BUREAU OF INDIAN STANDARDS (Southern Regional Office) · 2018. 12. 10. · IS 101(Part 4/Sec 3):1988 Part 4 Optical Tests on paint films ,Sec 3 Light fastness test (third revision)

BUREAU OF INDIAN STANDARDS

(Southern Regional Office)

Our Ref: 60/CM 1 10 03 2014

Subject: Preparation & Review of Product Manuals for Product Certification

This has reference to CMD-I’s circular CMD-1/31 dated 11 Nov 2013 on the above subject.

In this connection, the draft Product Manual in respect of IS 5410: 1992 allotted to SRO has been prepared. The same is attached herewith for hosting on the BIS Intranet for inviting suggestions and comments for a period of 15 days.

The comments may be sent to SRO/BNBO.

(E. Devendar)

Sc.G & DDGS

HITSD

5410/Draft Manual

DRAFT MANUAL FOR CERTIFICATION OF CEMENT

PAINT AS PER IS 5410

(FIRST ISSUE)

BUREAU OF INDIAN STANDARDS MANAK BHAWAN, 9, BAHADUR SHAH

ZAFAR MARG, NEW DELHI – 110002

5410/Draft Manual

Amendment Sheet S.No. Amendment No Reference no Date of Issue Date of implementation

5410/Draft Manual

FOREWORD . The present manual attempts in highlighting various requirements and providing handy and significant information related to “Cement Paint”. It elaborates the principle raw materials, manufacturing processes and desired controls, involved inspection and testing as need be practiced by BIS licencees and further monitoring thereof expected to be exercised by BIS Inspecting Officials during planned visits to those units and monitoring of BIS Certification Marks activities. Different tests as contained in relevant standards and referred standards thereof need be carried out at the licensee’s laboratory by the visiting officer with knowledge and background possessed by the individual. Since such inspecting officers come from different educational and technical background and may not be experienced or even having basic knowledge in the relevant field or product category, such documentation of sectoral manual aims in providing basic inputs and all essential aspects with the expectation of bringing uniformity of vision and enabling adoption of rational practices by concerned BIS officials during their visits for inspections to such sector as well as follow up actions

IS 5410/Draft manual

5410/Draft Manual

TABLE OF CONTENTS Section No/ Title Page no Para No 0 Amendment Sheet 0 Foreword

Section 1.0 Product Description Para 1.1. Latest Indian Standard Number with Product Title and

Number of Amendments Para 1.2 List of referred Indian Standards Para 1.3 Check-list for submission of an application for grant

of licence Section 2.0 Raw materials/ Components

Section 3.0 Manufacturing Process and In- Process Quality Controls Para 3.1 Manufacturing Process Para 3.2 Infrastructure for production

Section 4.0 Certification criteria Para 4.1 Identification of Critical Requirements of the Indian

Standard Para 4.2 Scheme of Testing and Inspection Para 4.3 Marking fee Rates Para 4.4 Grouping guidelines Para 4.5 Guidelines for writing Scope of Licence

Para 4.6 Guidelines for inclusion of new varieties Para 4.7 Sample size required to be sent to independent lab for

Testing Para 4.8 Manner of sealing of samples Para 4.9 Procedure of disposal of remnants of Tested Samples Para 4.10 Procedure to be followed if sample does not meet the

specified norm as per Indian Standard during regular Production

Section 5.0 Inspection and Testing Para 5.1 Packing Material for packing/dispatch of samples Para 5.2 List of test equipment/ Facilities with requirement and

frequency of Calibration Para 5.3 Status of Test Facilities in BIS labs/OSLs Para 5.4 Grant of Licence Para 5.5 Details of tests to be carried out in the factory

APPENDIX 1 : SCHEME OF TESTING AND INSPECTION


SECTION – I

1.0. Description of product: CEMENT PAINT

Cement paint is covered under powder paints and is applied to either exterior or interior masonry cemented surfaces. It gives the following excellent properties to any masonry surface.

Cement paints gives very good protection from the ultraviolet rays present in sun rays.

It also gives very good protection from severe climatic conditions like rain, heat, water, humidity.

