3958 6th Ave. NW Seattle WA 98107
P: 206-632-6206 F: 206-632-6017
E: [email protected] www.brooksrand.com
Report of Trace Metals Analyses in Water Samples Project: Anchor/Newtown Creek
(Alpha Job Number L1204660) Samples Collected: March 19-21, 2012 Report Date: April 20, 2012 Prepared for: Cindy McQueen Alpha Analytical 320 Forbes Blvd. Mansfield, MA 02048 Brooks Rand Labs Project ID: AAL-MN1101
BRL Report 1212016
Page 1 of 274
Table of Contents
Case Narrative ..................................................................................................................3
Report Information.............................................................................................................6
Sample Information ...........................................................................................................7
Batch Summary .................................................................................................................8
Sample Results .................................................................................................................9
Accuracy & Precision Summary .......................................................................................12
Method Blanks & Reporting Limits ...................................................................................17
Instrument Calibration ......................................................................................................22
Sample Containers ...........................................................................................................27
Shipping Containers .........................................................................................................33
Sample Calculations.........................................................................................................34
Chain-of-Custody Forms ..................................................................................................35
Waybills ............................................................................................................................38
Total Mercury Data Sequence 1200235, Batch B120480 ................................................41
Total Mercury Data Sequence 1200251, Batch B120509 ................................................67
Methylmercury Data Sequence 1200258, Batch B120524 ...............................................93
Methylmercury Data Sequence 1200272, Batch B120565 .............................................145
Selenium Data Sequence 1200243, Batch B120537 .....................................................176
BRL Report 1212016
Page 2 of 274
Case Narrative
Shipping and Receiving Water samples included in this report were received by Brooks Rand Labs (BRL) on three (3) different days and logged-in to one (1) work order:
BRL Work Order Number
Date Received
Time Received
Number of Samples
Cooler Temp
1212016 3/21/2012 9:30 AM 4 2.4 °C 3/22/2012 9:30 AM 5 1.0 °C 3/23/2012 9:30 AM 4 2.9 °C
The chain-of-custody (COC) forms requested analysis for total and di ssolved mercury (Hg), methylmercury (MeHg), and total and dissolved selenium (Se). A container was not submitted for MeHg analysis for sample SW-RB-20120321. A split was taken from the corresponding THg sample bottle and was preserved and logged-in for MeHg analysis. The samples were received and stored securely according to BRL standard operating procedures (SOP) and EPA methodology.
Preservation and Holding Time All method and SOP requirements for preservation and holding time were satisfied.
Total Mercury in Water by EPA Method 1631 (BRL SOP #BR-0006) All samples are prepared and anal yzed in accordance with EPA Method 1631. Samples are oxidized with bromine monochloride (BrCl) and then analyzed with stannous chloride (SnCl2) reduction, single gold amalgamation, and c old vapor atomic fluorescence spectroscopy (CVAFS) detection using a BRL Model III CVAFS Mercury Analyzer.
The results have not been method blank-corrected, contrary to the method described in the calculations section of the relevant BRL SOPs and may have been evaluated using reporting limits that have been adjusted to account for sample aliquot size. Please refer to the Sample Results page for sample-specific MDLs, MRLs, and other details. Sample results greater than the MDL, but less than or equal to the MRL, have been reported qualified B.
Sequence 1200235, Batch B120480 Instrument calibration, meeting all quality control criteria, was successfully achieved on the day of sample analysis.
All data was reported without further qualification and a ll associated quality control sample results met the acceptance criteria.
BRL Report 1212016
Page 3 of 274
Sequence 1200251, Batch B120509 The analysis of the 4th calibration standard produced an abnormal peak shape; however, this calibration standard result still yielded a 100% recovery. All calibration standard recoveries in this sequence ranged from 99% to 101%. On this basis, reanalysis of the calibration standard was not warranted. Instrument calibration, meeting all quality control criteria, was successfully achieved on the day of sample analysis.
Sample SW-RB-20120321 (1212016-21) was identified as a rinse blank and y ielded a detectable Hg concentration of 0.77 ng/L. Since half of this sample was split off for MeHg analysis (see Shipping and Receiving section above), reanalysis of this sample for confirmation was not possible.
All data was reported without further qualification and a ll associated quality control sample results met the acceptance criteria.
Methylmercury in Water by EPA Method 1630 (BRL SOP #BR-0011) Water samples are prepared by distillation. Distillates are analyzed by ethylation, Tenax trap collection, gas chromatography separation, isothermal decomposition, and c old vapor fluorescence spectroscopy (CVAFS).
The results have not been method blank-corrected, contrary to the method described in the calculations section of the relevant BRL SOPs and may have been evaluated using reporting limits that have been adjusted to account for sample aliquot size. Please refer to the Sample Results page for sample-specific MDLs, MRLs, and other details. Sample results equal to our less than the MDL have been reported at the MDL and qualified U. Sample results greater than the MDL, but less than or equal to the MRL, have been reported qualified B.
Sequence 1200258, Batch B120524 Instrument calibration, meeting all quality control criteria, was successfully achieved on the day of sample analysis. CCV6 and CCBA were part of a group of samples that were not ethylated. These samples were reanalyzed in sequence 1200272 (batch B120565), and CCV6 and CCBA were not reported.
The first method blank, B120524-BLK1, produced a high result (0.045 ng/L) that was determined to be a Grubb’s Outlier at < 5% risk of false rejection. As this BLK was detectable, and as the data for this project is being reported without the benefit of method blank-correction, all data was judged against this outlier BLK result. Most of the reported data is below the MDL and has not been further qualified. However, all detectable results that produced a concentration that was within 10x of the concentration of BLK1 have been reported qualified X as per BRL’s Comprehensive Quality Control Plan.
Samples 1212016-23 and 1212016-25 were not ethylated prior to analysis and have not been reported from this sequence/batch. The samples were rebatched for analysis in sequence 1200272 (batch B120565).
All data was reported without further qualification and a ll associated quality control sample results met the acceptance criteria.
BRL Report 1212016
Page 4 of 274
Sequence 1200272, Batch B120565 Instrument calibration, meeting all quality control criteria, was successfully achieved on the day of sample analysis.
All data was reported without further qualification and a ll associated quality control sample results met the acceptance criteria.
Trace Metals EPA Method 1638 modified (BRL SOP #BR-0060) Analysis is performed by EPA Draft Method 1638 (modified) using inductively coupled plasma - mass spectrometry (ICP-MS). Prior to analysis, the samples are preserved to 1% with ultra-pure nitric acid. Furthermore, samples for total recoverable analysis are heated overnight at 85 °C. Aliquots of digested sample are analyzed utilizing internal standardization. This method incorporates ionization of the sample in an inductively-coupled RF plasma, with detection of the resulting ions by mass spectrometer on t he basis of their mass-to-charge ratio. ICP-MS interference correction equations and background correction were applied. Raw data (counts-per-second) are reported prior to application of background correction. The results have not been method blank-corrected, contrary to the method described in the calculations section of the relevant BRL SOPs and may have been evaluated using reporting limits that have been adjusted to account for sample aliquot size. Please refer to the Sample Results page for sample-specific MDLs, MRLs, and ot her details. Due to the salinity of the samples, all samples were analyzed at a dilution. All sample results produced concentrations of Se that are equal to our less than the dilution-adjusted MDL and ha ve been r eported at the dilution-adjusted MDL and qualified U.
Sequence 1200243, Batch B120537 Instrument calibration, meeting all quality control criteria, was successfully achieved on the day of sample analysis.
In instances when the native sample and/or the corresponding duplicate (DUP) produced non-detectable results the relative percent difference (RPD) was not calculated (N/C).
All data was reported without further qualification and a ll associated quality control sample results met the acceptance criteria.
We certify that this data package is in compliance with the terms and conditions of the contract, both technically and f or completeness, for other than the conditions detailed above. BRL, an accredited laboratory, certifies that the reported results of all analyses for which BRL is NELAP accredited meet all NELAP requirements. For more details, please see the Report Information page in your report. Please feel free to contact us if you have any questions regarding this report.
___________________________ Michelle L. Briscoe
VP of Analytical Services [email protected]
___________________________ Amanda Royal
Project Manager [email protected]
BRL Report 1212016
Page 5 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Definition of Data Qualifiers(Effective 9/23/09)
Laboratory AccreditationBRL is accredited by the National Environmental Laboratory Accreditation Program (NELAP) through the State of Florida
Department of Health, Bureau of Laboratories (E87982) and is certified to perform many environmental analyses. BRL is
also certified by many other states to perform environmental analyses. For a current list of our
accreditations/certifications, please visit our website at <http://www.brooksrand.com/default.asp?contentID=586>. Results
reported relate only to the samples listed in the report.
Report Information
BLK
BRL
BS
CAL
CCV
CRM
D
DUP
ICV
MSD
ND
NR
PS
REC
RPD
RSD
SCV
SOP
method blank
Brooks Rand Labs
laboratory fortified blank
calibration standard
continuing calibration verification
certified reference material
dissolved fraction
duplicate
initial calibration verification
matrix spike duplicate
non-detect
non-reportable
post preparation spike
percent recovery
relative percent difference
relative standard deviation
secondary calibration verification
standard operating procedure
MDL
MRL
MS
method detection limit
method reporting limit
matrix spike
SRM
T
COC
standard reference material
total recoverable fraction
chain of custody record
Common Abbreviations
These qualifiers are based on those previously utilized by Brooks Rand, Ltd., those found in the EPA SOW ILM03.0,
Exhibit B, Section III, pg. B-18, and the USEPA Laboratory Data Validation Functional Guidelines for Evaluating Inorganic
Analyses; USEPA; July 2002. These supersede all previous qualifiers ever employed by BRL.
Detected by the instrument, the result is > the MDL but ≤ the MRL. Result is reported and considered an estimate.B
E An estimated value due to the presence of interferences. A full explanation is presented in the narrative.
H Holding time and/or preservation requirements not met. Result is estimated.
J Estimated value. A full explanation is presented in the narrative.
J-M Duplicate precision (RPD) for associated QC sample was not within acceptance criteria. Result is estimated.
J-N Spike recovery for associated QC sample was not within acceptance criteria. Result is estimated.
M Duplicate precision (RPD) was not within acceptance criteria. Result is estimated.
N Spike recovery was not within acceptance criteria. Result is estimated.
R Rejected, unusable value. A full explanation is presented in the narrative.
U Result is ≤ the MDL or client requested reporting limit (CRRL). Result reported as the MDL or CRRL.
X Result is not BLK-corrected and is within 10x the absolute value of the highest detectable BLK in the batch.
Result is estimated.
Field Quality Control SamplesPlease be notified that certain EPA methods require the collection of field quality control samples of an appropriate type
and frequency; failure to do so is considered a deviation from some methods and for compliance purposes should only be
done with the approval of regulatory authorities. Please see the specific EPA methods for details regarding required field
quality control samples.
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 6 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Sample Information
Report Matrix Type ReceivedSampledSample Lab IDAlias
1212016-01WC001SW-C-20120319 03/19/2012 03/21/2012SampleWaterL1204660-01
1212016-02WC001SW-C-20120319 03/19/2012 03/21/2012SampleWaterL1204660-01
1212016-03WC001SW-A-20120319 03/19/2012 03/21/2012SampleWaterL1204660-03
1212016-04WC001SW-A-20120319 03/19/2012 03/21/2012SampleWaterL1204660-03
1212016-05NC068SW-A-20120319 03/19/2012 03/21/2012SampleWaterL1204660-05
1212016-06NC068SW-A-20120319 03/19/2012 03/21/2012SampleWaterL1204660-05
