Disclosure to Promote the Right To Information

Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public.

इंटरनेट मानक

“!ान $ एक न' भारत का +नम-ण”Satyanarayan Gangaram Pitroda

“Invent a New India Using Knowledge”

“प0रा1 को छोड न' 5 तरफ”Jawaharlal Nehru

“Step Out From the Old to the New”

“जान1 का अ+धकार, जी1 का अ+धकार”Mazdoor Kisan Shakti Sangathan

“The Right to Information, The Right to Live”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता है”Bhartṛhari—Nītiśatakam

“Knowledge is such a treasure which cannot be stolen”

“Invent a New India Using Knowledge”

है”ह”ह

IS 75 (1973): Linseed Oil, Raw and Refined [FAD 13: Oilsand Oilseeds]

Gr2

IS: 75 -1973

Indian StandardSPECIFICATION FOR

LINSEED OIL, RAW AND REFINED

(Second Revision)Second Reprint OCTOBER 2008

(IncorporatingAmendmentNo. I and IncludingAmendments No.2. 3 & 4)

UDC 665.345.4

© Copyright 1984

BUREAU OF INDIAN STANDARDSMANAK BHA VAN, 9 BAHADUR SHAH ZAFAR MARG

NEW DELHI 110002

December 1973

(Reafnrmed20)xxxx2010

18:75-1973

Indian StandardSPECIFICATION FOR

LINSEED OIL, RAW AND REFINED

(Second Revision)

Oils and Oilsceds Sectional Committee, Ct\FIJC .1

CI.airmanDR .I. S. B'\O.~Mt

RepresentingSwa~1 ik Household and 1ndustrial Products

Private LtJ, B(unhay

(CSIR ),

Members

Sum R.. M. DF;sA I ( Altrrnnte ton« J. S. Bad;ul\i)

DR N. R. BHOW Solvent Extractors' Association of India, BombaySHRl O. P. S.\XF:N.\ (Alttrnalt)

SURI S. K. Bos..~ National Test House; CalcuttaSURI K. M. CHAT1' ..:nJE"~ ( Altrrnati)

SURf D. S. C:HAOII.o\ Central Committee for Food Standards ( Ministry ofHealth & Family Planning). New Delhi

Sunr P. V. GUJ .\n.\THT Khadi & Vrllage Industries Commission, BombaySlUU V. L\KRH:\tlK .\NTHAN (Altrrnatt)

Slun H. P. (;UltTA East India Oil Millers' Association, CalcuttaSHUt R. H". Muss vnr t Alternate ; .

SHIH B. V. K'~T.\K Godrej Soaps Private Ltd, BombayDR A, S. K.\Jt'1'HA Indian Council of Agr icultural Research, New DelhiSURI R. D. K.\'YA1'RA Directorate General of Technical Development,

New DelhiHindustan Lever Ltd, BombavH,,('~ional Research Lvhora tory

Hl1ubanes war

DR A. P. MAJI.\n.J·~VAN'

n« S. N. MAHAP.\TR.\

Dn C~. Stuxrv vsur.u (AlternlZtf)SHRI N. S. ~I.~J~ I Directorate of Oilseeds Development (Ministry of

Agriculture ). HyderabadSInH H.\R ISH SETHI ( Alternate )

SHRI F. (-;. T. rtlJo;SJ·:1.Jo-;~ Directorate of Sugar & Vanaspati {Ministry ofAgrieulture }, N~\\' Delhi

SHUt Rue KIS}r<lJt.~ (AU"nlllf) ,DR S. K. MUKEUJ Jo~F: Indian Agricultural Research Institute, New DelhiSURf J. P. PATIUI Iralab Private Ltd, Bombay

SUR] J. (:. DE\" t Alternat« I )SHIH S. S. J--Iobl.~v.-\ K ( ....ltrmnte II )

( C~;1Wtd 011 fJGIt 2 )

e Copyright 1984

BUREAU OF INDIAN STANDARDS"fhi, publicanon i' protected under the Indi.,. COPY"I" Ad (XIV of 1957) aDdreproduction in whole or in part by a~y ~eans except with ~ritten permission .of thepublisher shall be deemed to be an infringement of copyrlgbt under the said .Art.

