AP42 chapter 9 reference...4500 Ball Road N.E. Circle Pines, Minnesota 55014-1819 TEL: (612) 766-6020 FAX: (612; 786-7854 RESULTS OF THE NOVEMBER 9 - 11, 1993 AIR EMISSION TESTING

Y 4P42 Section:

3ackground Chapter qeference:

M e :

~

9.1 0.1.2

4 20

Results of the November 9-1 1, 1993, Air Emission Testing of Process Sources at the American Crystal-Sugar East Grand Forks Plant, Interpoll Laboratories, Inc., Circle Pines, MN,

December 3, 1993..

EPA

Text Box

Note: This is a reference cited in AP 42, Compilation of Air Pollutant Emission Factors, Volume I Stationary Point and Area Sources. AP42 is located on the EPA web site at www.epa.gov/ttn/chief/ap42/ The file name refers to the reference number, the AP42 chapter and section. The file name "ref02_c01s02.pdf" would mean the reference is from AP42 chapter 1 section 2. The reference may be from a previous version of the section and no longer cited. The primary source should always be checked.

APPENDIX s

REPORT EXCERPTS FROM REFERENCE 20

(American Crystal Sugar Company, December 3, 1993)

\

i

... I II I

.I1 1

Report Number 3-1636 December 3, 1993 SP/slp

Interpoll Laboratories, Inc. 4500 Ball Road N.E.

Circle Pines, Minnesota 55014-1819

TEL: (612) 766-6020 FAX: (612; 786-7854

RESULTS OF THE NOVEMBER 9 - 11, 1993 AIR EMISSION TESTING OF PROCESS SOURCES

AT THE AMERICAN CRYSTAL SUGAR EAST GRAND FORKS PLANT

Submitted to:

AMERICAN. CRYSTAL SUGAR COMPANY Business Highway 220

P.O. Box 357 East Grand Forks, Minnesota 56721

Attention:

Bruce Keifenheim

Approved by:

. a+- Daniel De en .-;.';'I bianager

\ .? : Stationary Source Testing Department

I \

i

I

I I

. j . . 1

1

1 I

II

I I

I I

1 I

...

.I

1 INTRODUCTION

in East Grand Forks, Minnesota:

2 "E" Pellet Cooler S 6

7

Pellet Loadout Stack 8

st. Coordination between testing activities

determinations of the gas

rnple withdrawal. An

in the above-cited

the large irnpinger version of EPA Method 6.

1

:: 1

- m Y VI

a L

w v o m r - m 3 0 0- - L - w L E .

w o m r VI

m q m n o

m o (Y m s

m - 4 - K

- x -2% - 0 - L U X a l c n L a 0 E L L w ( u =. au O L K

m w

z o m

m a K o -

m .-(

w

R

I-

F

m

m 0, I 4 rl I 4 - m 0, I - - I 4 4

m

I m 4 .-I I 4 4

o VI w o e 0

W 4J m 0

U m m 4 x 0 m N 4

m 0 N 4 . 0 0 .4 .-I

l. m 0 4 x 0 m m

I

cn a X - W K 0 U

0 L W 3 VI C 3 L

w E I- .r

r - m o u m o - U m N

m

N - W

m m m

r P

5 000 m m m w m m . . .

- 4 -

m w m w o 0 0 000 4 -01 .-t N m m m . N O YI l.0 N . . . 4

m a , 0 0 0 0 0 - m o m a - 4 w w , w m . N m U

u m . LOW N . . . . m w m m o 00 a, O N 4

UlN U 4l. 4 . . .-(

L

0

N 0 4

r - m U U ml. 0 0 . .

m m

m 4

- IL I U W 0 -

0) L 3 o

L (u a E W 4.2

vl

m

m U

> x > A. -

o K 0 *-' K 0 0

al L 3 o VI 7

0 z

7

- a L U

> x w > U

VI

m U

K 0 - o m

L

5 m

0 c o 0 C

Y 0 VI H

-

-- ILL v u

o x o - a x

K ~ W

o u a m - u I - * K e w o - a K L o - m o m u

w o r n

m m v l

3 c o 0 0

r 3 0

o L

- m a

S C m

0 L 0 VI

VI +

0 ,-

7

E 2 n w

.. o L a,

Y 0 m

a z

W

x -0 c W a a 4

.C

W W v)

I

' S 0 Y .r

m E 0 'c S - W U

p: m

L 0 LL

OXIDES OF NITROGEN COMPLIANCE STNUS \

1 No. 1 Boiler

2 No. 2 Boiler

c i e

6

7

m

a c VI

L w v c m~ - m 3 0 0 - - L c w L E . m a m n e

rnw w m r

m -

w o m r VI

K

- r 4 Y " 0 -

m u I L e x w m L 1 1 0 E LLL w w > a u

,I O L C

o : c m 0 0

w o r u - l e -

W L I e c c o m

d rl

W

11 7

m c

1

0

I m - 4

I 4 4

m

I 4 4 I 4 4

m

m

I 4 4 I 4 4

m

U YI

W c v- 0

W c

0 m

0 m m 4 . 0 m N 4

m 0 N 4 . 0 0 4 4

r- m 0 4 . 0 m 01

m E x - W K 0 U

W L W 3

YI K 3 L

W E

c 7

r - m m w 0 0 0 0 o m N 0 0 4 m % m e . N m 4 m 0 N . . . . N m w . - - m w m m o 00 u YIN m -i- - . . 4

w o 0 0 0 0 0 4 m u m r-al 4 N m m m . m m o i-0 N . . . . 4 NU) * 4 u m m m N 0 0 0 m YIN m d m 4 . . 4

m m u o 0 0 0 4 O b m m - rl w w w o m . r-N 0 m w N . . . . m m m . O N 4 ' w m m 0 0 0 w m N 0 A i - - . . 4

W

x

m e V I W W E 0 3 0 - I O

m L

e In m U

- > > . x -

e (3 W c 8 0 0

W L 3 * VI

- > L U .

- x 0

U K 8 W o s ~ m - r o w 0 u n m c 7 L w,* VI m x - o v o c n E 0 0

VI

7

m . U

C 0 -

* W C

1 0 Ln H

.,-

-- LLU v u

0.0 . - D : . c o o : L - r Y K

am

m -u

W v u S L 0- m v m u w - m 3 c

c u c m a - - e L m n

.r -0 S W n c 4

D: W aJ v1 I:

- .

8

1 I

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.: ,.., 1 :. 1 1

I.. 7 _1

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. .

..

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0 0 0 w m - m m N L o . N m w m i - m m 0 0 0

N P- - m m m m w N . . . . 0) u m r(

r-u N - r - . . m m .

N

m

I 0

I

m

-I

r(

rl

m m I 0

I r(

4

4

m I 0 .+ I

m

-I 4

e m W u

r 0

W 42 m 0

4

Lo m 4 . 0 Lo m 4

N m m 4 \

m 4 -4

0

W 0 rl 4 . m 0 m

- v) (L

I - W C 0 U

W L W 3

m s 3 L

W E

+ c

- m u YI

L w v u m c - m s 0 0.- .-L u w L E .

w o m c m

m q m n o

m u w m c - o c

m - - x

O X

O m N

N m 4 N

0 0 0 o m m

m8-m . . . 4 h

0 m u W N

w m w m 0 0 . .

m m a a m

0 0 0 m N O

3 . .

m a m N

N U .+I. m w w w

I

l

a Li

' I - C

m O N

0 m 0 0 0

U r l L o m Lo

a 4

. . m N

W

x U c? .- e m

m m c O I W

o - r - w s x u m u w w o

0 0 w o T o 2 u w

w u el- c O m

C F * o n I- m m L E m m E - 0) S E X m w v )

m c m

~

aJ a x 2

, " - 0 o W

W LL I U W 0 -

5, L U

> \ w > V - 7

. a I . 2 m

L L L 0 0

-0 a m

01 44 m L

C 0 .- In m .r

E W

+ L m n

.. 0 -

U 3 L o - m

- m u w L 3 C u urn m o v u L r m l n

L w u m w W E 0 3 0 7 '

L O a > *

u w m o u - 8 L

u c W

u c C W o c c m - o w 0 crn m L c L > u

m x - 0 0 0 s Q E 0 u

W L 3 u m L W

E W

a

L 0 - m m o m u 2. s s

w u m 0 u 0 + - m m w

4 C 0 0

m N

W

n - m I-

)

W L 3 u VI

w z s o X U O L m m u n

VI m U

0 r

9

Table 9. Summary of the Results of the November 9 - 11, 1993 Sulfur Dioxide Emission

Compliance Tests at the American Crystal Sugar Plant in East Grand Forks,

Minnesota.

Concentration Emission Rate

Date Time (DDm,d (LBIH R)

(A -.Pulp Dryer Stack)

11-1 1-93 0930-1037 21 4.73

11-1 1-93 1100-1208 16 3.92

1 1-1 1-93 1230-1 334 16 3.91

Average 18 4.19

(B - Pulp Dryer Stack)

11-10-93 0905-1 106 ' 18 7.76

11-10-93 1130-1332 16 7.32

11-10-93 1350-1551 14 5.99

Average 16 7.02

(C - Pulp Dryer Stack)

11-09-93 1030-1235 19 4.80

1 1-09-93 1315-1 51 7 12 3.08

11-09-93 1535-1738 25 5.87

Average 19 4.58

J 23

I I

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I .I1 '1 1 3

. . 1 1 '1 . I a 3 1.

... I 1

I I

-1

- m e VI 5, .L

w v e m r - a 3 v 0- 7 L urn L E . m < m n e

m e w m s

a -

w o m r m

- 4 - c - I -1 d V - L e x w m L n o E e u w 3 > 0 - 0 o u s. z m m

O L w 2 0 8 e w e

W V I

0 - w W

4 4 . - - w 38-0 m e w w e

0 0 w o z e d e m

w U ' "I- c o m c -

m m

L - m

V I ~ S

a c m

h o n L -

E w m E - 0, 3 E 3 m w v )

2- m

m m L

w

R

t-

7

m

/

d

I , d d

m

I 4 4 I d 4

m

m

I m d d

I rl r(

v)

W e

" 0

W e m n

rl N I- d x 0 N W 4

m U VI r(

x VI w

d

cn IY I - W 8 0 U

w L W 3

VI C 3 L

W E

I- 7

\: N m

4 0 m w

0

V I 0 ml.

0

- -/

/ L

- m 3

m

*

m o p 1 o m 0 o o m . . . NP.

m o r . orno o o m . . . NPI

m o l - o m 0

e S W e. S 0 V

w L 3 +I VI 7

0 x

0

0 0 rl

0

0 0 d

. . . o o m

NP.

=-# L. U . > \ w > u I - - x

0

u s S (u o s s m - o w 0 e n m L - L =-#+I

VI m x - O V O S Q E 0 0

m

-

m 0

3 0 w

0 0 . .

I

0 t . .

m m o m m I- 4 4 o 0 0 . 0 0 0 . .

\ ILL a 0 0 r

c a m x o x o m - IYx -I eCIa -

U m

m L

5

0 e o w e VI

VI

e - w 3 s o

1 4 4 e O L L

- 7

m m m

W

x U c a, Q c <

.r

*

22

W W v)

Table 10. Summary of the Results of the November 9 - 11, 1993 Oxides of Nitrogen

Emission Compliance Tests at the American Ctystal Sugar Plant in East Grand

Forks, Minnesota.

I

I

7

... 1 1 I


Date Time (o0m.d) [LB/HR) (A - Pulp Dryer Stack)

11-11-93 0930-1037 95 15.3

11-11-93 1100-1208 99 17.2

11-1 1-93 1230-1334 100 17.2

Average 98 16.6


11-10-93 0905-1 106 69 21.3

11-10-93 1130-1332 67 21.5

11-10-93 1350-1551 66 20.8

Average 67 21.2


11-09-93 1030-1 235 97 17.2

11-09-93 1315-1517 98 17.8

11-09-93 1535-1 738 90 15.1

Average 95 16.7

(No. 1 Boiler Stack)

11-10-93 0810-0917 284 186

11-10-93 0948-1053 273 179

1 1-1 0-93 1 1 15-1 220 2 78 179

Average 278 181


11-1 1-93 0830-0947 3 19 186

11-11-93 1011-1124 335 200

11-1 1-93 1146-1257 329 192

Average 328 193

I

1 'i

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I

- 1

I , '1 I I

.I ?

I I - . I I 3 1 ,,

I ... I 1

I I

..

:)

Table 11. Summary of the Results of the November 9 - 11, 1993 Total Hydrocarbon

Emission Compliance Tests at the American Crystal Sugar Plant in East Grand

Forks, Minnesota.

. . Concentration Emission Rate

Date Time (oDrnC,w) (LBIHR)

(A - Pulp Dryer Stack)

310 22.4

264 19.6

11-1 1-93 0930-1037

11-1 1-93 1100-1208

11-1 1-93 1230-1334 246 18.1

2 73 20.0 Average


106 11.2 11-10-93 0905-1 106

11-10-93 1130-1332

11-10-93 1350-1551 72 7.70

65 6.80

Average 01 8.57


123 8.61

177 12.2

172 12.0

11-09-93 1030-1235

1 1-09-93 1315-1 51 7

1 1-09-93 1535-1 738

157 10.9 Average

25

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I "1

I I ,

'- . . 1 I I

::\

.. 1 ..I 1 3 ;,3 1 3 ,.

I ;J

1

...

)

1

Table 12. Summary of the Results of the November 9 - 11, 1993 Carbon Monoxide

Emission Compliance Tests at the American Crystal Sugar Plant in East Grand

Forks, Minnesota.


Date Time (DDm,d) (LBIHR)

11-1 1-93 0930-1037 540 ' 53.3

11-11-93 1100-1208 500 52.5

11-1 1-93 1230-1334 450 47.2

Average 497 51.0

(A - Pulp Dryer Stack)


11-10-93 0905-1 106 750 142

11-10-93 1130-1332 830 162

11-10-93 1350-1551 590 112

Average 723 139


11-09-93 1030-1235 240 26.0

11-09-93 1315-1517 260 28.8

1 1-09-93 1535-1 738 290 29.7

Average 263 28.2


11-10-93 0810-091 7 319 128

11-10-93 0948-1053 336 134

1 1-1 0-93 1 1 15-1 220 330 130

Average 328 131


11-1 1-93 0830-0947 580 206

11-1 1-93 1011-1124 535 194

11-1 1-93 1146-1257 3 75 134

Average 497 178

26

..:I i ... 1 1 - ' 'I . . I

1

I

Table 13. Summary of the Flow Rate Determinations performed in

November 9 - 11, 1993 Tests at the American Crystal

Plant.

\

(Test 1 - C Hopper

nest 5 - B Recycle Duct)

11-10-93

11-10-93

11-10-93

11-10-93

1 27

I n t e r p o l 1 L a b s R e p o r t No. 3 -1636 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s , ! l i n n e s o t a

T e s t No. 9 A - P u l p D r y e r S t a c k

R e s u l t s o f P a r t i c u l a t e L o a d i n g D e t e r m i n a t i o n s - - - - - - - M e t h o d 5

D a t e o f run

T i m e r u n s t a r t / e n d . . . . . ( H R S )

S t a t i c p r e s s u r e . . . . . . ( I N . W C ) C r o s s s e c t i o n a l a r e a ( S Q . F T ) P i t o t t u b e c o e f f i c i e n t . . . . . . W a t e r i n s a m p l e g a s

c o n d e n s e r . . . . . . . . . . i m p i n g e r s . . . . . . . . . . d e s i c c a n t . . . . . . . . . . t o t a l . . . . . . . . . . . . . .

T o t a l p a r t i c u l a t e m a t . . . . . . . . . . c o l l e c t e d

Gas m e t e r c o e f f i c i e n t B a r o m e t r i c p r e s s u r e . . A v g . o r i f . p r e s . d r o p . . A v g . g a s m e t e r t e m p . .