1212016-07NC068SW-C-20120319 03/19/2012 03/21/2012SampleWaterL1204660-07
1212016-08NC068SW-C-20120319 03/19/2012 03/21/2012SampleWaterL1204660-07
1212016-09MC008SW-A-20120320 03/20/2012 03/22/2012SampleWaterL1204660-11
1212016-10MC008SW-A-20120320 03/20/2012 03/22/2012SampleWaterL1204660-11
1212016-11DK011SW-C-20120320 03/20/2012 03/22/2012SampleWaterL1204660-13
1212016-12DK011SW-C-20120320 03/20/2012 03/22/2012SampleWaterL1204660-13
1212016-13DK011SW-A-20120320 03/20/2012 03/22/2012SampleWaterL1204660-15
1212016-14DK011SW-A-20120320 03/20/2012 03/22/2012SampleWaterL1204660-15
1212016-15NC046SW-A-20120320 03/20/2012 03/22/2012SampleWaterL1204660-18
1212016-16NC046SW-A-20120320 03/20/2012 03/22/2012SampleWaterL1204660-18
1212016-17NC046SW-C-20120320 03/20/2012 03/22/2012SampleWaterL1204660-20
1212016-18NC046SW-C-20120320 03/20/2012 03/22/2012SampleWaterL1204660-20
1212016-19EB010SW-A-20120321 03/21/2012 03/23/2012SampleWaterL1204660-22
1212016-20EB010SW-A-20120321 03/21/2012 03/23/2012SampleWaterL1204660-22
1212016-21SW-RB-20120321 03/21/2012 03/23/2012Rinse BlankDIWL1204660-24
1212016-22SW-RB-20120321 03/21/2012 03/23/2012Rinse BlankDIWL1204660-24
1212016-23NC034SW-A-20120321 03/21/2012 03/23/2012SampleWaterL1204660-26
1212016-24NC034SW-A-20120321 03/21/2012 03/23/2012SampleWaterL1204660-26
1212016-25NC034SW-C-20120321 03/21/2012 03/23/2012SampleWaterL1204660-28
1212016-26NC034SW-C-20120321 03/21/2012 03/23/2012SampleWaterL1204660-28
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 7 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Batch Summary
Analyte Prepared Analyzed SequenceBatchLab Matrix Method
B12048003/23/2012 04/03/2012 1200235Water EPA 1631Hg
B12050903/30/2012 04/09/2012 1200251Water EPA 1631Hg
B12052404/09/2012 04/11/2012 1200258Water EPA 1630MeHg
B12056504/16/2012 04/18/2012 1200272Water EPA 1630MeHg
B12053704/03/2012 04/05/2012 1200243Water EPA 1638 DRCSe
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 8 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Sample Results
Sample Sequence Result MDL MRL Unit BatchQualifierAnalyte FractionReport Matrix
DK011SW-A-20120320
ng/L6.94T 1200235B120480Water 0.520.201212016-13 Hg
ng/L4.52D 1200235B120480Water 0.400.151212016-14 Hg
ng/L0.019T U 1200258B120524Water 0.0480.0191212016-13 MeHg
µg/L1.16T U 1200243B120537Water 3.431.161212016-13 Se
µg/L1.16D U 1200243B120537Water 3.431.161212016-14 Se
DK011SW-C-20120320
ng/L2.42T 1200235B120480Water 0.530.201212016-11 Hg
ng/L0.28D B 1200235B120480Water 0.400.151212016-12 Hg
ng/L0.020T U 1200258B120524Water 0.0490.0201212016-11 MeHg
µg/L1.16T U 1200243B120537Water 3.431.161212016-11 Se
µg/L1.16D U 1200243B120537Water 3.431.161212016-12 Se
EB010SW-A-20120321
ng/L8.87T 1200251B120509Water 0.540.201212016-19 Hg
ng/L1.17D 1200251B120509Water 0.400.151212016-20 Hg
ng/L0.159T X 1200258B120524Water 0.0510.0201212016-19 MeHg
µg/L0.929T U 1200243B120537Water 2.750.9291212016-19 Se
µg/L0.929D U 1200243B120537Water 2.750.9291212016-20 Se
MC008SW-A-20120320
ng/L3.71T 1200235B120480Water 0.540.201212016-09 Hg
ng/L0.40D B 1200235B120480Water 0.400.151212016-10 Hg
ng/L0.066T X 1200258B120524Water 0.0490.0201212016-09 MeHg
µg/L1.16T U 1200243B120537Water 3.431.161212016-09 Se
µg/L1.16D U 1200243B120537Water 3.431.161212016-10 Se
NC034SW-A-20120321
ng/L3.63T 1200251B120509Water 0.540.201212016-23 Hg
ng/L0.55D 1200251B120509Water 0.400.151212016-24 Hg
ng/L0.056T 1200272B120565Water 0.0500.0201212016-23 MeHg
µg/L1.16T U 1200243B120537Water 3.431.161212016-23 Se
µg/L1.16D U 1200243B120537Water 3.431.161212016-24 Se
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 9 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Sample Results
Sample Sequence Result MDL MRL Unit BatchQualifierAnalyte FractionReport Matrix
NC034SW-C-20120321
ng/L32.1T 1200251B120509Water 0.540.201212016-25 Hg
ng/L1.02D 1200251B120509Water 0.410.151212016-26 Hg
ng/L0.081T 1200272B120565Water 0.0510.0201212016-25 MeHg
µg/L1.16T U 1200243B120537Water 3.431.161212016-25 Se
µg/L1.16D U 1200243B120537Water 3.431.161212016-26 Se
NC046SW-A-20120320
ng/L3.06T 1200235B120480Water 0.490.181212016-15 Hg
ng/L0.36D B 1200235B120480Water 0.400.151212016-16 Hg
ng/L0.020T U 1200258B120524Water 0.0500.0201212016-15 MeHg
µg/L1.16T U 1200243B120537Water 3.431.161212016-15 Se
µg/L1.16D U 1200243B120537Water 3.431.161212016-16 Se
NC046SW-C-20120320
ng/L4.77T 1200235B120480Water 0.510.191212016-17 Hg
ng/L0.29D B 1200235B120480Water 0.400.151212016-18 Hg
ng/L0.020T U 1200258B120524Water 0.0500.0201212016-17 MeHg
µg/L1.16T U 1200243B120537Water 3.431.161212016-17 Se
µg/L1.16D U 1200243B120537Water 3.431.161212016-18 Se
NC068SW-A-20120319
ng/L4.30T 1200235B120480Water 0.510.191212016-05 Hg
ng/L0.29D B 1200235B120480Water 0.400.151212016-06 Hg
ng/L0.020T U 1200258B120524Water 0.0500.0201212016-05 MeHg
µg/L1.16T U 1200243B120537Water 3.431.161212016-05 Se
µg/L1.16D U 1200243B120537Water 3.431.161212016-06 Se
NC068SW-C-20120319
ng/L4.97T 1200235B120480Water 0.530.201212016-07 Hg
ng/L0.28D B 1200235B120480Water 0.400.151212016-08 Hg
ng/L0.019T U 1200258B120524Water 0.0480.0191212016-07 MeHg
µg/L1.16T U 1200243B120537Water 3.431.161212016-07 Se
µg/L1.16D U 1200243B120537Water 3.431.161212016-08 Se
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 10 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Sample Results
Sample Sequence Result MDL MRL Unit BatchQualifierAnalyte FractionReport Matrix
SW-RB-20120321
ng/L0.77T 1200251B120509DIW 0.400.151212016-21 Hg
ng/L0.21D B 1200251B120509DIW 0.410.151212016-22 Hg
ng/L0.020T U 1200258B120524DIW 0.0490.0201212016-21 MeHg
µg/L0.023T U 1200243B120537DIW 0.0690.0231212016-21 Se
µg/L0.023D U 1200243B120537DIW 0.0690.0231212016-22 Se
WC001SW-A-20120319
ng/L3.31T 1200235B120480Water 0.540.201212016-03 Hg
ng/L0.34D B 1200235B120480Water 0.400.151212016-04 Hg
ng/L0.020T U 1200258B120524Water 0.0500.0201212016-03 MeHg
µg/L1.16T U 1200243B120537Water 3.431.161212016-03 Se
µg/L1.16D U 1200243B120537Water 3.431.161212016-04 Se
WC001SW-C-20120319
ng/L8.97T 1200235B120480Water 0.540.201212016-01 Hg
ng/L0.32D B 1200235B120480Water 0.400.151212016-02 Hg
ng/L0.022T X, B 1200258B120524Water 0.0500.0201212016-01 MeHg
µg/L1.16T U 1200243B120537Water 3.431.161212016-01 Se
µg/L1.16D U 1200243B120537Water 3.431.161212016-02 Se
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 11 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Accuracy & Precision Summary
Batch: B120480
Analyte Result UnitsNative Spike REC & Limits RPD & Limits
Method: EPA 1631
Lab Matrix: Water
Sample
Certified Reference Material (1213013, NIST 1641d 1000x dilution)B120480-SRM1
15.68 101%ng/L 85-115Hg 15.83
Matrix Spike (1212016-01)B120480-MS2
40.05 108%ng/L 71-125Hg 52.398.97
Matrix Spike Duplicate (1212016-01)B120480-MSD2
40.18 109%ng/L 71-125 240.7%Hg 52.788.97
Matrix Spike (1212016-17)B120480-MS3
18.90 104%ng/L 71-125Hg 24.404.77
Matrix Spike Duplicate (1212016-17)B120480-MSD3
19.14 105%ng/L 71-125 242%Hg 24.824.77
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 12 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Accuracy & Precision Summary
Batch: B120509
Analyte Result UnitsNative Spike REC & Limits RPD & Limits
Method: EPA 1631
Lab Matrix: Water
Sample
Certified Reference Material (1213013, NIST 1641d 1000x dilution)B120509-SRM1
15.68 100%ng/L 85-115Hg 15.65
Matrix Spike (1212016-19)B120509-MS1
40.38 101%ng/L 71-125Hg 49.668.87
Matrix Spike Duplicate (1212016-19)B120509-MSD1
40.23 100%ng/L 71-125 241%Hg 49.188.87
Matrix Spike (1212016-23)B120509-MS3
13.36 99%ng/L 71-125Hg 16.823.63
Matrix Spike Duplicate (1212016-23)B120509-MSD3
13.43 98%ng/L 71-125 240.2%Hg 16.863.63
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 13 of 274
Project ID: AAL-MN1101 Client PM: Cindy McQueen PM: Amanda Royal Client PO: Signed LSA
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
Accuracy & Precision Summary Batch: B120524 Lab Matrix: Water Method: EPA 1630
Sample Analyte Native Spike Result Units REC & Limits RPD & Limits B120524-BS1 Laboratory Fortified Blank (1211027) MeHg 1.001 0.871 ng/L 87% 67-133
B120524-BS2 Laboratory Fortified Blank (1211027) MeHg 0.9891 0.888 ng/L 90% 67-133
B120524-MS2 Matrix Spike (1212016-11) MeHg ND 0.05091 0.060 ng/L 82% 65-135
B120524-MSD2 Matrix Spike Duplicate (1212016-11) MeHg ND 0.04917 0.065 ng/L 96% 65-135 8% 35
BRL Report 1212016
Page 14 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Accuracy & Precision Summary
Batch: B120537
Analyte Result UnitsNative Spike REC & Limits RPD & Limits
Method: EPA 1638 DRC
Lab Matrix: Water
Sample
Laboratory Fortified Blank (1210062)B120537-BS1
4.040 102%µg/L 75-125Se 4.107
Certified Reference Material (1132016, NIST 1643e)B120537-SRM1
11.97 103%µg/L 75-125Se 12.32
Duplicate (1212016-05)B120537-DUP1
µg/L 20N/CSe NDND
Matrix Spike (1212016-05)B120537-MS1
50.51 107%µg/L 75-125Se 54.80ND
Matrix Spike Duplicate (1212016-05)B120537-MSD1
50.51 105%µg/L 75-125 202%Se 53.91ND
Duplicate (1212016-09)B120537-DUP2
µg/L 20N/CSe 1.385ND
Matrix Spike (1212016-09)B120537-MS2
50.51 110%µg/L 75-125Se 56.21ND
Matrix Spike Duplicate (1212016-09)B120537-MSD2
50.51 106%µg/L 75-125 203%Se 54.36ND
Duplicate (1212016-19)B120537-DUP3
µg/L 20N/CSe NDND
Matrix Spike (1212016-19)B120537-MS3
50.51 95%µg/L 75-125Se 48.55ND
Matrix Spike Duplicate (1212016-19)B120537-MSD3
50.51 92%µg/L 75-125 203%Se 47.03ND
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 15 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Accuracy & Precision Summary
Batch: B120565
Analyte Result UnitsNative Spike REC & Limits RPD & Limits
Method: EPA 1630
Lab Matrix: Water
Sample
Laboratory Fortified Blank (1216002)B120565-BS1
1.005 94%ng/L 67-133MeHg 0.944
Laboratory Fortified Blank (1216002)B120565-BS2
0.9854 90%ng/L 67-133MeHg 0.882
Matrix Spike (1213006-01)B120565-MS1
0.2525 107%ng/L 65-135MeHg 0.289ND
Matrix Spike Duplicate (1213006-01)B120565-MSD1
0.2504 106%ng/L 65-135 352%MeHg 0.284ND
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 16 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Method Blanks & Reporting Limits
Batch: B120480
Method: EPA 1631
Matrix: Water
Analyte: Hg
Result UnitsSample
B120480-BLK1 ng/L0.10
B120480-BLK2 ng/L0.03
B120480-BLK3 ng/L0.04
B120480-BLK4 ng/L0.03
MDL: 0.15Average: 0.05 Standard Deviation: 0.03
Limit: 0.10Limit: 0.50 MRL: 0.40
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 17 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Method Blanks & Reporting Limits
Batch: B120509
Method: EPA 1631
Matrix: Water
Analyte: Hg
Result UnitsSample
B120509-BLK1 ng/L0.08
B120509-BLK2 ng/L0.09
B120509-BLK3 ng/L0.09
B120509-BLK4 ng/L0.06
MDL: 0.15Average: 0.08 Standard Deviation: 0.01
Limit: 0.10Limit: 0.50 MRL: 0.40
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 18 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Method Blanks & Reporting Limits
Batch: B120524
Method: EPA 1630
Matrix: Water
Analyte: MeHg
Result UnitsSample
B120524-BLK1 ng/L0.045
B120524-BLK2 ng/L0.007
B120524-BLK3 ng/L0.010
B120524-BLK4 ng/L0.003
MDL: 0.020Average: 0.016 Standard Deviation: 0.019
Limit: 0.015Limit: 0.045 MRL: 0.049
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 19 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Method Blanks & Reporting Limits
Batch: B120537
Method: EPA 1638 DRC
Matrix: Water
Analyte: Se 78
Result UnitsSample
B120537-BLK1 µg/L0.010
B120537-BLK2 µg/L0.009
B120537-BLK3 µg/L0.005
B120537-BLK4 µg/L0.012
MDL: 0.023Average: 0.009 Standard Deviation: 0.003
Limit: 0.023Limit: 0.069 MRL: 0.069
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 20 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Method Blanks & Reporting Limits
Batch: B120565
Method: EPA 1630
Matrix: Water
Analyte: MeHg
Result UnitsSample
B120565-BLK1 ng/L0.002
B120565-BLK2 ng/L-0.001
B120565-BLK3 ng/L0.007
B120565-BLK4 ng/L0.007
MDL: 0.020Average: 0.004 Standard Deviation: 0.004
Limit: 0.015Limit: 0.045 MRL: 0.051
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 21 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Instrument Calibration
Sequence: 1200235
Method: EPA 1631Instrument: THG-10
Date: 04/03/2012
Total Mercury and Mercury Speciation by CVAFS
Analyte: Hg
REC & LimitsResultTrue ValueLab ID Units1200235-IBL1 5.26 pg of Hg
1200235-IBL2 5.25 pg of Hg
1200235-IBL3 5.27 pg of Hg
1200235-IBL4 5.03 pg of Hg
1200235-CAL1 25.00 25.86 pg of Hg 103%
1200235-CAL2 100.0 99.45 pg of Hg 99%
1200235-CAL3 500.0 483.5 pg of Hg 97%
1200235-CAL4 2500 2440 pg of Hg 98%
1200235-CAL5 10000 9888 pg of Hg 99%
1200235-ICV1 1568 1583 pg of Hg 101% 85-115
1200235-CAL6 500.0 504.1 pg of Hg 101%
1200235-CCB1 5.00 pg of Hg
1200235-CCV1 500.0 499.8 pg of Hg 100% 77-123
1200235-CCB2 3.75 pg of Hg
1200235-CCV2 500.0 524.8 pg of Hg 105% 77-123
1200235-CCV3 500.0 498.1 pg of Hg 100% 77-123
1200235-CCV4 500.0 498.7 pg of Hg 100% 77-123
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 22 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Instrument Calibration
Sequence: 1200243
Method: EPA 1638 DRCInstrument: ICP-MS-2
Date: 04/05/2012
Trace Metals by ICP-DRC-MS
Analyte: Se 78
REC & LimitsResultTrue ValueLab ID Units1200243-ICB1 0.000 µg/L
1200243-CAL1 0.05000 0.049 µg/L 98%
1200243-CAL2 0.1000 0.104 µg/L 104%
1200243-CAL3 0.2500 0.245 µg/L 98%
1200243-CAL4 1.000 0.996 µg/L 100%
1200243-CAL5 5.000 5.106 µg/L 102%
1200243-CAL6 25.00 24.98 µg/L 100%
1200243-CAL7 125.0 124.9 µg/L 100%
1200243-CAL8 500.0 489.3 µg/L 98%
1200243-ICB2 0.133 µg/L
1200243-ICV1 10.00 10.31 µg/L 103% 85-115
1200243-ICB3 0.026 µg/L
1200243-IBL1 0.016 µg/L
1200243-IBL2 0.013 µg/L
1200243-IBL3 0.019 µg/L
1200243-IBL4 0.025 µg/L
1200243-SCV1 11.97 12.32 µg/L 103% 75-125
1200243-CCV1 1.000 1.029 µg/L 103% 75-125
1200243-CCB1 0.025 µg/L
1200243-CCV2 1.000 0.970 µg/L 97% 75-125
1200243-CCB2 0.005 µg/L
1200243-CCV3 1.000 0.980 µg/L 98% 75-125
1200243-CCB3 0.015 µg/L
1200243-CCV4 1.000 1.018 µg/L 102% 75-125
1200243-CCB4 0.0008 µg/L
1200243-CCV5 1.000 1.001 µg/L 100% 75-125
1200243-CCB5 0.007 µg/L
1200243-CCV6 1.000 0.979 µg/L 98% 75-125
1200243-CCB6 0.007 µg/L
1200243-CCV7 1.000 1.006 µg/L 101% 75-125
1200243-CCB7 0.005 µg/L
1200243-CCV8 5.000 5.352 µg/L 107% 75-125
1200243-CCB8 0.006 µg/L
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 23 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Instrument Calibration