ts:75·1973

( Continued from tagt I )

~\ftmbt'S R'F,s,nti",SHRI T. S. RAMASWAMY The Tata Oil MiIJsCo Ltd, Bombay

SIIBI V. PARAME8WARAN ( Alternate)SIIRI P. RAMDA8 Central Warehousing Corporation, New DelhiSURI N. K. MURAJ.1DBARA RAO Directorate of Marketing & Inspection (Ministry of

Agriculture), NagpurSHIU K. L. CHATTEUJEE ( Alternate )

DR B. R. REDTJY Oil Technological Research Institute, AnantapurSURI S. C. SINuJfAI. The Vanaspati Manufacturers' Association of India,

Bombay "DR M. R. SunDARAM Regional Research Laboratory (CSIR), HyderabadSHRJ L. R. SUD Ministry of Defence (DGI )

SURI P. N. '\OAltWAl. ( Alternat« )SURI D. DAB GUPTA, Director General, lSI ( Ex-nJlicin Membtr)

Deputy Director General

Secretary

SItUI R. K. SINGH

Assistant Director ( Chern ), lSI

Oils and Fats Subcommittee, CJ\FDC 5 : 1

CO"l,entr

Dn S. M. PATJi~L Hindusran Lever Ltd, Bombay

Snm R. D. K"·ATltA

Dn G. LAK8HMINARAYANA

SHRI F. G. T. MENEZJt:S

MembersSnRI GOKULCRAND J. AOARWAI. Bombay Oilseeds and Oils Exchange Ltd, Dombay

Sum C. V. ~1 A H 1\\'Al.A (Altlrnale)SIIRl V. P. ANAl\TA~AnAYAN"'S Dil('ctc:ratc' of Marketing & Inspection (l\'1inistry

of Agriculture), NagpurSHIH V. L:HANOnA)IOtIJ.Y i Alternate ]

SHRl S. C. (iI-HiS):: Indian Soap and Toiletries Makers' Association,Calcutta

Directorate General of Technical Developmentl':ew Delhi '

Regional Research Laboratory (CSIR), HyderabadDirectorate of Sugar & Vanaspati (Ministry of

Agriculture ), New D~lhi

Swn RUl' KJSBORE (.AlJt",at~)SDKI B. S. MODI Tho Vanaspat i Manufacturers' A~sociatiQll of India,

BombayDB K. S. MUR'f1 Tungabhadra Industries Ltd, KurnoolSUltl RAJESHWAB PRASAD Oil Technologists Association of India, Kanpur

DB N. S. RAJAGOPAL (AUmaolt)SRRI1·. S. RAMASWAMY :rhc 1"ata Oil Mill~ CAl l.td, Bombay

SHKt V. PABAJrlB8WABAN (Alternate)SoBJ ~l. N. RAO Indian Paint Association, Calcutta

SnBI G. S. GUI. (Allmud' )SUBI L. R. SUI> Ministry of Defence (DGI )

2

AMENDMENT NO. % JANUARY 1MTO

IS : 7S - 1973 SPECIFICATION FOR LINSEED OIL,RAW AND REFINED

( Second Rel'ision )

( Pflge S, claus~ 4.3 ) - Substitute the roUowinS ror the exiltina claue:

'4.3 AaafDare wJtll 0dIer 0111- The material shaD be free from admixtureof other oils.

4.3.1 The material sball be free from non-edible oils, when tested inaccordance with 9, 10, 11, 12, 14, 15 and 16 of IS : 548 ( Part 2 )-1976·:

( Pag. S, clause 6.2 ) - Add the rollowinS new clause after 6.2:

'6.2.1 The containers may also be marked with the Standard Mark.

NOTE - The use of the Standard Mark is loverned by the provisions of theBureau of Indian Standard. Act, 1986 and the Rule. and Re,ulations madethereunder. The Standard Mark OD products covered by an Indian Standardconveys the assurance tbat they have been produced to comply with the require­ments of that standard under a well-defined system or inspection. testiq andquality control which is devised and supervised by SIS and operated by tbeproducer. Standard marked products are also contiauously checked by DIS(or conformity to that standard as a further sareauard. Details of ccnditlcnsUDder which a licence for the use of the Standard Mark may be .ranted tomaoufaeturers or producers, may be obtained from the Buroau of IDdianStandards.'