V o l u m e t h r o u g h g a s me

. . (ML) G R A M S ) GRAMS) G R A M S )

r i a l . . g r a m s )

. . . . . . I N . H G ) IN.WC) DEF-F)

e r . . . . a t m e t e r c o n d i t i o n s . . . ( CF) s t a n d a r d c o n d i t i o n s . ( D S C F )

T o t a l s a m p l i n g t i m e . . . N o z z l e d i a m e t e r . . . . . . . A v g . s t a c k g a s t e m p . . V o l u m e t r i c f l o w r a t e .

a c t u a l . . . . . . . . . . . . . . d r y s t a n d a r d . . . . . . .

I s o k i n e t i c v a r i a t i o n .

. ( M I N 1 . . ( I N ] D E G - F )

. . . . . . (ACFM) DSCFM)

. . . ( * )

P a r t i c u l a t e c o n c e n t r a t i o n . . . a c t u a l . . . . . . . . . . . . (GR/ACF) d r y s t a n d a r d . . . . . (GR/DSCF)

P a r t i c l e mass r a t e . . . ( L B / H R )

Run 1 11-11-93

9 3 0 / 1 0 3 7

- 0 . 7 0 1 2 . 0 5

. a 4 0

0 . 0 6 1 7 . 0

1 7 . 0 6 3 4 . 0

0 . 2 5 8 5

0 . 9 9 8 5 2 9 . 3 0

1 . 7 8 7 7 . 2

4 3 . 4 9 4 1 . 9 7

60.00 . 2 5 5 214

5 0 5 8 5 2 2 6 1 8

1 0 5 . 1

0 . 0 4 2 4 8 0 . 0 9 5 0 4

1 8 . 4 2 6

Run 2 11-1.1 - 9 3

1 1 0 0 / 1 2 0 8

- 0 . 7 0 1 2 . 0 5

. 8 4 0

0 . 0 5 7 5 . 0

1 3 . 0 5 8 8 . 0

0 . 1 9 6 8

0 . 9 9 7 5 2 9 . 3 0

1 . 7 4 7 8 . 8

4 4 . 7 4 4 3 . 0 0

6 0 . 0 0 . 2 5 5 214

5 1 7 7 6 2 4 0 9 0

101.1

0 . 0 3 2 8 5 0 . 0 7 0 6 2

1 4 . 5 8 3

Run 3 11-11-93

1 2 3 0 / 1 3 3 4

- 0 . 7 0 1 2 . 0 5

.E40

0 . 0 5 7 4 . 0

1 2 . 0 5 8 6 . 0

0 . 2 0 8 9

0 . 9 9 7 5 2 9 . 3 0

1 . 7 2 7 8 . 2

4 4 . 9 9 4 3 . 2 8

60.00 . 2 5 5 2 1 5

5 1 5 0 7 2 4 0 4 3

1 0 2 . 0

0 . 0 3 4 7 5 0 . 0 7 4 4 7

1 5 . 3 4 7

55 1

I I I I

I n t e r p o l 1 L a b s R e p o r t No. 3-1636 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s , M i n n e s o t a

8 - P u l p D r y e r S t a c k T e s t ?

P a r t i c u l a t e L o a d i n g

. . . . . . . . . . . ( IN .WC) -0.98

C r o s s a r e a ( S Q . F T ) 18.99 . . . . . . .840

c o n d e n s e r . . . . . . . . . . . ( M L ) i m p i n g e r s . . . . . . . . (GRAMS) d e s i c c a n t . . . . . t o t a l . . . . . . . . .

T o t a l p a r t i c u l a t e . . . . . . . . . . c o l l e c

B a r o m e t r i c p r e s s u r e . . Awg. o r i f . p r e s . d r o p . . A v g . g a s m e t e r t e m p . .

Vo lume t h r o u g h g a

s t a n d a r d c o n

N o z z l e d i a

f l o w r a t e . . . . . . . . . . . . . . . . . . . . . (ACFM) n d a r d . . . . . . . (DSCFM)

.840

0.0 334.0 11.0

345.0

0.2343

0.9975 29.55 0.79 85.0

60.62 57.95

120.00 .198 234

76312 44674

96.0

. . . . . . . . . . . . . . . 03651

. . . . . . . .

P a r t c u l a t e c o n c e n t r a t i o n a t u a l (GR/ACF) 0.02827

P a t i c l e mass r a t e ( L B / H R ) 18.526

d Y s t a n d a r d ( G R / D S C F ) 0.04982 i

Run 3 11-10-93

1350 / 155 1

-0.98 18.99 .e40

0.0 336.0 15.0

351.0

0.2098

0.9975 29.55 0.80 80.0

60.91 58.77

120.00 .198 232

74513 43695

99.6

0.03229 0.05509

20.631

53

I n t e r p o l 1 R e p o r t No. 3-1636 A m e r i c a n C r y s t a l S u g a r


T e s t N o . 9 A - P u l p D r y e r S t a c k

R e s u l t s o f S u l f u r D i o x i d e D e t e r m i n a t i o n s - - - - - - - - - - - - M e t h o d 6

Run 1 Run 2 Run 3

D a t e o f r u n 11-11-93 11-11-93 11-11-93

T i m e run s t a r t / e n d . . . . . (HRS) 0930-1037 1100-1208 1230-1334

B a r o m e t r i c p r e s s u r e . . (IN.HG) 29.30 29.30 29.30

M e t e r t e m p e r a t u r e . . . . ( D E G - F ) 77.20 78.80 78.20

M e t e r c o r r e c t i o n c o e f f i c i e n t 0.9985 0.9975 0.9975

Vo lume t h r o u g h g a s m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) 43.490 44.740 44.990

T o t a l s a m p l i n g t i m e . . . . ( M I N ) 60.0 60.0 60.0

s t a n d a r d c o n d i t i o n s . . ( S C F ) 41.967 42.997 43.283

M o i s t u r e c o n t e n t . . . . . .( % V / V ) 41.60 39.20 38.96

O x y g e n c o n t e n t . . . . ( % V / V D R Y ) 13.60 13.80 13.90

M i l l i e q u i v a l e n t s o f SO4 i n . . g a s s a m p l e . . . . . . . . . . . . . . . . 2.0700 1.6500 1.6600

S u l f u r d i o x i d e c o n c e n t r a t i o n

. . . . . . . . . . . . . . . . . 0.0190 (MG/DSCM) . . . . . . . . . . . . . . . . . 56 43 43 ( P P M - D R Y ) . . . . . . . . . . . . . . . . . 21 16 16 (PPM-WET) . . . . . . . . . . . . . . . . . 12 10 10

SO2 E m i s s i o n r a t e . . . . ( L B / H R ) 4.73 3.92 3.91

0.0190 (GR/DSCF) 0.0244

~

62 1

I n t e r p o l l R e p o r t N o . 3-1636 Amer ican C r y s t a l S u g a r

E a s t Grand F o r k s , b ! i n n e s o t a

T e s t N o . 5 8 - p u l p D r y e r S t a c k

R e s u l t s o f S u l f u r D i o x i d e

M e t e r c o r r e c t i o n c o e f f i c i e n t 0 . 9 9 7 5

Volume t h r o u g h g a s m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) 6 0 . 6 2 0 s t a n d a r d c o n d i t i o n s . . ( S C F ) 5 7 . 9 4 8

T o t a l s a m p l i n g t i m e . . . . ( HI

R u n 3

1 1 - 1 0 - 9 3

1350-1551

2 9 . 5 5

a o . oo

0 . 9 9 7 5

~ ~

6 0 . 9 1 0 5 8 . 7 6 6

1 2 0 . 0

2 1 . 9 1

1 7 . 2 0

1 . 9 0 0 0

0 , 0 1 9 1 0 . 0 1 6 0 4 4 3 1

. . . . . . . . . . . . . . 1 4 11

i a 16 '

7 . 1 6 7 . 3 2 * 5 . 9 9

\ (GR/DSCF) 0 . 0 2 0 9 (MG/DSCM) 4 a

(PPM-WET) 1 4 1 3

J

61

f

I n t e r p o l 1 L a b s R e p o r t No. 3 - 1 6 3 6 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d ? o r ! < $ , I.Iinne5o:i.


R e s u l t s o f O x i d e s o f N i t r o g e n (NOx) D e t e r m i n a t i o n s - - - - - - - - - M e t h o d 7

Run 1 A Run 1 0 R u n 1C Run 1 0

D a t e o f r u n . . . . . . . . . . . . . . . . 1 1 - 1 1 - 9 3 1 1 - 1 1 - 9 3 1 1 - 1 1 - 9 3 11-11-93 T i m e o f r u n . . . . . . . . . . . . (HRS) 9 3 0 9 4 5 1 0 0 0 1 0 1 5

Vo lume o f f l a s k . . . . . . . . . ( M L ) 2 0 6 0 2 0 4 8 2 0 4 5 2 0 6 7

D a t a : t i m e o f s a m p l i n g

F l a s k n u m b e r . . . . . . . . . . . . . . . . 1 3 1 4 1 5 1 6

f l a s k t e m p e r a t u r e . . (DEG-F) 40.00 , 4 0 . 0 0 3 8 . 0 0 3 7 . 0 0 b a r . p r e s s . . . . . . . . . (1N.HG) 2 9 . 3 0 2 9 . 3 0 2 9 . 3 0 2 9 . 3 0 f l a s k vacuum . . . . . . . ( I N . H G ) 2 7 . 6 5 2 7 . 6 0 2 7 . 6 5 2 7 . 6 0 f l a s k a b s . p r e s s . . . ( I N . H G ) 1 . 6 5 1 . 7 0 1 . 6 5 1 . 7 0

D a t a : T i m e o f F l a s k O p e n i n g

f l a s k t e m p e r a t u r e . . ( D E G - F ) 7 2 . 0 0 7 2 . 0 0 7 2 . 0 0 7 2 . 0 0 l a b . b a r . p r e s s . . . . ( 1 N . H G ) 2 9 . 1 6 2 9 . 1 6 2 9 . 1 6 2 9 . 1 6 f l a s k s t a t i c p r e s s . ( 1 N . H G ) - 0 . 4 0 0 . 2 0 - 0 . 2 0 -0.10 f l a s k a b s . p r e s s . . . ( 1 N . H G ) 2 8 . 7 6 2 9 . 3 6 2 8 . 9 6 2 9 . 0 6

Vo lume g a s s a m p l e d . . . . (DSML) 1 8 2 2 1 8 4 8 1 8 2 2 1 8 4 4

M o i s t u r e c o n t e n t . . . . . . ( f V / V ) 4 1 . 5 9 4 1 . 5 9 4 1 . 5 9 4 1 . 5 9 0xyge.n c o n t e n t . . . . ( f V / V . D R Y ) 1 3 . 6 0 1 3 . 6 0 1 3 . 6 0 1 3 . 6 0

N i t r a t e i n g a s s a m p l e . . . ( I G ) 4 4 3 . 0 4 6 0 . 0 4 4 1 . 0 4 4 5 . 0 NO2 i n g a s s a m p l e . ...... ( J G ) 3 2 8 . 7 3 4 1 . 3 3 2 7 . 2 3 3 0 . 2

NOx C o n c e n t r a t i o n

(GR/DSCF) . . . . . . . . . . . . . . . . . 0 . 0 7 8 8 0 . 0 8 0 7 0 . 0 7 8 5 0 . 0 7 8 2 ( M G / D S C M ) . . . . . . . . . . . . . . . . . 1 8 0 1 8 5 1 8 0 1 7 9 ( P P M - D R Y ) . . . . . . . . . . . . . . . . . 9 4 9 7 9 4 94 ( P P M - W E T ) . . . . . . . . . . . . . . . . . 5 5 5 6 5 5 5 5

NOX E m i s s i o n r a t e . . . . ( L B / H R ) 1 5 . 2 8 1 5 . 6 5 1 5 . 2 2 1 5 . 1 7

N O x e m i s s i o n f a c t o r . . . . . . . . . . . . . . . . . . . . . . . . . (LB /MMBTU)* 0 . 3 1 5 0 . 3 2 3 0 . 3 1 4 0 . 3 1 3

* F = 9 7 8 0 DSCF/MMBTU

... - 64

I n t c r p a l l L a b s R e p o r t No. 3 -1636 A m e r i c a n C r y s t a l S u g a r

Ea:: G r z n i ! Fork ; , ? i ; c n ? s o ~ ~


R e s u l t s o f O x i d e s o f N i t r o g e n (NOx) D e t e r m i n a t i o n s - - - - - - - - -

Run 2A Run 2 8 , Run 2C

D a t e o f r u n . . . . . . . . . . . . . . . . 1 1 - 1 1 - 9 3 1 1 - 1 1 - 9 3 1 1 - 1 1 - 9 3 T i m e o f r u n . . . . . . . . . . . . ( H R S ) 1 1 0 5 1 1 3 0 1 1 4 5

F l a s k n u m b e r . . . . . . . . . . . . . . . . 1 7 1 8 7 3 Vo lume o f f l a s k . . . . . . . . . ( M L ) 2 0 5 4 2 0 4 5 2 0 6 5


f l a s k t e m p e r a t u r e . . ( D E G - F ) 3 7 . 0 0 3 8 . 0 0 4 0 . 0 0 b a r . p r e s s . . . . . . . . . (1N.HG) 2 9 . 3 0 2 9 . 3 0 2 9 . 3 0 f l a s k v a c u u m . . . . . . . ( I N . H G ) 2 7 . 6 5 2 7 . 6 5 . 2 7 . 6 0 f l a s k a b s . p r e s s . . . ( 1 N . H G ) 1 . 6 5 1 . 6 5 1 . 7 0


f l a s k t e m p e r a t u r e . . ( D E G - F ) 7 2 . 0 0 7 2 . 0 0 7 2 . 0 0 l a b . b a r . p r e s s . . . . (1N.HG) 2 9 . 1 6 2 9 . 1 6 2 9 . 1 6 f l a s k s t a t i c p r e s s . ( I N . H G ) 0 .30 0.10 0.10 f l a s k a b s . p r e s s . . . ( 1 N . H G ) 2 9 . 4 6 2 9 . 2 6 2 9 . 2 6

Vo lume g a s s a m p l e d . . . . ( DSML) 1 8 6 3 1 8 4 2 1 8 5 7

M o i s t u r e c o n t e n t . . . . . . ( t V / V ) 3 9 . 2 0 3 9 . 2 0 3 9 . 2 0 O x y g e n c o n t e n t . . . . ( % V / V , D R Y ) 1 3 . 8 0 1 3 . 8 0 1 3 . 8 0

N i t r a t e i n g a s s a m p l e . . . ( J G ) 4 5 5 . 0 4 5 8 . 0 5 0 0 . 0 NO2 i n g a s s a m p l e . . . . . . . ( J G ) 3 3 7 . 6 3 3 9 . 8 3 7 1 . 0


. . . . . . . . . . . . . . . . . 0 . 0 8 7 3 (GR/DSCF) 0 . 0 7 9 2 0 . 0 8 0 6

. . . . . . . . . . . . . . . . . 1 0 4 (PPM-DRY) 9 5 9 6 (MG/DSCM) . . . . . . . . . . . . . . . . . 1 8 1 1 8 5 2 0 0

(PPM-WET) . . . . . . . . . . . . . . . . . 5 8 59 6 4

NOX E m i s s i o n r a t e . . . . ( L B / H R ) 1 6 . 3 5 1 6 . 6 5 1 8 . 0 3

NOx e m i s s i o n f a c t o r . . . . . . . . . . . . . . . . . . . . . . . . . (LB/MMBTU) ' 0 . 3 2 6 0 . 3 3 2 0 . 3 5 9

- M e t h o d 7

Run 2 0

1 1 - 1 1 - 9 3 1155

74 , 2 0 7 1

3 9 . 0 0 2 9 . 3 0 2 7 . 6 0

1 . 7 0

7 2 . 0 0 2 9 . 1 6 -0 .60 2 8 . 5 6

1 8 1 5

3 9 . 2 0 1 3 . 8 0

4 7 9 . 0 3 5 5 . 4

0 . 0 8 5 6 1 9 6 1 0 2

6 2

1 7 . 6 7

0 . 3 5 2

F = 9 7 8 0 DSCF/MMBTU

6 5

I n t ? r p , o l l L a b s R e p o r t No. 3 - 1 5 3 6 A m e r i c a n C r y s t a l S u g a r

Ea;' G r a n d F o r k ; , f . l i n n e s o t ;

T e s t N O . 9 A - P u l p D r y e r S t a c k


D a t e o f r u n . . . . . . . . . . . . . . . . T i m e o f r u n . . . . . . . . . . . . . ( H R S )

F l a s k n u m b e r . . . . . . . . . . . . . . . . V o l u m e o f f l a s k . . . . . . . . . ( M L )


f l a s k t e m p e r a t u r e . . ( D E G - F ) b a r . p r e s s . . . . . . . . . ( 1 N . H G ) f l a s k vacuum . . . . . . . (1N.HG) f l a s k a b s . p r e s s . . . ( I N . H G )

Da ta : T i m e o f F l a s k O p e n i n g

f l a s k t e m p e r a t u r e . . (DEG-F) l a b . b a r . p r e s s . . . . (1N.HG) f l a s k s t a t i c p r e s s . ( I N . H G ) f l a s k a b s . p r e s s . . . ( I N . H G )

V o l u m e g a s s a m p l e d . . . . (DSML)

M o i s t u r e c o n t e n t . . . . . . ( f V / V ) O x y g e n c o n t e n t . . . . ( % V / V . D R Y )

N i t r a t e i n g a s s a m p l e . . . ( J G ) NO2 i n g a s s a m p l e . . . . . . . ( J G )


( G R / D S C F ) . . . . . . . . . . . . . . . . . (MG/OSCH). . . . . . . . . . . . . . . . . (PPM-DRY) . . . . . . . . . . . . . . . . . (PPM-WET) . . . . . . . . . . . . . . . . .

