Name: IEA Contract: 63-WS-Q045 I
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO*
Matrix: (soil/water) WATER Lab'Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0911407
Level: (low/med) LOW ' Date Received: 8/26/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/30/89
Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/11/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 2 (ug/L or ug/Kg) UG/L
iCAS NUMBER I COMPOUND NAME
_,,,.,!-, _,..„, — , ___ — j.UNKNSW T— •• - — • ————————————————2 . 128-37-0 [ Phenol, 2 , 6-bis 1 1 , 1 -dimethyl3. i4. . i5. 16. 17. i8. !9. 1
10. I11. 112. I13. i14. I15. I16. I17. i18. i19. 120. !21. I22. 123. 124. 125. I26. 127. 128. 129. i30. I
1
RT
!„ , _£._£5_19.18
EST. CONC.£>3>-7 D
'"*"*> 20'.
Q
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*FORM I SV-TIC _ 1/87
"
IS EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ____________TENTATIVELY IDENTIFIED COMPOUNDS [ —————————————
I CCH08Lab Name: IEA - Contract: 6S-W8-OG45 I
Lab Code: IEA Case No.: 12544 SAS No.: - SDG No.: CCHOO
Matrix: (soil/water) WATER - Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML , Lab File ID: 0831306
Level: (low/med) LOW Date Received: 8/26/89
% Moisture: not dec.100. ; . Date Analyzed: 8/31/89
Column: (pack/cap) CAP ]- Dilution Factor: 1.00
~- CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/L
CAS NUMBER
1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.15.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
COMPOUND NAME | RT
1111111
- 111111111111111111111I11
EST. CONC. Q
FORM I VOA-TIC ' 1/87 Re
- . - - ' ftR3Q2935.
IF EPA SAMPLE N(SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ____________
TENTATIVELY IDENTIFIED COMPOUNDS . II CCH08
Lab Name: IEA Contract: 63-W8-OQ45 _______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHQl
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0911409
Q Level: (low/med) LOW • Date Received: 8/26/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/23/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/11/89
'• GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 3 (ug/L or ug/Kg) UG/L
i : i i————\——————jI CAS NUMBER I COMPOUND NAME I RT I EST. CONC. I <
. 1.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
- - [UNKNOWN———— - —— - — f UNKNOWN —————————————————————
- - [UNKNOWN CYCLOHEXANE1tIf1Ii11!I1IIAIIff!!11II1I[
8.45[,. .._9_2.5_
9.92
7-, 9-.JZttL, ,40, ..UtWtf 10.
t*l/*M>t
fo~ rt Z** *~Zo*s
—————— 1
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FORM I SV-TIC 1/87 RflR302986
i - IE " E£»A SAMPLE NO-VOLATILE ORGANICS ANALYSIS DATA SHEET _____________TENTATIVELY IDENTIFIED COMPOUNDS _ I
| CCH09Lab Name: IEA : Contract: 68-W3-0045 I_____
Lab Code: IEA Case No.: 12544 SAS No.: . . SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML Lab File ID: 0831307
Level: (low/med) LCW Date Received: 8/26/89
% Moisture: not dec.100. Date Analysed: 8/31/89
Column: (pack/cap) CAP Dilution Factor: 1.00
-CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/L
CAS NUMBER
1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
| COMPOUND NAME
---
;'.
iiiiiii
RT
1
EST. CONC. Q
FORM I VOA-TIC 1/87 Re<
IF EPA SAMPLE NSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ___________
TENTATIVELY IDENTIFIED COMPOUNDS I1 CCH09
Lab Name: IEA Contract: 68-W8-0045 |______
Lab Code: IEA Case No.: 12544 SAS No.: SDG'NO.: CCHOcJB)
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000, (g/mL) ML Lab File ID: 0911410
Level: (low/med) LOW - Date Received: 8/26/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/28/89
Extraction: (SepF/Cont/Sonc) CONT ' Date Analyzed: 9/11/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 4 (ug/L or ug/Kg) UG/L
1CAS NUMBER i COMPOUND NAME
1. - - [UNKNOWN"1 ! TrkTT \T("*r "ITi- • I U-4*^—JUW.i
3. - - [UNKNOWN CYCLOHEXANE4. 128-37-0 [Phenol, 2,6-bis(l,l-dimethyl5. I6. I7. I8. 19. 1
10. 111. !12. !13. I14. 115. I16. I17. I18. 119. 120. !21. 122. I23. I24. I25. - 126. I27. 128. I29. I30. I
1
RT
8.4591 *™• -* 39.92
19.17
EST. CONC.
8.P— ' *** -» n—— K. —— . ——— ,HTT — " —///*-a/^»T <t n10 .
20.
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k-_LFORM I SV-TIC 1/87 I
flR3Q2988
page x of 2ORGANIC DATA VALIDATION SUMMARY
Date Review Completed: 29 November 1989 Contract Lab.: IEACase No.: 12544 Contract No.: 68-W8-0045Site Name: DELTA QUARRIES Lab DPO: Tom Bennett, Jr.Sample Nos. : CCHOO through CCH09 Reviewer: Doug Mclnnes
From: Region III/ESATPhone: (301) 266-9887
CONCENTRATIONMATRIX ! low jmed Jhiahj MATRIX RELATED COMMENTSsoil/solid ! ! ! ]aaueous j 10 j j j| other ! ! ! !
7OLATILESGC/MS TUNING — BFBInitial CalibrationContinuina CalibrationSurroaate RecovervMatrix SpikesReaaent BlanksHoldina times
OK | FYI 'ActionY * I———— £ —— i ——————— i ———————i x !
» Y 1———————— i ———— £ —— j ———————Y i i——— £ —— I —————— I ——————1 y 1
1 x i—————— I ——— £ —— j ——————Y 1 11 ———— £• ——— 1 ——— .__„.. i.,,. „ ,
COMMENT
See notes 1 and 2See notes 1 and 2
See note 3See note 4
SEMI-VOLATILES.
Initial Calibrationjcontinuina Calibration j jj Surroaate Recoverv } !Matrix Soikes _
XXXX
{Reaaent Blanks { x {i Holdina Times { X }
SeeSee
j SeeSee
notenotenotenote
2256
—————— 1 ————————————————————— t
PESTICIDESj Instrument Performance iInitial Calibration jjcontinuina Calibration jSurrocrate Recovery jMatrix SpikesJReaaent Blanks jJHoldina Times j
OVERALL CASE f! Compound Identification!Data Completeness }
v
XXXXXX t
! 1
———— 1 ————————————————— 1———— 1 ————————————————— 1———— , ______________ |———— 1 ———————————— 1———— 1 ————————————————— |
i
OK PYI Action!XX
1—————————— , ———————————————————————————————————— |.,, „ 1 ———— „.,..„.„.,.,„..„ ,,.,..„. ,.,— ————————— 1
REVIEWERrS COMMENTS:
DOCUMENTATION ATTACHED (see following pages)
SR302990
Case 12544 - . . . . : . Page 2 of 2
ORGANIC DATA VALIDATION SUMMARY
Note 1 - The response factor (RF) for 2-butanone was less than0.05 in the initial and/or continuing calibrations. (SeeTable 1 in Appendix F).
Note 2 - The %RSD and %D values for several compounds exceededprecision criteria in the initial and/or continuingcalibrations. (See Table 1 in Appendix F) .
Note 3 - The volatile MS/MSD analyses of sample CCH03 had a totalof four (4) out of ten (10) spike recoveries outside theQC limits. (See Appendix F),
Note 4 - The maximum concentration of the common laboratorycontaminant acetone found in the method blanks is 12j-g/L. (See Appendix F) .
Note.5 - Two samples, CCHOO and CCH01, had surrogate recoveriesfor 2-fluorophenol outside the QC limits. (See AppendixF).
Note 6 - The semivolatile MS/MSD analyses of sample CCH03 had atotal of one (1) out of eleven (11) RPD values outsidethe QC limits. (See Appendix F).
DCN - DM911A05
AR3Q2991
- " DPO:" I ] ACTION K( FYI
CJRGA&TC fSCpOtfAL BATA ASSESSMENT SVMMAX?
CASE NO. )7-$LiH __________ LABORATORY ______2
SDG NO. ££ gQ___________ DATA USER Tom g gU gr-r, JV.
SOW >/^-^______-________ " REVIEW COMPLETION DATE _££
NO. OF SAMPLES / Q MATRIX
REVIEWER [ ] ESD M H3AT [ ] OTHER,
VOA SNA PEST OTHER
1. HOLDING TIMES O O & ____
2. GC-MS TUNS/ GC PERFORMANCE O O ® ____
3. INITIAL CALIBRATIONS X X ^ ————
4. CONTINUING CALIBRATIONS * X p ____
5. FIELD BLANKS 0?* - not applicable) X O & ————
6. LABORATORY BLANKS X 0 ^ ————
7. SURROGATES O O ® ____
S, MATRIX SPKE/-DUPLICATES O Q ^ ___
9. REGIONAL QC C?* « sot applicable) _____ _____ _____ ___
10. INTERNAL STANDARDS O & ———
11. COMPOUND IDENTIFICATION O. ® & ———
1Z COMPOUND QUANTITATSON / T O... . ^ ——,
is. SYSTEM PERFORMANCE" P Q ^ ——14. OVERALL ASSESSMENT X X O ———
O * No problems or minor problems that do not affect data usability.X « No more than about 5% of the data points are qualified as either estimated or unusable.M ** More than about 5% of the data points are qualified as (estimated.Z « More than about 5% of the data points are qualified as unusable.A «• D?0 action requested; use in conjunction with one of the above codes.
DPO ACTION ITEMS;
AREAS OF CONCERN:
TTT Rev,8/8
TASLS I P«g«_l of bPftOTECriOM ASSHCY REStOH III
CALI33ATIOX QUTLIEXS_ VOLATILE HSL COHPQUMOS
CASI/SAS Mo. / -t-a. 7_______C3MT3ACTQR _____________J~ & f t _ _ _ _ _ _ _ _ _ _ _ _ _*—•-'
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S I
E3VISCSMEHWL PROTECTION AG2HCT HEGIQHCALIBRATION OUTLISSS
S2*I7QLATH,2 HSL COMPOUNDS (Part 1 of 2)^ m-/ ________ CONTRACTOR
i Inscr^ent* fr^t.I DATI/TrXE;: !
IKF !*3o^a^/o ' i. . .~..u _ > tb is ( -Chloroethvl) ether f !2-ChIoroohenol ! !t . —Dichlorobenzene ! !1 , -Diohlorobensene { • !Hensvl alcohol ! !1 ,2-Qichlorobensene ! !2-Methvlohenol ! !bis (2-Chloroisooroovl) ether! !H-Methvlohenol ! !tf— Mitroso— di— i— oroovlami^e ! !Ksxaohloroe thane : ! !Nitrobenzene • ! !Isoohorone ! !2-ttitroohenol ! !2 . --Dinethvlohenol ! !Benzole acid ! !bis(2-Chloroethoxv)methane { !2 . --Dichloroohenol ! !1.2, -Trichlorobenzene ! !Naohthalene ! !U-Chloroaniline f !Hexachlorobutadiene \ !4-Chloro-^-Methylohenol ! !2-MethvlnaDhthalene ! !Kexachlorocyctooentadiene [ !2.^.6-Triohloroohenol ! !2.4. 5-Trichioroohenol ! !2-Chloronaohthalene ! !2-?Titroarrline ! !Diaethvlohthalate ! . !Aeenachthvlsne • ! !2.6-Dinitrotoluene ! !^-tt-'troaniline ! !Acenaohthene • I !2,fc-Dinitroohenol ? fU-Mitroohenol f !
iAFFECTED !SAMPLES: !,.„,
[Reviewer J,Cnitials/Date: J>s" liters* \
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TABL3 I page_
ENVIRONMENTAL PROTECTION AGSNCT REGION inCALIBRATION OUTLIERS
SZJCTCLATILH ESL COMPOUNDS (Part 2 of 2)CASE/SAS No._L£vS_^i________CONTRACTOR_____________*£&#
! "-scr-js €"^--i JTa-ft Cal! DATE/TIME: !; , « RF t *rtSD i *! Diber.sofuras l> ! !! 2,^-Dinitrotoluene ! ! !! DietsvloctSialate ! ! !! --Chloroonesvl-chenYlether ! f !! Fluor*n« ! I I! a-Mitroaniline i 1 !! tt,6-Diaitro-2-aethrlBhenol I ! !1 tf-tfitrQsodlohesvlamine ! ! ff .fc-Brooooherrvl-ohenvlether 1 f f! Hexachlorobenzene ! \ \! Pentachloroohenol ! f fi . Phenanthrene ! ! f! Anthracene ! 1 !! .Di-n-butvi_hthaiata ! ! I1 ..Fluoranthene I ! f1 Pvrtr.e | I I! ButvlbenzTlonthaiate I ! !! 3.^-Dichiorobenzidine f ! fI B@nzo(a)anthrmcene f ! f| r*Vtw*r«a>*t A I I f
! bis(2-EthvlheTVl)Dhthalata ! ! f1 Di-n-octvlohthalate. ! ! If Benzo(o) fluoranthene f ! ff Benzo(lc) f luormnthene ! ! !! Benzofalovrene ! ! !! IndenoC 1.2. ^— cd) Dvrene ! f !f Dibeiz a h^s^itGrscsns ! ! !! Benzo (ff.h.i)oervlene ! I f
iAFFECTED !SAMPLES: !
4, Jl _____ m
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* Sat last page of this table for DEFINITION OF CODES.
• " " K : ^i-TA3L2 I1.. . oage 7 of
ENVIRONMENTAL PROTECTION AGENCT REGION IIICALIBRATION OOTLI22S
SH-OTCLATILZ HSL COMPOUNDS (Part 1 of 2)*^ _____ CONTRACTOR
• Cal.fCont. eal.JCont-. Cal. f Coot. Cal.!Zz/*±
!» I3F f,P f* fgp ftp Ift fHF !JP f* ISF I
bisi^-ChloroethvDether2-Chlorochenol7 .^-Dichlorobenzane______f { If | f | | j j j f ! j f. -Oichlorobensene
Ser.zvl alcohol1 . 2-Dichlorobensene2-Methvlshesolb is (2-Chloroi3ooroDvl) ether! f^-Methvlohenol
Hexachloro ethaneMi t rob enzereIso.ohorone2-Mitroohenol2 . fc-.Benzole acid____ _L L5"* 3 EP L _!_ J_~ L L £ I I __I f 1 !bisC2-Chloroet&oy70agthane If f I ! I ! ! ! ! I f ! t I t.g.tt-OiQhloroohenol L ! ! _L _L L L L !_ ! L i ! t i !1.2. -TrichlorobenzeneNaohthaleneii-ChloroanilineKexachlorobutadieneft-Chloro-1-Methylohenol ! f ! f ! ! I ! f ! f ! L I I2-Methvlnaohthalene ! ! ? ! ! ! ! ! ! ! ! ! ! I !Rexachlorocvclooentadiene !2^^6-trichloroohenol If f [ I I ! ! I ! ! ! L I fS.aj-TrichloroDhenol ?! ! \ I L L f ! I ! ? f i f2-Chloronaphthalene______I ! f i t ! I ! f f ! I !2-Nitro aniline___________! ! _ I !Diaethylohtaalate_______! * ! ! 'j———J——L———L.Acenaohthvlene2. 6-Dinitrotoluene_______f f
Ac snaoh there2.U-Dinitropheaol_______! ! ! ! ! I ? !
I a-Mitrooheaol___________I f f I ! I ? I ! I ! ! I
AFFECTEDSAMPLES:
^ReviewerInitials/Date;
70e,fe page of f.h^c, feahia for PP?T^TTTOM OF CQnffS.firto'uzygy
TABLE I page.
ENVIRONMENTAL PROTECTION AGENCT REGION IIICALIBRATION OUTLIERS
SHMI7CLATIL3 HSL COMPOUNDS (Part 2 of 2) „CONTRACTOR _________________.