-Methods of sampling aDd te,t for oils and fats: Part 2 Pu.iI, test.

(CAFDC S)

AMENDMENT NO. 3 AUGUST 1995TO

IS 7S: 1973 SPECIFICATION FOR LINSEED OIL,RAW AND REFINED ·

( Second Revision)

( Page 3, Foreword, clause 0.4 ) - Add the following clause 0.5 afterclause 0.4 and renumber the subsequent clause:

·0.5 A scheme for labelling environment friendly products to be known as ECOMark has heen introduced at tbe instance of tbe Ministry of Environment andForests ( MEF). The ECO Mark shall be administercd by tbe Bureau of IndianStandards ( BIS ) under the BIS A,..t, 1986 as per tbe Resolution No. 71 dated 20Fehruary 1991 as published in the Gazette of the Government of India vide GSR85(E) dated 21 Fcbrua ry 1Y91. For a product to be eligible for marking with theECO Mark it shall also carry the Standard Mark of BIS for quality besidesmeeting additional optional environment friendly ( EF ) requirements. The EFrequirements for linseed oil, raw and refined are therefore being includedthrough an amendment.

This amendment is based on the Gazette Notification No. 678 dated 30 AugustlYY4 for Labelling Edible Oils, Tea and Coffee as environment friendlyproducts, published by the Ministry of Environment and Forests.' .

(Ptl/{e 5, clause 4.4 ) - Add the following clauses after clause 4.4:

'4.5 Optional Requirements for I~CO Mark

4.5.1 General Requirements

4.5.1.1 The product shall conform 10 the requirements of quality prescribedunder clauses 4.1 104.4.

4.5.1.2 The manufacturcrs shaII produce to BIS environmental consentclearance from the concerned Slate Pollution Control Board as per the norms laiddown under the \VlIlt'r ( Prevention lind Control of Pollution) Act, 1974;Air ( Prevention lind Control of Pollution ) Act, 1981; and Waler ( Preventionand Control of Polllltion) Cess Act, 1977 respectively, along with theauthorization, if required under the Environment ( Protection) Act, 1986, whileapplying for ECO Mark.

4•.5.2 SIJccific Requirements

Amend No.3 to IS 75 : 1973

4.5.2.1 The product shall not contain aflatoxin, more tban 5 mg/kg, when testedby the method prescribed in Appendix A.

4.5.2.2 The pesticide residues, if any, shall not exceed tbe tolerance llnuts asprescribed in the Prevention of Food Adulteration Act, 1954 and Rules madethereunder.

4.5.2.3 Only permitted antioxidants not exceeding the quantities specifiedagainst each as prescribed under the Prevention of Food Adulteration Act, 1954and Rules made thereunder, shall be used, if required.

4.5.2.4 The product shall not contain any of tbe toxic metals in excess of thequantities prescribed in Table 2.

TABLE 2 LIl\1ITS I'"()R TllXIC l\tliALS

Sl.No. CllARAC'J'ERIS'nC RfQl1lREM l:NT

i) Lead,mg/kg. Max 5.0

ii) Arsenic, mg/kg. Max 0.5

iii) Cadmium. mglkg. McIX 1.0

iv) Mercury(total) 0.25mg/kg, Max

MEntOO OF TEsT, REF ro

15 of IS 1699 : 1995·

do

do

do

• Methods of sampling and lest for food colours ( second revision ).

(Page 5, clause S.I ) - Add the following clause S.I.1 after clause 5.1:

'S.l~1 For ECO Mark the product shall be packed in such packages which aremade from recyclable ( that is which can be re-processed to mauufacture anyuseful product ) or biodegradable materials.'