Sequence: 1200251
Method: EPA 1631Instrument: THG-05
Date: 04/09/2012
Total Mercury and Mercury Speciation by CVAFS
Analyte: Hg
REC & LimitsResultTrue ValueLab ID Units1200251-IBL2 4.37 pg of Hg
1200251-IBL3 3.99 pg of Hg
1200251-IBL4 3.64 pg of Hg
1200251-CAL1 25.00 24.95 pg of Hg 100%
1200251-CAL2 100.0 100.7 pg of Hg 101%
1200251-CAL3 500.0 505.8 pg of Hg 101%
1200251-CAL4 2500 2482 pg of Hg 99%
1200251-CAL5 10000 9911 pg of Hg 99%
1200251-ICV1 1568 1565 pg of Hg 100% 85-115
1200251-CCB1 8.66 pg of Hg
1200251-IBL5 5.17 pg of Hg
1200251-CCV2 500.0 487.8 pg of Hg 98% 77-123
1200251-CCV3 500.0 468.4 pg of Hg 94% 77-123
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 24 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Instrument Calibration
Sequence: 1200258
Method: EPA 1630Instrument: MMHG-09
Date: 04/11/2012
Total Mercury and Mercury Speciation by CVAFS
Analyte: MeHg
REC & LimitsResultTrue ValueLab ID Units1200258-IBL1 0.144 pg MeHg
1200258-IBL2 0.121 pg MeHg
1200258-IBL3 0.141 pg MeHg
1200258-CAL1 0.5005 0.491 pg MeHg 98%
1200258-CAL2 1.001 0.999 pg MeHg 100%
1200258-CAL3 2.002 1.888 pg MeHg 94%
1200258-CAL4 10.01 9.682 pg MeHg 97%
1200258-CAL5 50.05 49.92 pg MeHg 100%
1200258-CAL6 250.2 258.6 pg MeHg 103%
1200258-CAL7 1001 1086 pg MeHg 109%
1200258-CCB1 0.817 pg MeHg
1200258-ICV1 99.99 101.5 pg MeHg 102% 80-120
1200258-CCB2 1.40 pg MeHg
1200258-CCV1 25.02 25.38 pg MeHg 101% 67-133
1200258-CCB3 0.453 pg MeHg
1200258-CCB4 0.374 pg MeHg
1200258-CCB5 0.197 pg MeHg
1200258-CCV2 25.02 25.20 pg MeHg 101% 67-133
1200258-CCB6 0.230 pg MeHg
1200258-CCV3 25.02 24.32 pg MeHg 97% 67-133
1200258-CCB7 0.115 pg MeHg
1200258-CCV4 25.02 23.60 pg MeHg 94% 67-133
1200258-CCB8 0.456 pg MeHg
1200258-CCV5 25.02 23.07 pg MeHg 92% 67-133
1200258-CCB9 0.161 pg MeHg
1200258-CCV7 25.02 23.41 pg MeHg 94% 67-133
1200258-CCBB 0.148 pg MeHg
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 25 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Instrument Calibration
Sequence: 1200272
Method: EPA 1630Instrument: MMHG-09
Date: 04/18/2012
Total Mercury and Mercury Speciation by CVAFS
Analyte: MeHg
REC & LimitsResultTrue ValueLab ID Units1200272-IBL1 0.128 pg MeHg
1200272-IBL2 0.060 pg MeHg
1200272-IBL3 0.177 pg MeHg
1200272-CAL1 0.5005 0.466 pg MeHg 93%
1200272-CAL2 1.001 1.025 pg MeHg 102%
1200272-CAL3 2.002 1.918 pg MeHg 96%
1200272-CAL4 10.01 9.321 pg MeHg 93%
1200272-CAL5 50.05 51.74 pg MeHg 103%
1200272-CAL6 250.2 260.5 pg MeHg 104%
1200272-CAL7 1001 1099 pg MeHg 110%
1200272-CCB1 0.796 pg MeHg
1200272-ICV1 99.99 109.9 pg MeHg 110% 80-120
1200272-CCB2 1.35 pg MeHg
1200272-CCV1 25.02 23.85 pg MeHg 95% 67-133
1200272-CCB3 0.419 pg MeHg
1200272-CCB4 0.298 pg MeHg
1200272-CCB5 0.196 pg MeHg
1200272-CCV2 25.02 25.94 pg MeHg 104% 67-133
1200272-CCB6 0.087 pg MeHg
1200272-CCV3 25.02 25.12 pg MeHg 100% 67-133
1200272-CCB7 0.173 pg MeHg
1200272-CCV4 25.02 24.64 pg MeHg 98% 67-133
1200272-CCB8 0.181 pg MeHg
1200272-CCV5 25.02 25.15 pg MeHg 101% 67-133
1200272-CCB9 0.124 pg MeHg
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 26 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Sample Containers
Lab ID: 1212016-01 Report Matrix: Water
Sample Type: Sample Received: 03/21/2012Sample: WC001SW-C-20120319
Collected: 03/19/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Coolernone n/a250 mLBottle FLPE Hg-T
B 71470160
10
Cooler1 mL 9N H2SO4 (PP) 1208042 <2250 mLBottle FLPE Hg-SP
C 1048890 Cooler0.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-02 Report Matrix: Water
Sample Type: Sample Received: 03/21/2012Sample: WC001SW-C-20120319
Collected: 03/19/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Coolernone n/a250 mLBottle FLPE Hg-T
B 1048890 Cooler0.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-03 Report Matrix: Water
Sample Type: Sample Received: 03/21/2012Sample: WC001SW-A-20120319
Collected: 03/19/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Coolernone n/a250 mLBottle FLPE Hg-T
B 71470160
10
Cooler1 mL 9N H2SO4 (PP) 1208042 <2250 mLBottle FLPE Hg-SP
C 1048890 Cooler0.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-04 Report Matrix: Water
Sample Type: Sample Received: 03/21/2012Sample: WC001SW-A-20120319
Collected: 03/19/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Coolernone n/a250 mLBottle FLPE Hg-T
B 1048890 Cooler0.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 27 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Sample Containers
Lab ID: 1212016-05 Report Matrix: Water
Sample Type: Sample Received: 03/21/2012Sample: NC068SW-A-20120319
Collected: 03/19/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Coolernone n/a250 mLBottle FLPE Hg-T
B 71470160
10
Cooler1 mL 9N H2SO4 (PP) 1208042 <2250 mLBottle FLPE Hg-SP
C 1048890 Cooler0.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-06 Report Matrix: Water
Sample Type: Sample Received: 03/21/2012Sample: NC068SW-A-20120319
Collected: 03/19/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Coolernone n/a250 mLBottle FLPE Hg-T
B 1048890 Cooler0.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-07 Report Matrix: Water
Sample Type: Sample Received: 03/21/2012Sample: NC068SW-C-20120319
Collected: 03/19/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Coolernone n/a250 mLBottle FLPE Hg-T
B 71470160
10
Cooler1 mL 9N H2SO4 (PP) 1208042 <2250 mLBottle FLPE Hg-SP
C 1048890 Cooler0.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-08 Report Matrix: Water
Sample Type: Sample Received: 03/21/2012Sample: NC068SW-C-20120319
Collected: 03/19/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Coolernone n/a250 mLBottle FLPE Hg-T
B 1048890 Cooler0.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 28 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Sample Containers
Lab ID: 1212016-09 Report Matrix: Water
Sample Type: Sample Received: 03/22/2012Sample: MC008SW-A-20120320
Collected: 03/20/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 2none n/a250 mLBottle FLPE Hg-T
B 71470160
10
Cooler 21 mL 9N H2SO4 (PP) 1208042 <2250 mLBottle FLPE Hg-SP
C 1048890 Cooler 20.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-10 Report Matrix: Water
Sample Type: Sample Received: 03/22/2012Sample: MC008SW-A-20120320
Collected: 03/20/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 2none n/a250 mLBottle FLPE Hg-T
B 1048890 Cooler 20.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-11 Report Matrix: Water
Sample Type: Sample Received: 03/22/2012Sample: DK011SW-C-20120320
Collected: 03/20/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 2none n/a250 mLBottle FLPE Hg-T
B 71470160
10
Cooler 21 mL 9N H2SO4 (PP) 1208042 <2250 mLBottle FLPE Hg-SP
C 1048890 Cooler 20.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-12 Report Matrix: Water
Sample Type: Sample Received: 03/22/2012Sample: DK011SW-C-20120320
Collected: 03/20/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 2none n/a250 mLBottle FLPE Hg-T
B 1048890 Cooler 20.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 29 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Sample Containers
Lab ID: 1212016-13 Report Matrix: Water
Sample Type: Sample Received: 03/22/2012Sample: DK011SW-A-20120320
Collected: 03/20/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 2none n/a250 mLBottle FLPE Hg-T
B 71470160
10
Cooler 21 mL 9N H2SO4 (PP) 1208042 <2250 mLBottle FLPE Hg-SP
C 1048890 Cooler 20.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-14 Report Matrix: Water
Sample Type: Sample Received: 03/22/2012Sample: DK011SW-A-20120320
Collected: 03/20/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 2none n/a250 mLBottle FLPE Hg-T
B 1048890 Cooler 20.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-15 Report Matrix: Water
Sample Type: Sample Received: 03/22/2012Sample: NC046SW-A-20120320
Collected: 03/20/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 2none n/a250 mLBottle FLPE Hg-T
B 71470160
10
Cooler 21 mL 9N H2SO4 (PP) 1208042 <2250 mLBottle FLPE Hg-SP
C 1048890 Cooler 20.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-16 Report Matrix: Water
Sample Type: Sample Received: 03/22/2012Sample: NC046SW-A-20120320
Collected: 03/20/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 2none n/a250 mLBottle FLPE Hg-T
B 1048890 Cooler 20.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 30 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Sample Containers
Lab ID: 1212016-17 Report Matrix: Water
Sample Type: Sample Received: 03/22/2012Sample: NC046SW-C-20120320
Collected: 03/20/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 2none n/a250 mLBottle FLPE Hg-T
B 71470160
10
Cooler 21 mL 9N H2SO4 (PP) 1208042 <2250 mLBottle FLPE Hg-SP
C 1048890 Cooler 20.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-18 Report Matrix: Water
Sample Type: Sample Received: 03/22/2012Sample: NC046SW-C-20120320
Collected: 03/20/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 2none n/a250 mLBottle FLPE Hg-T
B 1048890 Cooler 20.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-19 Report Matrix: Water
Sample Type: Sample Received: 03/23/2012Sample: EB010SW-A-20120321
Collected: 03/21/2012
Comments: DIL Se: 40x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 3none n/a250 mLBottle FLPE Hg-T
B 71470160
10
Cooler 31 mL 9N H2SO4 (PP) 1208042 <2250 mLBottle FLPE Hg-SP
C 1048890 Cooler 30.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-20 Report Matrix: Water
Sample Type: Sample Received: 03/23/2012Sample: EB010SW-A-20120321
Collected: 03/21/2012
Comments: DIL Se: 40x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 3none n/a250 mLBottle FLPE Hg-T
B 1048890 Cooler 30.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 31 of 274
Project ID: AAL-MN1101 Client PM: Cindy McQueen PM: Amanda Royal Client PO: Signed LSA
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
Sample Containers Lab ID: 1212016-21 Report Matrix: DIW Collected: 03/21/2012 Sample: SW-RB-20120321 Sample Type: Rinse Blank Received: 03/23/2012 Des Container Size Lot Preservation P-Lot pH Ship. Cont. Bottle FLPE Hg-T A 250 mL 71470160 none n/a Cooler 3 10 Bottle FLPE Hg-SP B 125 mL 71402520 0.5 mL 9N H2SO4 (BRL) 1208042 <2 N/A 10 Bottle HDPE ICP-W C 125 mL 1048890 0.1% HNO3 (BRL) 1202050 <2 Cooler 3
Lab ID: 1212016-22 Report Matrix: DIW Collected: 03/21/2012 Sample: SW-RB-20120321 Sample Type: Rinse Blank Received: 03/23/2012 Des Container Size Lot Preservation P-Lot pH Ship. Cont. Bottle FLPE Hg-T A 250 mL 71470160 none n/a Cooler 3 10 Bottle HDPE ICP-W B 125 mL 1048890 0.1% HNO3 (BRL) 1202050 <2 Cooler 3
Lab ID: 1212016-23 Report Matrix: Water Collected: 03/21/2012 Sample: NC034SW-A-20120321 Sample Type: Sample Received: 03/23/2012 Comments: DIL Se: 50x Des Container Size Lot Preservation P-Lot pH Ship. Cont. Bottle FLPE Hg-T A 250 mL 71470160 none n/a Cooler 3 10 Bottle FLPE Hg-SP B 250 mL 71470160 1 mL 9N H2SO4 (PP) 1208042 <2 Cooler 3 10 Bottle HDPE ICP-W C 125 mL 1048890 0.1% HNO3 (BRL) 1202050 <2 Cooler 3
Lab ID: 1212016-24 Report Matrix: Water Collected: 03/21/2012 Sample: NC034SW-A-20120321 Sample Type: Sample Received: 03/23/2012 Comments: DIL Se: 50x Des Container Size Lot Preservation P-Lot pH Ship. Cont. Bottle FLPE Hg-T A 250 mL 71470160 none n/a Cooler 3 10 Bottle HDPE ICP-W B 125 mL 1048890 0.1% HNO3 (BRL) 1202050 <2 Cooler 3
BRL Report 1212016
Page 32 of 274
Project ID: AAL-MN1101
PM: Amanda Royal
Client PM: Cindy McQueen
Client PO: Signed LSA
Sample Containers
Lab ID: 1212016-25 Report Matrix: Water
Sample Type: Sample Received: 03/23/2012Sample: NC034SW-C-20120321
Collected: 03/21/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 3none n/a250 mLBottle FLPE Hg-T
B 71470160
10
Cooler 31 mL 9N H2SO4 (PP) 1208042 <2250 mLBottle FLPE Hg-SP
C 1048890 Cooler 30.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Lab ID: 1212016-26 Report Matrix: Water
Sample Type: Sample Received: 03/23/2012Sample: NC034SW-C-20120321
Collected: 03/21/2012
Comments: DIL Se: 50x
Ship. Cont.pHP-LotPreservationLotSizeContainerDesA 71470160
10
Cooler 3none n/a250 mLBottle FLPE Hg-T
B 1048890 Cooler 30.1% HNO3 (BRL) 1202050 <2125 mLBottle HDPE ICP-W
Shipping Containers
Cooler
Tracking No: 1Z 19E 18E 01 4806 6254 via UPS
Temperature: 2.4 °C
Coolant Type: Ice
Description: Cooler
Damaged in transit? No
Returned to client? No
Custody seals present? No
Custody seals intact? No
COC present? Yes
Received: March 21, 2012 9:30
Cooler 2
Tracking No: 1Z 19E 18E 01 4710 0306 via UPS
Temperature: 1.0 °C
Coolant Type: Ice
Description: Cooler 2
Damaged in transit? No
Returned to client? No
Custody seals present? No
Custody seals intact? No
COC present? Yes
Received: March 22, 2012 9:30
Cooler 3
Tracking No: 1Z 19E 18E 01 4925 4352 via UPS
Temperature: 2.9 °C
Coolant Type: Ice
Description: Cooler 3
Damaged in transit? No
Returned to client? No
Custody seals present? No
Custody seals intact? No
COC present? Yes
Received: March 23, 2012 9:30
3958 6th Avenue NW Seattle WA 98107 · P(206) 632-6206 · F(206) 632-6017 · [email protected] · www.brooksrand.com
BRL Report 1212016
Page 33 of 274
Sample Calculations
Page 1 of 1
CVAFS
EPA 1631, Water
𝐶𝐶𝐶𝐶𝐶𝐶𝐴𝐴 ∗ 𝐼𝐼
1− (𝑅𝑅𝐵𝐵𝐵𝐵𝐶𝐶𝐵𝐵 /100%)− �
𝐵𝐵𝑓𝑓𝐴𝐴𝐴𝐴𝐴𝐴
∗ 𝑅𝑅𝐵𝐵𝐵𝐵𝐶𝐶𝐵𝐵 �
C – result produced at the instrument, pg F – final volume of the sample preparation, mL D – dilution factor of any dilution of the preparation made at the instrument A – analyzed volume of the prep or dilution of the prep, mL Bf - the mean of the method blank instrument results, pg AAV - the mean of the analyzed volumes of the method blanks, mL RBrCl – percentage of BrCl in the sample preparation I – aliquot of sample prepared, mL.
EPA 1630, Water
𝐶𝐶𝐶𝐶𝐶𝐶𝐴𝐴 − 𝐵𝐵𝐶𝐶𝑑𝑑
𝐴𝐴𝑑𝑑𝐼𝐼
∗ 𝐸𝐸
C – result produced at the instrument, pg F – final volume of the sample preparation, mL D – dilution factor of any dilution of the preparation made at the instrument A – analyzed volume of the prep or dilution of the prep, mL B – the mean of the method blank instrument result, pg Fd – default final prep volume for the method used for the method blanks, 58 mL Ad – default analyzed volume for the method used for the method blanks, 30 mL E – the empirically derived correction factor I – aliquot of sample prepared, mL.