It prevents growth of fungus and bacteria on masonry surfaces. It also hides out various surface irregularities, hair lining, roughness etc...

thereby giving smooth, pleasing and matt finish on all masonry surfaces. 1.1. Latest Indian Standard Number with Product Title and Number of

Amendments: Latest Standard: IS 5410 Title: Cement Paint No. of Amendments:

1.2 List of referred Indian Standards for raw materials/ components and test methods: The following standards contain provisions which through reference in this text, constitute provisions of this standard. At the time of publication, the editions indicated were valid. All standards are subject to revision and parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the standards indicated below:

IS No. Title

IS 101(Part 1/Sec 1):1986

Methods of sampling and Tests for paints varnishes and related products. Part 1 Test on liquid paints(general and physical) Sec 1 Sampling (Third revision)

IS 101(Part 2/Sec 1):1987

Part 2 Test on liquid paints(Chemical examination) Sec 1 Water Content (Third revision)

IS 101(Part 2/Sec 2):1987

Part 2 Test on liquid paints(Chemical examination) Sec 2 Volatile matter (Third revision)

IS 101(Part 3/Sec 4):1989 Test on paint film formation, Sec 4 Finish (Third revision)


IS 101(Part 4/Sec 2):1989 Part 4 Optical Tests on paint films ,Sec 2 Color (third revision)

IS 101(Part 4/Sec 3):1988 Part 4 Optical Tests on paint films ,Sec 3 Light fastness test (third revision)

IS 101(Part 6/Sec 2):1990 Part 6 Durability Tests ,Sec 2 Keeping properties (third revision)

IS 269:1976 Ordinary and low heat Portland cement.

IS 650: 1966 Standard sand for testing of cement

IS 1070:1992 Reagent grade water – Specification (Third Revision)

IS 1303:1983 Glossary of paints relating to paints(second revision)

IS 1650:1973 Colors for building and decorative finishes


1.3 Check-list for submission of an application for grant of licence: The following check-list is required to be submitted with all the applications for grant of BIS licence under the Product Certification Scheme of BIS. Please tick (√) in the relevant box.

Whether applied under: Simplified Procedure Normal Procedure

Note: Refer BIS website or details of “Simplified Procedure” and “Normal Procedure” for grant of licence. No. Check-point Requirement Observations Page

No.

General Is the application form completely filled?

Name & Is the name and address of applicant Address (manufacturing unit applying for licence) same in the application as given in the attached document of Central/State Government Status of a. Has it been indicated whether the applicant is Applicant a large scale or small scale unit?

b. In case the applicant is a small scale unit, does the applicant hold valid Registration Certificate from the Local / State authority or from a Chartered Accountant, and is the certificate attached. c. Has it been indicated whether the applicant is a Public Sector or a Private Sector company? IS No. & a. Has applicant recorded the applicable Indian Varieties Standard with correct title of the Standard? b. Where applicable, has applicant mentioned designation, grade, type, variety, size, etc., of the product for which the BIS licence is sought? History a. Where applicable, has the applicant provided

information regarding earlier BIS licence(s) held

by them and / or cancelled in the past? b. Where applicable, has the applicant provided information regarding BIS licences currently held by them?


Signature a. Is the application signed by the CEO of the applicant? b. In case the application is signed by a person other than the CEO, is the application signed by the authorized signatory of the applicant and his authorization is attached by the authorized signatory? Machinery a. Does applicant possess requisite manufacturing infrastructure to manufacture the product as per the Indian Standard? b. Is installed capacity of production indicated in the application? c. Does applicant have all machineries installed as per manufacturing process at the applicant’s manufacturing premises? d. If answer to ‘c’ above is no, does the applicant outsource any of its manufacturing processes and possesses valid agreement(s) with other manufacturing units for the outsourced processes and traceability of material, thus produced, etc.? e. If answer to‘d’ above is yes, does the applicant has any control over such outsourced activity? Are these outsourced process will ensure testing the quality of final product for all requirements at the applicant's manufacturing premises? Test a. Does applicant possesses requisite test Equipment facilities in-house as per the relevant Indian & Standard at its factory address?

Calibration

b. Are valid calibration certificates for relevant test equipment attached are complete and valid at least 3 months after the date of recording? c. If reply to ‘a’ above is no, does applicant have arrangement with a BIS recognized outside lab for testing of the requirements for which it does not possess test facilities in-house? Is the consent letter as attached by applicant in this regard in order?