(Page 5, clause 6.% ) - Add the following clause 6.3 after clause 6.2:

"6.3 For ECO Mark the containers shall be marked with the followinginfonnation:

a) List of identified critical ingredients in descending order of quantity,percent by mass, which shall include 'made from pure linseed oil';

b) The brief criteria for which the product has been labelled for ECO Mark;and

e) Shelf life of the product."

2

v x m

Amend No.3 to IS 75 : 1973

(Page 6, Table 1 ) - Add the following Appendix after Table 1:

'APPENDIX A(Clause 4.5.2.1 )

DETERMINATION OF AFLATOXIN

A-I REAGENTS

A-I.I Acetone, 70 Percent - 700 ml acetone in 300 ml distilled water.

A-t.2 Acetone, 20 Percent - 200 ml acetone in 800 ml distilled water.

A-l.3 Lead Acetate, 20 Percent - 200 g neutral acetate in distilled water and3 ml glacial acetic acid, diluted to one litre.

A-Z PROCEIlURE

A-Z.l Dissolve 30 g sample in 100 ml hexane.

A-Z.Z Extract with 3 x 50 ml 70 percent acetone.

A-Z.3 To the extract add 60 ml distilled water and 20 ml lcad acetate.

A-Z.4 Boil to reduce volume to 150 ml. Cool to about 20°C.

A-Z.5 Filter and wash with 20 percent acetone.

A-2.6 Extract filtrate and washings with 3 x 50 ml chloroform,

A-Z.7 Pass chloroform layer through anhydrous sodium sulphate.

A-2.8 Concentrate to 50 ml and spot on TLC plate.

A-) (:AIJClJLAl·I()N

. V x s )( 1 000Aflatoxin, rug/kg ::

where

v = VOIUIIlC of extract in ml,

v =volume of extract giving minimum observable fluorescence in ~1I,

m =mass of sample in g, and

s = standard toxin giving minimum observable fluorescence in ug.'

(FAD 44)ReprographyUnit, HIS. NewDelhi, ladi.·

3

AMENDMENT NO. 4 MARCH 2002TO

IS 7S: 1973 SPECIFICATION FOR LINSEED OII.J,RAW AND REFINED

( Second Revision)

( Amendment No.3. page 2. clause 4.5.2.1 ) - Substitute '5 Jl g/kg' for'5 mglkg t.

(FAD 44 )Reprosraphy Unit. BIS,·New Delhi....lndia

IS: 75-1973

Indian StandardSPECIFICATION FOR

LINSEED OIL, RAW AND REFINED

(Second Revision)

o. FOR E \\' a R D

0.1 This Indian Standard (Second Revision) was adopted by theIndian Standards Institution on 17 August 1973, after the draft finalizedby the Oils and Oilseeds Sectional Committee had been approved by theChemical Division Council and the Ag-ricultural and Food Products])ivision Council.

0.2 Linseed oil is used in th» ruanufact ure of varnishes, paints, putty, oilcloth, facrice, linoleum, printing inks, artificial rubber, tracing cloth, andpatent leather. It is applied to paper and fahrics to render them water­proof and tough. Certain grades of the oil are also used fill" edihle andpharrnaccuticnl purposes.

0.3 This standard was first published in 1950 and then revised in 1967 byamalgamating lS:76-1950·, IS:55B-1954t and IS:3·174-1966~. In thesecond revision the Iirnit for iodine value is being changed from 175 Min to170 Min in view of the data available and the experience gained. Thischange brings this requirement in line with the provisions of thePrevention of Food Adulterat ion Act, 1952 of the Government of India.

0.4 The pharrnaccurical grade of linseed oil is covered in Pharmacopoeiaof India ('The Indian Pharrnacopoeia ). The Raw Grade 2, specifiedin this standard, corresponds to this grade. The boiled and pale-boiledtypes of linseed oils are covorr-d in IS: i7-1 ~68§.

0.5 For the purpose of deriding whether a particular requirement ofthis standard is complied with, the final value, observed or calculatedexpressing the result of a test or analysis, shall be rounded off inaccordance with IS: 2-1 ~160!l. The numbe-r of significant places retainedin the rounded off value should he the same as that of the specifiedvalue in this standard. '

.Specifil·ation for linseed oil, refined, for paints.tSpecifl(:ation for linseed oil, pharmaceutira l.:Spccif1ciltion for solvent-extracted linseed oil.§5pecHiration for linseed oil, boiled, for paints CIi"Ht ltl'iH'IJ11 ).