ICP-MS Metals
EPA 1638, Water
(𝐶𝐶 − 𝐶𝐶𝑠𝑠𝐵𝐵)𝐶𝐶
𝐼𝐼 − (𝐼𝐼 ∗ 𝑅𝑅𝑁𝑁/100%)
C – concentration of the sample preparation, corrected for the dilution at the instrument, µg/L Ds – dilution factor of the sample B – the mean of the method blank instrument result, µg/L F – final volume of the prep, mL I – aliquot of sample prepared, mL (this volume includes the HNO3 used in the prep of the sample) RN – percentage of HNO3 in the sample preparation
BRL Report 1212016
Page 34 of 274
BRL Report 1212016
Page 35 of 274
BRL Report 1212016
Page 36 of 274
BRL Report 1212016
Page 37 of 274
BRL Report 1212016
Page 38 of 274
BRL Report 1212016
Page 39 of 274
BRL Report 1212016
Page 40 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200235
THG-10Instrument:
Batch # Source ID
Brooks Rand Labs
1200235-IBL1 QC 11200235 -
1200235-IBL2 QC 21200235 -
1200235-IBL3 QC 31200235 -
1200235-IBL4 QC 41200235 -
1200235-CAL1 QC 5 12130061200235 -
1200235-CAL2 QC 6 12130071200235 -
1200235-CAL3 QC 7 12130081200235 -
1200235-CAL4 QC 8 12130091200235 -
1200235-CAL5 QC 9 12130101200235 -
1200235-ICV1 QC 10 12130121200235 -
B120480-SRM1 QC 11B120480 -
1200235-CAL6 QC 12 12130081200235 -
B120480-BLK1 QC 13B120480 -
1200235-CCB1 QC 141200235 -
B120480-BLK2 QC 15B120480 -
B120480-BLK3 QC 16B120480 -
B120480-BLK4 QC 17B120480 -
1200235-CCV1 QC 18 12130111200235 -
1200235-CCB2 QC 191200235 -
1212026-01 Hg-W-BrCl-CVAFS-TR 20B120480 MEL-YA0801 4/3/2012
1212026-01 Hg-W-BrCl-CVAFS-NoMB-Diss 21 BatchQCB120480 MEL-YA0801 1/1/1980
1212026-01 Hg-W-BrCl-CVAFS-NoMB-TR 22 BatchQCB120480 MEL-YA0801 1/1/1980
1212027-01 Hg-W-BrCl-CVAFS-TR 23B120480 MEL-YA0801 4/3/2012
1212011-02 Hg-W-BrCl-CVAFS-TR 24B120480 AXS-BC1201 4/11/2012
1212016-01 Hg-W-BrCl-CVAFS-TR 25 BatchQCB120480 AAL-MN1101 1/1/1980
1212016-01 Hg-W-BrCl-CVAFS-NoMB-Diss 26 BatchQCB120480 AAL-MN1101 1/1/1980
Page 1 of 3Printed: 4/4/2012 3:33:21PM
BRL Report 1212016
Page 41 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200235
THG-10Instrument:
Batch # Source ID
Brooks Rand Labs
1212016-01 Hg-W-BrCl-CVAFS-NoMB-TR 27B120480 AAL-MN1101 4/10/2012
1212016-03 Hg-W-BrCl-CVAFS-NoMB-TR 28B120480 AAL-MN1101 4/10/2012
1212016-05 Hg-W-BrCl-CVAFS-NoMB-TR 29B120480 AAL-MN1101 4/10/2012
1212016-07 Hg-W-BrCl-CVAFS-NoMB-TR 30B120480 AAL-MN1101 4/10/2012
1212016-09 Hg-W-BrCl-CVAFS-NoMB-TR 31B120480 AAL-MN1101 4/10/2012
1212016-11 Hg-W-BrCl-CVAFS-NoMB-TR 32B120480 AAL-MN1101 4/10/2012
1212016-13 Hg-W-BrCl-CVAFS-NoMB-TR 33B120480 AAL-MN1101 4/10/2012
B120480-MS1 QC 34B120480 1212026-01
B120480-MSD1 QC 35B120480 1212026-01
B120480-MS2 QC 36B120480 1212016-01
B120480-MSD2 QC 37B120480 1212016-01
1212011-02RE1 Hg-W-BrCl-CVAFS-TR 38 Added 4/4/2012 by MSUB120480 AXS-BC1201 4/11/2012
1200235-CCV2 QC 39 12130111200235 -
1212016-15 Hg-W-BrCl-CVAFS-NoMB-TR 40B120480 AAL-MN1101 4/10/2012
1212016-17 Hg-W-BrCl-CVAFS-TR 41 BatchQCB120480 AAL-MN1101 1/1/1980
1212016-17 Hg-W-BrCl-CVAFS-NoMB-Diss 42 BatchQCB120480 AAL-MN1101 1/1/1980
1212016-17 Hg-W-BrCl-CVAFS-NoMB-TR 43B120480 AAL-MN1101 4/10/2012
1212011-01 Hg-W-BrCl-CVAFS-TR 44B120480 AXS-BC1201 4/11/2012
1212016-02 Hg-W-BrCl-CVAFS-NoMB-Diss 45B120480 AAL-MN1101 4/10/2012
1212016-04 Hg-W-BrCl-CVAFS-NoMB-Diss 46B120480 AAL-MN1101 4/10/2012
1212016-06 Hg-W-BrCl-CVAFS-NoMB-Diss 47B120480 AAL-MN1101 4/10/2012
1212016-08 Hg-W-BrCl-CVAFS-NoMB-Diss 48B120480 AAL-MN1101 4/10/2012
1211017-01 Hg-W-BrCl-CVAFS-TR 49 reconstituted freeze dried urine samplesB120480 INS001 4/11/2012
1211017-02 Hg-W-BrCl-CVAFS-TR 50 reconstituted freeze dried urine samplesB120480 INS001 4/11/2012
1211017-03 Hg-W-BrCl-CVAFS-TR 51 reconstituted freeze dried urine samplesB120480 INS001 4/11/2012
B120480-MS3 QC 52B120480 1212016-17
Page 2 of 3Printed: 4/4/2012 3:33:21PM
BRL Report 1212016
Page 42 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200235
THG-10Instrument:
Batch # Source ID
Brooks Rand Labs
B120480-MSD3 QC 53B120480 1212016-17
1200235-CCV3 QC 54 12130111200235 -
1212016-10 Hg-W-BrCl-CVAFS-NoMB-Diss 55B120480 AAL-MN1101 4/10/2012
1212016-12 Hg-W-BrCl-CVAFS-NoMB-Diss 56B120480 AAL-MN1101 4/10/2012
1212016-14 Hg-W-BrCl-CVAFS-NoMB-Diss 57B120480 AAL-MN1101 4/10/2012
1212016-16 Hg-W-BrCl-CVAFS-NoMB-Diss 58B120480 AAL-MN1101 4/10/2012
1212016-18 Hg-W-BrCl-CVAFS-NoMB-Diss 59B120480 AAL-MN1101 4/10/2012
1200235-CCV4 QC 60 12130111200235 -
Page 3 of 3Printed: 4/4/2012 3:33:21PM
BRL Report 1212016
Page 43 of 274
BRL Report 1212016
Page 44 of 274
BRL Report 1212016
Page 45 of 274
BRL Report 1212016
Page 46 of 274
BRL Report 1212016
Page 47 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes1 IBL SEQ-IBL1 1 55,470 5.26 5.26 < 40 accept
Notes
Date:Time:
4/3/1212:15 PM
Peak rt Area1 1.19 55,470
0
200
400
600
800
1,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes2 IBL SEQ-IBL2 1 55,349 5.25 5.25 < 40 accept
Notes
Date:Time:
4/3/1212:20 PM
Peak rt Area1 1.15 55,349
0
200
400
600
800
1,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes3 IBL SEQ-IBL3 1 55,551 5.27 5.27 < 40 accept
Notes
Date:Time:
4/3/1212:34 PM
Peak rt Area1 1.16 55,5512 2.56 12
0
200
400
600
800
1,000
0 1 2 3
1 2
Page 1 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 48 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes4 IBL SEQ-IBL4 1 53,035 5.03 5.03 < 40 accept
Notes
Date:Time:
4/3/1212:44 PM
Peak rt Area1 1.19 53,035
0
200
400
600
800
1,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes5 CAL SEQ-CAL1 1 327,429 25.9 103 80-120 accept
Notes
Date:Time:
4/3/1212:56 PM
Peak rt Area1 1.19 327,429
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes6 CAL SEQ-CAL2 1 1,103,065 99.4 99.4 80-120 accept
Notes
Date:Time:
4/3/121:02 PM
Peak rt Area1 1.15 1,103,065
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Page 2 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 49 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes7 CAL SEQ-CAL3 1 5,151,337 484 96.7 80-120 reject
Notes
Date:Time:
4/3/121:11 PM
Peak rt Area1 1.14 5,151,3372 1.66 1,339,500
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1 2
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes8 CAL SEQ-CAL4 1 25,773,763 2,440 97.6 80-120 accept
Notes
Date:Time:
4/3/121:17 PM
Peak rt Area1 1.18 25,773,763
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes9 CAL SEQ-CAL5 1 104,280,648 9,890 98.9 80-120 accept
Notes
Date:Time:
4/3/121:21 PM
Peak rt Area1 1.15 104,280,648
0
400,000
800,000
1,200,000
1,600,000
2,000,000
0 1 2 3
1
Page 3 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 50 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes10 ICV SEQ-ICV1 1 16,735,916 1,580 101 85-115 accept
Notes
Date:Time:
4/3/121:25 PM
Peak rt Area1 1.16 16,735,916
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes11 CAL SEQ-CAL6 1 5,367,831 504 101 80-120 accept
Notes
Date:Time:
4/3/121:30 PM
Peak rt Area1 1.19 5,367,831
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes12 S B120480-BLK1 1 157,668 9.75 0.00 < HS accept
Notes
Date:Time:
4/3/121:38 PM
Peak rt Area1 1.20 157,668
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 4 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 51 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes13 CCB SEQ-CCB1 1 52,702 5.00 5.00 < 40 accept
Notes
Date:Time:
4/3/121:42 PM
Peak rt Area1 1.21 52,702
0
200
400
600
800
1,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes14 S B120480-BLK2 1 90,048 3.34 0.00 < HS accept
Notes
Date:Time:
4/3/121:48 PM
Peak rt Area1 1.19 90,0482 2.00 1623 2.58 6,0314 2.59 769
0
200
400
600
800
1,000
0 1 2 3
1 2 34
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes15 S B120480-BLK3 1 92,451 3.57 0.00 < HS accept
Notes
Date:Time:
4/3/121:52 PM
Peak rt Area1 1.19 92,451
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 5 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 52 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes16 S B120480-BLK4 1 83,141 2.68 0.00 < HS accept
Notes
Date:Time:
4/3/121:56 PM
Peak rt Area1 1.17 83,141
0
200
400
600
800
1,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes17 CCV SEQ-CCV 1 5,323,211 500. 100. 77-123 accept
Notes
Date:Time:
4/3/122:49 PM
Peak rt Area1 1.16 5,323,211
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes18 CCB SEQ-CCB 1 39,560 3.75 3.75 < 40 accept
Notes
Date:Time:
4/3/122:53 PM
Peak rt Area1 1.13 39,5602 1.66 3483 1.86 5414 1.96 1,2735 2.07 2,5546 2.19 3,7407 2.33 10,3008 2.60 23,5259 2.70 7,948
10 2.84 25,80811 2.97 4,669
0
200
400
600
800
1,000
0 1 2 3
1 2 3 4 5 6 7 8 9 10 11
Page 6 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 53 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes19 S 1212026-01 1 10,162,132 959 0.00 < HS accept
Notes
Date:Time:
4/3/123:01 PM
Peak rt Area1 1.16 10,162,132
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes20 S 1212027-01 1 5,561,408 522 0.00 < HS accept
Notes
Date:Time:
4/3/123:05 PM
Peak rt Area1 1.18 5,561,408
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes21 S 1212011-02 1 251,475 18.7 0.00 < HS accept
Notes
Date:Time:
4/3/123:10 PM
Peak rt Area1 1.16 251,475
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 7 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 54 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes22 S 1212016-01 1 7,061,836 665 0.00 < HS accept
Notes
Date:Time:
4/3/123:15 PM
Peak rt Area1 1.15 7,061,836
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes23 S 1212016-03 1 2,641,427 245 0.00 < HS accept
Notes
Date:Time:
4/3/123:20 PM
Peak rt Area1 1.14 2,641,427
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes24 S 1212016-05 2 3,643,585 340. 0.00 < HS accept
Notes
Date:Time:
4/3/123:24 PM
Peak rt Area1 0.76 5132 1.18 3,643,585
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1 2
Page 8 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 55 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes25 S 1212016-07 1 3,984,189 373 0.00 < HS accept
Notes
Date:Time:
4/3/123:36 PM
Peak rt Area1 1.18 3,984,189
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes26 S 1212016-09 1 2,966,396 276 0.00 < HS accept
Notes
Date:Time:
4/3/123:40 PM
Peak rt Area1 1.18 2,966,396
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes27 S 1212016-11 1 1,975,773 182 0.00 < HS accept
Notes
Date:Time:
4/3/123:45 PM
Peak rt Area1 1.15 1,975,773
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Page 9 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 56 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes28 S 1212016-13 1 5,654,909 531 0.00 < HS accept
Notes
Date:Time:
4/3/123:50 PM
Peak rt Area1 1.14 5,654,909
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes29 S B120480-MS1 1 59,606,278 5,650 0.00 < HS accept
Notes
Date:Time:
4/3/123:56 PM
Peak rt Area1 1.14 59,606,278
0
400,000
800,000
1,200,000
1,600,000
2,000,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes30 S B120480-MSD1 1 60,798,174 5,760 0.00 < HS accept
Notes
Date:Time:
4/3/124:00 PM
Peak rt Area1 1.16 60,798,174
0
400,000
800,000
1,200,000
1,600,000
2,000,000
0 1 2 3
1
Page 10 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 57 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes31 S B120480-MS2 1 41,421,187 3,920 0.00 < HS accept
Notes
Date:Time:
4/3/124:04 PM
Peak rt Area1 1.17 41,421,187
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes32 S B120480-MSD2 1 41,593,013 3,940 0.00 < HS accept
Notes
Date:Time:
4/3/124:08 PM
Peak rt Area1 1.14 41,593,013
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes33 S 1212011-02RE1 1 2,016,037 186 0.00 < HS accept
Notes
Date:Time:
4/3/124:15 PM
Peak rt Area1 1.18 2,016,037
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Page 11 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 58 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes34 CCV SEQ-CCV 1 5,585,908 525 105 77-123 accept
Notes
Date:Time:
4/3/124:21 PM
Peak rt Area1 1.14 5,585,908
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes35 S 1212016-15 1 2,677,657 249 0.00 < HS accept
Notes
Date:Time:
4/3/124:25 PM
Peak rt Area1 1.20 2,677,657
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes36 S 1212016-17 1 3,988,027 373 0.00 < HS accept
Notes
Date:Time:
4/3/124:29 PM
Peak rt Area1 1.22 3,988,027
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Page 12 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 59 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes37 S 1212011-01 1 2,408,834 223 0.00 < HS accept
Notes
Date:Time:
4/3/124:36 PM
Peak rt Area1 1.19 2,408,8342 1.70 4,968
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1 2
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes38 S 1212016-02 1 392,638 32.0 0.00 < HS accept
Notes
Date:Time:
4/3/125:10 PM
Peak rt Area1 1.14 392,638
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes39 S 1212016-04 1 408,122 33.5 0.00 < HS accept
Notes
Date:Time:
4/3/125:14 PM
Peak rt Area1 1.17 408,122
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 13 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 60 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes40 S 1212016-06 1 361,204 29.1 0.00 < HS accept
Notes
Date:Time:
4/3/125:22 PM
Peak rt Area1 1.17 361,204
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes41 S 1212016-08 1 347,811 27.8 0.00 < HS accept
Notes
Date:Time:
4/3/125:29 PM
Peak rt Area1 1.17 347,811
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes42 S 1211017-01 1 22,194,132 2,100 0.00 < HS accept
Notes
Date:Time:
4/3/125:34 PM
Peak rt Area1 1.12 22,194,132
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Page 14 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 61 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes43 S 1211017-02 1 3,589,189 335 0.00 < HS accept
Notes
Date:Time:
4/3/125:38 PM
Peak rt Area1 1.15 3,589,189
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes44 S 1211017-03 1 40,693,085 3,860 0.00 < HS accept
Notes
Date:Time:
4/3/125:45 PM
Peak rt Area1 1.10 40,693,085
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes45 S B120480-MS3 1 20,468,098 1,940 0.00 < HS accept
Notes
Date:Time:
4/3/125:50 PM
Peak rt Area1 1.13 20,468,098
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Page 15 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 62 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes46 S B120480-MSD3 1 20,554,965 1,940 0.00 < HS accept
Notes
Date:Time:
4/3/125:56 PM
Peak rt Area1 1.13 20,554,965
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes47 CCV SEQ-CCV 1 5,305,185 498 99.6 77-123 accept
Notes
Date:Time:
4/3/126:00 PM
Peak rt Area1 1.17 5,305,185
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes48 S 1212016-10 1 473,626 39.7 0.00 < HS accept
Notes
Date:Time:
4/3/126:05 PM
Peak rt Area1 1.20 473,626
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 16 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 63 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes49 S 1212016-12 1 348,126 27.8 0.00 < HS accept
Notes
Date:Time:
4/3/126:10 PM
Peak rt Area1 1.20 348,126
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes50 S 1212016-14 1 4,790,188 449 0.00 < HS accept
Notes
Date:Time:
4/3/126:17 PM
Peak rt Area1 1.20 4,790,1882 2.75 3583 2.78 779
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1 23
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes51 S 1212016-16 1 428,880 35.5 0.00 < HS accept
Notes
Date:Time:
4/3/126:22 PM
Peak rt Area1 1.17 428,880