T^gc-^m^t^ £ X"T# Y
! DATE/TIMS:ii!. Dibensofuran! 2 . &-Dlnitro£oluen@I DieshylsbthaiateU-Chiorooherivl-ohenTletherFluorine-?Titro anilineH . S-^initro-2-methylDhenoTN-Nitro30di3henvlamine^-Broooohenvl-ohenvletherHexachlorobenzenePentachioroohenolPher.anthrana
_ Anthracene_ Di-r.-butvlohthalateFluoranthenePvrsneButvlbenzvlohthalate^ . -DichlorobenzidineBanzo(m) anthraceneChrvsenebisC2-EthvliiexTl)ohthalateDI-n-octTlohthalateBenzo(b) fluorantheneBenzo Iclf luorantheneB @nzo f & / ovr @rsIndenoC 1.2. ~cd ) oyrensDxbenzC a. n / *yi "racene
' Benzo f s.h. i)o@rylene
AFFECTEDSAMPLES:
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flR3Q2998
OEfXXlT.QJI OF COOES USED XN TABLE I
I - Saso exceeded 30S in tht initial calibration, "positiveresult* are qualified -a", and qu«ntf tatf on Uaits «r«qu«l f f f *d »UJ".
C » XO •xe«*d*d 25 X In tht contfnufng calibration, Po*f tfv*results art qualified »J- and quant (tat ion " U«f ts are qualfffed
f » «F less than 0.05 in all ca I f brat f ons. 'AU quantisation limitsare qualified "R«. ; ..-..*.——
* * The "S- qualifier denoting blank eontaninat I on supersedes thequalifier issued in this table.
AR302999
6AVOLATILE CRGANICS INITIAL CALIBRATION DATA
Lab Name: IEA . Contract: 63-W8-0045
Lab Coda: IEA Case No.: 12544 SAS No.: SDG No.: CCHQQ
Instr-oment ID: EXTR3 Calibration Date(s): 8/10/89 8/10/89
Matrix: (soil/water) WATER Level: (low/med): LOW Column: (pack/cap) CAP
Min RR5 for SPCC(t) = .300 (0.250 for Bromoform) Max %RSD for CCCC*) = 30.
LAB FILE ID: RRF20 = 0810G04 RRF50 = 081QC02s 081QG01 ... - RRF150= 0810G02 RRF20Q= 0810GQ5
COMPOUND
Chloromethane|Bromomethane_iVinyl Chloride1ChloroethaneIMethylene ChlorideAcetone
,BromodichloromethaneJ1,2-Dichloropropane __|cis-1f3-DichloropropeneTrichloroethene|Dibramochloromethane_j1,1,2-Trichloroethane!Benzeneitrans-1,3-Dichloropropene _\Bromoform ________4-Methyl-2-?entanone2-HexanoneITetrachloroethene _____[1,1/2,2-Tetrachloroethanej Toluene
|RRI?20 IRRFSO IRHF100 1RRF150 1RRF20Q i
[Carbon Disulfide_11/1-Dichloroethene11,1-Dichloroethane^________11,2-Dichloroethene (total)_| Chloroform_____________* 3j 1,2-Dichloroethane_______ 1I2-Butanone_________11,1,1-Trichloroethane|Carbon TetrachlorideIVinyl Acetate
1Chlorobenzene__________S .953[ 1.0191 1.0151 1.0021 1.010| 1.0001 2.'[Ethylbenzene____________* .5051 .5471 .531| .567| .528| .5361 4.IStyrene ________________| 1.0031 1.1191 1.1771 1.211| 1.248| 1.1521 8.:IXylene (total)__________| .6371 .7311 -7531 .770| .764| .7311 7.!
IToluene-dS_______________| 1.222| 1.400] 1.376| 1.396| 1.351| 1.349| _IBromofluorobenzene_______1 .561] .617| .619| .587| .6271 .6021 4.'|l,2-Dichloroethane-d4 ____| 1.887| 1.924| 1.920| 1.834] 1.7951 1.8721 3.'
FORM VI VOA flR303000
7AVOLATILE CONTINUING CALIBRATION CEECX
Lab Name: IEA _* | Contract: 68-W8-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Instrument ID: EXTR3 ; Calibration Date: 8/22/89 Time: 7:52
Lab File ID: 0822301 Init. Calib. Date(s): 8/10/89 8/10/89
Matrix: (soil/water) WATER Level: (low/med): LOW Column: (pack/cap) CAP
Min RRF50 for SPCC(t) = .300 (0.250 for Bromoform) Max %D for CCC(*} is 2.
COMPOUND
t Chloramethanej Bromcme thane_I Vinyl Chloride1Chloroethane____[Methylene ChlorideAcetone[Carbon Disulfide_11,1-Dichioroethenei lf 1-Dichloroethane__ ___!1,2-Dichloroethene (total)_. Chlorof orm_____"_" _____*1 f 2-Dichloroethane2-Butanone11,1,1-Trichloroethane[Carbon Tetrachloridej Vinyl Acetate| Bromodichlorome thane11,2-Dichloropropane __j cis-1 f 3-DichloropropeneTrichloroethene[ Dibromochloromethane_[1,1,2-TrichlorqethaneBenzene
! trans-1,3-Dichloropropene _;Bromoform ________4-Methyl-2-Pentanone2-Hexanone
I Tetrachloroethene11,1,2,2-Tetrachloroethane _I Toluene ________ * 1[Chlorobenzene __________#IEthylbenzene___________StyreneXylene (total)
Toluene-d3Bromofluorobenzene1 , 2-Dichloroethane-d4
1.1521.7311
1.3491.602]
1.8721i
1.0841.720]
1.4451.6121
1.963|!
5.91.5
7.11.64.9
flR30300
r7A
VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: IEA Contract: 63-W8-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOQ
Instrument: ID: EXTR3 Calibration Date: 8/31/89 Time: 9:22
Lab File ID: 0831301 Init. Calib. Date(s): 8/10/89 8/10/89
Matrix: (soil/water) WATER Level: (low/med): LOW Column: (pack/cap) CAP
Min RRF50 for SPCC(i) = .300 (0.250 for Bromoform) Max %D for CCC(*J is 2
COMPOUND [ RRF IRRF50 | %D1 ——— ——— —— —————————( Chloromethane J! Bromome thane[Vinyl Chloride1 ChloroethaneIMethylene ChlorideI Acetone[Carbon Disulfide1 1 , 1-Dichloroethene :1 1 , 1-Dichloroethane \1 1 , 2-Dichloroethene ( total ) _1 Chloroform 31 1 , 2-Dichloroethane1 2-Butanone11,1, 1-Trichloroethane[ Carbon Tetrachloride[Vinyl AcetateI Bromodichlorome thanej 1 f 2-Dichloropropane *jcis-l,3-Dichloropropene __I Trichloroethenej Dibromochlorome thane11,1, 2-Trichloroethane1 BenzeneI trans-1 e 3 -Dichloropropene _JBromofara :I 4-Methyl-2-Pentanone1 2-Kexanone1 Tetrachloroethene11,1,2,2-Tetrachloroethane _J[Toluene '1 Chlorobenzene i1 Ethylbenzene *IStyrene[Xylene (total)1 - - - - - "— - ————————————[Toluene-dS1 Bromof luorobenzenei 1 , 2-Dichloroethane-d4I
t 11 1* 11 11 1
6* 21 34
* 31(
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—— I-2631994)681|5091772|469!565|995|474|780|178|3Z8|Q3$\T87|444|599|515|419|987|360|504|459(3571429!322]357]171 1321!4631981|9741436)04716751
389!577[904]
I
115105516555618152._!(25T312378512136
15
1452997
241
.6
.2
.0
.3
.0
.7
.1
.0
.1
.5
.6
.0
.8
.3-frT.1.1.8.5.0.3.8.5.3.3.5.4.3.6-2.0.6
,9.2.7
*1*ii*i1*
)*
FORM VII VGA . 1/87 ReflR303002 " *m<
r63
SEMIVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: IEA - •*- ' 'Contract: 68-W8-0045
Lab Code: IEA Case No.s 12544 SAS~No.: ' SDG No.: CCHOO
Instrument ID: EXTR4 Calibration Date(s): 8/25/89 8/25/89
Mia RRF for SPCC(f) = .050 \ Max %RSD for CCC(*J = 30
LAS FILE ID: RRF20 = 0825402 RRF50 = 0825403 [RRF80 = 0825404 RRF120= 0825405 ._ „. _RRF16Q= 0825401 1
COMPOUND
' Phenol______________bis(2-Chloroethyl)ether2-Chlorophenoli1,3-Dichlorobenzene1,4-DichlorobenseneBenzyl alcohol1,2-Dichlorobenzene2-Methylphenol_bis (2-Chloroisopropyl) ether4-Methylphenol| N-Nitroso-di-n-propylamine_I Hexachloroethane_; Nitrobenzene___~ilsophorone2-Nitrophenol ___
! 2,4-Dimethylphenol_Benzoic acid| bis (2-Chloroethoxy) methane_j 2,4-Dichlorophenol____[1,2,4-Trichlorobenzene(Naphthalene
i I 1 I I __ I %RRF20 IRRF50 |RRF80 |RJRF120 [RRF1601 RRF [ RS
_4-Chloroaniline __[Hexachlorobutadiene __|4-Chloro-3-methylphenolj 2-Methylnaphthalene _ _1 Hexachlorocyclopentadiene __12,4,6-Trichlorophenol - *[2,4,5-Trichlorophenolj2-Chloronaphthalenej 2-Nitroaniline__1 Dime thy Iphthalate| Acenaphthylene2,6-Dinitrotoluene13-Nitroaniline1Acenaphthene2,4-Dinitrophenol4-Nitrophenol ___
1.4921 12.3231 2.352
&R303003FORM VI SV-1 M 1/87 K
6CSEMIVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: IEA . Contract: 6S-W8-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHO<
Instrument ID: EXTR4 Calibration Date(s): 8/25/89 8/25/39
Min RRF for SPCC(S) = .050 Max %RSD for CCC(*) = 3C
;LAB FILE ID: RRF20 = 0325402 RRTSQ - 0325403i'RRFSO = 0825404 RRF120= 0825405 RRF160= 0825401
COMPOUND 1RRF20 (RRF50 (RRF80 [RRF1201RRF160
; DibenzofuranI 214-Dinitrotoluene_j Diethylphthalate4-Chlorophenyl-phenylether_IFluorene______________| 4-Nitroaniline__________j 4/6-Dinitro-2-methylphenol_j N-Nitrosodiphenylamine (1) _j 4-Bromophenyl-phenylether _j Hexachlorobenzene _______I Pentachlorophenol _______;j Phenanthrene____________j Anthracene______________JDi-n-butylphthalate _____j Fluoranthene____________•j Pyrene_________________I Butylbenzylphthalate_____j 3 f 3 ' -Dichlorobenzidine____j Benzo(a)anthracene_______j Chrysene_______________j bis (2-Ethylhexyl) phthalate_JDi-n-octylphthalate _____:j Benzo (b) f luoranthene_____Benzo(k)fluoranthene_____| Benzo (a) pyrene__________* 1.713 1Indeno (1,2,3 -[Dibenz(a,h)anthracene[ Benzo(g,h,i)perylene
JNitrobenzene-d5 ___j 2-Fluorobiphenyl___JTerphenyl-dl4 _____IPhenol-dS ________I 2-Fluorophenol_____[2,4,6^-Tribromophenol
1.9731 1.740.460[
1.3111.8831
1.7031
.705)
.3321
.3321
1,572]1.464]1.441]1.628]1.570].5501.4601
1.50611.4071 1.334).721] .865]
1.37511.86911.902)
834]268]
1.7251.763
1.8291.473)1.564) 1.7631 1.5661 1.3481 1.3691 1.522] 11
.491] .4661 -369| .3751 .3851 .4171 131.6191 1.4011 1.2971 1.1781 1.087] 1.3161 15.988] 1.0251 .9171 .8711 -873) .9351 7
2.504] 2.5681 1.9841 2.099) 2.014) 2.2341 121.955) 1.904] 1.5471 1.6421 1.560| 1.722] 11.335] .2791 -266) .223) .2221 .265) 17
(1) Cannot be separated from_Diphenylamine
FORM VI SV-2 1/87 F
AR3Q3QQU
735EHIVOIATJLE CONTINUING CALIBRATION CHECK
Lab Name: IEA Contract: 68-W8-0045
Lab Code: IEA Case No:: J.2544 iSAS No.: SDG No.: CCHOO
Instrument ID: EXTR4 • Calibration Date: 8/28/89 Time: 8:27
Lab File ID: 0823401 ; Init. Calib. Date(s): 8/25/89 8/25/89
Min RRF50 for SPCC(i) = .050 ^ Max %D for CCC(*J is 2
I .. . I1 COMPOUND __ ..._J_
I Phenol *i bis (2-Chloroethyl) ether __ 11 2-Chlorophenol 111,3 -Dichlorobensene [1 1 , 4-Dichlorobensene *I Benzyl alcohol ._._[i 1 , 2 -Dichlorobenzene „ 11 2-Methylphenol 1I bis ( 2-Chloroisopropyl ) ether |1 4-Methylphenol . 1I N-Nitroso-dirn-propylamine^fI Hexachloroethane . 11 Nitrobenzene 1llsophorone |I 2-Nitrophenol *[ 2 , 4-Dimethylphenol 1IBenzoic acid ' 11 bis ( 2-Chloroethoxy } methane_ |j 2 , 4-Dichlorophenol *1 1 , 2 , 4-Trichldrobenzene I1 Naphthalene - - 11 4-Chloroaniline 1j Hexachlorobutadiene *I 4-Chloro-3-methylphenol __ *1 2-Methylnaphthalene 1IHexachlorocyclopentadiene _#12,4, 6-Trichlorophenol - *12,4, 5-Trichlorophenol 11 2-Chloronaphthalene 1I 2-Nitroaniline I1 Dimethylphthalate 11 Acenaohthvlene 11 2 , 6-Dinitrotoluene 11 3 -Nitroaniline 1I Acenaphthene *1 2 , 4-Dinitroohenol #1 4-Nitrophenol #1 I
.RRF ...
2.4881.8551.7751.7141.7361.1671.6441.7551.9881.8531.201.689.367.731.270.355.230.554.375.364
1.157.534..188.336.773.309.437.465
1.114.3351.2781.854.319.417
1.020.198.126
1 1IRRF50 I
I 2.9481| 2.440]| 2.317]I 2.032]I 1.984!1 1.392]| 2.04811 2.1611I 2.1311I 2.2361[ 1.501[! -897!1 -42911 -851!1 -271]i -363]1 .219]1 -622]1 -4101I .3921| 1.26911 -53111 -19211 -413]I .854]I -309|1 .467[1 -5401| 1.22511 -3961| 1.4061[ 1.97911 -34311 - 477 1I 1.1961| ,20211 .13911 1
%D
18.5 *
§S518.514.3 *19.324.623.17.2
20.62^0 :
16.89.0.3 *2.14.7
12.49.2 *7.89.8S.82.3 *
22.7 *10.4 I
.2 %6.8 *
15.99.9
18.210.06.77.614.417.3 *1.9 *
10.4 J
CC14
FORM VII SV-1 1/87
- : SR303005 ''•
7C- SSMIVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: IEA Contract: 68-W3-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG'No.: CCHOO fc
Instrument ID: EXTR4 Calibration Date: 8/23/89 Time: 8:27
Lab File ID: 0823401 Init. Calib. Date(s): 8/25/89 8/25/89
Min RRF50 for SPCC(t) = .050 , Max %D for CCC(*) is
COMPOUND
[Dibenzofuran____________I 2,4-Dinitrotoluene_______i Diethylphthalate________, 4-Chlorophenyl-phenylether_,Fluorene[4-Nitroaniline__________I 4,6-Dinitro-2-methylphenol_I N-Nitroscdiphenylamine (1) _I4-Bromophenyl-phenylather _Hexachlorobenzene
RRF IRRF50 | %D
1.612] 1.753] 9.1.403) .489) 21.3
1.163) 1.389) 19.4.6721 .7411 10.1
1.3371 1.4361 7.4.400) .418) 4.5.1821 .1791 1.9.594! .6401 7.8.270] .2821 4.7.280! .290! 3.4
|Pentachlorophenol _______* .1851 .1791 3.4IPhenanthrene ________1 1.1921 1.261] 5.8[Anthracene______________1 1.1701 1.3141 12.3IDi-n-butvlphthalate _____1 1.250) 1.433] 14.71 Fluoranthene____________* 1.316) 1.495] 13.6 *| Pyrene_________________] 1.410] 1.433] 5.2Butylbenzylphthalate3,3' -DichlorobenzidineBenzo ( a) anthraceneChrysenebis ( 2-Ethylhexyl ) phthalate_Di-n-octylphthalateBenzo (b) fluorantheneBenzo ( k} fluorantheneBenzo ( a 5 pyrene *Indeno (1,2,3 -cd ) pyreneDibenz ( a , h ) anthraceneBenzo ( g,h, i ) perylene
Nitrobenzene-d52 -F luorobipheny 1Terphenyl-dl4I?henol-d52-Fluoroohenol2,4, 6-Tribromophenol
11
* 111
k 1111
1
21
.578)
.456]
.339)
.229]
.761)
.465]
.693)
.581]
.580)
.604]
.462)
.522]
.417)
.316]
.935)
.2341
.7221
.26511
.
