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PROLAS 1 Project PROLAS - Final Report Annex containing additional material by Alexander Kaplan, LTU, June 2014 Content: 1. Selected slides from a survey presentation on PROLAS (3 pages) 2. List of publications, and title pages of selected publications (10 pages) 3. Guideline “Introduktion till lasersvetsning” (Swedish version, 36 pages) 4. The final technical report - from Oulu University (in English, 48 pages) 1. Selected slides from a survey presentation on PROLAS Four EU regionally funded projects were recently carried out in laser materials processing, complementary to each other. The research carried out in PROLAS is of more fundamental and generalized nature than in FATLAS and IndLas where industrial applications were studied and spread, while FIF basically identified the industrial SME needs for when and how to implement advanced manufacturing technology. The Workpackages (WP) in PROLAS have generated results of the three types, as illustrated above: Developing cooperation, exploring and publishing scientific and technical results, a final guideline.

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  • PROLAS 1

    Project PROLAS - Final Report

    Annex containing additional material by Alexander Kaplan, LTU, June 2014

    Content: 1. Selected slides from a survey presentation on PROLAS (3 pages) 2. List of publications, and title pages of selected publications (10 pages) 3. Guideline “Introduktion till lasersvetsning” (Swedish version, 36 pages) 4. The final technical report - from Oulu University (in English, 48 pages)

    1. Selected slides from a survey presentation on PROLAS

    Four EU regionally funded projects were recently carried out in laser materials processing, complementary to each other. The research carried out in PROLAS is of more fundamental and generalized nature than in FATLAS and IndLas where industrial applications were studied and spread, while FIF basically identified the industrial SME needs for when and how to implement advanced manufacturing technology.

    The Workpackages (WP) in PROLAS have generated results of the three types, as illustrated above: Developing cooperation, exploring and publishing scientific and technical results, a final guideline.

  • PROLAS 2

    A web-conferencing culture between the Finnish and Swedish partners became established that enabled frequent distant meetings and in turn close cooperation at all levels.

    In WP2, the focused beams of two different types of modern high power lasers were measured, analyzed and compared, namely the Yb:fibre laser at LTU and the Yb:disc lasers at OU.

    As part of the state-of-the-art studies, Alexander Kaplan visited Japan in January 2014 and has seen welding by the today by far strongest industrial high power laser, a 100 kW Yb:fibre laser. In frame of an actual cooperation with the Japanese colleagues, common publications are planned.

  • PROLAS 3

    A significant part of the project comprised laser welding experiments, both at LTU and OU, to identify, understand and suppress laser welding defects, which was published, reported and entered in the developed guideline.

    Knowledge published in literature and discovered in the project was not only entered in State-of-the-Art-manuscripts and in the guideline but for the first time also expanded in a new format of documentation developed at LTU, by subway-system orientation and in a visualizing systematic flow-chart.

    Final seminar of the projects PROLAS and FIF in Tornio.

  • PROLAS 4

    2. List of publications and title pages of selected publications International scientific journal publications fully or partially accomplished (June 2014) in PROLAS, as acknowledged in most of the papers. Marked yellow: joint publications between OU and LTU; Laser beam (main topic) 1. Kaplan, A. F. H: Analysis and modeling of a high power Yb:fibre laser beam, Optical Engineering,

    v 50, n 5, p 054201 (2011). 2. Kaplan, A. F. H.: Comparison of beam profiles for keyhole modelling of laser welding, Journal of

    Laser Applications, v 23, pp 042005 (9 p) (2011). High speed imaging of the keyhole front 3. Eriksson, I., J. Powell, A. F. H. Kaplan: Measurements of fluid flow inside laser welding keyholes,

    Sci. Techn. Weld. Join., v 16, n 7, pp 636-641 (2011). 4. Eriksson, I., J. Powell, A. F. H. Kaplan: Melt behavior on the keyhole front during high speed laser

    welding, Optics and Lasers in Engineering, v 51, n 6, pp735-739 (2013). Absorption laser beam at keyhole front 5. Kaplan, A. F. H.: Local absorptivity modulation of a 1 µm-laser beam through surface waviness,

    Applied Surface Science , v 258. n 8, pp 9732-9736 (2012). 6. Kaplan, A. F. H.: Fresnel absorption of 1 µm- and 10 µm-laser beams at the keyhole wall during

    laser beam welding: Comparison between smooth and wavy surfaces, Applied Surface Science (IF 1,73), v 258, n 8, 3354-3363 (2012).

    7. Kaplan, A. F. H.: Absorptivity modulation on wavy molten steel surfaces; the influence of laser wavelength and angle of incidence, Applied Physics Letters (IF 3,77), v 101, pp 151605 (4 p) (2012). doi: 10.1063/1.4759126

    8. Kaplan, A. F. H.: Laser absorptivity on wavy molten metal surfaces: Categorization of different metals and wavelengths, J. Laser Appl., v 26, pp 012007 (9 p) (2014).