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 17 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 64 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes52 S 1212016-18 1 357,482 28.7 0.00 < HS accept
Notes
Date:Time:
4/3/126:26 PM
Peak rt Area1 1.18 357,482
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes53 CCV SEQ-CCV 1 5,311,726 499 99.7 77-123 accept
Notes
Date:Time:
4/3/126:32 PM
Peak rt Area1 1.12 5,311,7262 1.40 53,1583 2.25 9,3834 2.34 12,217
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes54 S DIW 1 118,647 6.05 0.00 < HS accept
Notes
Date:Time:
4/3/126:37 PM
Peak rt Area1 1.12 118,647
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 18 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 65 of 274
Peak ReportBatch Number: B120480
Method Number: CVAFS BR-0006Project Number(s): 1200235 Date Analyzed: 4/3/12Instrument ID: BR-10 Analyst Name: MSU
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes55 S A 1 117,313 5.93 0.00 < HS accept
Notes
Date:Time:
4/3/126:42 PM
Peak rt Area1 1.12 117,313
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes56 S B 1 149,414 8.97 0.00 < HS accept
Notes
Date:Time:
4/3/126:47 PM
Peak rt Area1 1.14 149,414
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 19 of 19 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 66 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200251
THG-05Instrument:
Batch # Source ID
Brooks Rand Labs
1200251-IBL1 QC 11200251 -
1200251-IBL2 QC 21200251 -
1200251-IBL3 QC 31200251 -
1200251-IBL4 QC 41200251 -
1200251-CAL1 QC 5 12130061200251 -
1200251-CAL2 QC 6 12130071200251 -
1200251-CAL3 QC 7 12130081200251 -
1200251-CAL4 QC 8 12130091200251 -
1200251-CAL5 QC 9 12130101200251 -
1200251-ICV1 QC 10 12130121200251 -
B120509-SRM1 QC 11B120509 -
1200251-CCV1 QC 12 12130111200251 -
B120509-BLK1 QC 13B120509 -
1200251-CCB1 QC 141200251 -
B120509-BLK2 QC 15B120509 -
B120509-BLK3 QC 16B120509 -
B120509-BLK4 QC 17B120509 -
1200251-IBL5 QC 181200251 -
1212016-21 Hg-W-BrCl-CVAFS-NoMB-TR 19B120509 AAL-MN1101 4/10/2012
1212016-22 Hg-W-BrCl-CVAFS-NoMB-Diss 20B120509 AAL-MN1101 4/10/2012
1212016-19 Hg-W-BrCl-CVAFS-TR 21 BatchQCB120509 AAL-MN1101 1/1/1980
1212016-19 Hg-W-BrCl-CVAFS-Diss 22 BatchQCB120509 AAL-MN1101 1/1/1980
1212016-19 Hg-W-BrCl-CVAFS-NoMB-Diss 23 BatchQCB120509 AAL-MN1101 1/1/1980
1212016-19 Hg-W-BrCl-CVAFS-NoMB-TR 24B120509 AAL-MN1101 4/10/2012
1213025-05 Hg-W-BrCl-CVAFS-TR 25B120509 ECA-GJ1001 4/9/2012
1214016-01 Hg-W-BrCl-CVAFS-TR 26B120509 H2M-MV1101 4/6/2012
Page 1 of 4Printed: 4/9/2012 7:24:11PM
BRL Report 1212016
Page 67 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200251
THG-05Instrument:
Batch # Source ID
Brooks Rand Labs
1212011-03 Hg-W-BrCl-CVAFS-TR 27B120509 AXS-BC1201 4/11/2012
1213025-01 Hg-W-BrCl-CVAFS-TR 28B120509 ECA-GJ1001 4/9/2012
1213025-01 Hg-W-BrCl-CVAFS-Diss 29 BatchQCB120509 ECA-GJ1001 1/1/1980
1213025-01 Hg-W-BrCl-CVAFS-NoMB-Diss 30 BatchQCB120509 ECA-GJ1001 1/1/1980
1213025-01 Hg-W-BrCl-CVAFS-NoMB-TR 31 BatchQCB120509 ECA-GJ1001 1/1/1980
1213037-01 Hg-W-BrCl-CVAFS-TR 32B120509 HCL-MU0801 4/4/2012
1213030-01 Hg-W-BrCl-CVAFS-TR 33B120509 MAX-CA1201 4/9/2012
1213009-09 Hg-W-BrCl-CVAFS-Diss 34B120509 ACC-SJ1201 4/6/2012
1213009-11 Hg-W-BrCl-CVAFS-Diss 35B120509 ACC-SJ1201 4/6/2012
1212016-20 Hg-W-BrCl-CVAFS-NoMB-Diss 36B120509 AAL-MN1101 4/10/2012
1214016-01RE1 Hg-W-BrCl-CVAFS-TR 37 Added 4/9/2012 by TKEB120509 H2M-MV1101 4/6/2012
B120509-MS1 QC 38B120509 1212016-19
B120509-MSD1 QC 39B120509 1212016-19
B120509-MS2 QC 40B120509 1213025-01
B120509-MSD2 QC 41B120509 1213025-01
1213009-09RE1 Hg-W-BrCl-CVAFS-Diss 42 Added 4/9/2012 by TKEB120509 ACC-SJ1201 4/6/2012
1213009-11RE1 Hg-W-BrCl-CVAFS-Diss 43 Added 4/9/2012 by TKEB120509 ACC-SJ1201 4/6/2012
1200251-CCV2 QC 44 12130111200251 -
1214016-02 Hg-W-BrCl-CVAFS-TR 45B120509 H2M-MV1101 4/6/2012
1214016-03 Hg-W-BrCl-CVAFS-TR 46B120509 H2M-MV1101 4/6/2012
1214016-04 Hg-W-BrCl-CVAFS-TR 47B120509 H2M-MV1101 4/6/2012
1212016-23 Hg-W-BrCl-CVAFS-TR 48 BatchQCB120509 AAL-MN1101 1/1/1980
1212016-23 Hg-W-BrCl-CVAFS-Diss 49 BatchQCB120509 AAL-MN1101 1/1/1980
1212016-23 Hg-W-BrCl-CVAFS-NoMB-Diss 50 BatchQCB120509 AAL-MN1101 1/1/1980
1212016-23 Hg-W-BrCl-CVAFS-NoMB-TR 51B120509 AAL-MN1101 4/10/2012
1212016-24 Hg-W-BrCl-CVAFS-NoMB-Diss 52B120509 AAL-MN1101 4/10/2012
Page 2 of 4Printed: 4/9/2012 7:24:11PM
BRL Report 1212016
Page 68 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200251
THG-05Instrument:
Batch # Source ID
Brooks Rand Labs
1212016-25 Hg-W-BrCl-CVAFS-NoMB-TR 53B120509 AAL-MN1101 4/10/2012
1212016-26 Hg-W-BrCl-CVAFS-NoMB-Diss 54B120509 AAL-MN1101 4/10/2012
1213009-13 Hg-W-BrCl-CVAFS-Diss 55B120509 ACC-SJ1201 4/6/2012
1213009-15 Hg-W-BrCl-CVAFS-Diss 56B120509 ACC-SJ1201 4/6/2012
1212011-04 Hg-W-BrCl-CVAFS-TR 57B120509 AXS-BC1201 4/11/2012
1212011-04 Hg-W-BrCl-CVAFS-Diss 58 BatchQCB120509 AXS-BC1201 1/1/1980
1212011-04 Hg-W-BrCl-CVAFS-NoMB-Diss 59 BatchQCB120509 AXS-BC1201 1/1/1980
1212011-04 Hg-W-BrCl-CVAFS-NoMB-TR 60 BatchQCB120509 AXS-BC1201 1/1/1980
1214016-02RE1 Hg-W-BrCl-CVAFS-TR 61 Added 4/9/2012 by TKEB120509 H2M-MV1101 4/6/2012
1214016-03RE1 Hg-W-BrCl-CVAFS-TR 62 Added 4/9/2012 by TKEB120509 H2M-MV1101 4/6/2012
1214016-04RE1 Hg-W-BrCl-CVAFS-TR 63 Added 4/9/2012 by TKEB120509 H2M-MV1101 4/6/2012
B120509-MS3 QC 64B120509 1212016-23
B120509-MSD3 QC 65B120509 1212016-23
B120509-MS4 QC 66B120509 1212011-04
B120509-MSD4 QC 67B120509 1212011-04
1213009-13RE1 Hg-W-BrCl-CVAFS-Diss 68 Added 4/9/2012 by TKEB120509 ACC-SJ1201 4/6/2012
1200251-CCV3 QC 69 12130111200251 -
1212011-05 Hg-W-BrCl-CVAFS-TR 70B120509 AXS-BC1201 4/11/2012
1212011-06 Hg-W-BrCl-CVAFS-TR 71B120509 AXS-BC1201 4/11/2012
1212011-07 Hg-W-BrCl-CVAFS-TR 72B120509 AXS-BC1201 4/11/2012
1212011-08 Hg-W-BrCl-CVAFS-TR 73B120509 AXS-BC1201 4/11/2012
1212011-09 Hg-W-BrCl-CVAFS-TR 74B120509 AXS-BC1201 4/11/2012
1213025-02 Hg-W-BrCl-CVAFS-TR 75B120509 ECA-GJ1001 4/9/2012
1213025-03 Hg-W-BrCl-CVAFS-TR 76B120509 ECA-GJ1001 4/9/2012
1213025-04 Hg-W-BrCl-CVAFS-TR 77B120509 ECA-GJ1001 4/9/2012
1213027-01 Hg-W-BrCl-CVAFS-Diss 78B120509 ACC-SJ1201 4/9/2012
Page 3 of 4Printed: 4/9/2012 7:24:11PM
BRL Report 1212016
Page 69 of 274
BRL Report 1212016
Page 70 of 274
BRL Report 1212016
Page 71 of 274
BRL Report 1212016
Page 72 of 274
BRL Report 1212016
Page 73 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes1 IBL SEQ-IBL1 1 50,029 4.96 4.96 < 40 reject
Notes
Date:Time:
4/9/1210:34 AM
Peak rt Area1 1.03 50,0292 1.25 14,269
0
200
400
600
800
1,000
0 1 2 3
1 2
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes2 IBL SEQ-IBL2 1 44,089 4.37 4.37 < 40 accept
Notes
Date:Time:
4/9/1210:38 AM
Peak rt Area1 1.08 44,089
0
200
400
600
800
1,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes3 IBL SEQ-IBL3 1 40,190 3.99 3.99 < 40 accept
Notes
Date:Time:
4/9/1210:42 AM
Peak rt Area1 1.05 40,190
0
200
400
600
800
1,000
0 1 2 3
1
Page 1 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 74 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes4 IBL SEQ-IBL4 1 36,702 3.64 3.64 < 40 accept
Notes
Date:Time:
4/9/1210:46 AM
Peak rt Area1 1.07 36,702
0
200
400
600
800
1,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes5 CAL SEQ-CAL1 1 294,760 24.9 99.8 80-120 accept
Notes
Date:Time:
4/9/1210:52 AM
Peak rt Area1 1.08 294,760
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes6 CAL SEQ-CAL2 1 1,058,254 101 101 80-120 accept
Notes
Date:Time:
4/9/1210:56 AM
Peak rt Area1 1.06 1,058,254
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Page 2 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 75 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes7 CAL SEQ-CAL3 1 5,142,494 506 101 80-120 accept
Notes
Date:Time:
4/9/1211:01 AM
Peak rt Area1 1.04 5,142,494
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes8 CAL SEQ-CAL4 1 25,065,924 2,480 99.3 80-120 accept
Notes
Date:Time:
4/9/1211:06 AM
Peak rt Area1 1.10 25,065,924
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes9 CAL SEQ-CAL5 1 99,950,545 9,910 99.1 80-120 accept
Notes
Date:Time:
4/9/1211:11 AM
Peak rt Area1 1.02 99,950,545
0
400,000
800,000
1,200,000
1,600,000
2,000,000
0 1 2 3
1
Page 3 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 76 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes10 ICV SEQ-ICV1 2 15,824,450 1,570 99.8 85-115 accept
Notes
Date:Time:
4/9/1211:15 AM
Peak rt Area1 0.18 4222 1.04 15,824,450
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1 2
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes11 CCV SEQ-CCV 1 5,125,287 504 101 77-123 accept
Notes
Date:Time:
4/9/1211:19 AM
Peak rt Area1 1.02 5,125,287
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes12 S B120509-BLK1 1 121,770 7.79 0.00 < HS accept
Notes
Date:Time:
4/9/1211:24 AM
Peak rt Area1 1.05 121,770
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 4 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 77 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes13 CCB SEQ-CCB1 1 87,300 8.66 8.66 < 40 accept
Notes
Date:Time:
4/9/1211:31 AM
Peak rt Area1 1.06 87,300
0
200
400
600
800
1,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes14 S B120509-BLK2 1 131,041 8.71 0.00 < HS accept
Notes
Date:Time:
4/9/1211:43 AM
Peak rt Area1 1.08 131,041
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes15 S B120509-BLK3 1 136,630 9.26 0.00 < HS accept
Notes
Date:Time:
4/9/1211:47 AM
Peak rt Area1 1.04 136,630
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 5 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 78 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes16 S B120509-BLK4 1 101,076 5.73 0.00 < HS accept
Notes
Date:Time:
4/9/1211:51 AM
Peak rt Area1 1.04 101,076
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes17 IBL SEQ-IBL5 1 52,117 5.17 5.17 < 40 accept
Notes
Date:Time:
4/9/1211:58 AM
Peak rt Area1 1.09 52,117
-100
100
300
500
700
900
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes18 S 1212016-21 1 816,548 76.7 0.00 < HS accept
Notes
Date:Time:
4/9/1212:02 PM
Peak rt Area1 1.04 816,548
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Page 6 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 79 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes19 S 1212016-22 1 255,404 21.0 0.00 < HS accept
Notes
Date:Time:
4/9/1212:16 PM
Peak rt Area1 1.08 255,404
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes20 S 1212016-19 1 6,666,857 657 0.00 < HS accept
Notes
Date:Time:
4/9/121:18 PM
Peak rt Area1 1.10 6,666,857
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes21 S 1213025-05 1 173,051 12.9 0.00 < HS accept
Notes
Date:Time:
4/9/121:22 PM
Peak rt Area1 1.05 173,051
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 7 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 80 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes22 S 1214016-01 1 151,351 10.7 0.00 < HS accept
Notes
Date:Time:
4/9/121:30 PM
Peak rt Area1 1.07 151,351
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes23 S 1212011-03 1 3,348,974 328 0.00 < HS accept
Notes
Date:Time:
4/9/121:37 PM
Peak rt Area1 1.07 3,348,974
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes24 S 1213025-01 2 1,839,350 178 0.00 < HS accept
Notes
Date:Time:
4/9/121:43 PM
Peak rt Area1 0.56 2032 1.06 1,839,350
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1 2
Page 8 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 81 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes25 S 1213037-01 1 2,811,197 275 0.00 < HS accept
Notes
Date:Time:
4/9/121:52 PM
Peak rt Area1 1.10 2,811,197
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes26 S 1213030-01 1 961,627 91.1 0.00 < HS accept
Notes
Date:Time:
4/9/121:59 PM
Peak rt Area1 1.09 961,627
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes27 S 1213009-09 1 35,098 -0.811 0.00 < HS accept
Notes
Date:Time:
4/9/122:03 PM
Peak rt Area1 1.04 35,098
-200
0
200
400
600
800
0 1 2 3
1
Page 9 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 82 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes28 S 1213009-11 1 41,590 -0.167 0.00 < HS accept
Notes
Date:Time:
4/9/122:08 PM
Peak rt Area1 1.06 41,590
-200
0
200
400
600
800
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes29 S 1212016-20 1 1,206,608 115 0.00 < HS accept
Notes
Date:Time:
4/9/122:14 PM
Peak rt Area1 1.08 1,206,608
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes30 S 1214016-01RE1 1 579,651 53.2 0.00 < HS accept
Notes
Date:Time:
4/9/122:19 PM
Peak rt Area1 1.08 579,651
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Page 10 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 83 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes31 S B120509-MS1 1 37,238,446 3,690 0.00 < HS accept
Notes
Date:Time:
4/9/122:23 PM
Peak rt Area1 1.07 37,238,446
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes32 S B120509-MSD1 1 37,013,897 3,670 0.00 < HS accept
Notes
Date:Time:
4/9/122:28 PM
Peak rt Area1 1.07 37,013,897
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes33 S B120509-MS2 1 10,096,033 997 0.00 < HS accept
Notes
Date:Time:
4/9/122:34 PM
Peak rt Area1 1.04 10,096,033
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Page 11 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 84 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes34 S B120509-MSD2 1 10,032,048 991 0.00 < HS accept
Notes
Date:Time:
4/9/122:39 PM
Peak rt Area1 1.04 10,032,048
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes35 S 1213009-09RE1 1 437,113 39.1 0.00 < HS accept
Notes
Date:Time:
4/9/122:43 PM
Peak rt Area1 1.06 437,113
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes36 S 1213009-11RE1 1 81,640 3.81 0.00 < HS accept
Notes
Date:Time:
4/9/122:50 PM
Peak rt Area1 1.08 81,640
-200
0
200
400
600
800
0 1 2 3
1
Page 12 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 85 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes37 CCV SEQ-CCV2 1 4,961,170 488 97.6 77-123 accept
Notes
Date:Time:
4/9/122:55 PM
Peak rt Area1 1.07 4,961,170
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes38 S 1214016-02 1 158,769 11.5 0.00 < HS accept
Notes
Date:Time:
4/9/123:00 PM
Peak rt Area1 1.08 158,769
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes39 S 1214016-03 1 141,202 9.71 0.00 < HS accept
Notes
Date:Time:
4/9/123:04 PM
Peak rt Area1 1.04 141,202
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Page 13 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 86 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes40 S 1214016-04 1 61,230 1.78 0.00 < HS accept
Notes
Date:Time:
4/9/123:08 PM
Peak rt Area1 1.04 61,230
-200
0
200
400
600
800
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes41 S 1212016-23 1 2,772,793 271 0.00 < HS accept
Notes
Date:Time:
4/9/123:14 PM
Peak rt Area1 1.08 2,772,793
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes42 S 1212016-24 1 588,983 54.1 0.00 < HS accept
Notes
Date:Time:
4/9/123:19 PM
Peak rt Area1 1.07 588,983
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Page 14 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 87 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes43 S 1212016-25 1 24,158,035 2,390 0.00 < HS accept
Notes
Date:Time:
4/9/123:23 PM
Peak rt Area1 1.06 24,158,035
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes44 S 1212016-26 1 1,055,719 100. 0.00 < HS accept
Notes
Date:Time:
4/9/123:27 PM
Peak rt Area1 1.06 1,055,719