Note: Relaxation in in-house test facilities maybe allowed on submission of proper justification for requirements which are obligatory to gettested and for which frequency of testing, as prescribed in the relevant scheme of testing an inspection (STI),is, normally, one month or

more. QC personnel Does the applicant employ qualified & experienced Quality Control (QC) personnel on permanent basis and possess documentary evidence to establish the same? Are the copies of the qualification certificates and appointment letters of the QC personnel are in order Raw Materials Where ever requirements for raw materials/ and components used in the manufacturing of the Components product are specified in the standard, do test reports/suppliers’ test certificates, as submitted by the applicant show that these requirements are met as per the standard? Plant Layout Does copy of the plant (applicant manufacturing premises) layout clearly indicates locations of manufacturing machinery, laboratory, office, workshop, amenities, storage area, etc.? Test Report(s) a. Is the attached test report of in-house or from independent laboratory cover all requirements of the Indian Standard and is passing in such requirements? b. In case the application is filed under “simplified Procedure” is the test report(s), in original, as submitted a) from BIS or its recognized laboratories? b) the test report is not older than one month from the date of submission of application, c) covers all the requirements of the standard, and d) passes in all such requirements. Undertaking In case application is under simplified procedure, an undertaking shall be obtained from the applicant on his letter-head that the licence if granted against his application shall be put under Stop Marking by BIS if the verification sample(s) (any sample including the long duration test samples) drawn during visit of the BIS officer prior to grant of licence fail to conform to the requirements of relevant Indian

Standards. The licensee shall take necessarycorrective actions


and inform the same to BISalong with fresh samples (of rating/size/varietywhich facilitates verification of corrective actions on the reported failures) manufactured after taking the corrective actions

The resumption of marking in such cases shall be allowed only on the basis of independent satisfactory Test Reports of the fresh samples offered (including long duration tests where failures were in long duration tests). In case the fresh sample drawn by BIS for independent testing fails, or the licensee does not inform corrective actions taken and does not offer improved samples within 1 month of the date of Stop Marking, the licence shall be processed for cancellation and no further chance would be given to the licensee Application Has applicant paid requisite application fee of Fee Rs. 1000/-, in equivalent US$ (Rs. 1000/- plus 12.36% tax for applicants from SAARC countries)? Signature Is the application countersigned by the applicant’s Authorized Indian Representative? Nomination a. Has ‘Nomination Form’ of ‘authorized Indian representative (AIR)’ in the prescribed format on the firm’s letter-head, duly signed by the authorized signatory of the applicant and the AIR or the authorized person of the company of the AIR, been submitted with the application? b. Is the authorization to the signing authority to sign the ‘Nomination Form’ on behalf of the Indian Co. also submitted? c. Is address of the AIR in the ‘Nomination Form’ complete and evidence of nationality, address proof, contact details like phone / fax numbers and e-mail address of the AIR submitted? d. In case AIR is an Indian company, have copies of registration certificate and/or Memorandum of Articles along with authorization letter from top management of the Indian company in the name of a person acting as the AIR also been submitted with the


application? e. Has copy of Agreement between applicant and the Indian company / individual, nominated as the AIR, also been submitted? f. Are copies of valid RBI clearance certificate for Indian Office / Branch of the applicant or any other relevant document for establishment of its Office / Branch in India provided? Language Are English translations of all the documents, which are in languages other than English, also available? Preliminary Does the applicant undertake to bear inspection Inspection / charges for all the inspections to be carried out Visit Charges by BIS at its premises before the grant of licence, including the arrangements and costs incidental thereto for travel and stay, visa, insurance, etc.? Translation Does the applicant undertake to arrange, if Facility required, services of translator (for translation in English) during the visits of BIS officers to its factory? Agreement Does the applicant agree to sign a legally binding agreement with BIS in the prescribed format? Indemnity Does the applicant agree to submit an Indemnity Bond Bond to BIS in the prescribed format? Performance Does the applicant agree to furnish a Bank Performance Bank Guarantee to BIS of US $ Guarantee 10000/- (from a bank having its branch in India) in the prescribed format on the letter-head of the bank?