NOX E m i s s i o n r a t e . . . . ( L B / H R )

NOx e m i s s i o n F a c t o r . . . . . . . . . . . . . . . . . . . . . . . . . (LB /MMBTU)*

Run 3 A

1 1 - 1 1 - 9 3 1 2 3 5

75 2 0 6 6

40.00 2 9 . 3 0 2 7 . 6 0

1 . 7 0

7 2 . 0 0 2 9 . 1 6

0 . 2 0 2 9 . 3 6

' 1 8 6 5

3 8 . 9 6 1 3 . 9 0

4 8 7 . 0 3 6 1 . 3

0 . 0 8 4 7 1 9 4 10 1

6 2

1 7 . 4 5

0.353

Run 3 8

1 1 - 1 1 - 9 3 1 2 5 5

7 6 2 0 9 3

4 0 . 0 0 2 9 . 3 0 2 7 . 6 0

1 . 7 0

7 2 . 0 0 2 9 . 1 6

1 . 5 0 3 0 . 6 6

1 9 7 8

3 8 . 9 6 1 3 . 9 0

4 8 9 . 0 3 6 2 . 8

0 . 0 8 0 1 1 8 3

9 6 5 9

1 6 . 5 2

0 . 3 3 4

Run 3 C

1 1 - 1 1 - 9 3 1 3 1 0

77 2 1 0 4

4 0 . 0 0 2 9 . 3 0 2 7 . 6 0

1 . 7 0

7 2 . 0 0 2 9 . 1 6

0 .40 2 9 . 5 6

1 9 1 3

3 8 . 9 6 1 3 . 9 0

4 9 9 . 0 3 7 0 . 2

0 . 0 8 4 6 1 9 4 101

62

1 7 . 4 3

0 . 3 5 3

Run 30

1 1 - 1 1 - 9 3 1 3 2 5

7 8 2 0 1 7

40.00 2 9 . 3 0 2 7 . 6 0

1 . 7 0

7 2 . 0 0 2 9 . 1 6

0 . 7 0 2 9 . 8 6

1 9 0 9

3 8 . 9 6 1 3 . 9 0

4 9 9 . 0 3 7 0 . 2

0 . 0 8 4 8 1 9 4 101

6 2

1 7 . 4 7

0 . 3 5 3

* F = 9 7 8 0 DSCF/MMBTU

P u l p D r y e r S t a c k

I n t e r p o l l Labs R e p o r t No. 3-1636 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s , b l i n n a s o t a

/ O x i d e s o f N i t r o g e n ( N O x ) D e t e r m i n a t i o n s - - - - - - - - - H hod 7 /”

f 1 a s k t e m p e r a t u r

f l a s k a b s . p r e s s . . .

D a t a : T i m e o f F l a s k Open

l a b . b a r . p r e s s . . . . ( I N . H G

f l a s k abs. p r e s s . . . (IN.HG f l a s k s t a t i c p r e s s . ( I N . H G

Volume g a s s a m p l e d . . . . ( D S M

H o i s t u r e c o n t e n t . . .. O x y g e n c o n t e n t . . . . ( %

N i t r a t e i n g a s NO2 i n g a s samp

. . . . . . . . . . . . . . . . .

. . . . . . . . . . . . . . . . .

s i o n r a t e . . . . ( L B I H R )

. . . . . . . . . . . .

R u n 1 D

11-10-93 1055

28 2031

40.00 29.55 21.10 ~

1.85

72.00 29.16 -0.30 28.86

1789

23.42 11.10

280.0 207.8

0.0508 116 61 4 7

18.87

0.390

\ ‘ F = 9780 DSCF/MMBTU


E a s t G r a n d F o r k s . M i n n e s o t a

T e s t N o . 0 A - P u l p D r y e r S t a c k

R e s u l t s o f CO D e t e r m i n a t i o n s ...................... M e t h o d 10

Run 1 Run 2 Run 3

D a t e o f r u n 11-11-93 11-11-93 11-11-93

T i m e r u n s t a r t / e n d . . . . . ( H R S ) 0930/1037 1100/1208 123011334

T o t a l s a m p l i n g t i m e . . . . ( M I N )

M o i s t u r e c o n t e n t . . . . . . ( % V / V )

0 2 C o n c e n t r a t i o n . . . . . . ( % V / V )

V o l u m e t r i c f l o w r a t e ( O S C F M )

C O c o n c e n t r a t i o n . . . . . . . . . . . . (GR/DSCF) . . . . . . . . . . . . . . . . . (MG/DSCM) . . . . . . . . . . . . . . . . . ( P P M - W E T ) . . . . . . . . . . . . . . . . ( P P M - D R Y ) . . . . . . . . . . . . . . . . ( P P M - D R Y @ 7% 0 2 . . . . . . . . .

CO e m i s s i o n r a t e . . . . ( L B / H R )

6 0 . 0

41.60

13.60

22618

0.2748 629.10 315.36 540.00 1021.

53.268

60.0

39.20

13.80

24090

0.2544 582.50 304.00 500.00 972.22

52.532

C O = C a r b o n m o n o x i d e

A t r a i l i n g ' < ' s y m b o l i n d i c a t e s t h a t t h e t r u e v a l u e i s l e s s t h a n o r e q u a l t o t h e r e p o r t e d v a l u e

60.0

38.96

13.90

24043

0.2290 524.25 274.68 450.00 887.32

41.187

I n t e r p o l 1 Labs R e p o r t No. 3-1636 Amer ican C r y s t a l S u g a r

E a s t Grand F o r k s , b l i n n e s o t a

-Method 10 D e t e r m i n a t i o n s ....................

I S t a c k

Time run . . . . . T o t a l s a m p l i n g t i m . . . . ( M I N )

M o i s t u r e c o n t e n t . . ( % V / V ) 21.92

V o l u m e t r i c

C O c o n c e n t

02 C o n c e n t r a t i o n . . . . . . 17.50

f l o w r a t e 43382 44674

a t i o n ( G R / D S C F 0.4223 ( M G / D SCM 966.95 ( P P M - W E T 640.06 ( P P M - D R Y ) 830 .OO

. . . . . . . . . 2692. 3320.

C O e m i s s i o n , & a t e . . . . . ( L B / H R ) 1 4 1 . 9 0 3 16\716

R u n 3

11-10-93

1 3 50 / 155 1

120.0

21.97

17.20

43695

0.3002 607.35 460.38 590.00 2173.

112.436


A t r a i l i n g ’ < ’ symbol i n d i c a t e s t h a t t h e t r u e v a l u e i s l e s s t h a n o r e q u a l t o t h e r e p o r t e d v a l u e

I n te rpo l1 L a b o r a t o r i e s (612) 796-5J20

EPFI M e t h o d 5 D a t a R e p o r t i n g S h e e t I m p i n g e r C a t c h f M i n n e s o t a P r o t o c o l

Job Acs Sourca A ? b u. brvw Team L e a d e r SCP T e s t 5 i t e S-k.4" D a t e S,bmit ted / / - l z - q 3 E a t e o f T e s t t t 7 \ - ~ 3

D a t e of A n a l y s i s I I -zq-9 'J T e s t No. cr NO. o f R u n s C o m p l e t e d 3

Techn i c i an c - NL\ cso-

Tes t - R u n 0 D i s h No. F i e l d B l a n k D i s h T a r e W t . 9 Log N u m b e r D i s h + S a m p l e W t . 9 Commen t s Sample W t . 9

T e s t X R u n I D i s h No. 6, I 4 Log Number / b 3 6 - 10 D i s h T a r e W t . S la ' f 73n 9 Comments D i s h c S a m p l e W t . 51. So67 9

S a m p l e W t . o.fJ33-l 9

T e s t L R u n F D i s h No. 6 2

Comments D i s h + S a m p l e W t . Sue < / U s z 9 Sample W t . 0 - O W L 9

T e s t R u n 3 D i s h No. d.5 Log N u m b e r - 107 D i s h T a r e W t . y q . b S 6 6 9 Comments D i sh+Samp l e W t . q Y . 6 7 3 4 9

Sample W t . 0 . 0 l 6 b 9

9 Log Number - D i s h T a r e W t . 5 0 . H S O

0

1

2

3

4

5

~

Test- R u n __ D i s h No. Log N u m b e r D i s h T a r e W t . 9 Comments D i sh+Sampl e W t - 9

Sample W t . 9 ~ ~

T e s t - R u n __ D i s h No.

Log Number D i s h T a r e W t . 9 Comment s D i s h + S a m p l e U t . 9

Sample W t . 9

R e s u l t s : F i e l d B l k . R u n 1 R u n 2 R u n 3 R u n 4 R u n 5

-

0 "'.:

Pellet Loadouf

/

0

1

2

5

4

5

- -

I n t e r p o l 1 L a b o r a t o r i e s (512) 786-tQ70

EPCI M e t h o d 5 D a t a R e p o r t i n g Sheet Probe/Cycl one Wash

Job A C S Source A - * 13 c o P r A v - Team Leader S L O T e s t S i t e S - k . b D a t e S u b m i t t e d / / - / z -q3 D a t e of T e s t LI-\\-93 T e s t No. C a t s of F n a l y s i s l \ ' ~ % c i ' I T e c h n i c i a n c~ ~ ~ - L \ ~ C S U -