.1.1.1.1.1.1.1.1.1.1.
*1.1.2.1.•
678498535384045790849914711941600|499
480)4091043|822]998!270|
1
17.49.314.712.6
<J7-A>22718.921.18.321.09.41.5
15.17.111.6(2T6 . 3)rSTD1.9
(1) Cannot be separated from Diphenylamine
S&IK
C C i-fo-i f"-
FORM VII SV-2 ' 1/87 I
AR3Q30Q6 '
r . i:. 7B . _i:.v:: ../"SEHIVOIAXILS CONTINUING CALIBRATION. CHECK
Lab Name: IEA Contract: 63-W8-0045
Lab Code: IEA Case No.::,12544. *.SAS No.: SDG'No.: CCHOO
Instrument ID: EXTR4 Calibration Date: 9/ 1/89 Time: 9:48
Lab File ID: 0901401 - Init. Calib. Date(s): 8/25/39 8/25/89
Min RRF50 for SPCCU) = .050 .. Max %D for CCC(*) is 2
$ 5//CCcc
1 . . . . . . . 11 COMPOUND . |
- , — lI Phenol *I bis (2-Chloroethyl) ether __ )I 2-Chlorophenol I1 1 , 3-Dichlorobenzene . . . . 11 1 , 4 -Dichlorobenzene *[Benzyl alcohol 11 1,2-Dichlorobenzene _.._.__. __i1 2-Methylphenol .\\ bis ( 2-Chloroisopropyl ) ether )1 4-Methylphenol 1( N-Nitroso-di-n-propylamine_j1 Hexachloroethane 1[Nitrobenzene —— |1 Isophorone 11 2-Nitrophenol *[2,4 -Dimethylpheriol 1[Berizoic acid jj bis ( 2 -Chloroethoxy ) methane_ j1 2 , 4-Dichlorophenol - *11,2, 4-Trichlorobenzene 11 Naphthalene 11 4-Chloroaniline 11 Hexachlorobutadiene *[4-Chloro-3-methylphenol __ *I 2-Methylnaphthalene 1(Hexachlorocyclopentadiene __#12,4, 6-Trichlorophenol *I 2,4,5-Trichlorophenol 1I 2-Chloronaphthalene [I 2-Nitroaniline 1I Dimethylphthalate _. 11 Acenaphthylene 11 2 , 6-Dinitrotoluene 1I 3-Nitroaniline _ 1I Acenaphthene - •• *\ 2 , 4-Dinitrophenol %1 4-Nitrophenol iI 1
RRF
2.4881.8551.7751.7141.7361.1671.6441.7551.9881.8531.201.639.367.781.270.355.230.554.375.364
1.157.534.188.336.773.309.437.465
1.114.335
1.2781.854.319.417
1.020.198.126
i 1[RRF50 1
I 2.537|i 1.86011 1,750)1 1.621]I 1.557|| 1.134!| 1.462]I 1.672]i 2.364)i 1.664!] 1.2361| .660(| .38S|1 -764]1 -2391i -35111 .243]1 .523]1 -31311 -31511 1.045]I .44511 -16911 .33211 .6701I -257|1 -4351
.46011.0981.453] <
| 1.334]1.854|.2931.3211.9971.122] <•161|<
1
%D
2.0.31.45.410.32.811.04.718.910.22.94.25.62.211.51.25.95.616.513.49.616.69.91.213.416.6.4
1.11.455JP4.4.0
8.323.12.3sm2¥.rj•" — —
1
A
•
*
3
**
1*
**i
FORM VII SV-1 1/87
flRSQSOQ? "•
7CSEMIVOLATILE CONTINUING CALIBRATION CHECK.
Lab Name: IEA Contract: 68-W8-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO I
Instrument ID: EXTR4 Calibration Date: 9/ 1/89 Time: 9:48
Lab File ID: 0901401 Init. Calib. Date(s): 8/25/89 8/25/89
Min RRF50 for SPCC(S) = .050 • Max %D for CCC(*) is 2
11 COMPOUND
IDibenzofuran1 2,4-Dinitrotoluene1 Diethylphthalate| 4-Chlorophenyl-phenylether_I FluoreneI 4-Nitroaniline| 4 r 6-Dinitro-2-methylphenol_j N-Nitrosodipheny lamine ( 1 ) _j 4 -Bromophenyl-pheny lather _I HexachlorobenzeneI Pentachlorophenol1 Phenanthrene1 Anthracene1 Di-n-butylphthalatej Fluoranthene "I PyreneI Butylbenzylphthalate13,3' -DichlorobenzidineI Benzo ( a ) anthracene1 Chrysene[ bis ( 2-Ethylhexyl ) phthalate_I Di-n-octylphthalate "*I Benzo (b) fluorantheneI Benzo ( k ) fluoranthene1 Benzo ( a) pyrene *1 Indeno (1,2,3 -cd ) pyr ene1 Dibenz ( a , h ) anthracene1 Benzo ( g , h , i ) pery lene
1 Nitrobenzene-d51 2-Fluorobiphenyl1 Terphenyl-dl41 Phenol-d51 2-Fluorophenol12,4, 6-Tribromophenol1
1 __RRF
; 1.612.403
1.163.672
1.337.400.182
* .594.270.230
* .1351.1921.1701.250
* 1.3161.410.578.456
1.3391.229.761
' 1.4651.6981.581
* 1.5801-6041.4621.522
.4171.316.9352.2341.722.265
1 t1RRF50 1t - — .— —— i -I- f1 1.55111 .42611 1.235]I -622)| 1.34011 .3641I .14111 .55311 .24311 -263!| .164]) 1.158]I 1.042]1 1.132]) 1.317)I 1.25311 .55411 .27911 1.23411 1.1251] .801|| 1.610]| 1.646)1 1.6851I 1.43211 1.57411 1.3111| 1.2851
1 .431]| 1.28611 .8551I 2.2351[ 1.564J1 .24211 1
%D
3.85.36.27.5.39.2
22.56.9 *3.06.211.5 *2.810.99.4.1 *
11.14J.
Cp78>/ . o8.45.49.9 *3.06.69.4 *1.910.315.6
3.42.38.6.0
9.28.9
(1) Cannot be separated from Diphenylamine
cccc
FORM VII SV-2 1/87 E
flR303008 - "
63SEMIVOLATILE CRGAN1CS INITIAL , CALIBRATION DATA
Lab Name: IEA ... -= - --'Cohtr ct: 63-W8-0045
Lab Code: IEA l Case No.: 12544 SAS No.: , SDG No.: CCHOO
Instrument ID: EXTR4 Calibration Date(s) : 9/11/89 9/11/89
Min RRF for SPCC(S) = .050 Max %RSD for CCC(*) = 30
| LAS FILE ID: RRF20 = 0911402 RRF50 = 0911403 IIRRF30 = 0911404 RRF120= 0911405 RRF160= 0911401 1I _______________________________________________________________ I __1 I I I 1 1 I __ I %| COMPOUND . , |RRF20 |RRF50 [RRF30 [RRF120 |RRF160 | RRF | RS
IPhenol _________________ * 3.443) 2.7731 2.3811 2.447] 2.324] 2.6731 17|bis(2-Chloroethyl)ether _, _ 1 2.314] 2.169) 1.635) 1.6731 1.5991 1.8731 171 2-Chlorophenol __________ | 2.160) 1.8441 1.567] 1.559! 1.519) 1.7301 1511,3-Dichlorobenzene _____ | 1.984[ 1-720) 1.4001 1.468) 1.311] 1.5771 17|l,4-Dichlorobenzene _____ * 2.149] 1.828] 1.425] 1.467) 1.273) 1.630) 21[Benzyl alcohol _____ I 1.340| 1.155| .969| 1.009] .969| 1.089] 141 1,2-Dichlorobenzene _____ [ 1.9081 1.683J 1.3241 1.232] 1.2121 1.432] 2012-Methylphenol ________ | 2.135| 1.9911 1-5651 1.7051 1.597] 1.799] 14Ibis(2-Chloroisaprapyl)etheri 1.9111 2.438J 1.5271 1.4391 1.220] 1.707] 28|4-Methylphenol ___________ J 2.371] 1.854! 1,4561 1.645J 1.638] 1.7931 19|N-Nitroso-di-n-propylamine_# 1.497] 1.302] .9551 -9641 1.023] 1.1481 21[Hexachloroethane ____ I .769] .652) .571| .554) .558) .621) 14[Nitrobenzene ____________ 1 .426] .364] .343] .322] .3061 .3521 13[Isophorone ____________ _] .5151 .747] .724) ,649) .636[ .6541 13|2-Nitraphenol __________ * .2691 -2101 -226] .2201 .2031 .226] 1112,4-Dimethylphenol _____ __I .428) .337) .323] .2951 .3061 .3331 JJIBenzoic acid ________ _| _____ | .0611 -0861 .119] .2221 .122 1 (£8]bis(2-Chloroethoxy)methane_r .597] .499] .5091 .466] .4611 .5061 lU1 2,4-Dichlorophenol _______ * .354| .2941 -3031 .281| .2601 .2981 1111,2,4-Trichlorobenzene ____ | .386] .292) .287] .251] .246] .2921 IS[Naphthalene ____________ | 1.371] 1.057] 1.031] .8991 .935[ 1.0591 171 4-Chloroaniline _______ ___[ .6321 .505] .475) .4281 .429] .5041 201 Hexachlorobutadiene _____ * .185] .135] .137| ,126) .129) .143) 1714-Chloro-3-methylphenol __ * .3761 .2941 -274| .272] .275] .2931 14[2-Methylnaphthalene ____ _| .8401 -631| .533] .555) .552] .622] 20[Hexachlorocyclopentadiene _# .2561 .221] .219] .242) .238] .235] 6[2,4,6-Trichlorophenol ____ * .446] .388] .362J .3301 .3491 .3851 S12,4,5-Trichlorophenol ____ | ____ I .429[ .3831 .417) .375) .4011 6|2-Chloronaphthalene _____ |~1.272| 1-064) .957) .920] .891) 1.021) 15|2-Nitroaniline __________ | ____ I .3561 -3231 .328] .3131 .3301 5(Dimethylphthalate _______ f 1.265] 1.159| 1.033] .997| .950| 1.0811 11iAcenaphthylene __________ 1 1.972] 1.790] 1.545] 1.4531 1.4541 1.6431 14I 2 , 6-Dinitrotoluene _______ I . 313 1 . 285 | . 245 ] . 237 1 . 247 ] . 265 | 12|3-Nitroaniline __________ I ____ I .397] .3631 -342] .3531 .364] 6(Acenaphthene _____________ *~1.154[ ,980( .893] .798] .8041 -9261 15[2,4-Dinitrophenol _______ # _____ 1 .0871 .120] .1491 .168] .1311 27[4-Nitrophenol __________ $ _____ | .071! -1031 .108] .133| .1041 24
QRR3030099'n
6CSEMIVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: IEA Contract: 63-W8-Q045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOi
Instrument: ID: EXTR4 Calibration Date(s): 9/11/89 9/11/89
Min HRF for SPCC(i) = .050 Max %RSD for CCC(*) = 30
O | LAB FILE ID: RRF2Q = 0911402 : RRF50 = 0911403 I1RRF80 « 0911404 RRF120= 0911405 RRF160= 0911401 ]
O
11 COMPOUND
I Dibenzofuran1 2 , 4-Dinitrotoluene! Diethylphthalatej 4-Chlorophenyl-phenylether_IFluorene1 4-NitroanilineI 4 , 6-Dinitro-2-methylphenol1 N-Nitrosodiphenylamine ( 1 ) _j 4-Brcmophenyl-phenylether _1 Hexachlorobenzene| PentachloroohenolI PhenanthreneI Anthracene1 Di-n-butylphtihalateI Fluoranthene1 Pyrene1 Butylbenzylphthalate1 3 , 3 ' -Dichlorobenzidine1 Benzo ( a ) anthracene1 Chrysene| bis ( 2-Ethylhexyl ) phthalate_I Di-n-octylphthalate "1 Benzo ( b ) fluoranthene1 Benzo ( k) fluoranthene1 Benzo ( a ) pyr ene *1 Indeno (1,2,3 -cd) pyrene1 Dibenz ( a , h ) anthracenej Benzo ( g , h , i ) peryleneI . . - -- — . ,.-. ..... _.__.. .._1 Nitrobenzene-d51 2-FluorobiphenylJTerphenyl-dl4IPhenol-d5[ 2-Fluorophenol[2,4, 6-Tribroraophenol1
RRf
1..
1.
i!IT
lr
1.1.1.
* 1.1...
1.1.
i!i.i.i.i.i.i.9
i..3.2..
'20
744403080769426
693297301
340375208407331500419389236678420306985603592256319
037623870111304227
1IRR! ——il illll illlilli il il il il iill il ill il il il il il il ill il1 2i 2| •1
FSO
.528
.377
.992
.646
.265
.374
.124
.625
.274
.271
.105
.147
.225
.120
.215
.169
.454
.354]
.058)
.121]
.615)
.325
.6511
.6701
.449
.321]
.196]
.123]
.409]
.264]
.8071,475|.1911.2221
I
RRF80
1.197.357.963.615
1.122.365.152.561.249.253.116
1.0271.0701.0411.0691.097.470.3471.1001.083.678
1.4331.5091.7621.5101.4461.2371.238
.3891.100.783
2.0911.564.201
1IRRjss-1 l11111I11111 i1 i1 l1 i1 iiI1 i1 iI1 l1 i1 i1 i1 i1 i1 i11 iII 2i 111
F
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.••
.
.•*..
120
193293837536955320167642264231166124125124163170474370130012624537533584487383305054
381149855063594199
11RRF160
| 1.2871 .3261 .8891 .5451 1.0561 .353I .167I .5421 .235I .2471 .1861 .983| 1.001I 1.046| 1.008| 1.092) .486| .389| 1.109I 1.0281 .6201 1.4581 1.329) 1.5391 1.4181 .8361 .9401 .512
1 .369| 1.052I .756| 2.010| 1.481| .2011
_.5
1....
1..•«-..
1.1.1.1.1.