SECTION – II 2.0 List of Major Raw Materials:

Cement Paint is manufactured by mixing the following raw materials . a) Ordinary Portland Cement (binder) - MIN 65% by mass

b) Hydrated Lime - MAX 25% by mass

c)

d)

e)

f)

g)

Pigments*

Extenders**

Accelerators***

Water repellents****

Fungicides*****

-

In suitable proportions to

produce a material to satisfy

the requirements of IS 5410

h) Alkali Rsistance Solvent******

Note:


*The color of the cement paint is based on the color and quantity of the pigments added

to it. The prime pigments may be Titanium Di Oxide, Carbon Black, Phthalocyanin Blue,

Phthalocyanin Green, Red Oxide etc…

**The common extenders used are whiting, china clay in suitable quantity.

*** Calcium chloride is the most common extender used in cement paint industry.

**** Calcium / Aluminium stearate or Stearic Acid is used as water repellents.

***** Ethylene Diamine (EDA) fungicides are added in a very small quantity in the

formulation if needed.

****** Solvents like 2 Ethyl hexanol is added as alkali resisting pigment

SECTION – III 3.0 Manufacturing Process and In-process Quality Controls: 3.1 Manufacturing Process:

ORDINARY PORTLAND CEMENT

HYDRATED LIME

MIXING ALL WEIGHED INGREDIENTS IN A BALL MILL UNTIL DESIRED FINENESS AND DISPERSION IS ACHIEVED


PIGMENTS + ACCELERATORS+ WATER REPELLENTS+ EXTENDERS+ FUNGICIDES + ALKALI RESISTING SOLVENT (in suitable proportions )

If pass if fail

PACKING IN SUITABLE POLY ETHYLENE BAGS

RE-FORMULATE AS PER STANDARD OR REJECT

TESTING SAMPLES IN LABORATOTY AS PER IS 5410


3.2 Infrastructure for production:

SNo Name of Machine Capacity Make Date of purchase Quantity

1 WEIGHING MACHINE

As per production capacity

2 BALL MILL WITH BALLS 3 BAG STITCHING MACHINE 4 STORAGE SILO/BIN

SECTION – IV 4.0 Certification Criteria

4.1 Identification of Critical Requirements of the Indian Standard: (To be provided by a committee comprising the concerned officer from CMD, Member-Secretary of the concerned technical committee and an officer from central laboratory)

4.2 Scheme of Testing and Inspection: DOC: STI/5410/3/JAN 1994 (Please see Appendix-D)

4.3 Marking fee Rates Manufacturing Minimum marking Unit Unit rate Status of Industry fee per year

Large Scale Rs. 36200/- 100 Kilo gram Rs. 8.60

Small Scale Rs. 29200/- 100 Kilo gram Rs. 8.60

4.4 Grouping guidelines: There is no grouping guidelines exists as on date to consider Grant of license/inclusion of new varieties for this product.

4.5 Guidelines for writing Scope of Licence: Scope of the license shall contain the name of the product and relevant ISS 4.6 Guidelines for inclusion of new varieties: No any new variety exists

4.7 Sample size required to be sent to independent lab for testing: For complete testing 2 numbers of individual closed pack/bag of 1 kg is required. It shall be ensured that adequate sample is available for testing (and retesting wherever


needed) the requirements for which it is desired to be tested. The technical auditor shall anticipate all requirements of the laboratory on the basis of' the relevant Indian Standards and STI, and draw the required size of the sample. Counter samples of identical size shall be drawn and left with the applicant / licensee. 4.8 Manner of sealing: 4.8.1 Sealing - The individual packs/bag (2 nos x 1 kg ) shall be closed/stitched firmly and tied with a rope/thread. Then it shall be properly sealed with official seal on the knot of the rope/thread so that no substitution or tampering with the contents is possible subsequently. For the purpose of sealing, the technical auditor should always carry the brass seal, red wax, candle, matchbox, rope/ thread roll. 4.8.2 Packing - The technical auditor shall take every precaution to ensure that the sealed samples (2 x 1kg) is packed firmly in a durable packing material like wooden cardboard or carton box with expanded polystyrene or any other shock absorbing material to withstand hazards during handling and transportation. Wherever feasible, all original markings indicating the origin of the product would be removed / defaced from the sample with the objective of concealing the identity of the origin from the testing laboratory. Labelling- The sample shall be labeled to indicate (a)Cement paint (b)the relevant Indian Standard with its year (IS 5410) (c) Shade (d) quantity of sample(2x 1 kg); (e) batch No./Control Unit No./date of production (f) Sample code. Labels . 4.8.3 shall be tagged to the sample or on the Packing. 4.9 Procedure of disposal of remnants of Tested Samples: These remnant samples are non returnable and shall be disposed off. 4.10 Procedure to be followed if sample does not meet the specified norm as per Indian Standard during regular production: In case of sample does not meet the requirements specified in Indian standard, such control unit i.e. Batch/lot shall not be marked. Those rejected batches/lots shall be destroyed, A separate record shall be maintained giving information relating to the rejection of the production not conforming to the requirements of the specification