    9. Matti, R. S., T. Ilar and A. F. H. Kaplan: Analysis of laser remote fusion cutting based on a mathematical model, J. Appl. Phys, v 114, pp 233107-9 (2013).

    Spatter 10. Kaplan, A. F. H and J. Powell: Spatter in laser welding, J Laser Appl., v 32, n 3, 032005 (7 p)

    (2011). doi:10.2351/1.3597830 Hot cracks 11. Wiklund, G, O. Akselsen, A. J. Soegjerd and A. F. H. Kaplan: Geometrical aspects of hot-cracks in

    laser hybrid arc welding, Journal of Laser Applications, v 26, pp 012003 (6 p) (2014).

    Weld distortion 12. Eriksson, I., P. Haglund, J. Powell, M. Sjödahl, A. F. H. Kaplan: Holographic measurement of

    thermal distortion during laser spot welding, Optical Engineering Letters, v 51, 030501 (3 p) (2012). DOI:10.1117/1.OE.51.3.030501

  • PROLAS 5

    Weld surface shape 13. Karlsson, J., A. F. H. Kaplan: Analysis of a fibre laser welding case study, utilising a matrix flow

    chart, Applied Surface Science, v 257, n 9, pp 4113-4122 (2011).

    Influence of joint edge preparation 14. Sokolov, M. S., A. Salminen, A. F. H. Kaplan: Laser Welding of Structural Steels: Influence of the

    Edge Roughness Level, Optics & Laser Technology, v 44, pp 2064-2071 (2012). Measurement of fatigue crack growth through welds 15. Sundqvist, J., A. F. H. Kaplan1, J. Granström, K.-G. Sundin, M. Keskitalo, K. Mäntyjärvi, X. Ren:

    Identifying Residual Stresses in Laser Welds by Fatigue Crack Growth Acceleration Measurement, submitted to Measurement Science and Technology (2014).

    New technique - donut welding 16. Eriksson, I., J. Powell, A. F. H. Kaplan: Surface tension generated defects in full penetration laser

    keyhole welding, J. Laser Appl., v 26, pp 012006 (6 p) (2014). Weld metallurgy 17. Keskitalo, M., K. Mäntyjärvi, J. Sundqvist, J. Powell, A. F. H. Kaplan: The influence of shielding

    gas on the properties of laser welded duplex stainless steel, submitted to Journal of Materials Processing Technologies (2014).

    18. Keskitalo, M., J. Sundqvist, K. Mäntyjärvi, J. Powell, A. F. H. Kaplan: The influence of shielding gas and heat input on the properties of the EN 1.4521 type steel laser weld, under preparation for journal submission (2014).

    Guidelines for laser-arc hybrid welding 19. Eriksson, I., J. Powell and A. F. H. Kaplan: Guidelines in the choice of parameters for hybrid laser

    arc welding with fiber lasers, Proc. LIM, Munich, Germany and Physics Procedia, v 41, pp 119-127 (2013).

    (further journal publications are under preparation, in additional several conference papers exist) Joint publications between OU and LTU at peer-reviewed conferences: 20. Keskitalo, M., K. Mäntyjärvi, J. Sundqvist, I. Eriksson, A. F. H. Kaplan: The influence of shielding

    gas on the properties of laser welded stainless steel, Proc. NOLAMP 14, August 26-28, 2013, Gothenburg/Sweden (2013).

    21. Sundqvist, J., I. Eriksson, A. F. H. Kaplan, M. Keskitalo, K. Mäntyjärvi, J. Granström, K.-G. Sundin: Measuring the influence of laser welding on fatigue crack propagation in high strength steel, Proc. ICALEO, Miami (FL), Paper #2104 (2013).

    22. Sundqvist, J., I. Eriksson, A. F. H. Kaplan, M. Keskitalo and K. Mäntyjärvi: Influence of the metallurgy on fatigue crack propagation in welded high strength steel joints, Proc. NOLAMP 14, August 26-28, 2013, Gothenburg/Sweden (2013).