«
•
I-
1
•
1
1-
1
I-
1
1
1
1
21 11
ISF I RS
3901 173511 129531 96221 151651 153531 €152] 13613) 102641 82711 S.1431 27,1241 12,153 12.ioM e.17ZT13,1721 8477] 3376) 7157] 11,096[ 8,643| 5,4451 6.5761 11,708| 10.494] 4.326] 20.1871 12.049] (30
.317[ 49
.2391 18
.8141 5
.351! 19
.8271 21
.2101 61
(1) Cannot be separated from Diphenylaraine
FORM VI SV-2 .1/87 B
flR3030IO
i 7BSEMXVCLATILE CONTINUING CALIBRATION CHECK
Lab Name: IEA . __ ( .' ^pntract: 63-W8-0045
Lab Code: IEA Case No.: 12544 SAS No. : SDG No.: CCHOO
Instrument ID: EXTR4 - Calibration Date: 9/11/89 Time: 23:37
Lab File ID: 0911D01 Init. Calib. Date(s)? 9/11/89 9/11/89
Min RRF50 for SPCC(i) = .050 ' Max %D for CCC(*J is 2
iCOMPOUND
;Phenol______________: bis (2-Chioroethyl) ether2-Chloropheno1i1,3-Dichlorobenzene,1,4-DichlorobenzeneBenzyl alcohol1,2-Dichlorobenzene2-Methylphenol
I bis ( 2-Chloroisopropyl ) etherI 4-Methylghenbl_ ____I N-Nitroso-di-n-propylamine__i 1I Hexachloroe thane(NitrobenzeneI Isophorone ________I 2 -Nitr opheno 1; 2 , 4-DimethylpheriolBenzoic acid[ bis (2 -Chloroethoxy} methane_I 2,4-Dichlorophenol_______*11,2,4-Trichlorobenzene[Naphthalene|4-Chloroaniline.Hexachlorobutadiene; 4-Chloro-3-methylphenol2 -MethylnaphthaleneIHexachlorocyclopentadiene _jI 2,4,6-Trichlorophenol ____*I 2p4,5-Trichl6rophenolI 2-ChloronaphthaleneI 2-NitroanilineJDimethylphthalateI Acenaphthylene_I 2,6-Dinitrotoluene^13-Nitroaniline1Acenaphthene^2,4-Dinitrophenol4-Nitrophenol .
-274|.375
1.009].104.125
FORM VII SV-1 n n, n n o o I I i/87-; - i -:- flRSOoU I l
7CSEMIVCLATILE CONTINUING CALIBRATION CHECK
Lab Name: IEA Contract: 68-WS-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.:
Instrument ID: EXTR4 Calibration Date: 9/11/39 Time: 23:37
Lab File ID: 0911D01 Init. Calib. Date(s): 9/11/89 9/11/89
Min RRF50 for S2CC(S) = .050 - Max %D for CCC(*) is 2
11 COMPOUND
1 DibenzofuranI 2 , 4-Dinitrotoluene1 Diethylphthalate1 4-Chlorophenyl-phenylether_1 FluoreneI 4-NitroanilineI 4,6-Dinitro-2-methylphenol_j N-Ni troscdiphenylamine ( 1 ) _>! 4-3rcmophenyl-phenylether _I Hexachlorobenzene1 Pentachlcrophenol 5! Phenanthrenei Anthracene1 Di-n-butylphthalate1 Fluoranthene '1 Pyrene1 Butylbenzylphthalate13,3' -Dichlorobenzidine1 Benzo ( a } anthracene1 Chrysene1 bis ( 2-Ethylhexyl ) phthalate_1 Di-n-octylphthalate *1 Benzo ( b } fluoranthene1 Benzo ( k) fluoranthene1 Benzo ( a ) pyrene *1 Indeno {1,2,3 -cd } pyr eneI Dibenz ( a ,h) anthracene1 Benzo ( g , h , i ) perylene1 ^ '—— — — — -1 Nitrobenzene-d51 2-FluorobiphenylI Terphenvl-dl4IPhenol-d51 2-Fluorophenol12,4, 6-Tribromophenol1
RRF
1.390.351.953.622
1.165.353.152
* .613.264.271
* .1431.1241.1591.108
* 1.1721.172.477.376
1.1571.096.643
* 1.4451.5761.708
" 1.4941,3261.1871.049
.3171.239.814
2.3511.827.210
1IRRF50
| 1.492[ .3841 1.1531 .6041 1.2951 .4251 .140I .619I .2401 .239I .112I 1.153I 1.2221 1.230I 1.2391 1.279| .594I .4321 1.2461 1.2221 .836I 1.663I 1.602I 1.869I 1.4731 1.373I 1.1341 1.198
1 .4291 1.1721 .8441 2.343I 2.1891 .188I
11 %D
1 7.4I 9.31 20.91 2.91 11.11 20.21 8.01 1.0 *1 9-1I 11.7| 21.9 *1 2.6I 5.4I 11.11 5.7 *1 9.2] 24.5] 15.11 7.71 i-L_JI (29.J>1 1571 *| 1.61 9.41 1.1 *1 3.61 4.5) 14.2
1 <5C£>1 5.41 3.61 -31 19.8I 10.31
(1) Cannot be separated from Diphenylamine
FORM VII SV-2 . 1/87 !
flR3030i2
3AWATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: IEA - .._ , £aixtract: 6E-W8-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix Spike - EPA Sample No.: CCH03
COMPOUND
1 , 1-DichloroetheneTrichloroetheneBenzeneTolueneChlorobenzene
| SPIKE1 ADDEDI (UG/L )
= 1 ———————J 250.| 250.I 250.I 250.I 250.j
1 SAMPLEI CONCENTRATION1 (UG/L )
•1 —— • —————————1 o.i o.1 o.1 o.I o.
MS | MSCONCENTRATION 1 %- (UG/L ) ] REC
194.337.299.236.343.
— i ———U7-3—ft351120.
i<uzL-
1 QCILIMI#1 ESC
.161-1£[71-1|76-1176-1
*>[75-lI
COMPOUND
1 , 1-Dichloroethene ___TrichloroetheneBenzeneTolueneChlorobenzene
| SPIKE| ADDED1 (UG/L )
= | ————————I 250.
"l 250.1 250.| 250.| 250.i
I MSDI CONCENTRATION[ (UG/L )
1 203.I 342.I 315.| 299.1 350. |1
MSD |% j %
REC #| RPD_ ——— _ — i ————————— i ————81 1 4.<U?T3>| 2.126. [ 5.
<HH1 1*\i*« V . Jf £• .
1
11 QC
II RPD= 1 =
I 141 141 111 131 131
LIMITS| REC
|61-1|71-1176-1176-1175-11
$ Column to be used to flag recovery ,and RPD values with an asterisk
* Values outside of QC limits
RPD: 0 out of 5 outside limitsSpike Recovery: 4 out of 10 outside limits,
COMMENTS: , . . .... -
FORM III VOA-1 1/87 Re
BR3030I3
2CWATER SEMIVOLATILE SURROGATE RECOVERY
Lab Name: IEA Contract: 63-W8-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOQl
| EPA1 SAMPLE NO.
11SBLK7921S3LK8331S3LK8941CCH0251CCH036ICCH03MS71CCH03MSD81 CCHOO9|CCH0110IS3LK93111CCK05121CCH0613114115116117118]19120121122123]24125126]27)28]29130]
SI t S2(NB2)*l(FBP)|
63 1 6574 1 7770 1 7050 1 5559 1 6761 I 64
. 66 I 6889 | 8578 1 8062 1 6163 1 6683 1 77
ii1111111IIii11i !i11
S3(TPH)S
637367624342438991367970
,
S4(PHL)S
575159505341402316753926
l S5(2FP)#
5949605148233*-(13 *)Ctr 5763322
| S6;(Tsp)#61585554
[ 6451532414633728
.OTHER
Mii
TOou000c0001100c
*
QC LIMITSSI (NB2) = Nitrobensene-d5 (35-114)S2 (FBP) = 2-Fluorobiphenyl (43-116)S3 (TPK) = Terphenyl-dl4 (33-141)S4 (PHL) = Phenol-d5 (10- 94)S5 (2FP) = 2-Fluorophenol (21-100)S6 (TBP) = 2r4,6-Tribromophenol (10-123)
S Column to be used to flag recovery values
* Values outside of contract required QC limits
D Surrogates diluted out •
page 1 of 1FORM II SV-1 1/87
D P* o o o n r iARJ030 1 k
• " 3C - ' • : - - -
WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: IEA - -^Contract: 68-W8-0045
Lab Code: IEA Case No.: 12544 SAS No.: . SDG No.: CCHOO
Matrix Spike - EPA Sample No.: CCH03
i:l
COMPOUND [
Phenol : 12-Chlorophenol [1,4-Dichlorobenzene , IN-Nitroso-di-n-prop.'d) |1,2, 4-Trichlorobenzene |4-Chloro-3-methylphenollAcenaphthene I4-Nitrophenol j2 , 4-Dinitrotaluene |Pentachlorophenol |Pyrene . . I
1
SPIKEADDED(UG/L )
200.200.100.100.100.200.100.200.'100.200.100.
SAMPLECONCENTRATION
(UG/L )
72.0.0.0.0.0.0.0.0.0.0.
MS |CONCENTRATION]
(UG/L ) i_ — —— _ — — ——— . j161. I78. [47. 162. 155. 1
107. |64. |74. |67, 184. 168. |
1
MS%
REC
45.39.47.62.55.53.64.37.67.42.68.
1 CILKII R-T112-127-(36-141-139-123-|46-1 10-124-1 9-126-1
i ii - i| COMPOUND |
_-. ——— „ ^ K_, ._ _^ |
I Phenol II 2-Chlorophenol 1j 1,4-Dichlorobensene __ 1j N-Nitroso-di-n-prop. (1) |I 1,2, 4-Trichlorobenzene_ j1 4-Chloro-3-methylphenol |j Acenaphthene II 4-Nitrophenol 1[ 2 , 4-Dinitrotoluene 1j Pentachlorophenol I1 Pyrene 11 1
SPIKEADDED(UG/L )
200.200.100.100.100.200.100.200.100.200.100.
MSDCONCENTRATION
(UG/L )
196.91.55.59.58.113.66.124.70.114.66.
MSD%REC *
62.46.55. .59.58.56.66 .62.70.57.66.
%RPD i
33.15.15.5.5.5.2.
C50. i5.30.3.
QCRPD
42402838234231
F 5 0385031
LIMI:1 w112-|27-|36-|41-139-123-146-110-124-1 9-126-1
(1) N-Nitroso-di-n-propylamine
i Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 1 out of 11 outside limitsSpike Recovery: 0 out of 22 outside limits
•COMMENTS: , ... , - :
FORM III SV-1
ftR3030S5
1A EPA SAMPLE. NOVOLATILE CRGANICS ANALYSIS DATA SHEET
I| VBLK01
Lab Name: IEA . Contract: 63-W8-OQ45 j_______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML Lab File ID: 0322302
Level: (low/med) LOW Date Received: O/ O/ 0
% Moisture: not dec,100. Date Analyzed: 8/22/89
Column: (pack/cap) CAP Dilution Factor: 1-00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3—————Chlorcmethane _________74-83-9—————Bromcmethane____________75-01-4—————Vinyl Chloride_________75-00-3—————Chloroethane____________75-09-2—————Hethylene Chloride______67-64-1—————Acetone ______________75-15-0—————Carbon Disulfide________75-35-4—————1,1-Dichloroethene______75-34-3—————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total).67-66-3—————Chloroform_____________'107-06-2—————l,2-Dichloroethane___78-93-3—————2-3utanone_________71-55-6—————1,1,1-Trichloroethane56-23-5—————Carbon Tetrachloride_108-05-4—————Vinyl Acetate ______75-27-4—————3romodichloromethane_78-37-5—————1,2-Dichloropropane
10061-01-5—————cis-1,3-Dichloropropene79-01-6—————Trichloroethene ___..___124-48-1—————Dibromochloromethane__79-00-5—————3. f 112-Trichloroethane71-43-2—————Benzene .__________
10061-02-6—————trans-l,3-Dichloropropene75-25-2—————Bromoform ____________108-10-1—————4-Methyl-2-Pencanone____591-78-6—————2-Hexanone____________127-18-4—————Tetrachloroethene ______79-34-5—————1,1,2,2-Tetrachloroethane108-88-3—————Toluene _______________108-90-7—————Chlorobenzene _________100-41-4—————Ethylbenzene__________100-42-5—————Styrene ______________1330-20-7—————Xylene (total)_________
10. [U10. |U10. [U10. IU5. IU12. |5. IU5. )U5. IU5. IU5. [U5. |U10. (U5. [U5. IU10. IU5. IU5. IU5. ]U5. |U5. IU5. )U5. [U5. [U5. |U10. |U10. IU5. IU5. IU5. IU5. IU5. IU5. |U5. IU
FORM I VOAfi R 3 0 3 0 1 6 ' 1/87 R
V/3-
IE i E5A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SEEST ____________TENTATIVELY IDENTIFIED COMPOUNDS I
I VBLK01Lab Name: IEA Contract: 68-W8-0045 [
Lab Code: IEA Case No".: 12544 . VSAS No.: SDG No.: CCHQO
Matrix: (soil/water) WATER : Lab Sample ID:
Sample wt/vol: 5. (g/inL) ML . Lab File ID: 0822302
Level: (low/med) LOW - Date Received: O/ O/ 0
% Moisture: not dec.100. - Date Analyzed: 8/22/89
Column: (pack/cap) CAP _ __ Dilution Factor:. . 1.00
CONCENTRATION UNITS:Number TICs found: Q (ug/L or ug/Kg) UG/L
CAS NUMBER
1.2.3.4.D.6.7.3.9.10.11.12.13.14.15.16.17.18,19.20.21.22.23.24.25.26.27.28.29.30.
COMPOUND NAME
,
.
1RT | EST. CONC.
, ,!111
11111111111111111111I1111I
Q
FORM I ypA-TIC. 1/87 Re
' fl"R3Q3QI7
1A EEA SAMPLE NOVOLATILE CRGANICS ANALYSIS DATA SHEET ________
II' VBLK02
Lab Name: IEA . Contract: 63-W8-0045 j_______
Lab Code: IEA Case No.: 12544 SAS No.: " SDG No.: CCHQO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/mL) ML ' Lab File ID: 0831302
Level: (low/med) LCW Date Received: 0/0/0.
% Moisture: not dec. 100. Date Analyzed: 8/31/89
Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO, COMPOUND (ug/L or ug/Kg) UG/L Q
C
74-37-3—————Chlorcmethane __________74-83-9—————Bromome thane___________75-01-4—————Vinyl Chloride_________75-00-3—————Chloroerhane____________75-09-2—————Methylene Chloride______67-64-1—————Acetone ______________75-15-0—————Carbon Disulfide________75-35-4—————1,1-Dichlorcethene______75-34-3—————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total).67-66-3—————Chloroform____________'107-06-2——>———1,2-Dichloroethane______78-93-3—————2-Butanone. _....._.. ______71-55-6—-*~—>~1,1,1-Trichloroethane ___56-23-5—————Carbon Tetrachlaride____108-05-4—————Vinyl Acetate _________75-27-4—————Bromcdichlorome thane____78-87-5—————1,2-Dichloropropane
10061-01-5—————cis-1,3-Dichloropropene79-01-6—————Trichloroethene124-48-1—————Dibromochloromethane_79-00-5—————1,1,2-Trichloroethane71-43-2—————Benzene
[10061-02-6—————trans-1,3-Dichloropropene _75-25-2—————Bromoform
O | 108-10-1—--——4-Methyl-2-Pentanone591-78-6—————2-Hexanone______________127-18-4—————Tetrachloroethene ________79-34-5—————1,1,2,2-Tetrachloroethane _108-88-3—————Toluene _________________108-90-7—————Chlorofaenzene ___________100-41-4—————Ethylbenzene______________100-42-5—————Styrene _________________1330-20-7————Xylene (total)__________
10. IU10. |U10. |U10. |U5. |U
11* 15. IU5. )U5. | XT5. |U5. IU5. | XT10. )U5. |U5. |U10. | XT5. IU5. IU5. IU5, IU5. IU5. IU5. [U5. |U5. IU10. IU10. IU5. IU5. IU5, IU5. IU5. IU5. IU5- |U
BR30^FORM I VOA R SI O U o w i w 1/87
IE EPA SAMPLE NO.VOLATILE CRGANICS ANALYSIS DATA SHEET m____________TENTATIVELY IDENTIFIED COMPOUNDS [-
. - , . I VBLK02Lab Name: IEA Contract: 68-W8-0045 |
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHQO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5. (g/znL) ML 4 Lab File ID: 0831302
Level: (low/med) LOW . T "" Date Received: O/ O/ 0
% Moisture: not dec.100. ;_ Date Analysed: 8/31/89
Column: (pack/cap) CAP . . . . ;_ Dilution Factor: 1.00
CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/L
CAS NUMBER
1.2.3.4.5.6.7.3.9.10.11.12.13.14.15.16.17.18.19.20.21.22.