9 No. of R u n s C o m p l e t e d 3

n l Sol- ient CL buJ. T r a n s p o r t Leakage f i 5 E 3 D -

T e s t - R u n G l s h No. F i e l d B l a n k D i = h T a r e U t . 9 Log N u m b e r D i s h + S a m p l e W t . 9 'Jol. o f S o l v e n t m l S a m p l e W t . 9 + S o l v e n t R e s i d u e k u g / m l

~~~ ~

T e s t 4 R u n 1 D i s h No. '-I6 Vol. of S o l v e n t a m l D i s h T a r e W t . %.q7 3 7 r3 Log N u m b e r lb7L - ,004 D i s h + S a m p l e W t . y f , r q 02 9 Coinmen t s S a m p l e U t . 0.0ib 9 9

I ~

T e s t 9 R u n 2 D i s h No. , 97 'dol. of S o l v e n t ) \ O m l D i s h T a r e W t . Vp.Yk5K 1 Lag N u m b e r c t ? D i sh+Sampl e W t s , r l E b 3 9 Comment s S a m p l e W t . 0.0 205 9

Interpol 1 Laboratories (612) 785-bQ2P)

EPA Method 5 Data Reporting Sheet Filter Gravimetrics

01 LO%"/

J o b p c s Source A - s,c, Or4 cr Team Leader Date Submitted I - 1 2 4 3 Date of Test 11- \\-'I 3 Test No. 9 No. o f Runs Completed 3 Date of Analysis I \ -ZY-q3 Technician ' ~ L \ , ~ J ~

,< L P Test Site s t a c "

"

0, f 5 U 0.17 I I

0

1

2

- 3

4

c J

Test Run P) Fi 1 ter No. Field Blank Fi 1 ter Type Log Number Fi 1 ter Tare Wt. 9 Comments Fi 1 ter+Sampl e Wt. 9

Sample Wt. 9

Test 9 Run \ Fi 1 ter No. LO lq Log Number / b 3 b - roof Fi 1 ter Type ql\ G c Commen t s Filter Tare Wt. ,&'aL7 9

FiltertSample Wt.J,OWl 9 Sample Wt. 0 . ?d Pf 9

Test 9 Run 2 Fi 1 ter No. 9999 Log Number - lo ( f Fi 1 ter Type q" c F Comments Filter Tare Wt. .&l@r 9

Fi 1 ter+Sampl e Wt . f. 0351 9 Sample Wt. 0,1566 9

Test 9 Run 3 Fi 1 ter No. ss 53 Log Number -\OL F Filter Type qb-b F

9 Comments Filter Tare Wt. .Q2kl Filter+Sample Wt. I.OY98 9 Sample Wt. 0.17l1 9

Test Run Fi lter No. Lag Number Filter Type Comments Fi 1 ter Tare Wt. 9

Fi 1 ter+Sampl e Wt . 9 Sample Wt. 9

Run Fi 1 ter No. Test Log Number Fi 1 ter Type Comments Fi 1 ter Tare Wt. 9

Fi 1 ter+Sampl e Wt - 9 Sample Wt. 9

I

I i I I I I 1

I 1 1 I I I I I I

i

Filename: BEET20,WQl Date: 31-Jan-95

Facility: American Crystal Sugar

Source: Coal-fired pulp dryer 'A (several other sources were tested, but process data are not provided for these sources)

Location: East Grand Forks, Minnesota

Test date: November 11. 1993

)

I

13 1

I 3

The oxides of nitrogen samples were collected during the particulate determinations

using an all-glass Method 7 sampling train. A heated stainless steel probe was used to

extract the samples from the exhaust stream. A plug of glass-wool was used in the end of

the probe to remove particulate material.

The NO, samples were collected in volumecalibrated two-liter all-glass flasks. An

aliquot of 25 cc of absorbing solution was added to each flask on-site; th,e flask was closed;

inserted into the sampling train; and evacuated. The probe was then purged and the sample

collected over a 15 second interval. The flask was then closed; the flask removed from the

sampling train; shook for two minutes and then secured for transport to the laboratory.

Upon arrival at the laboratory, the NO, samples are logged in, placed in a designated

area and maintained at 72 "F for 24 hours to allow completion of the conversion of NO to

NO, and absorption in the acidified peroxide reagent. The flasks are then shook to complete

absorption; attached to a mercury manometer and the static pressure and temperature

recorded. The samples are then recovered and analyzed by ion chromatography.

Total gaseous hydrocarbon concentrations were determined instrumentally using a

Ratfisch Model RS55 heated flame ionization detector (HFID) calibrated against propane in

air standards. was continuously monitored by extracting a

slipstream of exhaust gas by means of a heated probe and filter holder. A heat-traced teflon

line was used to transport the sample gas from the filter holder outlet to the analyzer inlet.

The THC concentration

An integrated flue gas sample was extracted simultaneously with each particulate

sample using a specially designed gas sampling system. Integrated flue gas samples were

collected in 44-liter Tedlar bags housed in a protective aluminum container. After sampling

was complete, the bags were sealed and returned to the laboratory for Orsat analysis. Prior

to sampling, the Tedlar bags are leak checked at 15 IN.HC. vacuum with an in-line

rotameter. Bags with any detectable inleakage are discarded. The integrated flue gas

samples on the A, B, and C Pulp Dryers and the No. 1 and 2 Boilers were also analyzed for

carbon monoxide in accordance with EPA Method 10 (NDIR).

Testing on the "A" Pulp Dryer Stack was conducted from 2 test ports oriented at 90

degrees on the stack. The test ports are located diameters 2 downstream and 5.5 diameters

L

!

!

I I 1 1

. I 1 3 i I 1 3 1 3 I '1 1

1

upstream of the nearest flow disturbances. A 24-point traverse was used to collect representative particulate samples. Each traverse point was sampled 2.5 minutes to give a

total sampling time of 60 minutes per run. Visible emission determinations were unable to

be performed due to converging plumes.

Tesiing on the "B" Pulp Dryer Stack was conducted from 2 test ports oriented at 90

degrees on the stack. The test ports are located 2 diameters downstream of a flow

straightener and 2 diameters upstream of the nearest flow disturbances. A 24-point traverse

was used to collect representative particulate samples. Each traverse point was sampled 2.5

minutes to give a total sampling time of 60 minutes per run. Visible emission determinations

were unable to be performed due to converging plumes.

Testing on the "C" Pulp Dryer Stack was conducted from 2 test ports oriented at 90

degrees on the stack. The test ports are located 2 diameters downstream and 2 diameters

upstream of the nearest flow disturbances. A 24-point traverse was used to collect

representative particulate samples. Each traverse point was sampled 2.5 minutes to give a

total sampling time of 60 minutes per run. Visible emission determinations were unable to

be performed due to converging plumes.

~

)

Testing on the No. 1 Boiler Stack was conducted from 4 test ports oriented at 90

degrees on the stack. The test ports are located 4.5 diameters downstream and 2.4 diameters


representative particulate samples. Each traverse point was sampled 2.5 minutes to give a

total sampling time of 60 minutes per run.

Testing on the No. 2 Boiler Stack was conducted from 4 test ports oriented at 90



representative particulate samples. Each traverse point was sampled 2.5 minutes to give a total sampling time of 60 minutes per run.

Testing on the "E" Pellet Cooler Stack was conducted from 2 test ports oriented at 90



3

I

I representative particulate samples. Each traverse point was sampled 5 minutes to give a total

sampling time of 60 minutes per run.

Testing on the "W" Pellet Cooler Stack was conducted from 2 test ports oriented at

90 degrees on the stack. The test ports are located 4.2 diameters downstream and 2.1

diameters upstream of the nearest flow disturbances. A 12-point traverse was used to collect

representative particulate samples. Each traverse point was sampled 5 minutes to give a total

sampling time of 60 minutes per run.

Testing on the Pellet Loadout Stack was conducted from 2 test ports oriented at 90 degrees on the stack. The test ports are located approximately 7.9 diameters downstream

and 2.3 diameters upstream of the nearest flow disturbances. A 16-point traverse was used

to collect representative particulate samples. Each traverse point was sampled 4 minutes to

give a total sampling time of 64 minutes per run,

The important results of the test are summarized in Section 2. Detailed results are

presented in Section 3. Field data and al l other supporting information are presented in the

appendices.

3 1

1

4

2 SUMMARY AND DISCUSSION

The results of the air emission tests are summarized in. Tables 1 - 13. The

compliance status of each source in each parameter is presented in the tables below.

PARTICULATE COMPLIANCE STATUS '

EMISSION PM PM

POINT SOURCE €mission Limit Emission Rate

Number NAME (LBIHR) (LBIHR)

3

4

5 , 1

2

6

7

a

"A" Pulp Dryer

"B" Pulp Dryer

"C" Pulp Dryer

No. 1 Boiler

No. 2 Boiler

"E" Pellet Cooler

" W Pellet Cooler

Pellet Loadout

15.94

17.94

14.62

14.6

14.6

.15.94

15.94

8.22

16.12

21.02

14.51

35.9

47.9

3.5

11.2

0.077

SULFUR DIOXIDE COMPLIANCE STATUS

EMISSION so2 so* POINT SOURCE Emission Limit Emission Rate Number NAME (LBIHR) (LBIHR)

3 " A Pulp Dryer 8.84 4.19

4 "6" Pulp Dryer 11.16 7.02

5 "C" Pulp Dryer 8.84 4.58

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T e s t N o . 1. C - P u l p D r y e

R e s u l t s o f Vo

I n t e r p o l l L a b s R e p o r t No. 3 - 1 6 3 6 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s , k l i n n e s a t a

S t a c k

u m e t r i c F l o w R a t e Determinat ion- - - - - - -Method 2

D a t e o f D e t e r m i n a t i o n . . . . . . . . . . . . 1 1 - 0 9 - 9 3

T i m e o f D e t e r m i n a t i o n . . . . . . . (HRS) 9 2 1

B a r o m e t r i c p r e s s u r e . . . . . . . (1N.HG) 2 9 . 5 1

P i t o t t u b e c o e f f i c i e n t . . . . . . . . . . . . 8 4

Number o f s a m p l i n g p o r t s . . . . . . . . . T o t a l n u m b e r o f p o i n t s . . . . . . . . . . . Shape o f d u c t .................... S t a c k d i a m e t e r . . . . . . . . . . . . . . . ( I N )

Duc t a r e a . . . . . . . . . . . . . . . . . ( S Q . F T )

D i r e c t i o n o f f l o w . . . . . . . . . . . . . . . .

S t a t i c p r e s s u r e . . . . . . . . . . . (1N.WC)

A v g . g a s t e m p . . . . . . . . . . . . . (DEG-F)

M o i s t u r e c o n t e n t . . . . . . . . . . ( 2 V / V )

A v g . l i n e a r v e l o c i t y . . . . . ( FT /SEC)

G a s d e n s i t y . . . . . . . . . . . . . . ( L B / A C F )

2

2 4

Round

4 8

1 2 . 5 7

UP

- 1 . 0 2

2 1 5

3 3 . 6 1

6 3 . 2

. 0 5 1 1 5

M o l e c u l a r w e i g h t . . . . . . (LB /LBMOLE) 2 9 . 4 4

Mass f l o w o f g a s . . . . . . . . . .

V o l u m e t r i c f l o w r a t e . . . . . . a c t u a l . . . . . . . . . . . . . . . . . . d r y s t a n d a r d . . . . . . . . . . . .

L B / H R )

. . . . . . (ACFM) DSCFM)

1 4 6 2 9 0

4 7 6 6 7 2 4 3 5 4

31 1

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T e s t No. B - P u l p

5 r y e r

I n t e r p o l l L a b s R e p o r t N o . 3-1636 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s , L l i n n e s o t a

; t a c k

R e s u l t s o f V o l u m e t r i c F l o w R a t e D e t e r m i n a t i o n - - - - - - - M e t h o d 2

D a t e o f D e t e r m i n a t i o n . . . . . . . . . . . . T i m e o f D e t e r m i n a t i o n . . . . . . . (HRS)

B a r o m e t r i c p r e s s u r e . . . . . . . ( I N . H G )

P i t o t t u b e c o e f f i c i e n t . . . . . . . . . . .

Number o f s a m p l i n g p o r t s . . . . . . . . . T o t a l number o f p o i n t s . . . . . . . . . . . Shape o f d u c t .................... S t a c k d i a m e t e r . . . . . . . . . . . . . . . ( I N )

D u c t a r e a . . . . . . . . . . . . . . . . . (SQ' .FT)

D i r e c t i o n o f f l o w . . . . . . . . .

S t a t i c p r e s s u r e . . . . . . . . . . . A v g . gas t e m p . . . . . . . . . . . . . M o i s t u r e c o n t e n t . . . . . . . . . .

. . . . . .

I N . W C )

DEG-F)

% V / V )

Avg. l i n e a r v e l o c i t y . . . . . (FT /SEC)

G a s d e n s i t y . . . . . . . . . . . . . . (LB /ACF)

M o l e c u l a r w e i g h t . . . . . . (LB/LBMOLE)

Mass f l o w o f g a s . . . . . . . . . .


34

LB/HR)

. . . . . . (ACFM) D S C F M )

11 -10 -93

807

2 9 . 5 5

.84

2

2 4

Round

5 9

1 8 . 9 9

UP

-. 98

2 3 1

2 3 . 3 0

6 3 . 3

. 0 5 2 0 1

29 .23

225180

72162 41655

I I

i I !

I I

. .,

I

'I

.::I . I I .:I .- 1

I IJ 3 I I

. I . 1

I I

I n t e r p o l l Labs R e p o r t No. 3 - 1 6 3 6 ~ m e r i c a n C r y s r a l S u g a r

E a s t G r a n d F o r k s , :.IN

T e s t No. 10 E a s t P e l l e t C o o l s r S t a c k

R e s u l t s o f V o l u m e t r i c F l o w R a t e D e t e r m i n a t i o n - - - - - - - M e t h o d 2

D a t e o f D e t e r m i n a t i o n . . . . . . . . . . . . 1 1 - 1 1 - 9 3

T ime o f D e t e r m i n a t i o n . . . . . . . ( H R S ) 1 4 0 0