    Below the title pages of selected publications [13,16,7,15,21,22,17,20] are added:

  • PROLAS 6

    [13]:

  • PROLAS 7

    [16]

  • PROLAS 8

    [7]:

  • PROLAS 9

    [15]: Identifying Residual Stresses in Laser Welds by Fatigue Crack Growth Acceleration Measurement Jesper Sundqvist1, Alexander F. H. Kaplan1, Jan Granström1, Karl-Gustaf Sundin1, Markku Keskitalo2, Kari Mäntyjärvi2, Xiaobo Ren3

    1 Department of Engineering Sciences and Mathematics, Luleå University of Technology, Luleå, 971 87 Sweden

    2 Oulu Southern Institute, University of Oulu, Pajatie 5, Nivala, FI-85500, Finland

    3 SINTEF Materials and Chemistry, N-7465 Trondheim, Norway

    Abstract The fatigue life of laser welds is often governed by their surface topology which can act in a stress

    raising manner and in turn influence the crack initiation time. Residual stresses which are induced by

    the fast heating and cooling cycle can have a strong impact on the fatigue behaviour, often shortening

    the fatigue lifetime of the welded component. This paper describes how the standardized measurement

    method for the fatigue crack growth rate can be expanded to identify residual stress along the cracking

    path. Here the method is studied for a three-point bending fatigue testing of laser welds. The second

    derivative of the measured crack opening and in turn crack length over time, hence the acceleration

    turns out to correspond well with the residual stress distribution along the crack. Distinct acceleration

    maxima and minima can be identified, correlating with tensile and compressive stress, as was basically

    proven by numerical simulation. The method is easy to apply and provides valuable information, as

    was demonstrated for different situations, like different high strength steel and welding parameters and

    cracking across two parallel welds or along the weld. The method has potential for further extensions.

    It was shown that the combination with additional analysis methods can provide valuable

    complementary information on the cracking behaviour.

  • PROLAS 10

    [21]:

  • PROLAS 11

    [22]:

    INFLUENCE OF THE METALLURGY ON FATIGUE CRACK PROPAGATION IN WELDED HIGH STRENGTH STEEL JOINTS J. SUNDQVIST1, I. ERIKSSON1, A. F. H. KAPLAN1, M. KESKITALO2, K. MÄNTYJÄRVI2 1Luleå University of Technology, Luleå, Sweden. 2 University of Oulu, Nivala, Finland

    Abstract

    A literature study of high strength steels, fatigue and fatigue assessment of welds has been conducted and is briefly presented in this paper together with experiments on fatigue crack growth rates of laser welded high strength steel. It is well-known that the fatigue life of welded joints is heavily dependent upon the surface geometry and welding defects because of crack initiation from the high stress concentrations associated with these types of welding flaws. However, the crack propagation through different weld zones of laser-welded high strength steels and the corresponding impact from the metallurgy is not fully understood. The experiments comprise three-point bending fatigue tests on laser-welded high strength steel with machined surfaces. Measurement of the fatigue crack propagation rate transverse the weld and hence through the different metallurgy and hardness of the heat affected zone and of the weld can contain information on the impact of the metallurgy on the crack propagation speed. The influence of different high strength steel grades and of different welding parameters on the crack propagation and fatigue life is discussed.

    Keywords: fatigue crack propagation, weld, laser, high strength steel, fatigue testing

    1 Introduction

    For many welded products fatigue is the main load situation to be optimized. Many new high strength steel grades have been developed that basically enable improved product design, particularly weight reduction. However, welding usually lowers the strength and fatigue life of steel which hinders the reduction of plate thickness for dimensioning. For fatigue life assessment mainly the geometrical aspects of a weld like the weld shape and its stress raisers have been studied and considered, while the impact of metallurgy on fatigue crack propagation is not well understood yet. Therefore the present study aims at better measurement and understanding of the influence of the metallurgy of laser welded high strength steel on fatigue crack propagation. The first part of this paper is a review of the mechanisms affecting fatigue life of high strength steel after welding. A literature study on the current research in high strength steel and fatigue of laser welds was made and is presented in the beginning sections of this paper. The second part of the paper describes a method for measuring fatigue crack propagation through laser welds with constant stress intensity factor. The method is discussed based on first measurement results.

  • PROLAS 12

    [17]:

    THE INFLUENCE OF SHIELDING GAS ON THE PROPERTIES OF LASER WELDED DUPLEX STAINLESS STEEL M. Keskitalo1,* ,K. Mäntyjärvi1, J. Sundqvist 2, J. Powell2, A. F. H. Kaplan2 1University of Oulu, Oulu Southern Institute, Pajatie 5, FI-85500 Nivala, Finland 2Luleå University of Technology, Department of Engineering Sciences and Mathematics, SE-97 451 Luleå, Sweden

    *18]Corresponding author Tel.: +358407750337

    E-mail address: [email protected]

    Abstract

    Some grades of duplex stainless steel employ nitrogen as an alloying ingredient which

    promotes austenite formation in welds and improves toughness. During laser welding with

    argon as the shielding gas, nitrogen can be lost from the weld pool and this can have a

    deleterious effect on weld toughness. This paper investigates whether or not this effect can be

    remedied by using nitrogen as the shielding gas during laser welding. Preliminary results are

    very promising. Increased austenite levels in the weld metal and improved toughness levels

    have been noted if nitrogen rather than argon is employed as the shielding gas.