[ 23.; 24.25.26.27.28.29.30.
.COMPOUND NAME
— • -- - ' -
•
,
RT EST. CONC.
i
i
Q
-
FORM I VOA-TIC 1/87
AR3030l<?
1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ____________
j CCHQ3MSLab Name: IEA . Contract: 63-W8-QQ45 I_______
i Lab Code: IEA Case No.: 12544 SAS No.: SDG No-: CCHOO3
Matrix: (soil/water) WATER Lab Sample ID:
O Sample wt/vol: 5. (g/mL) ML • Lab File ID: 0822310
Level: (low/med) LCW Date Received: 8/18/89
% Moisture: not dec.100. Date Analyzed: 8/22/89
^ Column: (pack/cap) CAP Dilution Factor: 1.00
CONCENTRATION XJNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
O
ij 74-87-3 ————— Chloromethane1 74-83-9 ————— Bromomethane1 75-01-4 ————— Vinyl Chloride| 75-00-3 ————— Chloroethane| 1 «4 W — ' «• •-'•—I >_*i.J . >»«_.*•• 1_>**._.1_'_» f\ I|> il
W » W T ^ k *W *— «— JiJ,l—
75-15-0 ————— Carbon Disulfide75-35-4 ————— 1, 1-Dichloroethene75-34-3 ————— 1,1-Dichloroethane540-59-0 ————— 1,2-Dichloroethene (total) _67-66-3 ————— Chloroform107-06-2 ————— 1,2-Dichloroethane78-93-3 ————— 2-3utanone71-55-6 ————— 1 , 1 , 1-Trichloroethane56-23-5 ————— Carbon Tetrachloride
_W W W W _J i T B**_2 J« * * *— *— 1«* hat_>
75-27-4 ————— Bromodichloromethane78-87-5 ————— 1,2-Dichloropropane
10061-01-5 ————— cis-1, 3-Dichloropropene ___79-01-6 ————— Trichloroethene124-48-1 ————— Dibromochloromethane
10061-02-6 ————— trans-1, 3-Dichloropropene _75-25-2 ————— Bromoform
591-78-6 ————— 2-Hexanone127-18-4 ————— Tetrachloroethene79-34-5 ————— 1 ,1,2, 2-Tetrachlorbethane _
100-41-4 ————— Ethylbenzene100-42-5 ————— Styrene1330-20-7 ————— Xylene (total)
10.10.10.10.5.19.5.39.5.5.5.5.
180.5.5.10.5.5.5.67.5.5.
60-5.5.10.10.5.5.57.69.5.5.5.
1 \HI IIU Iiu 1iu liu lIB |IU J
Iu \\vIUiu1|UItriuiuiuiu1iu[U\iuiuiuiuiu|U1 ^1 1.IU 1iu 4iu 11 1
FOEHI VOA (\R303G20 ' 1/87
1A EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEET _______._____: ; .- i——————'
I CCH03MSDLab Name: IEA m. * Contract: 63-W8-0045 |
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHQO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5., (g/mL) ML , Lab File ID: 0822311
Level: (low/med) LCW Date Received: 8/18/89
% Moisture: not dec.100. i - - ""Date Analyzed: 8/22/89
Column: (pack/cap) CAP , : ,. , Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3—————Chloromethane ___74-83-9—————Sromome thane_____75-01-4—————Vinyl Chloride___75-00-3—————Chloroe-chane_____75-09-2—————Methylene Chloride^67-54-1—————Acetone ________*75-15-0—————Carbon Disulfide_75-35-4—————1,1-Dichloroethene75-34-3—————l,l-Dichloroethane-______540-59-0—————1,2-Dichloroethene {total)J67-66-3—————Chloroform107-06-2—————1,2-Dichloroethane__78-93-3—————2-Butanone_______.71-55-6—————1 f 1 f 1-Trichloroethane56-23-5—————Carbon Tetrachloride_108-05-4—————Vinyl Acetate .- - - -75-27-4—————3romodichloromethane_78-87-5—————1 r 2-Dichloropropane
10061-01-5—————cis-1,3-Dichloropropene ___79-01-6—————Trichloroethene124-48-1—————Dibromochloromethane^79-00-5—————1,1,2-Trichloroethane71-43-2—————Benzene
10061-02-6—————trans-1,3-Dichloropropene75-25-2—————Bromoform108-10-1—————4-Methyl-2-Pentanone_591-78-6—————2-Hexanone127-18-4—————Tetrachloroethene _____79-34-5—————1,1,2,2-Tetrachloroethane108-88-3—————Toluene __________'_'108-90-7—————Chlorobenzene _________100-41-4—————Ethylbenzene_________100-42-5—————Styrene ______________1330-20-7—————Xylene (total)_________
FORM I VOAflR30302
10. [U10. IU10. I XT10. | XT5. | XT
29. IB5. [U
41- I5. [U5. |U5. IU5. 1U
ISO. I5. IU5- |U10. |u5. IXT5- IXT5. |U
68. I5. [U5. |U
63. I5. |XT5. | XI
10. IXT10. IU5. |U5. IU
60. I70. I5. IXT5. .fU5. IUI
IB EPA SAMPLE NCSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ____________
I| SBLK79
Lab Name: IEA • Contract: 63-W8-0045 I_____
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828402
Level: (low/med) LOW Date Received: O/ O/ 0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/13/39
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 8/28/89
GPC Cleanup: (Y/N) N pK: 6.0 Dilution Factor: 1.00
CONCENTRATION XJNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2—————Phenol__________________111-44-4—————bis (2-Chloroethyl) ether ___95-57-8 ————— 2-Chlorophenol___________541-73-1————1,3-Dichlorobenzene ______106-46-7—————1, 4-Dichlorobenzene ______100-51-6—————Benzyl alcohol____________95-50-1—————1,2-Dichlorobenzene ______95-48-7 ————— 2-Methylphenol___________108-60-1—————bis (2-Chloroisopropyl) ether106-44-5 ————— 4-Methylphenol___________621-64-7—————N-Nitroso-di-n-propylamine_67-72-1—————Hexachloroethane_________98-95-3—————Nitrobenzene_____________78-59-1—————Isor>horone______________88-75-5—————2-Nitrophenol ___________105-67-9—————2,4-Dimethylphenol________65-85-0—————Benzoic acid____________111-91-1—————bis (2-Chloroethoxy) me thane_120-83-2—————2,4-Dichlorophenol________120-82-1—————1,2,4-Trichlorobenzene_____91-20-3—————Naphthalene ____________106-47-8 ————— 4-Chloroaniline _________87-68-3—————Hexachlorobutadiene ______59-50-7—————4-Chloro-3-methylphenol ___91-57-6—————2-Methylnaphthalene ______77-47-4—————Hexachlorocyclopentadiene _88-06-2—————2,4,6-Trichlorophenol ____95-95-4—————2,4,5-Trichlorophenol _____91-58-7—————2-Chloronaphthalene ______88-74-4—————2-Nitroaniline___________131-11-3—————Dime thy Iphthalate ________208-96-8—————Acenaphthylene^
1 606-20-2—————2,-6-Dinitrotoluene^
10. IU10. IU10. IU10. IU10. )U10. IU10. |U10. IU10. IU10. IU10. IU10. IU10. IU10. IU10. |U10. |U50. IU10. IU10, IU10, |U10. |U10. |U10. IU10. IU10. IU10. IU10. IU50. IU10. IU50. |U10. IU10. [U10. IU
FORM I SV-1 a p O ft 1 i}9 9 ' ' 1/87flnuuoucd. ^,.
r 1C " EPA SAMPLESSMIVOLATILI. ORGAN!CS ANALYSIS DATA SHEET
j S3LK79Lab Name: IEA Contract: 68-W8-0045
Lab Code: IEA Case No". :• 12544 ^. SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab "Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828402
Level: (low/med) LOW - Date Received: 0/0/0
% Moisture: not dec.100. dec. 0. Eate Extracted: 8/18/89
Extraction: (SepF/Cont/Sonc) CONT \ _:__Date Analyzed: 8/28/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2 ————— 3-Nitroaniline _____83-32-9—————Acenaphthene _____.51-28-5 ————— 2 r 4-Dinitrophenol ______100-02-7—————4-Nitrophenol _________132-54-9—————Dibenzofuran___________121-14-2 ————— 2,4-Dinitrotoluene - :___84-66-2————-Diethylphthalate________
7005-72-3 ————— 4-Chlorophenyl-phenylether86-73-7————-Fluorene_________;____[100-01-6—————4-Nitroaniline_________534-52-1—————4/6-Dinitro-2-methylphenol_8"6-30-6—————N-Nitrosodiphenylamine (1)~101-55-3 ————— 4-Bromophenyl-phenylether ~118-74-1—————Hexachlorobenzene ______"87-86-5—————Pentachlorophenol ... . . .85-01-8—————Shenanthrene___________120-12-7—————Anthracene_____________84-74-2—————Di-n-butylphthalate ____206-44-0—————Fluoranthene___________"129-00-0—————Pyrene____i___^_^______85-68-7—————Butylbenzylphthalate_____91-94-1—————3,3 '-Dichlorobenzidine___56-55-3—————Benzo (a) anthracene______218-01-9—————Chrysene______117-81-7—————bis(2-Ethylhexyl)phthalate117-84-0—————Di-n-octylphthalate ____"205-99-2—————Benzo (b) fluoranthene____~207-08-9—————Benzo (k) fluoranthene_____50-32-8—————Benzo (a)pyrene_____;_____~193-39-5—————Indeno (1,2,3-cd) pyrene___53-70-3—————Dibenzta,h)anthracene ___191-24-2—————Benzo (g,h,i)perylene_____
50. |U I10. |U I50. )U 150. IU 110. |U 110. |U 110. |U I10. |U 110. |U I50. IU I50. IU I10. |U 110. IU |10. |U I50. |U |10. IU 110. |U I10. IU 110. [U 110. (U I10. IU I20. IU 110. IU 110. [U 110. IU 110. IU I10. |U 110. |U 110. IU I10. IU 110. JU I10. IU I
(1) - Cannot be separated from diphenylamine
FORM I SV-2 1/87 Ij : flR303023
O
IF EPA SAMPLESEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _________
TENTATIVELY IDENTIFIED COMPOUNDS 1I SBLK79
Lab Name: IEA Contract: 68-W8-0045 I
Lab Cade: IEA Case No,: 12544 SAS No.: SDG No.:
Matrix: (soil/water) WATER Lab'Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828402
Level: (low/rued) LOW • Date Received: 0/0/0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/18/89
Extraction: (SepF/Cont/Sonc) CONT ' Date Analyzed: 8/28/89
GPC Cleanup: (Y/NJ N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION XJNITS:Number TICs found: 4 (ug/L or ug/Kg) UG/L
CAS NUMBER
1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
tI COMPOUND NAME
- ^UNKNOWN- [UNKNOWN- iUNKNOWN- {UNKNOWN CYCLOHEXANE
FtI\1Ii?1t\\I:11Ir\\ \t if it ii ii ii ii iS I
RT
8.639.439.6710.10
EST. CONC.
10.40.20.20.
————— <
—— i
QJJJJ^•L
_tFORM I SV-TIC 1/87
.._-.. flR303.02U '
IB - EPA SAMPISEMIVOLATILE ORGANICS ANALYSIS DATA SHEET '
] SBLK83Lab Name: IEA ^ -* Contract: 63-W8-0045 1
Lab Code: IEA Case No.: 12544 SAS No.: _ SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828404
Level: (low/med) LOW : Date Received: O/ O/ 0
% Moisture: not dec. 100. dec. 0. . Date Extracted: 8/21/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 8/28/89
GPC Cleanup: (Y/N) N pH: 6.0 : .Dilution Factor: 1.00
""- CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
1I1 1-44-4 — — — -j« _» ^ M ^Q~—^7-Q-------
541-73-1 ———— -106-46-7 ———— -100-51-6 ———— -Q ^ H — 1-O — OU-J.- — -----Q q. /i Q— 7-- —— - —108-60-1 —————106-44-5 —————621 -64-7 —————** *• -*> ™* /67-72-1 —————
7S — Q — 1 —— — — .. — _Q Q "7 C C88- / J-O- ——— ——105-67-9 —————65-85-0 —————
1 1 1 — QI -1 -------120-83-2 —————
106-47-8 —————Q7 £3— •? _ — _— _
QI — 7— £— -.—— — — _77-47-4 ——————/ * "» / Tt
Q s;-aq_ A _._----
88-74-4 —————131-11-3 —————OnQ— QC — Q— — — — — — —£ A C. "~J rt *1606 20-2 ——————
•Phenol•bis (2-Chloroethyl) ether ___•2-Chlorophenol•1 r 3 -Dichlorobenzene•1 , 4-DichlorobenzeneBenzyl alcohol•1 , 2-Dichlorobenzene•2-Methylphenolbis ( 2-Chloroisopropyl ) ether4-MethylphenolN-Nitroso-di-n-propylamine _HexachloroethaneNitrobenzeneIsophorone2-Nitrophenol2 , 4 -DimethylphenolBenzoic acidbis (2-Chloroethoxy)me thane _2 , 4-Dichlorophenol1,2,4 -Tr ichlorobenzerieNaphthalene4-ChloroanilineKexachlorobutadiene4-Chloro-3-methylphenol ___2-MethylnaphthaleneHexachlorocyclopentadiene _2,4, 6-Trichlorophenol2,4, 5-Trichlorophenol2 -Chloronaphthalene2-NitroanilineDimethvlphthalateAcenaphthylene2 , 6-Dinitrotoluene
10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.50.10.10.10.10.10.10.10.10.10.10.50.10.50.10.10.10.