B a r o m e t r i c p r e s s u r e . . . . . . . ( I N . H G ) 2 9 . 2 6

P i t o t t u b e c o e f f i c i e n t . . . . . . . . . . . . 8 4

Number o f s a m p l i n g p o r t s . . . . . . . . . T o t a l number O F p o i n t s . . . . . . . . . . . Shape o f d u c t .................... S t a c k d i a m e t e r . . . . . . . . . . . . . . . ( I N )

D u c t a r e a . . . . . . . . . . . . . . . . . . ( S Q . F T )

D i r e c t i o n o f f l o w . . . . . . . . . . . . . . . . )

2

1 2

Round

23

2 . 8 9

DOWN

S t a t i c p r e s s u r e . . . . . . . . . . . ( 1 N . W C )

Avg . gas temp . ............ (OEG-F)

. . . . . . . . ( S V / V )

- . 46

129

3 . 5 4 M o i s t u r e c o n t e n t . .

Avg . l i n e a r v e l o c

Gas d e n s i t y . . . . . . M o l e c u l a r w e i g h t . .

t y . . . . . ( FT/SEC)

. . . . . . . (LB /ACF)

. . . . (LB/LBMOLE)

8 2 . 0

.06469

2 8 . 8 4

Mass f l o w o f g a s . . . . . . . . . .


1

38

L B / H R )

. . . . . . ( A C F M ) D S C F M )

55103

14197 11987

~~ - ~ ~ ~~~ ~~ ~

I n ; ? r p o l l Labs R e p o r t No. 3-1636 A m e r i c a n C r y s t a l S u ~ a r

E a s t G r a n d F o r k s . I . l i n n e s o t a

T e s t No. 12 P e l l e t L o a d o u t S t a c k

i I R e s u l t s o f V o l u m e t r i c F l o w R a t e D e t e r m i n a t i o n - - - - - - - M e t h o d 2

I !

.-I ...

1 .I

D a t e O F D e t e r m i n a t i o n . . . . . . . . . . . . T i m e o f D e t e r m i n a t i o n . . . . . . . [ H R S )

B a r o m e t r i c p r e s s u r e . . . . . . . ( 1 N . H G )


N u m b e r o f s a m p l i n g p o r t s . . . . . . . . . T o t a l number o f p o i n t s . . . . . . . . . . . Shape o f d u c t . . . . . . . . . . . . . . . . . . . . S t a c k d i a m e t e r . . . . . . . . . . . . . . . ( I N )

D u c t a r e a . . . . . . . . . . . . . . . . . ( S Q . F T )

D i r e c t i o n o f f l o w . . . . . . . . . . . . . . . .

S t a t i c p r e s s u r e . . . . . . . . . . . ( 1 N . W C ) Avg . g a s t e m p . . . . . . . . . . . . . ( D E G - F )

M o i s t u r e c o n t e n t . . . . . . . . . . ( % V / V )

Avg . l i n e a r v e l o c i t y . . . . . ( F T / S E C )

Gas d e n s i t y . . . . . . . . . . . . . . (LB /ACF)

M o l e c u l a r w e i g h t . . . . . . (LB/CBMOLE)

Mass f l o w O F g a s . . . . . . . . . . ( L B I H R )

V o l u m e t r i c f l o w r a t e . . . . . . . . . . . . . a c t u a l . . . . . . . . . . . . . . . . . . . ( A C F M ) d r y s t a n d a r d . . . . . . . . . . . . (DSCFt4)

11-11-93

1430

29.3

.84

2

16

Round

25.75

3.62

-

U P I

- .062

0

0.74

18.9

.OB394

28.84

20643

4099 4573

4 39 1

I

I i I i I I 1 1 I I

J 1 I 3

1 I

I n t e r p o l l Labs R e p o r t No . 3-1636 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s . f4N

T ? s t No . 1 3 West P e l l e t C o o l e r S t a c k

R e s u l t s o f V o l u m e t r i c F l o w R a t e Determination....... M e t h o d 2

D a t e o f D e t e r m i n a t i o n . . . . . . . . . . . . T i me o f D e t e r m i n a t i o n . . . . . . . ( H R S 1

B a r o m e t r i c p r e s s u r e . . . . . . . ( 1 N . H G )


Number o f s a m p l i n g p o r t s . . . . . . . . . T o t a l number o f p o i n t s . . . . . . . . . . . Shape o f d u c t .................... S t a c k d i a m e t e r . . . . . . . . . . . . . . . ( I N )

D u c t a r e a . . . . . . . . . . . . . . . . . ( S Q . F T )

D i r e c t i o n of f l o w . . . . . . . . . . . . . . . .

S t a t i c p r e s s u r e . . . . . . . . . . . (1N.WC)

Avg . gas temp . . . . . . . . . . . . . ( D E G - F )

M o i s t u r e c o n t e n t . . . . . . . . . . ( S V / V )

Avg . l i n e a r v e l o c i t y . . ... ( F T / S E C )

Gas d e n s i t y . . . . . . . . . . . . . . (LB/ACF)

M o l e c u l a r w e i g h t . . . . . . (LB/LBMOLE)

Mass f l o w o f gas . . . . . . . . . . (LB/HR)

V o l u m e t r i c f l o w r a t e . . . . . . . . . . . . . a c t u a l . . . . . . . . . . . . . . . . . . . ( A C F M ) d r y s t a n d a r d . . . . . . . . . . . . (DSCFM)

11-11-93

905

29.26

.84

2

12

Round

23

2.89

DOWN

-.5

1 3 3

2.92

87.6

. 06438 28.84

58599

15169 12800

1 40

I n t e r p o l l L a b s R e p o r t No. 3-1636 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s , b l i n n e s o t a

T e s t N o . 1 C - P u l p D r y e r S t a c k

R e s u l t s o f O r s a t & M o i s t u r e A n a l y s e s - - - - - M e t h o d s 3 & 4 ( Z v / v )

D a t e o f r u n

D r y b a s i s ( o r s a t )

Run 1 Run .2 Run 3 .11-09-93 11-09-93 11-09-93

c a r b o n d i o x i d e . . . . . . . . . . . . 5.20

o x y g e n .................... 15.20

n i t r o g e n . . . . . . . . . . . . . . . . . . 79.60

Wet b a s i s ( o r s a t )

c a r b o n d i o x i d e . . . . . . . . . . . . 3.45

o x y g e n .................... 10.09

n i t r o g e n . . . . . . . . . . . . . . . . . . 52.85

w a t e r v a p o r . . . . . . . . . . . . . . . 33.61

D r y m o l e c u l a r w e i g h t . . . . . . . . 29.44

W e t m o l e c u l a r w e i g h t . . . . . . . . 25.60

S p e c i f i c g r a v i t y . . . . . . . . . . . . 0.884

W a t e r mass f l o w . . . . . . ( L B / H R ) 35310

F O 1.096

5.60 5.60

14.70 14.70

79.70 19.70 ~-

~~

3.86 3.52

10.12 9.24

54.89 50.08

31.13 37.16

29.48 29.48

25.91 25.22

0.895 0.871

32147 38896

1.107 1.107

42



T e s t N o . 5 B - P u l p D r y e r S t a c k

R e s u l t s o f O r s a t & M o i s t u r e A n a l y s e s - - - - - M e t h o d s 3 & 4(%v/v)

D a t e o f r u n


c a r b o n d i o x i d e . . . . . . . . . . . . o x y g e n .................... n i t r o g e n . . . . . . . . . . . . . . . . . .


c a r b o n d i o x i d e . . . . . . . . . . . . o x y g e n .................... n i t r o g e n . . . . . . . . . . . . . . . . . . w a t e r v a p o r . . . . . . . . . . . . . . .

D r y m o l e c u l a r w e i g h t . . . . . . . . Wet m o l e c u l a r w e i g h t . . . . . . . . S p e c i f i c g r a v i t y . . . . . . . . . . . . W a t e r mass f l o w . . . . . . ( L B / H R )

FO

Run 1 Run 2 Run 3 11-10-93 11-10-93 11-10-93

3.40

17.10

79.50

2.61

13.12

60.98

23.30

29.23

26.61

0.919

36957

1.118

3.00 3.30

17.50 17.20

79.50 79.50

2.34 2.57

13.66 13.42

62.07 62.03

21.92 21.97

29.18 29.22

26.73 26.75

0.923 0.924

35176 34517

1.133 1.121

44

~

i i

I

I . 1 I I

.:I . I

I ... -1 .. I 1

:a3 .f

1 I

.I

I I

!

I n t e r p o l l L z b s R e p o r t No. 3-1636 A m e r i c a n C r y s t a l S u g a r

E z s t G r s n d F o r k s , k l i n n e s o t a


R e s u l t s o f O r s a t & M o i s t u r e A n a l y s e s - - - - - M e t h o d s 3 13 4 ( % v / v )

D a t e of r u n


Run 1 Run 2 Run 3 11-11-93 11-11-93 11-11-93

c a r b o n d i o x i d e . . . . . . . . . . . . 6.60

o x y g e n .................... 13.60

n i t r o g e n . . . . . . . . . . . . . . . . . . 79.80



D r y m o l e c u l a r w e i g h t . . . . . . . . Wet m o l e c u l a r w e i g h t ........ S p e c i f i c g r a v i t y . . . . . . . . . . . . W a t e r mass f l o w . . . . . . ( L B / H R )

F O

46

3.85

7.94

46.60

41.60

29.60

24.17

0.856

45191

1.106

3.30

13.80

82.90

2.01

8.39

50.40

39.20

29.08

24.74

0.854

43571

2 . 1 5 2

6.30

13.90

79.80

3.85

8.48

48.71

38.96

29.56

25.06

0.866

43051

1 . 1 1 1

1

i

I n t r r p o l l L a b s R e p o r t N o . 3-1636 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F a r k s , IMN

T e s t N o . 10 E a s t P e l l e t C o o l e r S t a c k

R e s u l t s o f O r s a t & M o i s t u r e A n a l y s e s - - - - - M e t h o d s 3 & 4(2v/v)

D a t e o f r u n


Run 1 Run 2 Run 3 11-11-93 11-11-93 11-11-93

c a r b o n d i o x i d e . . . . . . . . . . . . 0 . 0 3

o x y g e n .................... 20.90

n i t r o g e n . . . . . . . . . . . . . . . . . . 79.07


c a r b o n d i o x i d e . . . . . . . . . . . . 0 . 0 3

o x y g e n .................... 20.16

n i t r o g e n . . . . . . . . . . . . . . . . . . 76.27

w a t e r v a p o r . . . . . . . . . . . . . . . 3.54

D r y m o l e c u l a r w e i g h t . . . . . . . . 28.84

Wet m o l e c u l a r w e i g h t ......... 28.46

S p e c i f i c g r a v i t y . . . . . . . . . . . . 0.983

W a t e r mass f l o w . . . . . . ( L B / H R ) 1221

'0.03 0.03

20.90 20.90

79.07 79.07

0.03 0.03

20.09 20.19

7s. 99 76.38

3.89 3.40

28.84 28.84

28.42 28.47

0.982 0.983

1353 1194

47 .I

I n t e r p o i l Labs R e p o r t N O . 3-1636 A m e r i c a n C r y s t a l S u g a r

E J i t G r a n d F o r k s , I . I i n n e ; o t ~

T e s t No. 1 2 P e l l e t L o a d o u t S t a c k

R e s u l t s o f O r s a t 8 M o i s t u r e A n a l y s e s - - - - - M e t h o d s 3

D a t e o f r u n


c a r b o n d i o x i d e . . . . . . . . . . o x y g e n .................... n i t r o g e n . . . . . . . . . . . . . . . . . .


c a r b o n d i o x i d e . . . . . . . . . . . . o x y g e n . . . . . . . . . . . . n i t r o g e n . . . . . . . . . w a t e r v a p o r , . . . . .

D r y m o l e c u l a r w e i g h

. . . . . . . .

........

. . . . . . . .

. . . . . . . . Wet m o l e c u l a r w e i g h t . . . . . . . . S p e c i f i c g r a v i t y . . . . . . . . . . . . W a t e r mass f l o w . . . . . . ( L B / H R )

Run 1 11-1 1-93

0 . 0 3

2 0 . 9 0

7 9 . 0 7

0 .03

2 0 . 7 s

7 0 . 4 9

0 . 7 4 *

2 8 . 0 4

2 0 . 7 6

0 . 9 9 3

1 0 6

Run 2 1 1 - 1 1 - 9 3

0 . 0 3

2 0 . 9 0

7 9 . 0 7

0 . 0 3

2 0 . 7 5

7 0 . 5 1

0 . 7 0 '

2 8 . 0 4

2 8 . 7 6

0 . 9 9 4

1 2 0

* F r e e o r c o n d e n s e d w a t e r i n t h e g a s s t r e a m .

8 4 ( % v / v )

Run 3 1 1 - 1 1 - 9 3

0.03

2 0 . 9 0

7 9 . 0 7 ~~~ ~~

0 .03

2 0 . 7 8

7 8 . 6 0

0.60*

2 8 . 0 4

2 0 . 7 0

0 . 9 9 4

1 1 4

i I I I

1 I I 1 1 I I 1 I

I I

I n t o r p o l l Labs R e p o r t No . 3-1036 A m e r i c s n C r y s t a l S u g a r

E a s t G r a n d F o r k s . I4N

T e s t No. 1 3 W e s t P e l l e t C o o l e r S t a c k

R e s u l t s o f O r s a t B M o i s t u r e Ana lyses- - - - - M e t h o d s 3 & 4 ( % v / v )

D a t e o f r u n


c a r b o n d i o x i d e . . . . . . . . . . . . o x y g e n . . . . . . . . . . . . . . . . . . . . n i t r o g e n . . . . . . . . . . . . . . . . . .



D r y m o l e c u l a r w e i g h t . . . . . . . . Wet m o l e c u l a r w e i g h t . . . . . . . . S p e c i f i c g r a v i t y . . . . . . . . . . . . W a t e r mass f l o w . . . . . . ( L B / H R )

Run 1 Run 2 Run 3 11-11-93 11-11-93 11-11-93

0.03 0.03 0.03

20.90 20.90 20.90

79.07 79.07 79.07

0.03

20.29

76.76

2.92

28.84

28.52

0.985

1089

0.03

20.13

76.14

3.70

28.84

28.44

0.982

1378

0.03

20.35

76.97

2.65

28.84

28.55

0.986

1002

49 J ~

I n t e r p o l 1 Labs R e p o r t N o . 3 - 1 6 3 6 A m e r i c a n C r y s t a l Sugar

E a s t G r a n d F o r k s , f . I i n n e s o t a

T e s t No. 1 C - P u l p D r y e r S t a c k

R e s u l t s o f P a r t i c u l a t e L o a d i n g D e t e r m i n a t i o n s - - - - - - - M e t h o d 5

1 1 I I

D a t e o f r u n

T ime r u n s t a r t / e n d . . . . . ( H R S )

S t a t i c p r e s s u r e . . . . . . ( 1 N . W C ) C r o s s s e c t i o n a l a r e a ( S Q . F T ) P i t o t t u b e c o e f f i c i e n t . . . . . . W a t e r i n samp le gas

c o nde n s e r . . . . . . . . . . . . . ( M L ) i m p i n g e r s . . . . . . . . . . (GRAMS) d e s i c c a n t . . . . . . . . . . (GRAMS) t o t a l . . . . . . . . . . . . . . (GRAMS)

T o t a l p a r t i c u l a t e m a t e r i a l . . . . . . . . . . . . c o l l e c t e d ( g r a m s )

Gas m e t e r c o e f f i c i e n t . . . . . . . B a r o m e t r i c p r e s s u r e . . ( I N . H G ) Avg . o r i f . p r e s . d r o p . . ( I N . W C ) Avg . gas m e t e r t e m p . . ( D E F - F )

Volume t h r o u g h gas m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) s t a n d a r d c o n d i t i o n s . ( D S C F )

T o t a l s a m p l i n g t i m e . . . . ( M I N ) N o z z l e d i a m e t e r . . ....... ( I N ) A v g . s t a c k gas temp . . ( D E G - F )

V o l u m e t r i c f l o w r a t e . . . . . . . . a c t u a l . . . . . . . . . . . . . . (ACFM) d r y s t a n d a r d . . . . . . . ( D S C F M )

I s o k i n e t i c v a r i a t i o n . . . . . 0 ; )