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes45 S 1213009-13 1 47,305 0.400 0.00 < HS accept
Notes
Date:Time:
4/9/123:34 PM
Peak rt Area1 1.02 47,305
-300
-100
100
300
500
700
0 1 2 3
1
Page 15 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 88 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes46 S 1213009-15 1 57,165 1.38 0.00 < HS accept
Notes
Date:Time:
4/9/123:39 PM
Peak rt Area1 1.05 57,165
-300
-100
100
300
500
700
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes47 S 1212011-04 1 2,773,098 271 0.00 < HS accept
Notes
Date:Time:
4/9/123:44 PM
Peak rt Area1 1.07 2,773,098
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes48 S 1214016-02RE1 1 652,190 60.4 0.00 < HS accept
Notes
Date:Time:
4/9/123:48 PM
Peak rt Area1 1.07 652,190
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Page 16 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 89 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes49 S 1214016-03RE1 1 518,427 47.1 0.00 < HS accept
Notes
Date:Time:
4/9/123:54 PM
Peak rt Area1 1.03 518,427
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes50 S 1214016-04RE1 1 123,859 7.99 0.00 < HS accept
Notes
Date:Time:
4/9/123:59 PM
Peak rt Area1 1.05 123,859
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes51 S B120509-MS3 1 12,740,286 1,260 0.00 < HS accept
Notes
Date:Time:
4/9/124:03 PM
Peak rt Area1 1.04 12,740,286
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Page 17 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 90 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes52 S B120509-MSD3 1 12,693,420 1,250 0.00 < HS accept
Notes
Date:Time:
4/9/124:08 PM
Peak rt Area1 1.07 12,693,420
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes53 S B120509-MS4 1 12,645,571 1,250 0.00 < HS accept
Notes
Date:Time:
4/9/124:15 PM
Peak rt Area1 1.11 12,645,571
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes54 S B120509-MSD4 1 12,296,063 1,220 0.00 < HS accept
Notes
Date:Time:
4/9/124:21 PM
Peak rt Area1 1.08 12,296,063
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3
1
Page 18 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 91 of 274
Peak ReportBatch Number: B120509
Method Number: CVAFS BR-0006Project Number(s): 1200251 Date Analyzed: 4/9/12Instrument ID: BR-05 Analyst Name: TE
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes55 S 1213009-13RE1 1 1,249,002 120. 0.00 < HS accept
Notes
Date:Time:
4/9/124:26 PM
Peak rt Area1 1.08 1,249,002
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes56 CCV SEQ-CCV3 1 4,765,620 468 93.7 77-123 accept
Notes
Date:Time:
4/9/124:39 PM
Peak rt Area1 1.02 4,765,620
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3
1
Run Trap Type Name/ID M B Peak Peak Area Analyzed Result Final Result QA Results Criteria Notes57 S 1212011-05 3 1,892,287 183 0.00 < HS accept
Notes
Date:Time:
4/9/124:43 PM
Peak rt Area1 0.18 1,8052 0.36 2053 1.08 1,892,287
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3
1 2 3
Page 19 of 26 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 92 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200258
MMHG-09Instrument:
Batch # Source ID
Brooks Rand Labs
1200258-IBL1 QC 11200258 -
1200258-IBL2 QC 21200258 -
1200258-IBL3 QC 31200258 -
1200258-CAL1 QC 4 12120281200258 -
1200258-CAL2 QC 5 12120291200258 -
1200258-CAL3 QC 6 12120301200258 -
1200258-CAL4 QC 7 12120311200258 -
1200258-CAL5 QC 8 12120321200258 -
1200258-CAL6 QC 9 12120331200258 -
1200258-CAL7 QC 10 12120341200258 -
1200258-CCB1 QC 111200258 -
1200258-ICV1 QC 12 12110081200258 -
1200258-CCB2 QC 131200258 -
1200258-CCV1 QC 14 12120351200258 -
1200258-CCB3 QC 151200258 -
1200258-CCB4 QC 161200258 -
1200258-CCB5 QC 171200258 -
B120596-BLK1 QC 18B120596 -
B120596-BLK2 QC 19B120596 -
B120596-BLK3 QC 20B120596 -
B120596-BLK4 QC 21B120596 -
B120596-BS1 QC 22B120596 -
B120596-BS2 QC 23B120596 -
B120596-BS3 QC 24B120596 -
B120596-BS4 QC 25B120596 -
B120596-BS5 QC 26B120596 -
Page 1 of 5Printed: 4/19/2012 1:42:22PM
BRL Report 1212016
Page 93 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200258
MMHG-09Instrument:
Batch # Source ID
Brooks Rand Labs
B120596-BS6 QC 27B120596 -
1200258-CCV2 QC 28 12120351200258 -
1200258-CCB6 QC 291200258 -
B120596-BS7 QC 30B120596 -
B120596-BS8 QC 31B120596 -
B120596-BS9 QC 32B120596 -
B120596-BSA QC 33B120596 -
B120596-BSB QC 34B120596 -
B120596-BSC QC 35B120596 -
B120596-BSD QC 36B120596 -
B120596-BSE QC 37B120596 -
1200258-CCV3 QC 38 12120351200258 -
1200258-CCB7 QC 391200258 -
B120524-BLK1 QC 40B120524 -
B120524-BLK2 QC 41B120524 -
B120524-BLK3 QC 42B120524 -
B120524-BLK4 QC 43B120524 -
1212016-21 MeHg-W-Dist-NoMB-TR 44B120524 AAL-MN1101 4/10/2012
B120524-BS1 QC 45B120524 -
B120524-BS2 QC 46B120524 -
1213011-17 MeHg-W-Dist-TR 47B120524 UME-OR1201 4/18/2012
1213011-18 MeHg-W-Dist-TR 48B120524 UME-OR1201 4/18/2012
1213011-19 MeHg-W-Dist-TR 49B120524 UME-OR1201 4/18/2012
1200258-CCV4 QC 50 12120351200258 -
1200258-CCB8 QC 511200258 -
1212014-03 MeHg-W-Dist-TR 52B120524 SFE-OA1103 4/12/2012
Page 2 of 5Printed: 4/19/2012 1:42:22PM
BRL Report 1212016
Page 94 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200258
MMHG-09Instrument:
Batch # Source ID
Brooks Rand Labs
1212014-04 MeHg-W-Dist-TR 53B120524 SFE-OA1103 4/12/2012
1212014-04 MeHg-W-Dist-NoMB-TR 54 BatchQCB120524 SFE-OA1103 1/1/1980
B120524-MS1 QC 55B120524 1212014-04
B120524-MSD1 QC 56B120524 1212014-04
1212016-01 MeHg-W-Dist-NoMB-TR 57B120524 AAL-MN1101 4/10/2012
1212016-03 MeHg-W-Dist-NoMB-TR 58B120524 AAL-MN1101 4/10/2012
1212016-05 MeHg-W-Dist-NoMB-TR 59B120524 AAL-MN1101 4/10/2012
1212016-07 MeHg-W-Dist-NoMB-TR 60B120524 AAL-MN1101 4/10/2012
1212016-09 MeHg-W-Dist-NoMB-TR 61B120524 AAL-MN1101 4/10/2012
1212016-11 MeHg-W-Dist-NoMB-TR 62B120524 AAL-MN1101 4/10/2012
1200258-CCV5 QC 63 12120351200258 -
1200258-CCB9 QC 641200258 -
B120524-MS2 QC 65B120524 1212016-11
B120524-MSD2 QC 66B120524 1212016-11
1212016-13 MeHg-W-Dist-NoMB-TR 67B120524 AAL-MN1101 4/10/2012
1212016-15 MeHg-W-Dist-NoMB-TR 68B120524 AAL-MN1101 4/10/2012
1212016-17 MeHg-W-Dist-NoMB-TR 69B120524 AAL-MN1101 4/10/2012
1212016-19 MeHg-W-Dist-NoMB-TR 70B120524 AAL-MN1101 4/10/2012
1212016-23 MeHg-W-Dist-NoMB-TR 71B120524 AAL-MN1101 4/10/2012
1212016-25 MeHg-W-Dist-NoMB-TR 72B120524 AAL-MN1101 4/10/2012
1213006-01 MeHg-W-Dist-NoMB-TR 73B120524 AAL-MN1101 4/18/2012
1213006-03 MeHg-W-Dist-NoMB-TR 74B120524 AAL-MN1101 4/18/2012
1200258-CCV6 QC 75 12120351200258 -
1200258-CCBA QC 761200258 -
1213006-05 MeHg-W-Dist-NoMB-TR 77B120524 AAL-MN1101 4/18/2012
1213006-07 MeHg-W-Dist-NoMB-TR 78B120524 AAL-MN1101 4/18/2012
Page 3 of 5Printed: 4/19/2012 1:42:22PM
BRL Report 1212016
Page 95 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200258
MMHG-09Instrument:
Batch # Source ID
Brooks Rand Labs
1213006-09 MeHg-W-Dist-NoMB-TR 79B120524 AAL-MN1101 4/18/2012
1212016-11 MeHg-W-Dist-TR 80 BatchQCB120524 AAL-MN1101 1/1/1980
1213006-11 MeHg-W-Dist-NoMB-TR 81B120524 AAL-MN1101 4/18/2012
1213006-13 MeHg-W-Dist-NoMB-TR 82B120524 AAL-MN1101 4/18/2012
1213006-15 MeHg-W-Dist-NoMB-TR 83B120524 AAL-MN1101 4/18/2012
1213006-15 MeHg-W-Dist-TR 84 BatchQCB120524 AAL-MN1101 1/1/1980
B120524-MS3 QC 85B120524 1213006-15
B120524-MSD3 QC 86B120524 1213006-15
1213006-17 MeHg-W-Dist-NoMB-TR 87B120524 AAL-MN1101 4/18/2012
1213006-19 MeHg-W-Dist-NoMB-TR 88B120524 AAL-MN1101 4/18/2012
1200258-CCV7 QC 89 12120351200258 -
1200258-CCBB QC 901200258 -
1213006-21 MeHg-W-Dist-NoMB-TR 91B120524 AAL-MN1101 4/18/2012
1213006-23 MeHg-W-Dist-NoMB-TR 92B120524 AAL-MN1101 4/18/2012
1213006-25 MeHg-W-Dist-NoMB-TR 93B120524 AAL-MN1101 4/18/2012
1213006-31 MeHg-W-Dist-NoMB-TR 94B120524 AAL-MN1101 4/18/2012
1213006-31 MeHg-W-Dist-TR 95 BatchQCB120524 AAL-MN1101 1/1/1980
B120524-MS4 QC 96B120524 1213006-31
B120524-MSD4 QC 97B120524 1213006-31
1213006-33 MeHg-W-Dist-NoMB-TR 98B120524 AAL-MN1101 4/18/2012
1213006-35 MeHg-W-Dist-NoMB-TR 99B120524 AAL-MN1101 4/18/2012
1200258-CCV8 QC 100 12120351200258 -
1200258-CCBC QC 1011200258 -
B120566-BLK1 QC 102B120566 -
B120566-BLK2 QC 103B120566 -
B120566-BLK3 QC 104B120566 -
Page 4 of 5Printed: 4/19/2012 1:42:22PM
BRL Report 1212016
Page 96 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200258
MMHG-09Instrument:
Batch # Source ID
Brooks Rand Labs
B120566-BLK4 QC 105B120566 -
1200258-CCBD QC 1061200258 -
B120566-SRM1 QC 107B120566 -
1211036-02 MeHg-B-KOH/Me 108B120566 ACF-SH1201 6/25/2012
B120566-DUP1 QC 109B120566 1211036-02
B120566-MS1 QC 110B120566 1211036-02
B120566-MSD1 QC 111B120566 1211036-02
1200258-CCV9 QC 112 12120351200258 -
1200258-CCBE QC 1131200258 -
1214009-01 MeHg-B-KOH/Me 114B120566 UME-OR1201 4/25/2012
1214009-02 MeHg-B-KOH/Me 115B120566 UME-OR1201 4/25/2012
1214009-03 MeHg-B-KOH/Me 116B120566 UME-OR1201 4/25/2012
1214009-04 MeHg-B-KOH/Me 117B120566 UME-OR1201 4/25/2012
1200258-CCVA QC 118 12120351200258 -
1200258-CCBF QC 1191200258 -
Page 5 of 5Printed: 4/19/2012 1:42:22PM
BRL Report 1212016
Page 97 of 274
BRL Report 1212016
Page 98 of 274
BRL Report 1212016
Page 99 of 274
BRL Report 1212016
Page 100 of 274
BRL Report 1212016
Page 101 of 274
BRL Report 1212016
Page 102 of 274
BRL Report 1212016
Page 103 of 274
BRL Report 1212016
Page 104 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes1 A Rins Rinse 2 62 0.203 0.00 0.00 < 0.05 accept
Notes
Date:Time:
4/11/1212:51 PM
Peak rt Height1 0.52 5522 1.12 623 2.44 356
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes2 B Rins Rinse 2 49 0.161 0.00 0.00 < 0.05 accept
Notes
Date:Time:
4/11/1212:58 PM
Peak rt Height1 0.53 6492 1.10 493 2.43 300
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes3 C Rins Rinse 2 46 0.151 0.00 0.00 < 0.05 accept
Notes
Date:Time:
4/11/121:05 PM
Peak rt Height1 0.52 8202 1.14 463 2.44 241
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 1 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 105 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes4 A CB SEQ-IBL 2 44 0.144 0.144 < 1.4 accept
Notes
Date:Time:
4/11/121:11 PM
Peak rt Height1 0.52 5352 1.10 443 2.45 2084 3.75 15 3.77 46 4.20 117 4.42 1
-100
100
300
500
700
900
0 1 2 3 4 5
1 2 3 45 6 7
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes5 B CB SEQ-IBL 2 37 0.121 0.121 < 1.4 accept
Notes
Date:Time:
4/11/121:18 PM
Peak rt Height1 0.53 5882 1.10 373 2.44 203
-100
100
300
500
700
900
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes6 C CB SEQ-IBL 2 43 0.141 0.141 < 1.4 accept
Notes
Date:Time:
4/11/121:25 PM
Peak rt Height1 0.52 8142 1.12 433 2.45 169
-200
0
200
400
600
800
0 1 2 3 4 5
1 2 3
Page 2 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 106 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes7 A STD SEQ-CAL1 2 191 0.491 98.2 65-135 accept
Notes
Date:Time:
4/11/121:31 PM
Peak rt Height1 0.52 5382 1.13 1913 2.45 208
-200
0
200
400
600
800
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes8 B STD SEQ-CAL2 2 346 0.999 99.9 65-135 accept
Notes
Date:Time:
4/11/121:38 PM
Peak rt Height1 0.52 5332 1.12 3463 2.43 185
-300
-100
100
300
500
700
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes9 C STD SEQ-CAL3 2 617 1.89 94.4 65-135 accept
Notes
Date:Time:
4/11/121:45 PM
Peak rt Height1 0.52 7352 1.14 6173 2.47 275
-300
-100
100
300
500
700
0 1 2 3 4 5
1 2 3
Page 3 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 107 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes10 A STD SEQ-CAL4 2 2,993 9.68 96.8 65-135 accept
Notes
Date:Time:
4/11/121:51 PM
Peak rt Height1 0.52 5182 1.13 2,9933 2.47 170
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes11 B STD SEQ-CAL5 2 15,260 49.9 99.8 65-135 accept
Notes
Date:Time:
4/11/121:58 PM
Peak rt Height1 0.53 5112 1.12 15,2603 2.44 196
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes12 C STD SEQ-CAL6 2 78,871 259 103 65-135 accept
Notes
Date:Time:
4/11/122:05 PM
Peak rt Height1 0.52 7522 1.14 78,8713 2.44 307
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3 4 5
1 2 3
Page 4 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 108 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes13 A STD SEQ-CAL7 2 331,161 1,090 109 65-135 accept
Notes
Date:Time:
4/11/122:11 PM
Peak rt Height1 0.53 9782 1.13 331,1613 2.43 318
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes14 B CCB SEQ-CCB 2 249 0.817 0.817 < 1.4 accept
Notes
Date:Time:
4/11/122:18 PM
Peak rt Height1 0.52 5232 1.11 2493 2.44 161
-600
-400
-200
0
200
400
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes15 C ICV SEQ-ICV 2 30,998 102 102 80-120 accept
Notes
Date:Time:
4/11/122:25 PM
Peak rt Height1 0.52 8062 1.14 30,9983 2.47 2,616
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3 4 5
1 2 3
Page 5 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 109 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes16 A CCB SEQ-CCB 2 426 1.40 1.40 < 1.4 accept
Notes
Date:Time:
4/11/122:31 PM
Peak rt Height1 0.52 7502 1.13 4263 2.47 193
-700
-500
-300
-100
100
300
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes17 B CCV SEQ-CCV 2 7,778 25.4 102 67-133 accept
Notes
Date:Time:
4/11/122:38 PM
Peak rt Height1 0.52 4962 1.12 7,7783 2.44 2164 4.58 23
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes18 C CCB SEQ-CCB 2 138 0.453 0.453 < 1.4 accept
Notes
Date:Time:
4/11/122:45 PM
Peak rt Height1 0.52 7682 1.14 1383 2.46 164
-800
-600
-400
-200
0
200
0 1 2 3 4 5
1 2 3
Page 6 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 110 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes19 A CCB SEQ-CCB 2 114 0.374 0.374 < 1.4 accept
Notes
Date:Time:
4/11/122:51 PM
Peak rt Height1 0.52 6552 1.13 1143 2.46 147
-900
-700
-500
-300
-100
100
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes20 B CCB SEQ-CCB 2 60 0.197 0.197 < 1.4 accept
Notes
Date:Time:
4/11/122:58 PM
Peak rt Height1 0.52 4802 1.12 603 2.44 281
-900
-700
-500
-300
-100
100
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes21 C S B120596-BLK1 2 264 0.730 0.00 < HS accept
Notes
Date:Time:
4/11/123:05 PM
Peak rt Height1 0.52 7332 1.14 2643 2.46 903
-1,000
-800
-600
-400
-200
0
0 1 2 3 4 5
1 2 3
Page 7 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 111 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes22 A S B120596-BLK2 2 118 0.251 0.00 < HS accept
Notes
Date:Time:
4/11/123:11 PM
Peak rt Height1 0.52 5962 1.13 1183 2.47 662
-1,000
-800
-600
-400
-200
0
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes23 B S B120596-BLK3 2 72 0.101 0.00 < HS accept
Notes
Date:Time:
4/11/123:18 PM
Peak rt Height1 0.52 4502 1.11 723 2.44 511
-1,100
-900
-700
-500
-300
-100
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes24 C S B120596-BLK4 2 105 0.209 0.00 < HS accept
Notes
Date:Time:
4/11/123:25 PM
Peak rt Height1 0.52 6942 1.14 1053 2.47 556
-1,100
-900
-700
-500
-300
-100
0 1 2 3 4 5
1 2 3
Page 8 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 112 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes25 A S B120596-BS1 2 446 1.33 0.00 < HS accept
Notes
Date:Time:
4/11/123:31 PM
Peak rt Height1 0.52 5802 1.13 4463 2.47 515
-1,200
-1,000
-800
-600
-400
-200
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes26 B S B120596-BS2 2 405 1.19 0.00 < HS accept
Notes
Date:Time:
4/11/123:38 PM
Peak rt Height1 0.53 4582 1.12 4053 2.45 602
-1,200
-1,000
-800
-600
-400
-200
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes27 C S B120596-BS3 2 272 0.757 0.00 < HS accept
Notes
Date:Time:
4/11/123:45 PM