IIU
IUIUiuIUIUIUIUiuIUIUIUIUIUIUIUIUIUIUiuIU[UIUIUIUIUIUIUJu|U1
sv-i ' „ n 'n n Q n 9 q • 1/87 ifiR303025
1C "" ESA SAMPLESEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
| SBLK33Lab Name: IEA Contract: 63-W8-0045 |______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab 'Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828404
Level: (low/med) LOW . Date Received: O/ O/ 0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/21/89
Extraction: (SepF/Cont/Sonc) CQNT Date Analyzed: 8/28/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2—————3-Nitroaniline_________83-32-9—————Acenaphthene___________51-28-5—————2,4-Dinitrophenol ______100-02-7—————4-Nitrophenol __________132-64-9—————Dibenzofuran___________121-14-2 ————— 2,4-Dinitrotoluene______84-66-2—————Diethylphthalate________
7005-72-3—————4-Chlorophenyl-phenyletherw86-73-7—————Fluorene_______________]100-01-6—————4-Nitroaniline_________534-52-1—————4,6-Dinitro-2-methylphenol^86-30-6—————N-Nitrosodiphenylamine (1)]101-55-3 ————— 4-Bromophenyl-phenylether ]118-74-1—————Hexachlorobenzene ______^87-86-5—————Pentachlorophenol ______85-01-8—————Phenanthrene___________120-12-7—————Anthracene_____________84-74-2—————Di-n-butylphthalate _____206-44-0—————Fluoranthene___________129-00-0—————Pyrene________________85-68-7—————Butylbenzylphthalate_____91-94-1—————3,3' -Dichlorobenzidine___56-55-3—————Benzo (a) anthracene______218-01-9—————Chrysene______________117-81-7—————bis (2-Ethylhexyl )phthalate_117-84-0—————Di-n-octylphthalate ____j205-99-2—————Benzo (b) fluoranthene_____207-08-9—————Benzo(k) fluoranthene____50-32-8—————Benzo (a) pyrene193-39-5—————Indenod, 2,3-cd) pyrene.53-70-3—————Dibenz(a,h)anthracene [191-24-2—————Benzo(g,h,i)perylene "
50. |U10. IU50. |U50. ]U10. IU10. IU10. |U10. ]U10. |U50. IU50, |U10. IU10. IU10. IU50. [U10. IU10. IU10. IU10. IU10. ]U10. IU20. 1U10. ]U10. (U10. IU10. IU10. IU10. IU10. ]U10. [U10. [U10. - IU
(1) - Cannot be separated from diphenylamine
FORM I SV-2 1/37 R
flR3G3026 "
, „ IF .. . . . . . . . . . . .. . EPA SAMPLESEMIVOLATXLE ORGAN! CS ANALYSIS DATA SHS2T _
TENTATIVELY IDENTIFIED COMPOUNDS l" "- . - . - I S3LK33
Lab Name: IEA t -;? - f Contract: 63-W8-Q045 I
Lab Code: IEA Case No.s 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab "sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828404
Level: (low/med) LOW ' Date Received: O/ O/ 0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/21/89
Extraction: (SepF/Cont/Sonc) CONT _ .___ _ Date Analyzed: 8/23/89
GPC Cleanup: (Y/N) N pH: 6.0 _ .Dilution Factor: 1.00
..: CONCENTRATION UNITS:Number TICs found: 3 (ug/L or ug/Kg) UG/L
1 _ . . . . . - : -CAS NUMBER | COMPOUND NAME
1. - - I UNKNOWN2. - - | UNKNOWN3 . - - 1 UNKNOWN4. 15. 16. 17. |8. 19. 110. |11. 112. I13. 114. I15. I16. |17. I18. |19. 1 . .20. I21. 1 • i I22. | |23. | -- |
I 24. I I1 25. | I[26. 1 - - • |
27. I I28. I I29. 1 • - |30. |
1 * ; 1
RT
8.629.43
10.10
EST. CONC.
3.30.10,
Q
JJJ
FORM I SV-TIC 1/87 I;;: .-91303027 , •
IB EPA SAMPLESEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I SBLK39Lab Name: IEA Contract: 68-W8-0045 I______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO^
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828405& Level: (low/med) LOW ' Date Received: O/ O/ 0
% Moisture: not dec. 100. dec. 0. Date Extracted: 8/22/89
Extraction: (SepF/Con-/Sonc) CONT Date Analyzed: 8/23/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
O
108-95-2 ————— Phenol111-44-4 ————— bis(2-Chloroenhyl)et:her ___95-57-8 ————— 2-Chlorophenol
541 —73-1- ——— --T 3-DichlQrohenz'an.e*ml T. — . * —* ^> ^ f -mJ *•/ •••*** ti_»*-* _• W_rf S»».fcA t* (_>**<*«•
106-46-7 ————— 1,4-Dichlorobenzene100-51-6 ————— Benzyl alcohol95-50-1 ————— 1,2-Dichlorobenzene95-43-7 ————— 2-Methylphenol108-60-1 ————— bis (2-Chloroisopropyl) ether10 6 — 44-5— — — — ---4— MethvlnhenolU_ W sj 1 — ' ^ fa *>_• <_>** T >J. t ** "*- '
621-64-7 ————— N-Nitroso-di-n-propylamine _67-72-1 ————— Hexachlo roe thane98-95-3 ————— Nitrobenzene78-59-1 ————— Isophorone88-75-5 ————— 2-Nitrophenol105-67-9 ————— 2,4-Dimethylphenol65-85-0 ————— Benzoic acid111-91-1 ————— bis (2-Chloroethoxy) methane _120-83-2 ————— 2,4-Dichlorophenol120-82-1 ————— 1,2,4-Trichlorobenzene91-20-3 ————— Naphthalene106-47-8 ————— 4-Chloroaniline87-68-3 ————— Kexachlorobutadiene59-50-7 ————— 4-Chloro-3-methylphenol91-57-6 ————— 2-Methylnaphthalene77-47-4 ————— Kexachlorocyclopentadiene _88-06-2 ————— 2.4,6-Trichlorophenol95-95-4 ————— 2 . 4 , 5-Trichlorophenol91-58-7 ————— 2-Chloronaphthalene88-74-4 ————— 2-Nitroaniline131-11-3 ————— Dimethylphthalate208-96-8 ————— Acenaphthylene606-20-2 ————— 2,6-Dinitrotolue'ne
10.10.10,10.10.10.10.10.10,10.10.10.10.10.10.10.50.10.10.10.10.10.10.10.10.10.10.50.10.50.10.10.10.
1
IUIUiuiu^ 1iuiuIUiuiuIU[UIUiuiuIUIUIUIUiuIUIUiuiu|UIUiuIS 11
FORM I SV-1 1/87 R
r 1C - EPA SAMPLE NSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET. ..:•-• - •• ---• .r ' . - i :————
- I SBLK89Lab Name: IEA Contract: 63-W8-0045 |
Lab Code: IEA Case No.: 12544 , SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER .v , _ Lab .Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828405
Level: (low/med) LOW . Date Received: O/ O/ 0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/22/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 8/28/89
GPC Cleanup: (Y/N) N . pH: 6.0 „ . Dilution Factor: 1.00
-- - "CONCENTRATION UNITS:CAS NO. COMPOUND . (ug/L or ug/Kg) UG/L Q
99-09-2—————3-Nitroaniline _ . ..... .. .83-32-9—————Acenaphthene___________51-28-5——'—"—2"f4-Dinitrqphenol ______100-02-7—————4-Nitrophenol __________132-64-9—————Dibenzofuran___________"121-14-2 ————— 2,4-Dinitrotoluene-_____84-66-2—————Diethylphthalate _____]
7005-72-3—————4-Chlorophenyl-phenylether_86-73-7—————Fluorene__________]____"100-01-6 ————— 4-Nitroaniline_____534-52-1—————4,6-Dinitro-2-methylphenolM86-30-6—————N-Nitrosodiphenylamine (1)~101-55-3—————4-3romophenyl-phenylether ^118-74-1—————Hexachlorobenzene ______"87-86-5—————Pentachlorophenol ______85-01-8—————Phenanthrene__________120-12-7—————Anthracene_____________84-74-2—————Di-n-butylphthalate _____206-44-0—————Fluoranthene____________129-00-0—————Pyrene ... _ _ _ _ , . '85-68-7—————Butylbenzylphthalate_____91-94-1—————3,3 ' -Dichlorobenzidine___|56-55-3—————Benzo (a) anthracene_______218-01-9—————Chrysene_____ " -- :117-81-7—————bis(2-Ethylhexyl)phthalate117-84-0—————Di-n-octylphthalate ____"205-99-2—————3enso(b) fluoranthene_____207-08-9—————Benzo (k) fluoranthene_____50-32-8—————Benzo(a)pyrene__________193-39-5—————Indeno (1,2,3-cd)pyrene___53-70-3—————Dibenz(a,h)anthracene ___191-24-2————Benzo (g,h,i) perylene_____
50. |U10. |U50. [U50. |U10. |U10. |U10. ]U10. IU10. IU50. |U50. IU10. |U10. IU10. IU50. |U10, |U10. |U10. IU10. |U10. |U10. IU20. |U10. IU10. [U10. (U10. |U10. [U10. )U10. |U10. |U10. IU10. IU
(1) - Cannot be separated from diphenylamine
FORM I SV-2 1/87 F
3Q3029 '*
IF EPA SAMPLESEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _
TENTATIVELY IDENTIFIED COMPOUNDS - II S3LK89
Lab Name: IEA Contract: 63-W8-0045 I
Lab Cede: IEA Case No.: 12544 SAS No.: SDG-No.:
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828405
O Level: (low/med) LOW Date Received: O/ Q/ 0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/22/89
Extraction: (SepF/Cont/Sonc) CONT . Date Analyzed: 8/28/89
^ GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: " 1.00
CONCENTRATION UNITS:Number TICs found: 1 (ug/L or ug/Kg) UG/L
CAS NUMBER
1. - -2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
COMPOUND NAME
UNKNOWN
'
RT
9.43
EST. CONC.
20.
QJ
*FORM I SV-TIC 1/87 I
AR303030 •"
rIB EPA SAMPLE NC
SEMIVOLAXILE ORGAJTICS ANALYSIS DATA SHEET _______________II SBLK93
Lab Name: IEA Contract: 63-W8-0045 |___________
Lab Code: IEA Case No.: 12544 SAS No.: , SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901408
Level: (low/med) LOW ,/ ; _ Date Received: O/ O/ 0
% Moisture: not dec.100. dec. 0. _ P§te Extracted: 8/25/39
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: .6.0 ,__ ..Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L Or ug/Kg) UG/L Q
s
111-44-4—————bis (2-Chloroethyl)ether ___95-57-8 ————— 2-Chlorophenol________541-73-1—————1,3-Dichlorobenzene ______106-46-7—————1,4-Dichlorobenzene ______100-51-6—————Benzyl alcohol___________95-50-1—————1,2-Dichlorobenzene ______95-48-7—————2-Methylphenol___________108-60-1—————his (2-Chloroisopropyl) ether106-44-5—————4-Methylphenol___________621-64-7————-N-Nitroso-di-n-propylamine_67-72-1—————Hexachloroethane________'98-95-3—————Nitrobenzene_____________78-59-1—————Isophorone______________88-75-5 ————— 2-Nitrophenol ___________105-67-9 ————— 2,4-Dimethylphenol_________65-85-0—————Benzoic acid____________111-91-1—————bis (2-Chloroethoxy)me thane_120-83-2 ————— 2,4-Dichlorophenol______'_120-82-1—————1,2,4-Trichlorobenzene_____91-20-3—————Naphthalene _______;______106-47-8 ————— 4-Chloroaniline __________87-68-3—————Kexachlorobutadiene ______59-50-7—————4-Chloro-3-methylphenol ___91-57-6—————2-Methylnaphthalene ______77-47-4—————Hexachlorocyclopentadiene _88-06-2 ————— 2,4,6-Trichlorophenol _____95-95-4—————2,4,5-Trichlorophenol ____91-58-7—————2-Chloronaphthalene ______88-74-4—————2-Nitroaniline___________131-11-3—————Dime thy Iphthalate ________208-96-8—————Acsnaphthylene___________606-20-2—————2,6-Dinitrotoluene________
FORM I SV-1 ~ - 1/87 R
1C " EPA SAMPLE NSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _____
| SBLK93Lab Name: IEA Contract: 68-WS-0045 |______
Lab Code: IEA Case No.: 12544 SAS No.: " SDG No.:
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901408
Level: (low/med) LOW . Date Received: O/ O/ 0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/25/89
Extraction: (SepF/Cont/Sonc) CCNT Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
1 \————————————j ,| 99-09-2—————3-Nitroaniline___________i 50. IU 1| 83-32-9—————Acenaphthene_____________| 10. [U 1| 51-28-5—————2,4-Dinitrophenol ________1 50. |U 11 100-02-7—————4-Nitrophenol ____________1 50. ]U |i 132-64-9—————Dibenzofuran 1 10. IU 1
121-14-2—————2,4-Dinitrotoluene______84-66-2—————Diethylphthalate________
7005-72-3 ————— 4-Chlorophenyl-phenylether^86-73-7—————Fluorene______________'_100-01-6—————4-Nitroaniline_________534-52-1—————4,6-Dinitro-2-methylphenol_86-30-6—————N-Nitrosodiphenylamine (1)]101-55-3—————4-Bromophenyl-phenylether ~118-74-1—————Hexachlorobenzene ______87-86-5—————Pentachlorophenol ______85-01-8—————Phenanthrene___________120-12-7—————Anthracene_____________84-74-2—————Di-n-butylphthalate _____206-44-0—————Fluoranthene___________129-00-0—————Pyrene________________85-68-7—————Butylbenzylphthalate_____91-94-1—————3,3 f -Dichlorobenzidine___56-55-3—————Benzo (a) anthracene______218-01-9—————Chrysene______________117-81-7—————bis(2-Ethylhexyl)phthalate117-84-0—————Di-n-octylphthalate ____"m205-99-2—————Benzo (b) fluoranthene_____207-08-9—————Benzo(k)fluoranthene_____50-32-8—————Benzo (a)pyrene__________193-39-5—————Indeno (1,2,3-cd) pyrene___53-70-3—————Dibenz(a,h)anthracene ___191-24-2—————Benzo (g ,h, i) perylene_____
10. |U10. IU10. |U10. |U50. IU50. IU10. [U10. |U10. IU50. IU10. IU10. IU10. IU10. IU10. |U10. |U20. |U10. IU10. JU10. IU10. IU10. IU10. IU10. [U10. IU10. |U10. .IU
(1) - Cannot be separated from diphenylamineFORM I SV-2 . 1/87
AR3Q3Q32 " "
IF EPA SAMPLE KSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _ _________
TENTATIVELY IDENTIFIED COMPOUNDS |"I SBLK9 3
Lab Name: IEA t Contract: 63-W8-0045 I__________
Lab Code: IEA Case No.: 12544" SAS Wo.: - SDG No.: CCHOO
Matrix: (soil/water) WATER . ... _^v. Lab_ Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0901408
Level: (low/med) LOW . Date Received: O/ O/ 0
% Moisture: not dec.100. dec. 0, „ Date Extracted: 8/25/S9
Extraction: (SepF/Cont/Sonc) CONT Data Analyzed: 9/ 1/89GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: • 1.00
; - - .-CONCENTRATION UNITS:Number TICs found: 2 . . (ug/L or ug/Kg) UG/L
1I CAS NUMBERI11. - -12. - -I 3.1 4.1 5.1 6.! 7.1 8.1 9.1 10.1 11.1 12.1 13.I 14.! 15.1 16.1 17.I 18.I 19.1 20.1 21. 11 22. 11 23. 11 24. 11 25. 11 26. 1i 27. Ii 28. I1 29. 11 30. 11 1
COMPOUND NAME
UNKNOWNUNKNOWN
.
;
1
„-. , _
|RT [ EST. CONC.
9.42 i 10.10.10 | 10.