SECTION – V 5.0 Inspection and Testing 5.1 Packing Material: The following materials shall be available with the firm for packing, sealing and dispatch of samples. The product shall be packed in polyethylene bags in suitable plastic or metal containers. 5.2 List of test equipment/ Facilities with requirement and frequency of Calibration: (To be prepared / provided by Central Laboratory)

5.3 Status of Test Facilities in BIS labs/OSLs:

Technical auditor shall ensurestatus of laboratory and availability of testing facilities at the time of visit from BIS intranet. 5.3.1 Testing Charges: (To be provided by Central Laboratory) 5.3.2 Approximate time required for testing by BIS labs/OSLs: (To beprovided by Central Laboratory) 5.4 Grant of Licence: Grant of licence would be on the basis on independent testing. 5.5 Details of tests to be carried out in the factory: Possible tests to be done within the duration of the visit. 5.5.3 In case of Market samples:

The laboratory shall conduct maximum possible tests in order to assess quality of the product or the tests prescribed in the test request. 5.5.4: In case of Raw Material:

As Portland cement is one of the main raw materials and it is a product under mandatory certification, it may be drawn and treated as market sample to assess the performance of the particular licencee.

APPENDIX-1: SCHEME OF TESTING AND INSPECTION

Doc.STI/5410/3 Jan 1994

SCHEME OF TESTING AND INSPECTIONFOR CERTIFICATION OF CEMENT PAINT

ACCORDING TO IS 5410:1992 (First Revision)

1. LABORATORY: A laboratory shall be maintained which shall be suitably

equipped and staffed where the tests shall be carried out in accordance with the methods given in the specification.

1.1 All the testing equipment shall be periodically checked and records of such

checks shall be maintained. 2. TEST RECORDS: All records of tests and analysis shall be kept in suitable

forms approved by the Bureau. 2.1 Copies of any records or charts that may be required by BIS shall be made

available at any time on request. 3. QUALITY CONTROL: It is recommended that as far as possible, Statistical

Quality Control (SQC) methods may be used for controlling the quality of the product during production as envisaged in this scheme, See IS:397 (Part 1)-1972, IS:397 (Part 2)-1985 and IS 397 (Part 3):1980.

3.1 QUALITY SYSTEMS: As far as possible the provisions of IS 140003:1988

“Quality systems – Model for Quality Assurance in final inspection and Test” may be complied with.

4. STANDARD MARK: The Standard Mark, as given in Column (1) of the First

Schedule of the license shall be printed on each container or on the label applied to the container; provided always that the material in each container on which this Mark is thus applied conforms to every requirement of the specification.

5. MARKING: In addition, the following information shall be given on each

container on or the label applied to it:

a) Name of the material b) Indication of source of manufacture; c) Mass of the material in the container; d) Control unit number; and e) Month and year of manufacture.

6. LEVELS OF CONTROL: The tests as indicated in Table 1 and at the levels of

control specified therein shall be carried out on the whole production of the factory covered by this scheme and appropriate records and charts maintained in accordance with paragraph 2 above. All the production which conforms to the Indian Standard and covered by this license shall be marked with Certification ark of the Bureau.

Doc.STI/5410/3 Jan 1994

6.1 CONTROL UNIT: For the purpose of this scheme, the entire quantity of the cement Paint produced in a batch mixer at a time shall constitute a control unit.

6.2 The control unit shall be considered fit for the purpose of marking if sample taken

from the control unit and tested as in Table 1, is found to conform to all the relevant requirements of the specification.