    Keywords: laser welding, duplex stainless steel, shielding gas. Nitrogen. Argon.

    1. Introduction

    This paper presents the results of an experimental program to compare the hardness and

    formability of Lean duplex stainless steel laser welds produced with either Argon or Nitrogen

    as the shielding gas. Duplex stainless steels are made up of a combination of austenite and

    ferrite and some grades of this material employ nitrogen as an alloying ingredient which

    promotes austenite formation in welds and improves toughness. In standard laser welding,

    using argon as a shield gas, nitrogen can be lost from the weld pool and the austenite content

    of the weld will be reduced. Kyröläinen and Lukkari (1999) and the welding handbook of

    Outokumpu Oyj (2010) has been noted that if the austenite content of a weld is too low, this

    can lead to nitride precipitation, which has a negative effect on weld corrosion properties and

  • PROLAS 13

    [20]:

    THE INFLUENCE OF SHIELDING GAS ON THE PROPERTIES OF LASER WELDED STAINLESS STEEL

    M. Keskitalo1, ,K. Mäntyjärvi1, J. Sundqvist 2, I. Eriksson 2, A. F. H. Kaplan2 1University of Oulu, Oulu Southern Institute, Pajatie 5, FI-85500 Nivala, Finland 2Luleå University of Technology, Department of Engineering Sciences and Mathematics, SE-97 451 Luleå, Sweden

    Abstract

    Argon is generally used as shielding gas for laser welding. As Argon is an inert gas it does not have influence on the microstructure of the weld material or on the heat input of the weld, whereas nitrogen has solubility to austenite. Therefore nitrogen as an interstitial atom increases the hardness of the weld. This has been detected when comparing the hardness profiles of nitrogen shielded welds of austenitic stainless steel with Argon shielded welds. Nitrogen as the shielding gas can compensate the softer structure of the weld in work-hardened and nitrogen-alloyed steels. For the duplex stainless steel grades the nitrogen additions promote formation of austenite in the weld, which decreases the risk of lowered toughness. In this study the influence of nitrogen shielding gas on the strength of the laser weld has been examined. The strength of laser welds of nitrogen alloyed work-hardened stainless steel seems to be slightly better when using nitrogen shielding gas compared to welds for argon shielding gas. It has also been verified that nitrogen as shielding gas decreases the risk of weak toughness of laser welded duplex stainless steel.

    Keywords: laser welding, stainless steel, shielding gas

    1 Introduction

    Nitrogen alloying is used in order to increase the strength of Austenitic stainless steel. The heat influence of welding can cause a nitrogen loss of the weld. The study will determine the influences of Nitrogen shielding gas on the hardness profiles of the laser weld and also on the strength properties of Nitrogen alloyed austenitic stainless steels. In addition the study will compare the formability of Lean duplex stainless steel laser welds which are welded with Argon and Nitrogen stainless steel. Low austenite content of a weld can cause a nitride precipitation which has a deleterious defect to the corrosion properties and toughness [1]. The target of the study is to increase the austenite content of the weld by using Nitrogen as shielding gas and backing gas [2]. The nitrogen as alloying element favours austenite according to WRC-92 equations (1) and (2) [3]. Ni-ekv = %Ni+35*%C+20*%N+0,25*%Cu (1) Cr-ekv = %Cr+%Mo+0,7*%Nb (2)

    17. Keskitalo, M., K. Mäntyjärvi, J. Sundqvist, J. Powell, A. F. H. Kaplan: The influence of shielding gas on the properties of laser welded duplex stainless steel, submitted to Journal of Materials Processing Technologies (2014).19. Eriksson, I., J. Powell and A. F. H. Kaplan: Guidelines in the choice of parameters for hybrid laser arc welding with fiber lasers, Proc. LIM, Munich, Germany and Physics Procedia, v 41, pp 119-127 (2013).(further journal publications are under preparation, in additional several conference papers exist)21. Sundqvist, J., I. Eriksson, A. F. H. Kaplan, M. Keskitalo, K. Mäntyjärvi, J. Granström, K.-G. Sundin: Measuring the influence of laser welding on fatigue crack propagation in high strength steel, Proc. ICALEO, Miami (FL), Paper #2104 (2013).22. Sundqvist, J., I. Eriksson, A. F. H. Kaplan, M. Keskitalo and K. Mäntyjärvi: Influence of the metallurgy on fatigue crack propagation in welded high strength steel joints, Proc. NOLAMP 14, August 26-28, 2013, Gothenburg/Sweden (2013).[17]:THE INFLUENCE OF SHIELDING GAS ON THE PROPERTIES OF LASER WELDED DUPLEX STAINLESS STEELAbstract1. IntroductionTHE INFLUENCE OF SHIELDING GAS ON THE PROPERTIES OF LASER WELDED STAINLESS STEELAbstract1 Introduction