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QJJ
FORM I JV-TIC _ _ l/_87•—•'---- flR303033 ''
r13 EPA SAMPLE
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET '•
I SBLK97Lab Name: IEA • Contract: 68-W8-0045 |
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHQO'
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0911408
Level: (low/med) LOW Date Received: O/ O/ 0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/28/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/11/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I I I II 108-95-2—————Phenol . 1 10. ]U 1
111-44-4—————bis (2-Chloroethyl)ether ___95-57-8 ————— 2-Chlorophenol___________541-73-1————-1,3-Dichlorobenzene ______106-46-7 ————— 1,4-Dichlorobenzene ______100-51-6—————Benzyl alcohol___________95-50-1—————1,2-Dichlorobenzene ______95-48-7—————2-Methylphenol___________108-60-1—————bis (2-Chloroisopropyl) ether106-44-5 ————— 4-Methylphenol___________621-64-7—————N-Nitroso-di-n-propylamine_67-72-1————Hexachlor oethane_________98-95-3—————Nitrobenzene____________78-59-1—————Isophorone______________88-75-5—————2-Nitrophenol ___________105-67-9—————2,4-Dimethylphenol________65-35-0—————Benzoic acid_____________111-91-1—————bis (2-Chloroethoxy) me thane_120-33-2—————2,4-Dichlorophenol________120-82-1—————1,2,4-Trichlorobenzene_____91-20-3—————Naphthalene ____________106-47-8—————4-Chloroaniline _________87-63-3—————Hexachlorobutadiene
O 1 59-50-7—————4-Chloro-3-methylphenolj 91-57-6—————2-Methylnaphthalene __
77-47-4—————Hexachlor ocyclopentadiene88-06-2—————2,4,6-Trichlorophenol __95-95-4—————2,4,5-Trichlorophenol __91-58-7—————2-Chloronaphthalene ____88-74-4—————2-Nitroaniline_________131-11-3—————Dimethylphthalate ______208-96-8—————Acenaphthylene_________606-20-2—————2,6-Dinitrotoluene_____
10. IU10. |U10. IU10. [U10. IU10. |U10. IU10. IU10. IU10. IU10. [U10. )U10. |U10. IU10. IU50. IU10. IU10. IU10. |U10. IU10. IU10. IU10. IU10. |U10. |U10. IU50. IU10. IU50. |U10. |U10. ' *IU10. IU
FORM I SV-
1C • EPA SAMPLESEMIVOLATILZ ORGANICS ANALYSIS. DATA SHEET , „
I S3LK97Lab Name: IEA Contract: 63-WS-Q045 |_______
Lab Cede: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab "Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0911408
Level: (low/med) LOW !1 "" /'"""Gate Received: O/ O/ 0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/28/89
Extraction: (SepF/Cont/Sonc) CONT Date Analyzed: 9/11/89
GPC Cleanup: (Y/N) N pH: 6.0 , Dilution Factor: 1.00
"CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or Ug/Kg) UG/L Q
99-09-2—————3-Nitroanilii83-32-9—————Acenaphthene
| 51-28-5 ————— 2,4-DinitrophenolI 100-02-7 ————— 4-Nitrophenol __
132-64-9—————Dibenzofuran121-14-2————-2,4-Dinitrotoluene
•Diethylphthalate________•4-Chlorophenyl-phenylether
86-73-7—————Fluorene______________100-01-6—————4-Nitroaniline________]534-52-1—————4,6-Dinitro-2-methylphenol_86-30-6—————N-Nitrosodiphenylamine (1)~101-55-3—————4-3romophenyl-phenylether118-74-1—————Hexachlorobenzene ______87-36-5—————Pentachlorophenol _______
-Phenanthrene________120-12-7—————Anthracene__________84-74-2—————Di-n-butylphthalate _206-44-0—————Fluoranthene . ....._.. :129-00-0—————Pyrene_____________85-68-7—————Butylbensylphthalate__91-94-1—————3 , 3 ' -Dichlorobenzidine
-Benzo(a)anthracene218-01-9—————Chrysene_______________117-81-7—————bis(2-Ethylhexyl)phthalate117-84-0—————Di-n-octylphthalate ____~205-99-2—————Benzo (b) fluoranthene_____
-Benzo (k) f luoranthene_•Benzo(a)pyrene
193-39-5—————Indeno (1,2,3-cd)pyrene_
191-24-2————Benzo(g,h,i)perylene
50. |U10. |U50. 1U50. IU10. (U10. |U10. |U10. |U10. (U50. |U50. |U10. IU10. |U10. )U50. |U.10. |U10. |U10. IU10. [U10. |U10. ]U20. IU10. (U10. IU10. IU10. [U10. [U10. IU10. |U10. IU10. IU10. . IU'I
(1) - Cannot be separated from diphenylamine
FORM I SV-2 1/87 J=
~ ftR303035
IF EPA SAMPLE NSEMIVOLATILE ORGA.NICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS1 S3LK97
Lab Name: IEA : Contract: 63-W8-OQ45 1
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.:
Matrix: (soil/water) WATER Lab 'Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0911408
Level: (low/med) LOW . Date Received: 0/0/0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/28/89
Extraction: (SepF/Cont/Sonc) CONT ' Date Analyzed: 9/11/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1*00
CONCENTRATION UNITS:Number Ties found: 1 (ug/L or ug/Kg) UG/L
CAS NUMBER
1. - -2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.
1 25.I 26.27.28.29.30.
ICOMPOUND NAME
UNKNOWN
RT
9.25
1
EST. CONC.
20.
i
QJ
*
—-fe_
FORM I SV-TIC 1/87 R
flR303036"
r-IB " EPA SAMPLE K-
SEMXVOLATILE ORGANICS ANALYSIS DATA SHEET ' " -
• "- -— I SBLK10Lab Name: IEA Contract: 63-W8-0045 I
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0911D10
Level: (low/med) LOW _ ...;. Date Received: 0/0/0
% Moisture: not dec.lOQ. dec. 0. Date Extracted: 8/30/89
„ Extraction: (SepF/Cont/Sonc) SEPF . Date Analyzed: 9/12/89
GPC Cleanup: (Y/N) N : pH: 6.0 Dilution Factor: 1.00
""'CONCENTRATION UNITS:CAS NO. COMPOUND . (ug/L or ug/Kg) UG/L Q
108-95-2—————Phenol^__________________________111-44-4 ———— -bis.( 2-Chloroethyl)ether ___95-57-8 ————— 2-Chlorophenol____541-73-1 ————— 1,3-Dichlorobenzene106-46-7—————1,4- _____100-51-6—————Benzyl alcohol _____95-50-1—————1,2-Dichlorobenzene ______95-48-7—————2-Methylphenol___________108-60-1—————bis (2-Chloroisopropyl) ether106-44-5—————4-Methylphenol___________621-64-7—————N-Nitroso-di-n-propylamine_67-72-1—————Hexachloroethane
•Nitrobenzene78-59-1—————Isonhorone____________88-75-5 ————— 2-Nitrophenol _________]105-67-9—————2,4-Dimethylphenol____'65-85-0—————Bensoic acid . . . . . _ . . . .111-91-1—————bis (2-ChloroethoxyJmethaneJ120-83-2—————2,4-Dichlorophenol______"120-82-1—————If 2, 4-Trichlorobenzene___"91-20-3—————Naphthalene ___________106-47-8 ————— 4-Chloroaniline ________.87-68-3—————Hexachlorobutadiene _____'59-50-7—————4-Chloro-3-methylphenol __91-57-6—————2-Methylnaphthalene _____77-47-4—————Hexachlorocyclopentadiene88-06-2—————2,4,6-Trichlorophenol _^__"
•2,4,5-Trichlorophenol ___'91-58-7—————2-Chloronaphthalene88-74-4—————2-Nitroaniline__131-11-3—————Dimethylphthalate208-96-8———•
•2,6-Dinitrotoluene
10. IU10. |U10. |U10. IU10. IU10. |U10. IU10. [U10. |U10. IU10. |U10. ]U10. |U10. |U10. [U10. [U50. IU10, |U10. IU10. IU10. |U10. [U10. IU10. |U10. |U10. 1U10. |U50. |U10. |U50. |U10. . |U10. '|U10. |U
FORM I SV-1 ' . 1/87 I_fiR3G3Q37
1C • EPA SAMPLESEMIVOLATILE CRGANICS ANALYSIS DATA SHEET _____
1 " S3LK10Lab Name: IEA Contract: 63-W8-0045 I_______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0911D10
Level: (low/med) LOW Date Received: O/ O/ 0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/30/89
Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/12/89
'3 GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
o
O
99-09-2—————3-Nitroaniline ! 50. IU83-32-9—————Acenashthene I 10. IU51-28-5 ————— 2,4-Dinitrophenol ________I 50. jU100-02-7————-4-Nitrophenol 50. U132-64-9—————Dibenzofuran I 10. |U
7005-72-3—————4-Chlorophenyl-phenylether_86-73-7—————Fluorene________________100-01-6-.————— 4-Nitroaniline_________.534-52-1—————4,6-Dinitro-2-methylphenol_86-30-6————N-Nitrosodiphenylamine (1)_101-55-3 ————— 4-3romoDhenyl-phenylether118-74-1—————87-86-5—————
•Phenanthrene120-12-7——————Anthracene________84-74-2—————Di-n-butylphthalate206-44-0—————Fluoranthene______129-00-0—————
121-14-2—————2,4-Dinitrotoluene________| 10. | U84-66-2————Diethylphthalate_________| 10. IU
10. IU10. IU50. |U50. [U10. |U10. IU10. |U50. IU10. IU10. (U10. IU10. IU10. IU10. IU20. |U10. |U10. IU10. IU10. ]U10. (U10. [U10. (U10. IU10. IU10. IU
91-94-1——————3.3 '-Dichlorobenzidine___56-55-3—————Benzo (a) anthracene______218-01-9—————Chrysene_______________117-81-7—————bis (2-Ethylhexyl )phthalate_117-84-0—————Di-n-octylphthalate
-99-2—————Benzo (b) fluoranthene,207-08-9—————Benzo(k) fluoranthene"
-Benzo(a)pyrene______•Indeno (1,2,3 -cd) pyrene_•Dibenz(a,h)anthracene
191-24-2—————Benzo (g,h,i)peryl
(1) - Cannot be separated from diphenylamine
FORM I SV-2 1/87 E
IF . . • EPA SAMPLESZMIVCLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS [I S3LK10
Lab Name: IEA •--: ---- ' Contract: 68-W8-0045
Lab Code: IEA Case No.: 12544 SAS No..: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML ' Lab File ID: 0911D10
Level: (low/med) LOW • Date Received: O/ O/ 0
% Moisture: not dec.100. dec. 0.. , :. Date Extracted: 8/30/89
Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/12/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
- CONCENTRATION UNITS:Number TICs found: 1 (ug/L or ug/Kg) UG/L
1 1 . ...._".......I CAS NUMBER | COMPOUND NAME
|1. - - I UNKNOWN1 2 . |1 3. I1 4. I1 5 . |1 6. I1 7. |1 8. |1 9- 11 10. |1 11. 11 12. |1 13. I1 14. Ii 15. !1 16. I1 17. |1 18. [i 19. 11 20. I1 21. I1 22. |1 23. I1 24. I1 25. I1 25. I1 27. |1 28. I1 29. |
30. I1
RT
9.23
EST. CONC.
8.
QJ
FORM I SV-TIC ' " 1/87flR303039 '
IB EPA SAMPLE fifeSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET "________
II CCH03MS
Lab Name: IEA . Contract: 63-W8-0045 I
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHQO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 10QQ. (g/mL) ML Lab File ID: 0828411
Level: (low/med) LOW Date Received: 8/13/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/22/89
Extraction: (SepF/Cont/Scnc) CCNT Date Analyzed: 8/23/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L 'Q
! I I i[ 108-95-2—————Phenol__________________I 160. 1 i| 111-44-4—————bis(2-Chloroethyl)ether ___1 10. IU |
95-57-8 ————— 2-Chlorophenol____ _______541-73-1—————1,3-Dichlorobenzene ______106-46-7—————1,4-Dichlorobenzene ______100-51-6—————Benzyl alcohol___________95-50-1—————Ir2-Dichlorobenzene ______95-4S-7—————2-Methylphenol___________108-60-1————bis (2-Chloroisopropyl) ether106-44-5—————4-Methylphenol___________621-64-7—————N-Nitroso-di-n-propylamine_67-72-1—————Kexachloroethane_________98-95-3—————Nitrobenzene_____________78-59-1—————Isophorone______________88-75-5——————2-Nitrophenol ____________105-67-9—————2,4-Dimethylphenol________65-85-0—————Benzoic acid111-91-1—————bis (2-Chloroethoxy) methane_120-83-2—————2, 4-Dichlorophenol________120-82-1—————1.2. 4-Trichlorobenzene_____91-20-3—————Naphthalene ____________106-47-8—————4-Chloroaniline _________87-68-3—————Hexachlorobutadiene ______59-50-7—————4-Chloro-3-methylphenol ___91-57-6—————2-Methylnaphthalene ______77-47-4—————Hexachlorocyclopentadiene _88-06-2—————2,4.6-Trichlorophenol ____95-95-4—————2,4,5-Trichlorophenol _____91-58-7—————2-Chloronaphthalene ______88-74-4——-^~-2-NitroaniIine___________131-11-3—-———Dimethylphthalate ________208-96-8—————Acenaphthylene___________606-20-2—————2f 6-Dinitrotoluene________
78. |10. |U47. |10. |U10. [U10. IU10. IU10. IU62. I10. IU10. |U10. IU10. |U10. IU50. IU10. |U10. IU55. |10. |U10. |U10. [U110. |10. IU10. IU10. IU50. ]U10. IU50. |U10. IU10. -IU10. IU 4
FORM I SV-1 _. . n . 1/87 F
1C . . -. EPA SAMPLE ISSEMIVOLATILE CRGANICS ANALYSIS DATA SHEET ___________
• ' ' ' . . :".. " " ' _ ———————I CCH03MS
Lab Name: IEA ^ _^ ... Contract: 63-W8-0045 I_______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828411
Level: (low/med) LOW Date Received: 8/18/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/22/39
Extraction: (SepF/Ccnt/Sonc) CONT Date Analyzed: 3/28/89
GPC Cleanup: (Y/N) N pK: 6.0 " Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2 ————— 3-Nitroaniline _____S3 -3 2-9-- ——— • Acenaphthene...51-28-5 ————— 2,4-Dinitrophenol ; _____100-02-7 ————— 4-Nitrophenol __________132-64-9 ————— Dibenzofuran _____121-14-2 ————— 2 , 4-Dinitrotoluene_ _____84-66-2 ————— Diethylphthalate
7005-72-3 —— ----4-Chlorophenyl-phenylether _*86-73-7—————Fluorene______________
100-01-6—————4-Nitroaniline__________534-52-1—————;4/6-Dinitro-2-methylphenol-
. 86-30-6—————N-Nitrosodiphenylamine (1)]3 , I 101-55-3 ————— 4-Bromophenyl-phenylether ~_