P a r t i c u l a t e c o n c e n t r a t i o n . . . a c t u a l . . . . . . . . . . . . ( G R / A C F ) d r y s t a n d a r d . . . . . ( G R / O S C F )


Run 1 11 - 0 9 - 9 3

1 0 3 0 / 1 2 3 5

- 1 . 0 2 1 2 . 5 7

. E 4 0

0 . 0 5 7 8 . 0

11.0 5 8 9 . 0

0 . 2 1 5 6

0 . 9 9 7 5 2 9 . 5 1

0 . 7 0 7 9 . 5

5 6 . 9 0 5 4 . 8 6

1 2 0 . 0 0

2 1 6 . i g a

4 8 7 5 9 2 4 8 6 7

108.1

0 . 0 3 0 9 1 0 . 0 6 0 6 4

1 2 . 9 2 5

Run 2 1 1 -'09 - 9 3

L 3 1 5 / 1 5 1 7

- 1 . 0 2 1 2 . 5 7

. E 4 0

0 . 0 4 6 8 . 0

10.0 4 7 8 . 0

0 . 2 2 3 1

0 . 9 9 7 5 2 9 . 5 1

0 . 5 7 7 8 . 0

5 1 . 5 9 4 9 . 8 6

1 2 0 . 0 0 .198 2 1 5

4 7 8 6 6 2 5 3 5 6

9 6 . 4

0 . 0 3 6 5 6 0 . 0 6 9 0 4

1 5 . 0 0 4

Run 3 1 1 - 0 9 - 9 3

1 5 3 5 / 1 7 3 8

- 1 . 0 2 1 2 . 5 7

. 8 4 0

0.0 6 3 1 . 0

1 0 . 0 6 4 1 . 0

0 . 2 5 7 1

0 . 9 9 7 5 2 9 . 5 1

0 . 6 1 8 2 . 1

5 3 . 2 7 51.10

1 2 0 . 0 0 . 1 9 8

216

48553 2 3 4 4 6

1 0 6 . 8

0 . 0 3 7 5 7 0 . 0 7 7 6 3

1 5 . 6 0 1

I 1 51

I n t e r p o l 1 Labs R e p o r t No. 3 - 1 6 3 6 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s , ).IN

T e s t No. E a s t P e

R e s u l t s

D a t e o f

10 l e t C o o l e r S t a c k

o f P a r t i c u l a t e L o a d i n g D e t e r m i n a t i o n s - - - - - - - M e t h o d 5

r u n

T ime r u n s t a r t / e n d . . . . . ( H R S )

S t a t i c p r e s s u r e . . . . . . ( I N . W C ) C r o s s s e c t i o n a l a r e a ( S Q . F T ) P i t o t t u b e c o e f f i c i e n t . . . . . . W a t e r i n sample g a s

c o n d e n s e r . . . . . . . . . . . . . (ML) i m p i n g e r s . . . . . . . . . . ( G R A M S )

t o t a l . . . . . . . . . . . . . . ( G R A M S )

. . . . . . . . . . c o l l e c t e d ( g r a m s )

d e s i c c a n t . . . . . . . . . . ( G R A M S )

T o t a l p a r t i c u l a t e m a t e r i a l . .

Gas m e t e r c o e f f i c i e n t . . . . . . . B a r o m e t r i c p r e s s u r e . . (1N.HG) Avg. o r i f . p r e s . d r o p . . ( I N . W C ) Avg . gas m e t e r t e m p . . ( D E F - F )

Vo lume t h r o u g h gas m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) s t a n d a r d c o n d i t i o n s . ( D S C F )

T o t a l s a m p l i n g t i m e . . . . ( M I N ) N o z z l e d i a m e t e r . . . . . . . . . ( I N ) A v g . s t a c k gas temp . . (DEG-F)

V o l u m e t r i c f l o w r a t e . . . . . . . . d r y s t a n d a r d . . . . . . . (DSCFM) a c t u a l . . . . . . . . . . . . . . (ACFM)

I s o k i n e t i c v a r i a t i o n . . . . . ( % )



Run 1 11-11-93

141511517

-0.46 2.89 .840

0.0 25.0 12.0 37.0

0.1021

, O . 9965 29.26 2.23 65.5

48.24 47.48

60.00 .188 134

14158 11849

100.0

0.02776 0.03318

3.370

aun 2 11-11-93

1545/1648

-0.46 2.89 .840

0 .0 27.0 14.0 41.0

0.1142

0.9965 29.26 2.28 71.5

49.08 47.77

60.00 .188 134

14278 11920

100.0

0.03078 0.03669

3.769

Run 3 1 1 - 1 1-93

1705/ 1808

-0.46 2.89 .040

0.0 23.0 13 .O 36.0

0.1012

0.9965 29.26 2.32 71.8

49.51 48.16

60.00 .188 128

14238 12073

99.6

0.02748 0.03242

3.355

56

- ~ ~~

I n t e r p o l 1 Labs R e p o r t No. 3 - 1 6 3 6 A m e r i c a n C r y s t a l Sugar

r c a s t G r a n d F o r k s , t 4 i n n e s o t a

T e s t No. 1 2 P e l l e t L o a d o u t S t a c k

R e s u l t s o f P a r t i c u l a t e L o a d i n g D e t e r m i n a t

D a t e o f r u n Run 1

1 1 - 1 1 - 9 3

T i m e r u n s t a r t l e n d . . . . . ( H R S ) 1 4 4 5 / 1 5 4 9

S t a t i c p r e s s u r e . . . . . . (1N.WC) C r o s s s e c t i o n a l a r e a ( S Q . F T ) P i t o t t u b e c o e f f i c i e n t . . . . . . W a t e r i n sample gas

c o n d e n s e r . . . . . . . . . . . . . ( ML) i m p i n g e r s . . . . . . . . . . ( G R A M S ) d e s i c c a n t . . . . . . , . . . (GRAMS) t o t a l . . . . . . . . . . . . . . ( G R A M S )


Gas m e t e r c o e . f F i c i e n t B a r o m e t r i c p r e s s u r e . . A v g . o r i f . p r e s . d r o p . . A v g . gas m e t e r t e m p . .

Vo lume t h r o u g h gas me a t m e t e r c o n d i t i o n s s t a n d a r d c o n d i t i o n s

T o t a l s a m p l i n g t i m e . . N o z z l e d i a m e t e r . . . . . . A v g . s t a c k g a s temp . . V o l u m e t r i c f l o w r a t e .

a c t u a l . . . . ......... d r y s t a n d a r d . . . . . . .

. . . . . . IN .HG) 1 N . W C ) DEF-F)

e r . . . . . . ( C F ) (OSCF)

. ( M I N )

. . ( I N ) DEG-F )

. . . . . . (ACFM) DSCFM)

I s o k i n e t i c v a r i a t i o n . . . . . ( % )

P a r t i c u l a t e c o n c e n t r a t i o n . . . a c t u a l . . . . . . . . . . . . ( G R l A C F ) d r y s t a n d a r d . . . . . (GR/OSCF)


- 0 . 0 6 3 . 6 2 . E 4 0

0 . 0 0 . 0

1 3 . 0 1 3 . 0

0 . 0 0 8 7

0 . 9 9 7 5 2 9 . 3 0

1 . 2 9 7 1 . 6

4 1 . 1 9 4 0 . 0 8

6 4 . 0 0 .310

3 7

4 2 0 4 4 3 4 4

9 9 . 5

0 . 0 0 3 4 6 0 . 0 0 3 3 5

0 . 1 2 5

Run 2 1 - 1 1 - 9 3

1 6 2 0 I 1 7 2 1

-0 .06 3 . 6 2 . 8 4 0

0 . 0 0 .0 9.0 9 . 0

0 . 0 0 4 6

0 . 9 9 7 5 2 9 . 3 0

1 . 3 5 8 6 . 2

4 2 . 7 1 4 0 . 4 5

6 4 . 0 0 . 3 1 0

3 5

4 2 1 1 4 3 6 4

100.0

0 .00182 0 . 0 0 1 7 5

0 . 0 6 6

Run 3 11 - 1 1 - 9 3

1 7 5 5 / 1 8 5 6

-0 .06 3 . 6 2 . a 4 0

0.0 0.0 8.0 8.0

0 . 0 0 2 8

0 . 9 9 7 5 2 9 . 3 0

1 . 4 0 8 9 . 1

4 3 . 6 6 4 1 . 1 4

6 4 . 0 0 .3 10

3 1

4 2 4 0 4 4 3 6

100.0

0.00110 0 . 0 0 1 0 5

3 . 0 4 0

5 7

I n t e r p o l 1 Labs R e p o r t No. 3-1636 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s , I.1N

T e s t No. 1 3 West P e l l e t Coo

R e s u l t s o f P a r t

e r S t a c k

c u 1 a t e L o a d i ng De t e r m i na t i ons-------He t h o d 5

D a t e o f r u n

T i m e r u n s t a r t l e n d . . . . . ( H R S ' )

S t a t i c p r e s s u r e . . . . . . (1N.WC) C r o s s s e c t i o n a l a r e a (SQ.FT) P i t o t t u b e c o e f f i c i e n t . . . . . . W a t e r i n samp le gas

c o n d e n s e r . . . . . . . . . . . . . (ML) i m p i n g e r s . . . . . . . . . . ( G R A M S ) d e s i c c a n t . . . . . . . . . . ( G R A M S ) t o t a l . . . . . . . . . . . . . . ( GRAMS)


Gas m e t e r c o e f f i c i e n t . . . . . . . B a r o m e t r i c p r e s s u r e . . ( 1 N . H G ) Avg . o r i f . p r e s . d r o p . . ( I N . WC) Avg . g a s m e t e r t e m p . . ( D E F - F )

Vo lume t h r o u g h gas m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) s t a n d a r d c o n d i t i o n s . ( D S C F )

T o t a l s a m p l i n g t i m e . . . . ( M I N ) N o z z l e d i a m e t e r . . . ...... ( I N ) A v g . s t a c k g a s temp . . ( D E G - F )

V o l u m e t r i c f l o w r a t e . . . . . . . . a c t u a l . . . . . . . . . . . . . . (ACFM) d r y s t a n d a r d . . . . . . .(DSCFM)

I s o k i n e t i c v a r i a t i o n . . . . . ( t )



Run 1 11-11-93

935/1038

-0.50 2.89 .e40

0.0 17.0 16.0 33.0

0.3116

0.9965 29.26 2.63 61.4

52.11 51.74

60.00 .188 124

15063 12908

100.1

0.07960 0.09293

10.281

Run 2 1 1 - 1.1 - 9 3

1103/ 1205

-0.50 2.89 .840

0.0 27 .O 15.0 42.0

0.3111

0.9965 29.26 2.63 64.5

52.18 51.51

60.00 .188 138

15396 12779

100.6

0.07732 0.09319

10.207

Run 3 11-11-93

1245 / 13 48

-0.50 2.89 .840

0.0 22.0 8.0 30.0

0.3909

0.9965 29.26 2.66 63.9

52.58 51.97

60.00 .180 135

15555 13123

90.8

0.09708 0.11606

13.055

I n t e r p o l l R e p o r t No. 3-1636 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F i r r k s . M i n n e s o t a


R e s u l t s o f S u l f u r D i o x i d e D e t e r m i n a t i o n s - - - - - - - - - - - - M e t h o d 6

Run 1

D a t e o f r u n 11-09-93

T i m e r u n s t a r t / e n d . . . . . ( H R S ) 1030-1235

B a r o m e t r i c p r e s s u r e . . (IN.HG)

M e t e r t e m p e r a t u r e . . .. (OEG-F)

M e t e r c o r r e c t i o n c o e f f i c i e n t

Vo lume t h r o u g h g a s m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) s t a n d a r d c o n d i

T o t a l s a m p l i n g t

M o i s t u r e c o n t e n t

Oxygen c o n t e n t . .

M i l l i e q u i v a l e n t s

i o n s . . ( S C F )

m e . . . . ( M I N )

. . ... ( S V / V )

. ( % V / V D R Y )

o f SO4 i n . , g a s s a m p l e . . . . . . . . . . . . . . . .

S u l f u r d i o x i d e c o n c e n t r a t i o n

(GR/DSCF) . . . . . . . . . . . . . . . . . ( M G I D S C M ) . . . . . . . . . . . . . . . . . (PPM-DRY) . . . . . . . . . . . . . . . . . (PPM-WET) . . . . . . . . . . . . . . . . .

SO2 E m i s s i o n r a t e . . . . ( LB/HR)

29.51

79.50

0.9975

56.900 54.860

120.0

33.61

15.20

2.5000

0.0225 52 19 1 3

4.80

R u n 2

11-09-93

1315-1517

29.51

78.00

0.9975

51.590 49.863

120.0

31.13

14.70

1.4300

0.0142 32 12 8

3.08

Run 3

11-09-93

1535-1738

29.51

82.10

0.9975

53.270 51.103

120.0

37.16

14.70

3 .a200

0.0292 67 25 16

5.87

60

i 1 ;

! ,! '

I n t e r p o l l Labs R e p o r t No. 3 - 1 6 3 6 A m e r i c a n C r y s t a l s u g a r


T e s t N O . 5 8 - P u l p D r y e r S t a c k

R e s u l t s of O x i d e s o f N i t r o g e n (NOx) D e t e r m i n a t i o n s - - - - - - - - - M e t h o d 7

Run 2A Run 2 8 Run 2C Run 2 0

D a t e o f run . . . . . . . . . . . . . . . . 1 1 - 1 0 - 9 3 1 1 - 1 0 - 9 3 1 1 - 1 0 - 9 3 1 1 - 1 0 - 9 3 T ime o f r un . . . . . . . . . . . . ( H R S ) 1 1 3 0 1 2 0 5 1 2 3 5 1310

F l a s k n u m b e r . . . . . . . . . . . . . . . . 2 9 3 0 3 1 32 Volume o f f l a s k . . . . . . . . . ( M L ) 2 0 6 8 2 0 7 1 2 0 0 9 2 0 9 2

. .


f l a s k t e m p e r a t u r e . . ( D E G - F ) 5 5 . 0 0 b a r . p r e s s . . . . . . . . . ( I N . H G ) 2 9 . 5 5 f l a s k vacuum . . . . . . . (1N.HG) 2 7 . 4 5 f l a s k a b s . p r e s s . . . ( 1 N . H G ) 2 . 1 0

D a t a : T ime of F l a s k O p e n i n g

f l a s k t e m p e r a t u r e . . ( D E G - F ) 7 2 . 0 0

f l a s k s t a t i c p r e s s . ( I N . H G ) 0 . 5 0 l a b . b a r . p r e s s . . . . (1N.HG) 2 9 . 1 6

f l a s k a b s . p r e s s . . . (1N.HG) 2 9 . 6 6

Volume gas s a m p l e d . . . . ( D S M L ) 1 8 6 2

M o i s t u r e c o n t e n t . . . . . . ( t V / V ) 2 1 . 8 8 Oxygen c o n t e n t . . . . ( f V / V . D R Y ) 1 7 . 5 0

N i t r a t e i n gas samp le . . . ( J G ) 3 1 9 . 0 NO2 i n g a s samp le . . . . . . . ( J G ) 2 3 6 . 7


( G R / D S C F ) . . . . . . . . . . . . . . . . . 0 . 0 5 5 5 (MG/DSCM) . . . . . . . . . . . . . . . . . 1 2 7 ( P P M - D R Y ) . . . . . . . . . . . . . . . . . 6 6 ( P P M - W E T ) . . . . . . . . . . . . . . . . . 5 2

NOX E m i s s i o n r a t e . ... ( L B / H R ) 2 1 . 2 7

N O x e m i s s i o n f a c t o r . . . . . . . . . . . . . . . . . . . . . . . . . (LE/MMETU)* 0 . 4 7 7

* F = 9 7 8 0 DSCF/MMETU

5 2 . 0 0 5 8 . 0 0 5 6 . 0 0 2 9 . 5 5 2 9 . 5 5 2 9 . 5 5 . 2 7 . 5 0 2 7 . 4 5 2 7 . 5 0

2 . 0 5 2 . 1 0 2 . 0 5

7 2 . 0 0 7 2 . 0 0 7 2 . 0 0 2 9 . 1 6 2 9 . 1 6 2 9 . 1 6 - 0 . 3 0 - 2 . 3 0 - 0 . 3 0 2 8 . 8 6 2 6 . 8 6 2 8 . 8 6

1 8 1 3 1 6 2 5 1 8 3 3

2 1 . 8 8 2 1 . 8 8 2 1 . 8 8 1 7 . 5 0 1 7 . 5 0 1 7 . 5 0

3 0 1 . 0 300.0 3 1 0 . 0 2 2 3 . 3 2 2 2 . 6 2 3 0 . 0

0 . 0 5 3 8 0 . 0 5 9 9 0 . 0 5 4 8 1 2 3 1 3 7 1 2 5

6 4 7 2 6 6 5 0 56 5 1

2 0 . 6 1 2 2 . 9 2 2 1 . 0 0

0 . 4 6 2 0 . 5 1 4 0 . 4 7 1

68

I n t e r p o l 1 L a b s R e p o r t No. 3 - 1 5 2 6 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s . I . l i n n e s o t a

(GR/OSCF) . . . . . . . . . . . . . . . . . 0.0521 0.0554 0.0548 0.0593 ,

(MG/DSCM) . . . . . . . . . . . . . . . . . 119 127 125 136 ( P P M - D R Y ) . . . . . . . . . . . . . . . . . 62 66 66 71 (PPM-WET) . . . . . . . . . . . . . . . . . 49 52 51 55

T e s t N o . 5 0 - P u l p D r y e r S t a c k

R e s u l t s o f O x i d e s o f N i t r o g e n ( N O x ) D e t e r m i n a t i o n s - - - - - - - - - M e t h o d 7

* F = 9780 OSCF/MMBTU i

69 1

!

I n t e r p u l l L a b s R e p o r t Nu. 3 - 1 6 3 6 A m e r i c a n C r y s t a l s u g a r

Ea; t G r a n d F a r k s . I4 inne;uta



D a t e O F run . . . . . . . . . . . . . . . . T ime O F r u n . . . . . . . . . . . . (HRS)

F l a s k number . . . . . . . . . . . . . . . . Volume o f f l a s k . . . . . . . . . ( t . 1L)


f l a s k t e m p e r a t u r e . . ( D E G - F ) b a r . p r e s s . . . . . . . . . ( I N . H G ) f l a s k vacuum . . . . . . . ( I N . H G ) F l a s k a b s . p r e s s . . . ( I N . H G )


F l a s k t e m p e r a t u r e . . ( D E G - F )

f l a s k s t a t i c p r e s s . ( 1 N . H G ) f l a s k a b s . p r e s s . . . ( I N . H G )