Peak rt Height1 0.52 6652 1.15 2723 2.48 428
-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2 3
Page 9 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 113 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes28 A S B120596-BS4 2 414 1.22 0.00 < HS accept
Notes
Date:Time:
4/11/123:51 PM
Peak rt Height1 0.52 5732 1.13 4143 2.46 5364 4.90 11
-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes29 B S B120596-BS5 2 397 1.17 0.00 < HS accept
Notes
Date:Time:
4/11/123:58 PM
Peak rt Height1 0.53 4122 1.12 3973 2.45 385
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes30 C S B120596-BS6 2 431 1.28 0.00 < HS accept
Notes
Date:Time:
4/11/124:05 PM
Peak rt Height1 0.52 6332 1.14 4313 2.46 479
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Page 10 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 114 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes31 A CCV SEQ-CCV 2 7,723 25.2 101 67-133 accept
Notes
Date:Time:
4/11/124:11 PM
Peak rt Height1 0.52 5292 1.13 7,7233 2.47 1614 4.81 12
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes32 B CCB SEQ-CCB 2 70 0.230 0.230 < 1.4 accept
Notes
Date:Time:
4/11/124:18 PM
Peak rt Height1 0.52 4002 1.11 703 2.45 144
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes33 C S B120596-BS7 2 394 1.16 0.00 < HS accept
Notes
Date:Time:
4/11/124:25 PM
Peak rt Height1 0.52 6302 1.14 3943 2.47 1,598
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 3
Page 11 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 115 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes34 A S B120596-BS8 2 414 1.22 0.00 < HS accept
Notes
Date:Time:
4/11/124:31 PM
Peak rt Height1 0.52 5202 1.14 4143 2.47 499
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes35 B S B120596-BS9 2 3,130 10.1 0.00 < HS accept
Notes
Date:Time:
4/11/124:38 PM
Peak rt Height1 0.52 3932 1.12 3,1303 2.45 5634 3.78 34
-1,000
0
1,000
2,000
3,000
4,000
0 1 2 3 4 5
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes36 C S B120596-BSA 2 418 1.24 0.00 < HS accept
Notes
Date:Time:
4/11/124:45 PM
Peak rt Height1 0.52 5772 1.15 4183 2.46 4884 4.07 155 4.44 276 4.93 0
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 3 4 5 6
Page 12 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 116 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes37 A S B120596-BSB 2 1,933 6.21 0.00 < HS accept
Notes
Date:Time:
4/11/124:51 PM
Peak rt Height1 0.52 5362 1.13 1,9333 2.47 1,4804 4.86 0
-1,500
-500
500
1,500
2,500
3,500
0 1 2 3 4 5
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes38 B S B120596-BSC 2 788 2.45 0.00 < HS accept
Notes
Date:Time:
4/11/124:58 PM
Peak rt Height1 0.52 4202 1.12 7883 2.45 4684 3.94 15 3.97 16 4.94 0
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 3 45 6
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes39 C S B120596-BSD 2 753 2.33 0.00 < HS accept
Notes
Date:Time:
4/11/125:05 PM
Peak rt Height1 0.52 6052 1.14 7533 2.47 3884 4.28 15 4.30 1
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 3 45
Page 13 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 117 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes40 A S B120596-BSE 2 697 2.15 0.00 < HS accept
Notes
Date:Time:
4/11/125:11 PM
Peak rt Height1 0.52 5352 1.13 6973 2.48 3644 3.63 15 3.66 16 4.24 24
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 3 45 6
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes41 B CCV SEQ-CCV 2 7,454 24.3 97.3 67-133 accept
Notes
Date:Time:
4/11/125:18 PM
Peak rt Height1 0.53 3762 1.12 7,4543 2.44 266
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes42 C CCB SEQ-CCB 2 35 0.115 0.115 < 1.4 accept
Notes
Date:Time:
4/11/125:25 PM
Peak rt Height1 0.52 6102 1.11 353 2.45 2314 3.94 15 3.96 1
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 3 45
Page 14 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 118 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes43 A S B120524-BLK1 2 358 1.04 0.00 < HS accept
Notes
Date:Time:
4/11/125:31 PM
Peak rt Height1 0.52 5122 1.13 3583 2.47 1,0574 4.31 15 4.33 1
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 3 45
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes44 B S B120524-BLK2 2 93 0.169 0.00 < HS accept
Notes
Date:Time:
4/11/125:38 PM
Peak rt Height1 0.52 3992 1.12 933 2.44 5624 4.74 15 4.76 1
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 3 45
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes45 C S B120524-BLK3 2 111 0.229 0.00 < HS accept
Notes
Date:Time:
4/11/125:45 PM
Peak rt Height1 0.52 6162 1.15 1113 1.73 14 1.75 15 2.46 650
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 34 5
Page 15 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 119 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes46 A S B120524-BLK4 2 62 0.0678 0.00 < HS accept
Notes
Date:Time:
4/11/125:51 PM
Peak rt Height1 0.52 4962 1.13 623 2.47 5134 4.85 15 4.87 1
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3 45
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes47 B S 1212016-21 2 63 0.0711 0.00 < HS accept
Notes
Date:Time:
4/11/125:58 PM
Peak rt Height1 0.52 3862 1.09 633 2.45 2774 3.65 25 3.69 16 4.54 17 4.56 1
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3 45 67
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes48 C S B120524-BS1 2 6,059 19.7 0.00 < HS accept
Notes
Date:Time:
4/11/126:05 PM
Peak rt Height1 0.52 6062 1.14 6,0593 2.46 2,082
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Page 16 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 120 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes49 A S B120524-BS2 2 6,328 20.6 0.00 < HS accept
Notes
Date:Time:
4/11/126:11 PM
Peak rt Height1 0.52 5012 1.13 6,3283 2.47 538
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes50 B S 1213011-17 2 5,583 18.2 0.00 < HS accept
Notes
Date:Time:
4/11/126:18 PM
Peak rt Height1 0.53 4072 1.12 5,5833 2.44 729
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes51 C S 1213011-18 2 6,378 20.8 0.00 < HS accept
Notes
Date:Time:
4/11/126:25 PM
Peak rt Height1 0.53 7522 1.14 6,3783 2.46 14,970
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Page 17 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 121 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes52 A S 1213011-19 2 22,272 72.9 0.00 < HS accept
Notes
Date:Time:
4/11/126:31 PM
Peak rt Height1 0.52 5442 1.13 22,2723 2.46 7944 4.25 15 4.27 1
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3 45
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes53 B CCV SEQ-CCV 2 7,235 23.6 94.4 67-133 accept
Notes
Date:Time:
4/11/126:38 PM
Peak rt Height1 0.53 4122 1.12 7,2353 2.42 2374 4.60 15 4.62 2
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3 45
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes54 C CCB SEQ-CCB 2 139 0.456 0.456 < 1.4 accept
Notes
Date:Time:
4/11/126:45 PM
Peak rt Height1 0.52 6432 1.14 1393 2.45 283
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Page 18 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 122 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes55 A S 1212014-03 2 1,851 5.94 0.00 < HS accept
Notes
Date:Time:
4/11/126:51 PM
Peak rt Height1 0.52 5262 1.13 1,8513 2.46 1,088
-1,500
-500
500
1,500
2,500
3,500
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes56 B S 1212014-04 2 1,185 3.75 0.00 < HS accept
Notes
Date:Time:
4/11/126:58 PM
Peak rt Height1 0.52 3992 1.12 1,1853 2.44 946
-1,500
-500
500
1,500
2,500
3,500
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes57 C S B120524-MS1 2 9,984 32.6 0.00 < HS accept
Notes
Date:Time:
4/11/127:05 PM
Peak rt Height1 0.52 6062 1.14 9,9843 2.46 879
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Page 19 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 123 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes58 A S B120524-MSD1 2 10,792 35.3 0.00 < HS accept
Notes
Date:Time:
4/11/127:11 PM
Peak rt Height1 0.52 5082 1.13 10,7923 2.46 9974 4.55 15 4.57 1
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3 45
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes59 B S 1212016-01 2 307 0.871 0.00 < HS accept
Notes
Date:Time:
4/11/127:18 PM
Peak rt Height1 0.52 3762 1.11 3073 2.43 1,128
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes60 C S 1212016-03 2 260 0.717 0.00 < HS accept
Notes
Date:Time:
4/11/127:25 PM
Peak rt Height1 0.52 6142 1.14 2603 2.46 823
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Page 20 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 124 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes61 A S 1212016-05 2 272 0.757 0.00 < HS accept
Notes
Date:Time:
4/11/127:31 PM
Peak rt Height1 0.52 4762 1.13 2723 2.46 564
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes62 B S 1212016-07 2 163 0.399 0.00 < HS accept
Notes
Date:Time:
4/11/127:38 PM
Peak rt Height1 0.52 3612 1.11 1633 2.44 1,003
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes63 C S 1212016-09 2 619 1.89 0.00 < HS accept
Notes
Date:Time:
4/11/127:45 PM
Peak rt Height1 0.53 5892 1.14 6193 2.46 1,183
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Page 21 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 125 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes64 A S 1212016-11 2 283 0.793 0.00 < HS accept
Notes
Date:Time:
4/11/127:51 PM
Peak rt Height1 0.52 4582 1.13 2833 2.46 557
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes65 B CCV SEQ-CCV 2 7,074 23.1 92.3 67-133 accept
Notes
Date:Time:
4/11/127:58 PM
Peak rt Height1 0.52 3352 1.11 7,0743 2.43 235
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes66 C CCB SEQ-CCB 2 49 0.161 0.161 < 1.4 accept
Notes
Date:Time:
4/11/128:05 PM
Peak rt Height1 0.52 5692 1.13 493 2.45 359
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Page 22 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 126 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes67 A S B120524-MS2 2 574 1.75 0.00 < HS accept
Notes
Date:Time:
4/11/128:11 PM
Peak rt Height1 0.52 4622 1.13 5743 2.46 526
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes68 B S B120524-MSD2 2 611 1.87 0.00 < HS accept
Notes
Date:Time:
4/11/128:18 PM
Peak rt Height1 0.52 3282 1.11 6113 2.44 617
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes69 C S 1212016-13 2 212 0.560 0.00 < HS accept
Notes
Date:Time:
4/11/128:25 PM
Peak rt Height1 0.52 5422 1.14 2123 2.46 635
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Page 23 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 127 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes70 A S 1212016-15 2 252 0.691 0.00 < HS accept
Notes
Date:Time:
4/11/128:31 PM
Peak rt Height1 0.52 4372 1.13 2523 2.46 666
-1,600
-1,400
-1,200
-1,000
-800
-600
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes71 B S 1212016-17 2 249 0.681 0.00 < HS accept
Notes
Date:Time:
4/11/128:38 PM
Peak rt Height1 0.53 3432 1.12 2493 2.44 1,222
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes72 C S 1212016-19 2 1,226 3.89 0.00 < HS accept
Notes
Date:Time:
4/11/128:45 PM
Peak rt Height1 0.53 5832 1.14 1,2263 2.46 974
-1,500
-500
500
1,500
2,500
3,500
0 1 2 3 4 5
1 2 3
Page 24 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 128 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes73 A S 1212016-23 0 -0.136 0.00 < HS accept
Notes
Date:Time:
4/11/128:51 PM
Peak rt Height1 0.52 438
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes74 B S 1212016-25 0 -0.136 0.00 < HS accept
Notes
Date:Time:
4/11/128:58 PM
Peak rt Height1 0.53 331
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes75 C S 1213006-01 0 -0.136 0.00 < HS accept
Notes
Date:Time:
4/11/129:05 PM
Peak rt Height1 0.53 582
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1
Page 25 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 129 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes76 A S 1213006-03 0 -0.136 0.00 < HS accept
Notes
Date:Time:
4/11/129:11 PM
Peak rt Height1 0.52 427
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes77 B CCV SEQ-CCV 0 -0.136 -0.542 67-133 reject
Notes
Date:Time:
4/11/129:18 PM
Peak rt Height1 0.52 3202 2.33 13 2.36 14 2.72 20
-1,500
-1,300
-1,100
-900
-700
-500
0 1 2 3 4 5
1 23 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes78 C CCB SEQ-CCB 0 0.00 0.00 < 1.4 accept
Notes
Date:Time:
4/11/129:25 PM
Peak rt Height1 0.52 5452 3.53 23 3.56 1
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 23
Page 26 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 130 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes79 A S 1213006-05 0 -0.136 0.00 < HS accept
Notes
Date:Time:
4/11/129:31 PM
Peak rt Height1 0.52 437
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes80 B S 1213006-07 0 -0.136 0.00 < HS accept
Notes
Date:Time:
4/11/129:38 PM
Peak rt Height1 0.52 333
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes81 C S 1213006-09 2 204 0.534 0.00 < HS accept
Notes
Date:Time:
4/11/129:45 PM
Peak rt Height1 0.52 5372 1.14 2043 2.46 6674 4.24 15 4.26 1
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3 45
Page 27 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 131 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes82 A S 1213006-11 2 215 0.570 0.00 < HS accept
Notes
Date:Time:
4/11/129:51 PM
Peak rt Height1 0.52 4272 1.12 2153 2.45 547
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes83 B S 1213006-13 2 237 0.642 0.00 < HS accept
Notes
Date:Time:
4/11/129:58 PM
Peak rt Height1 0.53 3322 1.12 2373 2.43 506
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes84 C S 1213006-15 2 186 0.475 0.00 < HS accept
Notes
Date:Time:
4/11/1210:05 PM
Peak rt Height1 0.52 5282 1.14 1863 2.45 745
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Page 28 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 132 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes85 A S B120524-MS3 2 510 1.54 0.00 < HS accept
Notes
Date:Time:
4/11/1210:11 PM
Peak rt Height1 0.52 4132 1.13 5103 2.46 740
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes86 B S B120524-MSD3 2 408 1.20 0.00 < HS accept
Notes
Date:Time:
4/11/1210:18 PM
Peak rt Height1 0.52 3022 1.11 4083 2.42 369
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes87 C S 1213006-17 2 217 0.576 0.00 < HS accept
Notes
Date:Time:
4/11/1210:25 PM
Peak rt Height1 0.52 5232 1.14 2173 2.46 807
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Page 29 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 133 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes88 A S 1213006-19 2 182 0.461 0.00 < HS accept
Notes
Date:Time:
4/11/1210:31 PM
Peak rt Height1 0.52 4162 1.12 1823 2.45 605
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes89 B CCV SEQ-CCV 2 7,177 23.4 93.6 67-133 accept
Notes
Date:Time:
4/11/1210:38 PM
Peak rt Height1 0.53 3112 1.12 7,1773 2.44 191
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes90 C CCB SEQ-CCB 2 45 0.148 0.148 < 1.4 accept
Notes
Date:Time:
4/11/1210:45 PM
Peak rt Height1 0.52 5082 1.13 453 2.44 203
-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2 3
Page 30 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 134 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes91 A S 1213006-21 2 376 1.10 0.00 < HS accept
Notes
Date:Time:
4/11/1210:51 PM
Peak rt Height1 0.52 4592 1.12 3763 2.45 2,825
-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes92 B S 1213006-23 2 247 0.675 0.00 < HS accept
Notes
Date:Time:
4/11/1210:58 PM