6.3 For composition, initially each control unit shall be tested till three consecutive

control units are found to be conforming to the specification requirements. From the subsequent production every tenth control unit shall be tested. Whenever a failure is encountered, the control unit shall not be marked and from the subsequent production, each control unit shall be tested till three consecutive control units are found to be conforming to the specification requirements whereupon the original frequency of testing every tenth control unit may be resumed.

6.4 In case of failure of the sample from a control unit to conform to any of the

requirements of the standard the entire material in the control unit shall be considered as unfit for the marking. The material however could be reprocessed and marked provided the sample drawn from the reprocessed control unit meetsall the requirements of the specification.

7. RAW MATERIAL: Routine analysis of various raw materials going into the

manufacture of cement paint shall be made on each lot received in the factory and appropriate records maintained. Alternatively raw materials of known composition may be used.

8. In respect of all other clauses of the specification, the factory shall maintain

appropriate controls and checks to ensure that their product conforms to the requirement of these clauses.

9. REJECTIONS: A separate shall be maintained giving information relating to the

rejection of paint not conforming to the specification and the method of its disposal. Such material shall not be stored together with that conforming to the specification.

10. SAMPLES: The licensee shall supply, free of charge, the samples required in

accordance with Regulations of the Bureau of Indian Standards from his factory or godown. BIS shall, however, pay for the samples taken by it from the open market.

11. REPLACEMENT: Whenever a complaint is received soon after the goods with

certification Mark have been purchased and used and if there is adequate evidence that the goods have not been misused, defective goods shall be replaced free of cost by the licensee in case the complaint is provide to be genuine and the warranty period (where applicable) has not expired. The final authority to judge conformity of the product to the Standard shall be with BIS.

Doc.STI/5410/3 Jan 1994

12. STOP MARKING: The marking of the product shall be stopped under intimation to BIS, if, at any time, there is some difficulty in maintaining the conformity of the product to the specification or the testing equipment goes out of order or if directed to do so by BIS for any reason. The marking may be resumed as soon as the defects are removed or when the Bureau gives the permission to do so. The information regarding resumption of marking shall also be sent to BIS.

13. PRODUCTION: The licensee shall send to BIS as per the enclosed proforma, a

statement of the quantity produced, marked and exported by him and the trade value thereof during the half-year ending 30 June and 31 December. This Statement is required to be forwarded to BIS on or before the 31st day of July and January for the preceding half-year.

Doc.STI/5410/3 Jan 1994

IS 8249:1994 ZINC SULPHATE HYPTAHYDRATE AGRICULTURAL GRADE

TABLE 1 LEVELS OF CONTROL (Para 6 of the Scheme of Testing and Inspection)

TEST DETAILS LEVELS OF CONTROL

Test Method Clause Requirements

Clause

Reference

No. of Samples Frequency

Remarks

4.1

Composition.

Annex IS 5410:1992

One

Every 10th control unit

Please refer to item 6.3 of the S.T.I.

4.1.1

Freedom from organic binders.

Annex C -do-

-do-

Each control unit.

4.2

Preparation for use.

4.2 -do-

-do-

-do-

4.5 & Table 1

Driving time and recoating properties.

Annex E -do-

-do-

-do-

-do-

Finish

IS 101(Part 3)/Sec 4:1989

-do-

-do-

-do-

Residue on sieve.

Annex F IS 5410:1992

One

-do-

-do-

Resistance to dry rubbine

Annex G -do-

One

-do-

-do-

Water repellancy

Annex H -do-

One

-do-

-do-

Pot life of mixed paint.

Annex J -do-

One

-do-

-do-

Keeping properties.

IS 101 (Part 4)/Sec 2:1990

One

Once in six months.

-do-

Fastness to light.

IS 101 (Part 4)/Sec 3:1988

One

Once in three months.

4.4

Durability

Annex D IS 5410:1992

One

Once in a year between last week of January and first week of March

Doc.STI/5410/3 Jan 1994

Documents

BUREAU OF INDIAN STANDARDS (Southern Regional Office) · 2018. 12. 10. · IS 101(Part 4/Sec 3):1988 Part 4 Optical Tests on paint films ,Sec 3 Light fastness test (third revision)