Vo lume gas s a m p l e d . . . . (DSML)

M o i s t u r e c o n t e n t . . . . . . ( t V / V ) Oxygen c o n t e n t . . . . ( ? V / V . D R Y )

N i t r a t e i n g a s sample . . . ( J G ) N O 2 i n g a s s a m p l e . . . . . . . ( J G )


l a b . b a r . p r e s s . . . . ( I N . H G )

( G R / D S C F ) . . . . . . . . . . . . . . . . . ( M G / O S C M ) . . . . . . . . . . . . . . . . . (PPM-DRY) . . . . . . . . . . . . . . . . . (PPM-WET) . . . . . . . . . . . . . . . . .

NOX E m i s s i o n r a t e . . . . ( L B / H R )

NOx e m i s s i o n f a c t o r . . . . . . . . . . . . . . . . . . . . . . . . . (LB/MMBTU) '

Run 1 A

11 - 0 9 - 9 3 1030

37 2 0 5 4

6 0 . 0 0 2 9 . 5 1 2 7 . 8 0

1 . 7 1

7 2 .OO 2 9 . 1 6

0 .00 2 9 . 1 6

1 8 4 4

3 3 . 6 1 1 5 . 2 0

4 3 8 . 0 3 2 5 . 0

0 . 0 7 7 0 1 7 6

9 2 6 1

1 6 . 4 2

0 . 3 9 5

Run 1 8

11 - 0 9 - 9 3 1 0 5 5

3 8 2 0 5 6

5 9 . 0 0 2 9 . 5 1 2 7 . 7 0

1 .81

7 2 . O O 2 9 . 1 6

1.10 3 0 . 2 6

1 9 1 3

3 3 . 6 1 1 5 . 2 0

4 6 5 . 0 3 4 9 . 0

0 . 0 7 8 8 1 8 0

9 4 63

1 6 . 8 0

0 . 4 0 4

Run 1 C

11 - 0 9 - 9 3 1 1 2 5

39 2 0 6 2

5 6 . 0 0 2 9 . 5 1 2 7 . 8 0

1 . 7 1

7 2 . 0 0 2 9 . 1 6 0.00

2 9 . 1 6

1 8 5 0

3 3 . 6 1 1 5 . 2 0

4 6 6 . 0 3 4 5 . 8

0 . 0 8 1 7 1 8 7

9 8 6 5

1 7 . 4 0

0 . 4 1 8

Run 1 0

1 1 - 0 9 - 9 3 1 1 5 5

40 2 0 9 3

5 5 . 0 0 2 9 . 5 1 2 7 . 8 5

1 . 6 6

7 2 . 0 0 2 9 . 1 6 - 1 . 4 0 2 7 . 1 6

1 7 8 6

3 3 . 6 1 1 5 . 2 0

4 7 0 . 0 3 4 8 . 7

0 . 0 8 5 3 1 9 5 1 0 2

6 8

1 8 . 1 9

0 . 4 3 7

" F = 9 7 8 0 O S C F / M M B T U

70

I n t e r p o l 1 Labs R e p o r t No. 3 - 1 6 3 6 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k i , t . I i n n e s a t a

T e s t N o . 1 C - P u l p D r y e r S t a c k


Run 2A Run 2 8 Run 2 C Run 2D

D a t e o f r u n . . . . . . . . . . . . . . . . 1 1 - 0 9 - 9 3 1 1 - 0 9 - 9 3 1 1 - 0 9 - 9 3 1 1 - 0 9 - 9 3 . . . . . . . . . . . . T ime o f run ( H R S ) 1 3 2 0 1 3 4 5 1 4 1 5 1 4 4 5

. . . . . . . . . . . . . F l a s k n u m b e r . . . 4 1 4 2 7 9 8 0 Vo lume o f f l a s k . . . . . . . . . ( H L ) 2 0 7 6 2 0 9 4 2 0 8 5 2 1 0 5


f l a s k t e m p e r a t u r e . .(DEG-F) 4 6 . 0 0 4 4 . 0 0 6 8 . 0 0 6 8 . 0 0

f l a s k vacuum ( 1 N . H G ) b a r . p r e s s . . . . . . . . . (1N.HG) 2 9 . 5 1 2 9 . 5 1 2 9 . 5 1 2 9 . 5 1

f l a s k a b s . p r e s s . . . ( 1 N . H G ) 1 . 7 1 1 . 7 1 1 . 7 1 1 . 7 1 . . . . . . . 2 7 . 8 0 2 7 . 8 0 2 7 . 8 0 2 7 . 8 0 =


f l a s k t e m p e r a t u r e . . ( D E G - F ) 7 2 . 0 0 7 2 . 0 0 7 2 . 0 0 7 2 . 0 0 l a b . b a r . p r e s s . . . . (1N.HG) 2 9 . 1 6 2 9 . 1 6 2 9 . 1 6 2 9 . 1 6 F l a s k ' s t a t i c p r e s s . (1N.HG) - 1 . 3 0 - 1 . 5 0 0.30 0 . 9 0

Vo lume g a s s a m p l e d . . . . ( D S M L ) 1 7 7 2 1 7 7 4 1 8 9 5 1 9 5 4

Moi s t u r e c o n t e n t . . . . . . ( t V / V ) 3 1 . 1 3 3 1 . 1 3 3 1 . 1 3 3 1 . 1 3 Oxygen c o n t e n t . . . . ( % V / V , D R Y ) 1 4 . 7 0 1 4 . 7 0 1 4 . 7 0 1 4 . 7 0

N i t r a t e i n g a s samp le . . . ( J G ) 4 8 2 . 0 4 8 7 . 0 4 4 0 . 0 4 4 7 . o

f l a s k a b s . p r e s s . ..(IN.HG) 2 7 . 8 6 2 7 . 6 6 2 9 . 4 6 3 0 . 0 6

NO2 i n g a s s a m p l e . . . . . . . ( J G ) 3 5 7 . 6 3 6 1 . 3 3 2 6 . 5 3 3 1 . 1


(GR/DSCF) . . . . . . . . . . . . . . . . . 0 . 0 8 8 2 0 .0890 0 . 0 7 5 3 0 . 0 7 4 2 (MG/DSCM) . . . . . . . . . . . . . . . . . 2 0 2 2 0 4 1 7 2 1 7 0 ( P P M - D R Y ) . . . . . . . . . . . . . . . . . 1 0 6 1 0 7 9 0 8 9

. . . . . . . . . . . . . . . . . 6 1 ( P P M - W E T ) 7 3 1 3 6 2

N O X E m i s s i o n r a t e . . . . ( L B / H R ) 1 9 . 1 6 1 9 . 3 5 1 6 . 3 7 1 6 . 1 2

N O x e m i s s i o n f a c t o r . . . . . . . . . . . . . . . . . . . . . . . . . (LB/MMETU) * 0 . 4 1 5 0 . 4 1 9 0 . 3 5 5 0 . 3 4 9

* F = 9 7 8 0 D S C F / M M E T U

71

I n t e r p o l l L a b s R e p o r t No. 3 - 1 6 3 6 A m e r i c a n C r y s t a l S u g a r


T ? s t N o . 1 C - P u l p D r y e r S t a c k


Run 3 A Run 3 8 Run 3 C Run 3 D

D a t e o f r u n . . . . . . . . . . . . . . . . 1 1 - 0 9 - 9 3 1 1 - 0 9 - 9 3 1 1 - 0 9 - 9 3 1 1 - 0 9 - 9 3 T ime o f r u n . . . . . . . . . . . . ( H R S ) 1 5 4 0 1 6 2 5 1 6 5 0 1 7 2 0

F l a s k number . . . . . . . . . . . . . . . . 8 1 8 2 8 3 8 4 Volume o f f l a s k . . . . . . . . . ( M L ) 2 0 9 3 2 0 9 0 2 0 6 0 2 0 8 9


f l a s k t e m p e r a t u r e . . ( D E G - F ) 7 9 . 0 0 7 6 . 0 0 7 5 . 0 0 7 0 . 0 0 b a r . p r e s s . . . . . . . . . ( 1 N . H G ) 2 9 . 5 1 2 9 . 5 1 2 9 . 5 1 2 9 . 5 1 f l a s k vacuum. . . . . . . ( I N . H G ) 2 7 . 7 5 2 7 . 8 0 2 7 . 8 0 2 7 . 8 0 f l a s k a b s . p r e s s . . . ( I N . H G ) 1 . 7 6 1 . 7 1 1 . 7 1 1 . 7 1


f l a s k t e m p e r a t u r e . . ( D E G - F ) 7 2 . 0 0 7 2 . 0 0 7 2 . 0 0 7 2 . 0 0 l a b . b a r . p r e s s . . . . ( I N . H G ) 2 9 . 1 6 2 9 . 1 6 2 9 . 1 6 2 9 . 1 6

f l a s k a b s . p r e s s . . . ( I N . H G ) 2 9 . 9 6 2 8 . 0 6 2 7 . 5 6 3 0 . 9 6 f l a s k s t a t i c p r e s s . ( I N . H G ) 0 .80 -1.10 - 1 . 6 0 1 . 8 0

Volume gas s a m p l e d . . . . ( DSML) 1 9 3 5 1 8 0 5 1 7 4 5 2 0 0 1

M o i s t u r e c o n t e n t . . . . . . ( % V / V ) 3 7 . 1 6 3 7 . 1 6 3 7 . 1 6 3 7 . 1 6 Oxygen c o n t e n t . . . . ( f V / V . D R Y ) 1 4 . 7 0 1 4 . 7 0 1 4 . 7 0 1 4 . 7 0

N i t r a t e i n gas samp le . . . ( J G ) 4 0 1 . 0 4 4 5 . 0 4 5 4 . 0 4 2 3 . 0 N O 2 i n gas samp le . ...... ( J G ) 2 9 7 , 5 3 3 0 . 2 3 3 6 . 9 3 1 3 . 9


(GR/OSCF) . . . . . . . . . . . . . . . . . 0 . 0 6 7 2 0 . 0 7 9 9 0 . 0 8 4 4 0 . 0 6 8 5 (MG/OSCM) . . . . . . . . . . . . . . . . . 1 5 4 1 8 3 1 9 3 1 5 7 ( P P M - D R Y ) . . . . . . . . . . . . . . . . . 8 0 9 6 101 8 2 ( P P M - W E T ) . 5 1 6 0 63 5 2

NOX E m i s s i o n r a t e . . . . ( LB/HR) 1 3 . 5 0 1 6 . 0 6 1 6 . 9 5 1 3 . 7 7

N O x e m i s s i o n f a c t o r . . . . . . . . . . . . . . . . . . . . . . . . . (LB/MM9TU]* 0 . 3 1 6 0 . 3 7 6 0 . 3 9 7 0 . 3 2 3

. . . . . . . . . . . . . . . . .

* F = 9 7 8 0 OSCF/MMBTU

72 -

I n t e r p o l l L a b s R e p o r t No. 3 - 1 6 3 6 A m e r i c a n C r y s t a l Sugar

E a s t G r a n d F o r k s , I 4 i n n e s o t a

T r s t No. 1 C - P u l p Dryer S t a c k

R e s u l t s o f C O D e t e r m i n a t i o n s - - - - - - - - - - - - - - - - - - - - - -Method 10

Run 1 Run 2 Run 3

D a t e o f r u n 1 1 - 0 9 - 9 3 1 1 - 0 9 - 0 3 1 1 - 0 9 - 9 3

T ime r u n s t a r t / e n d . . . . . ( H R S ) 1 0 3 0 / 1 2 3 5 1 3 1 5 / 1 5 1 7 1 5 3 5 / 1 7 3 8

T o t a l s a m p l i n g t i m e . . . . ( M I N ) 1 2 0 . 0 i z o . o 1 2 0 . 0

M o i s t u r e c o n t e n t . . . . . . ( S V / V ) 3 3 . 6 1 3 1 . 1 3 3 7 . 1 6

0 2 C o n c e n t r a t i o n . . . . . . [ % V / V ) 1 5 . 2 0 1 4 . 7 0 1 4 . 7 0

V o l u m e t r i c P l o w r a t e ( D S C F M ) 2 4 8 6 7 2 5 3 5 6 2 3 4 4 6

C O c o n c e n t r a t i o n . . . . . . . . . . . . ( G R I D S C F ) . . . . . . . . . . . . . . . . . 0 . 1 2 2 1 0 . 1 3 2 3 0 . 1 4 7 6 ( M G / O S C M ) . . . . . . . . . . . . . . . . . 2 7 9 . 6 0 3 0 2 . 9 0 3 3 7 . 8 5 (PPM-WET) . . . . . . . . . . . . . . . . . 1 5 9 . 3 4 1 7 9 . 0 6 1 8 2 . 2 4 ( P P M - D R Y ) . . . . . . . . . . . . . . . . . 2 4 0 . 0 0 2 6 0 . 0 0 2 9 0 . 0 0 ( P P M - D R Y @ 7 % 0 2 ) . . . . . . . . . 5 7 9 . 3 1 5 7 7 . 7 0 ,644.44

C O e m i s s i o n r a t e . . . . . ( L B / H R ) 2 6 . 0 2 9 2 8 . 7 5 2 2 9 . 6 5 4


A t r a i l i n g ' < ' symbo l i n d i c a t e s t h a t t h e t r u e v a l u e i s l e s s t h a n o r e q u a l to t h e r e p o r t e d v a l u e

84

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i I I

I I

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I

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I n t e r p o l l Labora to r les (512) 706-5320

€PA M e t h o d 5 D a t a R e p o r t i n g S h e e t I m p i n g e r C a t c h / M i n n e s o t a P ro toco l

Job M Sourca 6 ?4?.'p &c,

- S L U Team L e a d e r . . _ _ -

0

i ! , . .

D i s h No. D i s h T a r e U t . D i s h + S a m p l e U t . S a m p l e U t .

9 9 9

T e s t R u n O F i e l d B l a n k Log Number

3

4

5

I

S a m p l e WC

D i s h No. 9 D i s h T a r e U t . Yv.*Oi 9 D i sh+Sampl e U t . 'f 517.3 Comments 19. COO6 Y 9

Sample W t .

D i s h No. T e s t R u n 9 D i s h T a r e W t .

9 D i s h c S a m p l e W t . Log N u m b e r Comments 9

Sample U t .

D i s h No. T e s t - Run 9 D i s h T a r e W t . Lug N u m b e r 9 D i s h + S a m p l e E t . Comment 6 9 S a m p l e W t .

L I T e s t %Run- 3 -9 5 Log N u m b e r

B l a n k S o l v e n t U t . O . 9

Run 4 R u n 5 R u n 3 Results: F i e l d E l k - Run 1 R u n 2

O , , J 4 5 I .. LSC-03-! . . . . . , . .

0.0 t7.L

I n t e r p o l l L a b o r a t o r i e s (612) 735-6D2a

- T e s t R u n D D i s h No. F i e l d Y l a n l : D i z h T a r e W t . 9

D i s h + S a m p l e W t . 9 Val. of S o l v e n t - r n l Samp le W t . 9

D Log N u m b e r

+ S o l v e n t R e s i d u e Y.0 u g l r n l

T e s t R u n I D i s h No. 2 I V O ~ . of S o l v e n t &S- rnl D i s h T a r e W t . q b , r z s : ‘3

Log N u m b e d 6 3 6 ’ eK f‘ D i sh+Sampl e W t .yb.2s 7 7 9 Comments Sample W t . U . O Z 5 0 9

T e s t 5 R u n z D i s h No. 3 A 2 ‘‘01 - of S o l v e n t L m l D i s h T a r e W t . 37 .go 1q

Log N u m b e r B ’ r 3 D i s h + S a n p l e W t s%&-’iqx 9 Commen t= Samp le W t . 0.ayrc i 9

D i s h T a r e W t . 52. 1201 9 Log N u m b e r -70 P D i sh+Sampl e Ut=& 13 12 D Comments Sample W t . 0.0165 9

4 L ’o l . of S o l v e n t - m l C i s h T a r e W t . 9 Log N u m b s r D i s h + S a m p l e W t . 9 Comments Sample W t . 9

D i s h llo. .3 T e s t s R u n 3 3 V a l . of So lvent lor rnl

T e s t R u n D i s h No.

Tes t R u n D i s h No. 5 L’al. of S o l v e n t m l D i s h T a r e W t . Y

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+Solvant Residue-ug/ml=C ( S i m p l e W t . - 9) ( l a ~ ) I / L ’ o l . o f Sol.- In

EPA Method 5 D a t a R e p o r t i n g S h e e t P r o b o / C y c l o n e W a s h

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EPA Method 5 Data Repor t ing Sheet F i l t e r Grav imet r ics

u . / 8 3 3 a . / g 7 0 I

Job Acs Source 8 - 9 . s ~ p ih~‘ Team Leader 5c(5 Test S i t e CLC.

Date Submitted I I - l L ” f 3 Date o f Test l \ - \ O + 3 Test No. c No. of Runs Completed Date of Clnalysis 11-27-97 Technic ian c- L\.rc5 e -

0,1965

Test - R u n 8 F i 1 t e r No. F i e l d Blank F i 1 t e r Type Log Number 9 Comments F i l te r+Sample W t . 9

Sample W t . 9

F i 1 t e r Tare W t .

0.24 Y 3 1

T e s t c R u n I F i l t e r No. (le12 Log Number I b 36 - A& F F i l t e r Type V”Lf Comments F i l t e r Tare W t . d62D 9

F i l te rcSample W t . 1.01 6 2 9 Sample W t . d i t 5 V t 9

-~ T e r t L R u n 2 F i 1 t e r No. 6013

F F i l t e r Type c ( “ L i * I Log Number Commen t s 9 F i l t e r Tare W t .

F i 1 ter+Sampl e W t . 1,0379 9 Sample W t . d. JF 3 3 9

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Test 7 R u n 3 F i 1 t e r No. s9q1 Log Number - 9 0 F F i l t e r Type q-L F Comments F i l t e r Tare W t . ,&6

F i 1 ter+Sample w t . / . . p Sample W t . 0 1 70

Test- Run - F i l t e r No. Log Number F i l t e r Type Comment s F i 1 t e r Tare W t . 9

F i l ter+Sample W t . 9 Sample W t . 9

Test - R u n F i l t e r No. Log Number F i 1 t e r Type Comments Fi 1 t e r Tare W t . 9

F i l ter+Sample W t . 9 Sample W t . 9

7esul ts: F i e l d Elk. R u n 1 R u n 2 Run 3 R u n 4 Run 5

D-16 II

0

1

2

3

4

5

EPFI M e t h o d 5 D a t a R e p a r t i n g S h e e t Imp inger C a t c h / M I n n e s a t a P r o t o c o l

Saurca C P - C p Dr.c c c T e a m Leader SCr) T e s t i i t e ’S k Lk ., D a t e S u b m i t t e d //-fx-?3 C a t s o f T e s t [ [ -9 -T3

D a t e of Wtaly=is 11-22-’?3 T e c h n i c l a n c-&&u 0..

T e s t I R u n ( 1 D i s h Na. (SL F i e l d B l a n k C i s h T a r e W t . 9 9 .go 5- cf 9 Log Numbet-1636’ 17 D i sh+Sampl e W t . YV. 6-0 9

T e s t l R u n I D i s h No. 158 Log N u m b e r - 7Li D i s h T a r e W t . s O . Z z 27 9 C a m m e n t s D ish+Sample Wt.-<”* LY7? 9

S a m p l e W t . 0 , fJ l -yy 9

Jab Acs

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T o s t R u n 2 D i s h No. [b I Log N u m b e r - s = I D i s h T a r e W t . 4 4 . / 3 Y 5 9 C o m m e n t s DiehcSample W t . Y 9 . 1 S 6 L 9