Yltul~s for rounding olf numerical values ("("'ud).

3

1&175-1973

1. SCOPE

1.1 This standard prescribes requirements and methods or- sampling andtest for linseed oil.

2. TERMINOLOGY

2.1 For the purpose of this standard, the definitions given in 2 ofIS: 548-1964* and also those given below shall apply.

2.1.1 Alkali-Rejintd or Semirefined Linseed Oil - Linseed oil whichhas been refined by neutralization with alkali and bleached with bleachingearth or activated carbon or both, no other chemical agents being used.The oil may also be treated with mineral acid prior to alkali-refining.

2.1.2 Add-Refined Linseed Oil- Linseed oil which has been refinedusing mineral acid and bleached with bleaching earth Of activatedcarbon or both.

3. TYPES AND GRADES

3.1 The material shall be of .'VQ types, naTnel~, expressed and solvent­extracted, wi th grades as givP1\ below:

a) Expressed:1) Alkali refined,2) Acid refined,:~) Raw Grade 1.. and4) Raw Grade. 2.

b) SolfJiTlt-l~xtTa(tcd:

1) Scmircfined, and2) Ra\v.

3.1.1 Of these, alkali-refined grade and Raw Grade 1 of the expressedtype are suitable for edible usc.

NOTE - Although the alkali-refinod and the scmirefinerl grades are equivalent,the latter is not considered suitable fur direct edihh' consumption.

4. REqUIREMENTS

4.1 Description - The material shall be obtained from good qualitylinseed cake by solvent-extraction, or from clean and sound linseeds fromLinum flSitatissimum Linn., fame I ..inaceae, either by process of expression ot"solvent E'xtraction. .

4.1.1 Solvent-extracted linseed oil shall be produced by using solventhexane confortning to IS: 3470-196fi t .

• Methods of sampling anti test for oils and fatl ( ",:i.Jed).tSpeciftcation for hexane, food grade.

4

IS:7S-1f7!

4.2 The material shall be clear and free from rancidity, adulterants,sediment, suspended and other foreign matter, separated water andadded colouring and flavouring substances.

4.2.1 The clarity of the material shall be judged by the absence ofturbidity after keeping the filtered sample at 30°C for 24 hours.4.3 AdiDbt...e with Other Oil. - The material shall be free fromadmixture with other oils, when tested according to the methodsprescribed in 20 of IS: 548-1964*.".4 The material shall also comply with the requirements given inTable 1.

5. PACKING5.1 The material shall be supplied in suitable well-closed containers, asagreed to between the purchaser and the supplier.

6. MARKING6.1 The containers shall be marked with the following:

a) Name including the type and grade of material;b) Mass of the material in the container;c) Manufacturer's name and trade-mark, if any;d) Batch number; ande) Year of manufacture.

6.2 In the case of nonedible grades (see 3.1.1), the containers shall alsobe suitably marked 'FOR INDUSTRIAL NONEDI 81"E USES ONLv,(either printed on the label affixed to the container or lithographed orstencilled thereon with indelible ink) in a type size of not less than50 mm.7. SAMPLING7.1 Representative samples of the material shall be drawn ac; prescribedin 3 of IS : 548·1964* .

,. TEST METHODS8.1 Tests shall be carried out as prescribed in the relevant clauses of thestandards specified in col 9 of Table I.8.2 Q,aallty of RealeDts- Unless specified otherwise, pure chemicalsand distilled water. (ste IS : I070.1960t ) shall be used in tests.

NOTE -' Pure chemicals t shall mean chemicals that do not conta in impuritieswhich affect the results of analysis. .

9. 'CRlTERIA FOR CONFORMITY1.1 A lot shall be declared &41 conforming to this standard, if the testresults of thee omposite test sample satisfy the requirements prescribed in 4.

• Methods of aampling and tesl for oils and fats (rtl1iJtJ).t8pecification for water, distilled quality {"L,jstd }.

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