118-74-1—————Hexachlorobenzene . ..87-86-5 ————— Pentachlorophenol85-01-8 ————— Phenanthrene ______120-12-7 ————— Anthracene84-74-2 ————— Di-n-butylphthalate206-44-0 ————— Fluoranthene129-00-0 ————— Pyrene85-68-7 ————— Butylbenzylphthalate91-94-1 ————— 3 . 3 ' -Dichlorobenzidine __ _56-55-3 ————— Senzo ( a ) anthracene218-01-9 ————— Chrysene ______________117-31-7 ————— bis(2-Ethylhexyl)phthalate117-84-0 ————— Di-n-octylphthalate205-99-2 ————— Benzo (b) fluoranthene207-08-9 ————— Benzo(k) f luoranthene_50-32-8 ————— Benzo(a)pyrene193-39-5 ————— Indeno (1,2, 3 -cd) pyrene53-70-3 ————— Dibenz( a, h) anthracene ___191-24-2 ————— Senzo (g.h/i)perylene
50. IU64. I50. IU74. I10. |U67. |10. |U10. IU10. IU50. [U50. IU10. |U10. [U10. |U84. |10. (U10. IU10. |U10. |U63. |10. |U20. |U10. |U10. IU10. IU10. |U10. IU10. |U10. |U10. IU10. IU10. IU
(1) - Cannot be separated from diphenylamine
FORM I SV-2 1/87 3
IB EPA SAMPLE NCSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ____________,
I CCH03MSDLab Name: IEA Contract: 68-W8-0045 j.____
Lab Cede: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828412
Level: (low/med) LOW Date Received: 8/13/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/22/89
Extraction: (SepF/Cont/Sonc) CCNT Date Analyzed: 8/28/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I 1 I II 108-95-2—————Phenol___________________I 2 0 0 - 1 || 111-44-4—————bis(2-Chloroethyl)ether ___i 10. IU 1
95-57-8 ————— 2-Chloroohenol 91.541-73-1—————1,3-Dichlorobenzene ______| 10106-46-7 ————— 1,4-Dichlorobenzene 55100-51-5—————Benzyl alcohol__________95-50-1—————lf2-Dichlorobenzene ______95-48-7—————2-Methylphenol _____108-60-1—————bis (2-Chloroisopropyl) ether106-44-5—————4-Methylphenol__________621-64-7—————N-Nitroso-di-n-propylamine__67-72-1—————Hexachloroethane_________98-95-3—————Nitrobenzene __1-59-1—————Isophorone
83-75-5 ————— 2-Nitrophenol-67-9 ————— 2,4-Dimethylphenol
•Benzoic acid-91-1—————bis (2-Chloroethoxy) me thane_
120-83-2—————2,4-Dichlorophenol________120-82-1—————112 ,4-Trichlorobenzene_____91-20-3—————Naphthalene
•4-Chloroaniline'-68-3—————Hexachlorobutadiene
59-50-7—————4-Chloro-3-methylphenol ___91-57-6—————2-Methylnaphthalene ______77-47-4—————Hexachlorocyclopentadiene _88-06-2—————2,4,6-Trichlorophenol ____
-2.4,5-Trichlorophenol91-58-7—————2-Chloronaphthalene88-74-4—————2-Nitroaniline____131-11-3—————Dimethylphthalate __
-96-8—————Acenaphthylene_606-20-2—————2,6-Dinitrotoluene
10. ]U10. 1U10. IU10. |U10. |U59. 110. IU10. IU10. IU10. IU10. IU50. IU10. |U10. |U58. |10. [U10. IU10. IU
110. I10. |U10. IU10. IU50. IU10. IU50. IU10. • IU10. "IU10. IU
*
*FORM I SV-1 • 1/87 F
flB3030i42
: 1C EPA SAMPLESEMIVOLATILE ORGAN!CS ANALYSIS DATA SHEET ______^'
I ~~—————I CCH03MSD
Lab Name: IEA v'\r :--- -Contract: 63-W8-0045 |_________
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL) ML Lab File ID: 0828412
Level: (low/med) LOW Date Received: 8/18/89
% Moisture: not dec. 100. ; dec. 0. Date Extracted: 8/22/89
Extraction: {SepF/Cont/Sonc) CCNT Date Analyzed: 8/28/89
GPC Cleanup: (Y/N) 'N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
O—' -" W —' 4* —I fcl^W^UU.^A.J. . **>•— ____________________^_^____________ I
66
O
99-09-2————-3-Nitroaniline___________1 50. |U83-32-9—————Acsnaphthene51-28-5 ————— 2,4-Dinitrophenol ______100-02-7 ————— 4-Nitrophenpl13 2-64-9--———Dibenzofuran______121-14-2 ————— 2,4-Dinitrotoluene_______84-66-2—————Diethylphthalate________
7005-72-3 ————— 4-Chlorcphenyl-phenylether_86-73-J—————:Fluorene_________]____"100-01-6 ————— 4-Nitroaniline_________"534-52-1—————.4,6-Dinitro-2-methylphenol_i86-30-6—————N-Nitrosodiphenylamine (1)]101-55-3———:——4-3romophenyl-phenylether [118-74-1—————Hexachlorobenzene ______87-86-5—————Pentachlorophenol ______35-01-8—————Phenanthrene - . „„_120-12-7—————Anthracene______- . .____84-74-2—————Di-n-butylphthalat_e .._ .__ .206-44-0—————Fluoranthene____________129-00-0—————Pyrene____________85-58-7—————Butylbenzylphthalate____"91-94-1—————3 , 3' -Dichlorobenzidine___56-55-3—————Benzo (a) anthracene______218-01-9—————Chrysene______________~117-81-7—————bis (2-Ethylhexyl )phthalate_117-84-0—————Di-n-octylphthalate ____"205-99-2—————Benso(b) fluoranthene____~207-08-9—————Benzo(k)fluoranthene_____50-32-8—————Benzo (a) pyrene_________"193-39-5—————Indenod, 2,3-cd)pyrene___53-70-3—————Dibenz(a,h)anthracene ___191-24-2—————Benzo (g,hf i)perylene_____
50. |U120. |10. |U70. |10. ]U10. IU10. |U50. IU50. (U10. IU10. IU10. |U110. 110. [U10. IU10. IU10. IU66. |10. [U20. |U10. |U10, |U10. |U10. IU10. IU10. IU10. IU10. IU10. IU10. IU
(1) - Cannot be separated from diphenylamine
FORM I SV-2 1/87 I
ID EPA SAMPLE NOPESTICIDE CRGANICS ANALYSIS DATA SHEET
1 PBLK73Lab Name: IEA Contract: 63-W8-0045
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL)ML ' Lab File ID: DB5A4554
Level: (low/med) LOW Date Received: O/ O/ 0
% Moisture: not dec,100. dec. 0. Date Extracted: 8/17/39
Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
O
319-34-5————aloha-BHC | .050 [U319-85-7————beca-BHC I .050 IU319-86-3————delta-BEC I .050 [U58-89-9———gamma-BHC [ .050 (U76-44-3————Heptachlor | .050 IU309-00-2————Aldrin I .050 IU1024-57-3———Heptachlor epoxide j .050 JU959-98-8————Endosulfan I I .050 )U60-57-1————Dieldrin I .10 IU72-55-9————4,4r -DDE I . 10 IU72-20-8———Endrin I .10 IU
33213-65-9———Endosulfan II I .10 |U72-54-8————4.4'-DDD | .10 IU
1031-07-8———Endosulfan sulfate [ .10 IU50-29-3————4,4' -DDT I . 10 IU72-43-5———Methoxychlor I .50 JU
53494-70-5————Endrin ketone 1 .10 IU5103-71-9———alpha-Chlordane | .50 |U5103-74-2———gamraa-Chlordane j .50 JU8001-35-2————Toxaphene | 1.0 IU12674-11-2———Aroclor-1016 | . 50 | U11104-23-2————Aroclor-1221 I .50 [U11141-16-5———Aroclor-1232 | .50 IU53469-21-9————Aroclor-1242 [ .50 IU12672-29-6———Aroclor-1248 1 .50 |U11097-69-1———Aroclor-1254 I 1.0 IU11096-82-5————Aroclor-1260 I 1.0 IU
FORM I PEST 1/87 Re'
ID EPA SAMPLE NO-PESTICIDE ORGANICS ANALYSIS DATA SHEET
I PBLK79Lab Name: IEA r - Contract: 6S-W8-0045 I______
Lab Code: IEA Case No.: 12544 SAS No.: ' SDG No.: CCHOO
Matrix: (soil/water) WATER . ... r"~_. Lab Sample ID:
Sample wt/vol: 1000. (g/mL)ML ' Lab File ID: DB5A4556
Level: (low/med) LOW '. Date Received: 0/0/0
% Moisture: not dec.100. dec. 0. Date Extracted: 8/21/89
Extraction: (SepF/Conr/Sonc) SEPF _ ... : Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
- , • - - ,. CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
319-84-6———alpha-3HC I .050 |U319-35-7———ceta-3EC I .050 [U319-86-3———delta-BHC . [ .050 [U53-39-9———gamma-3HC I .050 IU76-44-3———Heptachlor I .050 |U309-00-2———Aldrin 1 .050 |U1024-57-3———Heatachlor eraoxide I .050 |U959-98-8———Sndosulfan I I .050 (U60-57-1———Dieidrin I .10 IU72-55-9————4f4r-DDE I .10 |U72-20-8———Endrin I . 10 | U
33213-65-9———Sndosulfan II [ .10 |U72-54-8————4,4f-DDD | .10 JU
1031-07-3———Endosulfan sulfate I .10 ]U50-29-3 ———— 4,4f-DDT I .10 IU72-43-5———Methoxychlor I • .50 [U
53494-70-5———Endrin ketone | .10 |U5103-71-9———alpha-Chlordane | .50 |U5103-74-2———gamma-Chlordane j .50 |U8001-35-2———Toxaphene I 1.0 (U12674-11-2————Aroclor-1016 I .50 [U11104-28-2———Aroclor-1221 | .50 JU11141-16-5———Aroclor-1232 I .50 IU53469-21-9———Aroclor-1242 1 .50 |U12672-29-6———Aroclor-1248 | .50 IU11097-69-1———Aroclor-1254 I 1.0 |U11096-82-5————Aroclor-1260 | 1.0 |U
FORM I PEST . 1/87 Re
r
ID ' EPA SAMPLE NO.PESTICIDE CRGANICS ANALYSIS DATA SHEET
~| "PBLK35Lab Name: IEA Contract: 63-WS-Q045 I
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mLJML ' Lab File ID: DB5A4563
Level: (Icw/med) LOW Date Received: O/ O/ 0
% Moisture: not dec.100. dec. 0. Date Extracted: 3/29/39
Extraction: (SepF/Conc/Sonc) SEP? Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
O
319-34-6————alpha-3HC319-85-7————beta-3HC319-86-8————delta-BHC53-89-9-———gamma-3HC76-44-8————Hentachlor309-00-2————Aldrin1024-57-3———Keotachlor epoxide959-98-8———Endosulfan I60-57-1———Dieldrin72-55-9————4,4' -DDE72-20-3————Sndrin
33213-65-9———Sndosulfan II72-54-8 ———— 4,4'-DDD
1031-07-8———Sndosulfan sulfate50-29-3———4.4' -DDT72-43-5———Methoxychlor
53494-70-5———Sndrin ketone5103-71-9————alpha-Chlordane5103-74-2———gamma-Chlordane8001-35-2————Toxaphene12674-11-2———Aroclor-101611104-28-2———Aroclor-122111141-16-5———Aroclor-123253469-21-9———Aroclor-124212672-29-6————Aroclor-124811097-69-1————Aroclor-125411096-82-5————Aroclor-1260
.050 IU
.050 [U
.050 (U
.050 |U
.050 |U
.050 |U
.050 |U
.050 |U.10 |U.10 |U.10 |U.10 IU.10 IU.10 |U.10 iy.50 IU.10 ju.50 IU.50 ]U1,0 |U.50 IU.50 ]U.50 |U.50 [U.50 |U1.0 [U1.0 IU
FORM I PEST 1/87 Re"
ID EPA SAMPLE NO,PESTICIDE ORGANICS ANALYSIS DATA SHEET _______
I PBLKS 3Lab Name: ISA Contract: 63-W3-0045 [______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1QOO. (g/mL)ML - Lab File ID: DB5A4567
Level: (low/med) LOW . Date Received: O/ O/ 0
% Moisture: not dec.100, dec. 0. __ Date Extracted: 8/28/89
Extraction: (SepF/Conc/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1,00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
i i i i| 319-84-5————alpha-BHC I .050 |U || 319-35-7————beta-BEC I .050 |U! 319-36-8————delta-3EC I .050 |U
53-89-9———gamma-BHC| 76-44-8———Heotachlor| 309-00-2———Aldrin1 1024-57-3———He-ntachlor epoxide! 959-98-3———Sndosulfan II 60-57-1———Dieldrin| 72-55-9————4,4'-DDEI 72-20-8———EndrinI 33213-65-9———Sndosulfan III 72-54-8————4,4 ' -DDDI 1031-07-8———Sndosulfan sulfate| 50-29-3 ———— 4,4'-DDTI 72-43-5———Methoxychlor[ 53494-70-5———Sndrin ketone| 5103-71-9———alpha-ChlordaneI 5103-74-2———gamma-Chlordanej 8001-35-2———ToxapheneI 12674-11-2———Aroclor-1016| 11104-23-2————Aroclor-1221| 11141-16-5———Aroclor-1232| 53469-21-9———Aroclor-1242| 12672-29-6————Aroclor-1248I 11097-69-1———Aroclor-1254| 11096-82-5———Aroclor-1260
.050 |U
.050 IU
.050 [U
.050 IU
.050 IU.10 IU.10 [U.10 |U.10 [U.10 IU.10 |U.10 IU.50 |U.10 ]U.50 IU.50 [U1.0 [U.50 |U.50 IU.50 [U.50 IU.50 [U1.0 |U1.0 |U
FORM I PEST ' 1/87 Re
' - : ; SR303QU '
ID EPA SAMPLE NO,PESTICIDE CRGANICS ANALYSIS DATA SHEET _____________
|• CCH03MSLab Name: IEA . Contract: 63-W3-0045 1______
Lab Code: IEA Case No.: 12544 SAS No.: SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL)ML • Lab File ID: DB5A4561
Level: (low/med) LOW Date Received: 8/18/39
% Moisture: not dec.lQQ. dec. 0. Date Extracted: 8/21/39
Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: 6.0 Dilution Factor: 1.00
CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
O
319-84-6————alpha-BBC319-85-7————beta-3HC319-86-3————delta-3EC58-89-9————gamma-BBC76-44-8———Heptachlor309-00-2————Aldrin1024-57-3———Heptachlor epoxide959-98-8———Endosulfan I60-57-1———Dieldrin72-55-9————4,4' -DDE72-20-3———Sndrin
33213-65-9———Endosulfan II72-54-3————4,4'-DDD
1031-07-8———Endosulfan sulfatef _
72-43-5———Methoxychlor53494-70-5———Sndrin ketone5103-71-9———alpha-Chlordane5103-74-2———gamma-Chlordane8001-35-2————Toxachene12674-11-2————Aroclor-101611104-28-2———Aroclor-122111141-16-5————Aroclor-123253469-21-9————Aroclor-124212672-29-6————Aroclor-124811097-69-1————Aroclor-125411096-82-5———Aroclor-1260
,050 |U,050 |U,050 IU.16 I• 14 |.14 [,050 [U,050 )U.33 1.10 IU.40 |.10 |U.10 ITT,10 [U.33 I.50 IU.10 ITT.50 IU.50 IU1.0 IU.50 IU.50 IU.50 IU.50 IU.50 |U1.0 IU1.0 IU
•
FORM I PEST . 1/87 Re-
BR3030U8
ID EPA SAMPLE NOPESTICIDE CRGANICS ANALYSIS DATA SHEET
: I CCH03MSDLab Name: IEA Contract: 68-W8-G045 I
Lab Code: IEA Case No.: 12544 SAS No.: ' SDG No.: CCHOO
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000. (g/mL)ML Lab File ID: DB5A4562
Level: (low/med) LOW Date Received: 8/18/89
% Moisture: not dec.100. dec. 0. Date Extracted: 8/21/89
Extraction: (SepF/Conz/Sonc) SEPF . Date Analyzed: 9/ 1/89
GPC Cleanup: (Y/N) N pH: "6.6"" " Dilution Factor: 1.00
' CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
319-34-6————alpha-BBC319-85-7————bera-3HC319-36-8————delta-3HC58-89-9————gamma-3KC76-44-3———Heptachlor309-00-2r——Aldrin1024-57-37-——Heptachlor epoxide959-93-8———Sndosulfan I60-57-1———Dieldrin72-55-9————4, 4' -DDE72-20-8———Sndrin
33213-65-9———Endosulfan II72-54-8————4,4'-DDD
1031-07-8———Sndosulfan sulfate50-29-3————4,4'-DDT72-43-5———Methoxychlor
53494-70-5———Sndrin ketone5103-71-9———alpha-Chlordane5103-74-2———gamma-Chlordane8001-35-2———Toxaphene12674-11-2————Aroclor-101611104-28-2————Aroclor-122111141-16-5———Aroclor-123253469-21-9———Aroclor-124212672-29-6———Aroclor-124811097-69-1———Aroclor-125411096-82-5———Aroclor-1260
.050 IU
.050 IU
.050 [U.18 I.13 1.13 I
.050 |U
.050 )U.33 |.10 IU.41 |.10 JU.10 IU.10 |U.32 [.50 IU.10 |U.50 |U.50 [U1.0 IU.50 |U.50 IU.50 IU.50 [U.50 IU1.0 IU1.0 |U
FORM I PEST 1/87 Re
flR3Q30*t9