S a m p l e W t . O . o Z I7 9

T e s t R u n 3 D i s h No. I75 Log N u m b e r - 83 D i s h T a r e W t . 5 3. c i q 9 9 C o m m e n t s D i s h + S a m p l e W t . 53. O Y Y t 9

S a m p l e U t . t l . d l q 3 9 ~ - ~

D i s h No. T e s t __ R u n - Log N u m b e r D i s h T a r e W t . 9 C o m n e n t s D i s h + S a m p l e W t . 9

S a m p l e W t . 9 ~~

Test- R u n - D i s h No. Log Number D i s h T a r e W t . 9 C o n m e n t s D i s h + S a m p l e E t . 9

S a m p l e W t . 9

B l a n k S o l v e n t E t . a*oodlg

Resu l t r : F i e l d B l k . R u n I R u n 2 R u n 3 R u n 4 R u n 5

LSC-03 I- . -

0

1

2

3

4

5

I , 9 , / 6 9 f I 0.17 l t I 0 . l - 0 r-7

Interpol 1 Laboratories (612) 796-6020

€PA Method 5 Data Reporting Sheet Filter Gravimetric5

I

Job A cs Source C P h ~ p D r d P r

Team Leader s C6 Test Site S f 4 C K V Date Submitted 11-1 L -3 Date of Test I I - Y - $ 3 Test No. I No. of Runs Completed 3 Date of Analysis 11-19.93 Technician c. H a l C C S O .

~

Test R u n L Fi 1 ter No. 5 ? 4 & Field Blank Fi 1 ter Type y" 6 F Log Number&?&- 7 3 F Filter Tare Ut. . k 7 ' l y 9 Comments Filter+Sample Wt.&7'/7 9

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Fi 1 ter No. 595.2

Comments Filter Tare Wt. . L ) t Y 6 9 Filter+Sample Wt. l .C?Y'-l 9 Sample Wt. 0, I G9&- 9

Test I R u n L - Log Number -1q r Fi 1 ter Type YSSC,F

T e r t R u n A Fi 1 ter No. s c 7 2

Comments Filter Tare Wt. . ?328 9 Filter+Sample Wt. I . I O q 0 9 Sample Wt. O O f 7 6 Z 9

Test I R u n -

Log Number - 7 5 i Filter Type ' i " 6 F

Fi 1 ter No. fvQ1.S 4°C F Log Number - 7 L t Fi 1 ter Type

Comments Filter Tare Wt. "87 37 9 Filter+Sample Wt. 1~081b 9 Sample Wt. &* 20 rY 9

Test - Run __ Filter No. Log Number Fi 1 ter Type Comments Filter Tare Wt. 9

Filter+Sample Wt. 9 Sample Wt. 9

Test Run - Fi 1 ter No. Log Number Fi 1 ter Type Comments Fi 1 ter Tare Wt. 9


Field B l k . Run 1 Run 2 Run 3 Run 4 Run 5

1 0.2156 I 0.ZZ 31 I 0.257 I LSC-02PR

D-19

I n t e r p o l 1 L a b o r a t o r i e s ( 6 1 1 ) 796-&3213

EPCI Method 5 Data Repor t i ng Sheet Impinger Catch/Minnesota P r o t o c o l

Job qcs sourcz Eqs-1 I'LL+ Icr Team Leader D Q Test 'Si te S k L k Date Submit ted I - I 2-r( 3 Este o f Test 11 .1,-q f

Test P!o. 10 No. o f Huns Completed 3 Date of A n a l y s i s \ \ - Z ? - ? s Techn ic ian C.HL\~C - SO"

Test L R u n Q D i s h No. i F i e l d Blank D i s h Tare W t . S L . q C ? $ 9 Log Number /LxL- l lLr Dish+Sample Wt.51.97 0 0

Comments Sample W t . O.b-W( 9

T e s t x R u n L D i s h No. 6 Log Number - 113 - r D i s h Tare W t . Y& ..1706 9

P T e s t ( D R u n L D ish No. 7 Log Number -11q r D i s h Tare W t . 5 @ . O \ ? Z 9 Comments Dish+Sample U t . ~ ~ O l 5 ~ 9

Sample W t . 0,OJ / b 9

Tes t [ O R u n L D i s h No. 12 Log Number -\\Sr D i s h Tare W t . 9. 1q 8CI 9 Comments Dish+Sample W t . Y f . l S J / 9

Sample W t . d.oel7 9

Log Number D i s h Tare W t . 9 Comments D i sh+Sample ' W t . 9

Sample W t . 9

9

9 Comments Dish+Sample W t . ' 7 3 5 Sample W t . 0.cJn.l y

Test- Run __ D i s h No.

0

1

2

3

4

5 Tes t __ R u n - Dish No. Log P!umber D i s h Tare W t . 9 Comments D i sh+Sampl e et. 9

Sample W t . 9

Blank So lvent U t . O . O U L J / ~

R e s u l t s : F i e l d B l k . Run 1 R u n 2 R u n 3 R u n 4 R u n 5

I n t e r p o l l L a b o r a t o r l r s (612) 786-tOZ0

EPC\ Method 5 D a t a Reportxng Sheet Probo/Cyclone Wash

Job A c s Source ea,+ f ‘ ~ L 4 CR2* \ cr Team Leader b b Test S i t e S+p,k Date Submit ted l l - b - 3 Date of Test N-\\-%3

Transpor t Leakage I X E 3 0

Test No. 10 No. of Runs Completed 3 Date of A n a l y s i s 11-r.i-43 Techn ic ian c . N c \ q u o s .

n l So lven t Ac*L,,U

D-27

- Test R u n 9 GI =h m. F i e l d B l a n k Dish Tare W t . 9 Log Numbar D i sh+Sampl e W t . 9 ‘Jol. o f Solvent- m l Sample W t . 9

Test 10 Run \ C i s h No. 6 6 V o l . o f So lven t 2so m l D ish Tare W t . %?, 3 3 $9 g

Comments Sample W t . d*# 71 3 g

Test 10 Run L D i s h No. 67 ‘201. of So lven t 175 m l D ish Tare W t . YCI. 5395 3 Log Number - e Dish+Sample Wt.$%booS 9 Conmen t 5 Sample W t . u,b 6 6 0 9

+Solvent Residue ’dsb u q / m l

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5

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Interpol 1 Laboratories (512) ~ ~ L , - ~ Q z o

EPCI Method 5 Data Reporting Sheet Fi 1 t er Gr av i met r i cs

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J o b 4 CS Team Leader D D Test Site Date Submitted / l - l z - 9 4 Date of Test [ \ - \ \ -93 Test No. \O No. of Runs Completed 3 Date of Analysis 11-zq-q 3 Technician '& U d r ~ S c k

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0. //Ut 0. i o 1 2

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Test Run Fi 1 ter No. Log Number Fi 1 ter Type Comments Filter Tare Wt. 9


Results: Field Elk. Run 1 Run 2 Run 3 Run 4 Run 5

I n t e r p o l l L a b o r a t o r i e s ( 5 1 1 ) ?SA-5320

EPA Method 5 D a t a R e p o r t i n g Sheet Imp inger C a t c h / M i n n e s o t a P r o t o c o l

Job S o u r c a U Z S , PtI\LS. C C O l P /

Tsam Leader D(3 T e s t 3 i t e S h C k I l-l-L-73 E a t e of Tes t - 11-q 3 D a t e S u b m i t t e d

T e s t PJo. 13 rlo. of Huns Completed 3 D s t e of f i n a l y s i s \ \ -Zq-q3 Techn 1 c i an c- HLttcrO-

u. 0334 0,oo 2 I 0 , O O I v

0

1

2

3

D-29

Test- R u n 0 D i s h No. F i e l d B lank D i s h T a r e W t . 9 L o q Number D ish tSamp le W t - 9 Comments Sample W t . 9

T e s t L R u n - D i s h N o . 3 ) Log Number l b x b ' 120 T D i s h T a r e W t . Y5,2710 9 Comments Dish+Sample W t . Y5.2.72-5 9

Sample W t . 0. ou 15 9

T e s t L R u n z D i s h No. 3 s Log Number -\z\ T D i s h T a r e W t . 51.o?lZ 9 Comments D i sh+Sampl e U t . Sl.09Y7 9

Sample W t . 0 , u03s 9

T e s t \ 3 R u n L D i s h No. 3 6 Log Number - 1 ZZX D i s h T a r e W t . 43.S635 9 Comments Dish+Sample W t . q 3 . 5657 9

Sample W t . d * , . W L Z 9

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4

D-29

5

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D i s h No. T e s t - R u n - Log Numbor D i s h Ta re W t . 9 C o m m e n t s D i sh+Sampl e ' W t . 9

Sample W t . 9 ~ ~ _ _ _

D i s h No. Test- R u n - Log Number D i s h Ta re WC. 9 Comment s Dish+Sample W t . 9

Sample W t . 9

Results: F i e l d B l k . Run 1 R u n 2 R u n 3 R u n 4 R u n 5

-

I 1

Q . 2 5 s - V u. 2L9l

0

1

2

i 3

4

5

D-30 SC-01 Y R 08 L Y 6 B

.

I n t e r p o l 1 L a b o r a t o r i e s ($12) 7 S b - t O Z O

€PA flethod 5 D a t a R e p o r t i n g S h e e t P r o b o / C y c l o n e Wash

Job .4c5 Source b ~ \ f p c\\c+ C-ol<r T s a m Lsader DB T e s t S l t e S C" ck D a t e S u b m i t t e d 1)-17-33 Date of T e s t 11-1\- 4 3 T e s t No. I3 No. of Huns C o m p l e t e d '3

ansp sport L e a k a g e e O an C a t a of C n a l y s i s / I -zq-q3 T e c h n i c i a n c, H d j u o h

m l So lven t A'4-4, YP

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Tes t I3 R u n L F i e l d B l a n k Log N u m b e r 16 36 - I I 4 f V a l . o f S o l v e n t - m l *So lvent R e s i d u e x u g / m l

G r s h Mo. f 0 2 D i s h T a r e !4 t .L tq , 3 2 Y 6 9 D i s h + S a m p l e W t Y Y . 3 250 9 Samp le W t . 0. uuo Y 9

T e s t 13 R u n V o l . o f S o l v e n t ZSO r n l Log N u m b e r -1L0 e

'3 9

- C i n h No. I IO D i s h T a r e W t . L

D i sh+Sampl e U t .?i.\:iJ C o m m e n t s Sample W t . O,Z%l 9

~~ ~ ~

T e s t 13 R u n 1 D i s h NO. V I 0

Log Plumber - 9 D i s h t S a m p l e wt50.81 b b J Commen t 5 S a m p l e W t . 0.25qS 9

'.'ol- o f S o l v e n t z m l D i s h T a r e U t . ' i ~ . S S - f r 3

T e s t 11 R u n ? V o l . of S o l v e n t c m l

D i s h rlo. G I b D i s h T a r e W t . 5O0.9Zs3 Y

L o 3 t l u m b e r -127-4 Di s h + S a m p l e W t SJ.1-I 6 b D C o m m e n t s S a m p l e W t . 0. rv77 9

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T e s t R u n ___ C i s h No. '201. o f Solvent- m l D i s h T a r e W t . Y Log Number Di s h + S a m p l e W t . D Coinmen t s Sample Ut. 4

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Interpol1 Laboratories (612) 756-61320

EPA Method 5 Data Reporting Sheet Filter Gravimetrics

I cc Job A c s Source LJ e 3 4 PLI\L+ - Team Leader OB Test Site S k L k Date Submitted I I - I 2 e 9.3 Date of Test I I - \ \ -13 Test No. 13 No. of Runs Completed 3 Date of Analysis I \ - L b - % s Techn i c i an e. h d . 5 ~ C L

T e s t A R u n Q Filter No. 5 r b l Field Blank Filter Type '4 ' 'bi Log Number 163b- 114F Filter Tare Wt. a q 1 7 n 9 Comments Filter+Sample Wt. . $ 3 Z @ 9

Sample Wt. 0.MJJd 9

T e s t k R u n \ Filter No. ( t w o 7 Log Number - I / 0 F Fi 1 ter Type V " 6 F Comments Filter Tare Wt. .6505 9

Fi 1 ter+Sample Wt. .93 I 6 9 Sample Wt. d . o S / I 9

T e s t L R u n Fi 1 ter No. & 0 0 b Log Number - I 2 \ f Filter Type L( '* 6 F Comments Filter Tare Wt. , (rs-lr 9

Filter+Sample Wt. ,40 31 9 Sample Wt. u, 0 r6rq 9

T e s t k R u n 3 Filter No. 1190 4 Log Number - 1 z r F Filter Type q ' " 4 F Comnen t s Filter Tare Wt. a t 6 2 9 9

Fi lter+Sample Wt./.@OY'l 9 Sample Wt. o.lyro 9

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I n t e r p o l l L a b o r a t s r l e s (512) 796-CJ213

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a . 0 0 1 0 D-32 LSC-03 GP

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Fi 1 ter+Sdmpl e W t - 9 Sample Wt. 4

R e s u l t s : Field Elk. Run 1 Run 2 Run 3 Run 4 Run 5

I 17-34

I n t e r p o l l Laboratories ( 6 1 2 ) 786-6020

EPA Method 6 S u l f u r Dioxide Ca lcu la t i on Data Sheet'

Job (4- cs Source A ?u/fi A*.,,, Team leader 5 i f i Test S i t e <-k '

Date submit ted / / - I t r L i 3 Date of Test / / - I ) + > Test Number Y No. of Runs Completed 3 Date o f ana lys is I / - t ? - l f + Techn i c i an c. Jc I,+<.(. . MEQ Ca7culat ion

DF = D i l u t i o n Factor

Vs = Volume o f T i t r a n t SamDle ( m l ) MEQ DF N ( V s - V b ) Vt N = Normali ty o f T i t r a n t

V. Vb = Volume of T i t r a n t Blank i r n i j Vs = F ina l Volume of sample (ml ) V. = Volume o f A1 i q u o t (rnl )

Water Catch

T e s t L R u n d

Tes t Z R u n 2

T e s t L R u n 3

3X Peroxide Catch

T e s t L R u n - /

T e s t q R u n L

T e s t x R u d -

T o t a l UEQ Per Run:

Comments:

1 Form to be used i n con junc t ion w i t h combination method 5 and 6 train. S-42 1 A

I n t e r p o l 1 Laboratories ( 6 1 2 ) 786-6020

EPA Method 6 S u l f u r Dioxide Ca lcu la t i on Data Sheet'

Job Kcs Source 6 Z+ .Lye, Team leader :j i- 13 Test S i t e >+a& k Date submit ted J I - I I % 3 Date o f Test I ) -lo 9 3 Test Number 5 No. o f Runs Completed -4 Date o f ana lys is /1-'-?-?3 Technician c. */p... -

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MEQ = DF N ( V a - v b ) VE N = Normali ty o f T i t r a n t V. Va = Volume o f T i t r a n t Sample (m1)

Vb Volume of T i t r a n t Blank ( m l ) V. = F ina l Volume o f sample (m1) V. Volume o f A l i q u o t (m l )

Water Catch

Test Z R u n L

Tes & R u n 2

T es t z R u n - 3

).% Peroxide Catch

Tes t r R u n - i

T e s t x R u n 2

Te s & R u n 3

Tota7 HE0 Per Run: Test- Run- 2.57 MEQ

Test- Run- L = 2 . 2 Y MEQ

T e s t r R u n A = 1 . 9 2 MEQ

1 Form to be used i n con junc t ion w i t h combination method 5 and 6 t r a i n . S-42 1 A

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I n t e r p o l l Laboratories ( 6 12 ) 786-6020

EPA Method 6 S u l f u r Dioxide C a l c u l a t i o n Data Sheet’

Job Acs Source L P-Ip Dcy<, Team leader - 5 ~ 3 Test S i t e S%t= Date submi t ted 11-1-43 Date o f Test I 1 - ? - ’ i >

Test Number I No. o f Runs Completed 3 Date of ana lys i s / l # l ? - ’ l 3 Technician C-H 4 2 0

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Water C a t c h

T e s t l R u n l

T e s t L R u n L

T e s t \ R u n&

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T e s t L R u n L

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T e s t l R u n i - - 2, 5.0 MEQ

T e s t l R u n L = 1.43 MEQ

T e s t I R u n L = 3 s o r MEQ

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Documents

AP42 chapter 9 reference...4500 Ball Road N.E. Circle Pines, Minnesota 55014-1819 TEL: (612) 766-6020 FAX: (612; 786-7854 RESULTS OF THE NOVEMBER 9 - 11, 1993 AIR EMISSION TESTING