Peak rt Height1 0.53 3392 1.12 2473 2.44 2,269
-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes93 C S 1213006-25 2 176 0.442 0.00 < HS accept
Notes
Date:Time:
4/11/1211:05 PM
Peak rt Height1 0.52 4872 1.14 1763 2.45 489
-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2 3
Page 31 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 135 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes94 A S 1213006-31 2 201 0.524 0.00 < HS accept
Notes
Date:Time:
4/11/1211:11 PM
Peak rt Height1 0.52 4242 1.12 2013 2.45 542
-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes95 B S B120524-MS4 2 512 1.54 0.00 < HS accept
Notes
Date:Time:
4/11/1211:18 PM
Peak rt Height1 0.52 3002 1.11 5123 2.43 598
-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes96 C S B120524-MSD4 2 501 1.51 0.00 < HS accept
Notes
Date:Time:
4/11/1211:25 PM
Peak rt Height1 0.52 4972 1.14 5013 2.45 623
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Page 32 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 136 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes97 A S 1213006-33 2 179 0.452 0.00 < HS accept
Notes
Date:Time:
4/11/1211:31 PM
Peak rt Height1 0.52 4042 1.12 1793 2.45 848
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes98 B S 1213006-35 2 195 0.504 0.00 < HS accept
Notes
Date:Time:
4/11/1211:38 PM
Peak rt Height1 0.53 3072 1.11 1953 2.43 795
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes99 C CCV SEQ-CCV 2 7,166 23.4 93.5 67-133 accept
Notes
Date:Time:
4/11/1211:45 PM
Peak rt Height1 0.52 4782 1.14 7,1663 2.44 175
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Page 33 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 137 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes100 A CCB SEQ-CCB 2 52 0.171 0.171 < 1.4 acceptNotes
Date:Time:
4/11/1211:51 PM
Peak rt Height1 0.52 3912 1.12 523 2.45 1904 4.91 15 4.93 1
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3 45
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes101 B S B120566-BLK1 2m 44 0.00875 0.00 < HS acceptNotes
Date:Time:
4/11/1211:58 PM
Peak rt Height1 0.52 281
2m 1.12 443 1.12 24 2.44 176
-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2m3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes102 C S B120566-BLK2 2 46 0.0153 0.00 < HS acceptNotes
Date:Time:
4/12/1212:05 AM
Peak rt Height1 0.52 4642 1.13 463 2.44 2214 3.01 15 3.80 16 3.83 1
-1,400
-1,200
-1,000
-800
-600
-400
0 1 2 3 4 5
1 2 3 4 56
Page 34 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 138 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes103 A S B120566-BLK3 2 45 0.0120 0.00 < HS acceptNotes
Date:Time:
4/12/1212:11 AM
Peak rt Height1 0.52 3862 1.14 453 1.43 14 1.97 85 2.08 16 2.45 2737 3.61 18 3.63 19 4.88 1
10 4.90 1-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2 3 4 5 6 78 910
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes104 B S B120566-BLK4 2 47 0.0186 0.00 < HS acceptNotes
Date:Time:
4/12/1212:18 AM
Peak rt Height1 0.52 2762 1.07 473 2.44 2324 4.24 23
-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes105 C S SEQ-CCB 2 42 0.00219 0.00 < HS acceptNotes
Date:Time:
4/12/1212:25 AM
Peak rt Height1 0.52 4592 1.10 423 2.46 2074 4.55 15
-1,300
-1,100
-900
-700
-500
-300
0 1 2 3 4 5
1 2 3 4
Page 35 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 139 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes106 A S B120566-SRM1 2 75,560 248 0.00 < HS acceptNotes
Date:Time:
4/12/1212:31 AM
Peak rt Height1 0.52 4762 1.12 75,5603 2.45 6604 4.63 25 4.67 1
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3 4 5
1 2 3 45
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes107 B S 1211036-02 2 222,889 731 0.00 < HS acceptNotes
Date:Time:
4/12/1212:38 AM
Peak rt Height1 0.52 2,0652 1.11 222,8893 2.43 85,441
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes108 C S B120566-DUP1 2 218,840 718 0.00 < HS acceptNotes
Date:Time:
4/12/1212:45 AM
Peak rt Height1 0.53 1,5572 1.14 218,8403 2.45 86,829
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3 4 5
1 2 3
Page 36 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 140 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes109 A S B120566-MS1 2 385,586 1,260 0.00 < HS rejectNotes
Date:Time:
4/12/1212:51 AM
Peak rt Height1 0.52 2,3412 1.12 385,5863 2.46 96,504
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes110 B S B120566-MSD1 2 389,287 1,280 0.00 < HS rejectNotes
Date:Time:
4/12/1212:58 AM
Peak rt Height1 0.52 3,0092 1.11 389,2873 2.44 93,018
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes111 C CCV SEQ-CCV 2 9,217 30.1 120. 67-133 acceptNotes
Date:Time:
4/12/121:05 AM
Peak rt Height1 0.52 9392 1.14 9,2173 2.46 1,145
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Page 37 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 141 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes112 A CCB SEQ-CCB 2 543 1.78 1.78 < 1.4 rejectNotes
Date:Time:
4/12/121:11 AM
Peak rt Height1 0.52 1,0542 1.12 5433 2.45 400
-1,200
-1,000
-800
-600
-400
-200
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes113 B S 1214009-01 2 4,987 16.2 0.00 < HS acceptNotes
Date:Time:
4/12/121:18 AM
Peak rt Height1 0.52 1,4332 1.11 4,9873 2.43 1,631
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes114 C S 1214009-02 2 2,368 7.63 0.00 < HS acceptNotes
Date:Time:
4/12/121:25 AM
Peak rt Height1 0.52 7752 1.14 2,3683 2.45 1,588
-1,000
0
1,000
2,000
3,000
4,000
0 1 2 3 4 5
1 2 3
Page 38 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 142 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes115 A S 1214009-03 2 2,293 7.39 0.00 < HS acceptNotes
Date:Time:
4/12/121:31 AM
Peak rt Height1 0.52 9102 1.12 2,2933 2.45 2,720
-1,000
0
1,000
2,000
3,000
4,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes116 B S 1214009-04 2 2,085 6.70 0.00 < HS acceptNotes
Date:Time:
4/12/121:38 AM
Peak rt Height1 0.52 1,1322 1.11 2,0853 2.43 2,711
-1,000
0
1,000
2,000
3,000
4,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes117 C CCV SEQ-CCV 2 7,142 23.3 93.2 67-133 acceptNotes
Date:Time:
4/12/121:45 AM
Peak rt Height1 0.52 7312 1.14 7,1423 2.45 231
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Page 39 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 143 of 274
Peak ReportBatch Number: B120524, B120596, B120566
Method Number: CVAFS BR-0011Project Number(s): 1200258 Date Analyzed: 4/11/12Instrument ID: BR-09 Analyst Name: AC
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes118 A CCB SEQ-CCB 2 114 0.374 0.374 < 1.4 acceptNotes
Date:Time:
4/12/121:51 AM
Peak rt Height1 0.52 7572 1.13 1143 2.45 220
-1,200
-1,000
-800
-600
-400
-200
0 1 2 3 4 5
1 2 3
Page 40 of 40 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 144 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200272
MMHG-09Instrument:
Batch # Source ID
Brooks Rand Labs
1200272-IBL1 QC 11200272 -
1200272-IBL2 QC 21200272 -
1200272-IBL3 QC 31200272 -
1200272-CAL1 QC 4 12160371200272 -
1200272-CAL2 QC 5 12160381200272 -
1200272-CAL3 QC 6 12160391200272 -
1200272-CAL4 QC 7 12160401200272 -
1200272-CAL5 QC 8 12160441200272 -
1200272-CAL6 QC 9 12160421200272 -
1200272-CAL7 QC 10 12160431200272 -
1200272-CCB1 QC 111200272 -
1200272-ICV1 QC 12 12160461200272 -
1200272-CCB2 QC 131200272 -
1200272-CCV1 QC 14 12160451200272 -
1200272-CCB3 QC 151200272 -
1200272-CCB4 QC 161200272 -
1200272-CCB5 QC 171200272 -
B120642-BLK1 QC 18B120642 -
B120642-BLK2 QC 19B120642 -
B120642-BLK3 QC 20B120642 -
B120642-BLK4 QC 21B120642 -
B120642-BS1 QC 22B120642 -
B120642-BS2 QC 23B120642 -
B120642-BS3 QC 24B120642 -
B120642-BS4 QC 25B120642 -
B120642-BS5 QC 26B120642 -
Page 1 of 6Printed: 4/19/2012 11:28:11AM
BRL Report 1212016
Page 145 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200272
MMHG-09Instrument:
Batch # Source ID
Brooks Rand Labs
B120642-BS6 QC 27B120642 -
1200272-CCV2 QC 28 12160451200272 -
1200272-CCB6 QC 291200272 -
B120642-BS7 QC 30B120642 -
B120642-BS8 QC 31B120642 -
B120642-BS9 QC 32B120642 -
B120642-BSA QC 33B120642 -
B120642-BSB QC 34B120642 -
B120642-BSC QC 35B120642 -
B120642-BSD QC 36B120642 -
B120642-BSE QC 37B120642 -
1200272-CCV3 QC 38 12160451200272 -
1200272-CCB7 QC 391200272 -
B120565-BLK1 QC 40B120565 -
B120565-BLK2 QC 41B120565 -
B120565-BLK3 QC 42B120565 -
B120565-BLK4 QC 43B120565 -
B120565-BS1 QC 44B120565 -
B120565-BS2 QC 45B120565 -
1212016-23RE1 MeHg-W-Dist-NoMB-TR 46 From B120524 by MSU on 04/13/12B120565 AAL-MN1101 4/10/2012
1212016-25RE1 MeHg-W-Dist-NoMB-TR 47 From B120524 by MSU on 04/13/12B120565 AAL-MN1101 4/10/2012
1213006-01RE1 MeHg-W-Dist-NoMB-TR 48 From B120524 by MSU on 04/13/12B120565 AAL-MN1101 4/18/2012
B120565-MS1 QC 49B120565 1213006-01RE1
1200272-CCV4 QC 50 12160451200272 -
1200272-CCB8 QC 511200272 -
B120565-MSD1 QC 52B120565 1213006-01RE1
Page 2 of 6Printed: 4/19/2012 11:28:11AM
BRL Report 1212016
Page 146 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200272
MMHG-09Instrument:
Batch # Source ID
Brooks Rand Labs
1213006-03RE1 MeHg-W-Dist-NoMB-TR 53 From B120524 by MSU on 04/13/12B120565 AAL-MN1101 4/18/2012
1213006-05RE1 MeHg-W-Dist-NoMB-TR 54 From B120524 by MSU on 04/13/12B120565 AAL-MN1101 4/18/2012
1213006-07RE1 MeHg-W-Dist-NoMB-TR 55 From B120524 by MSU on 04/13/12B120565 AAL-MN1101 4/18/2012
1214002-43 MeHg-W-Dist-Diss 56B120565 AEC-WE1203 4/24/2012
B120565-MS2 QC 57B120565 1214002-43
B120565-MSD2 QC 58B120565 1214002-43
1214002-49 MeHg-W-Dist-Diss 59B120565 AEC-WE1203 4/24/2012
1214002-50 MeHg-W-Dist-TR 60B120565 AEC-WE1203 4/24/2012
1214002-51 MeHg-W-Dist-Diss 61B120565 AEC-WE1203 4/24/2012
1200272-CCV5 QC 62 12160451200272 -
1200272-CCB9 QC 631200272 -
1214002-52 MeHg-W-Dist-TR 64B120565 AEC-WE1203 4/24/2012
1214002-53 MeHg-W-Dist-Diss 65B120565 AEC-WE1203 4/24/2012
1214002-54 MeHg-W-Dist-TR 66B120565 AEC-WE1203 4/24/2012
1214002-55 MeHg-W-Dist-Diss 67B120565 AEC-WE1203 4/24/2012
1214002-56 MeHg-W-Dist-TR 68B120565 AEC-WE1203 4/24/2012
1214002-57 MeHg-W-Dist-Diss 69B120565 AEC-WE1203 4/24/2012
1214002-58 MeHg-W-Dist-TR 70B120565 AEC-WE1203 4/24/2012
1214002-59 MeHg-W-Dist-Diss 71B120565 AEC-WE1203 4/24/2012
1214002-60 MeHg-W-Dist-TR 72B120565 AEC-WE1203 4/24/2012
1214002-61 MeHg-W-Dist-Diss 73B120565 AEC-WE1203 4/24/2012
1200272-CCV6 QC 74 12160451200272 -
1200272-CCBA QC 751200272 -
1214002-62 MeHg-W-Dist-TR 76B120565 AEC-WE1203 4/24/2012
1214002-63 MeHg-W-Dist-Diss 77B120565 AEC-WE1203 4/24/2012
1214018-01 MeHg-W-Dist-TR 78B120565 EBM-OA1001 4/26/2012
Page 3 of 6Printed: 4/19/2012 11:28:11AM
BRL Report 1212016
Page 147 of 274
BRL Report 1212016
Page 148 of 274
BRL Report 1212016
Page 149 of 274
BRL Report 1212016
Page 150 of 274
BRL Report 1212016
Page 151 of 274
BRL Report 1212016
Page 152 of 274
BRL Report 1212016
Page 153 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes1 A Rins Rinse u 30 0.113 0.00 0.00 < 0.05 accept
Notes
Date:Time:
4/18/1211:04 AM
Peak rt Height1 0.52 4772 2.46 300u 1.08 30
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2u
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes2 B Rins Rinse 2 26 0.0981 0.00 0.00 < 0.05 accept
Notes
Date:Time:
4/18/1211:11 AM
Peak rt Height1 0.52 3852 1.15 263 1.41 14 2.45 168
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes3 C Rins Rinse u 16 0.0603 0.00 0.00 < 0.05 accept
Notes
Date:Time:
4/18/1211:17 AM
Peak rt Height1 0.52 4482 1.92 13 1.94 14 2.46 1145 4.01 36 4.04 2u 1.07 16
0
200
400
600
800
1,000
0 1 2 3 4 5
1 23 4 56u
Page 1 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 154 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes4 A CB SEQ-IBL 2 34 0.128 0.128 < 1.4 accept
Notes
Date:Time:
4/18/1211:24 AM
Peak rt Height1 0.52 4782 1.14 343 1.39 14 2.48 140
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes5 B CB SEQ-IBL u 16 0.0603 0.0603 < 1.4 accept
Notes
Date:Time:
4/18/1211:31 AM
Peak rt Height1 0.52 3392 2.43 1183 3.24 1u 1.14 16
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3u
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes6 C CB SEQ-IBL 2 47 0.177 0.177 < 1.4 accept
Notes
Date:Time:
4/18/1211:37 AM
Peak rt Height1 0.52 4432 1.20 473 2.48 127
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 2 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 155 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes7 A STD SEQ-CAL1 2 156 0.466 93.3 65-135 accept
Notes
Date:Time:
4/18/1211:44 AM
Peak rt Height1 0.52 4522 1.14 1563 2.47 144
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes8 B STD SEQ-CAL2 2 304 1.02 102 65-135 accept
Notes
Date:Time:
4/18/1211:51 AM
Peak rt Height1 0.52 3062 1.12 3043 2.40 119
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes9 C STD SEQ-CAL3 2 541 1.92 95.9 65-135 accept
Notes
Date:Time:
4/18/1211:57 AM
Peak rt Height1 0.52 4392 1.15 5413 2.49 192
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 3 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 156 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes10 A STD SEQ-CAL4 2 2,504 9.32 93.2 65-135 accept
Notes
Date:Time:
4/18/1212:04 PM
Peak rt Height1 0.52 3822 1.14 2,5043 2.46 185
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes11 B STD SEQ-CAL5 2 13,753 51.7 103 65-135 accept
Notes
Date:Time:
4/18/1212:11 PM
Peak rt Height1 0.52 3252 1.12 13,7533 2.45 497
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes12 C STD SEQ-CAL6 2 69,104 260. 104 65-135 accept
Notes
Date:Time:
4/18/1212:17 PM
Peak rt Height1 0.53 5012 1.15 69,1043 2.48 1,763
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3 4 5
1 2 3
Page 4 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 157 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes13 A STD SEQ-CAL7 2 291,333 1,100 110. 65-135 accept
Notes
Date:Time:
4/18/1212:24 PM
Peak rt Height1 0.52 9902 1.14 291,3333 2.48 6,194
0
100,000
200,000
300,000
400,000
500,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes14 B CCB SEQ-CCB 2 211 0.796 0.796 < 1.4 accept
Notes
Date:Time:
4/18/1212:31 PM
Peak rt Height1 0.52 3332 1.12 2113 2.44 80
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes15 C ICV SEQ-ICV 2 29,163 110. 110. 80-120 accept
Notes
Date:Time:
4/18/1212:37 PM
Peak rt Height1 0.52 5012 1.15 29,1633 2.47 993
0
20,000
40,000
60,000
80,000
100,000
0 1 2 3 4 5
1 2 3
Page 5 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 158 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes16 A CCB SEQ-CCB 2 359 1.35 1.35 < 1.4 accept
Notes
Date:Time:
4/18/1212:44 PM
Peak rt Height1 0.52 6432 1.14 3593 2.48 136
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes17 B CCV SEQ-CCV 2 6,356 23.8 95.4 67-133 accept
Notes
Date:Time:
4/18/1212:51 PM
Peak rt Height1 0.53 3242 1.12 6,3563 2.45 296
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes18 C CCB SEQ-CCB 2 111 0.419 0.419 < 1.4 accept
Notes
Date:Time:
4/18/1212:57 PM
Peak rt Height1 0.52 4682 1.16 1113 2.43 104
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 6 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 159 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes19 A CCB SEQ-CCB 2 79 0.298 0.298 < 1.4 accept
Notes
Date:Time:
4/18/121:04 PM
Peak rt Height1 0.52 5312 1.12 793 2.50 101
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes20 B CCB SEQ-CCB 2 52 0.196 0.196 < 1.4 accept
Notes
Date:Time:
4/18/121:11 PM
Peak rt Height1 0.52 2572 1.12 523 2.46 294
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes21 C S B120642-BLK1 2 96 0.240 0.00 < HS accept
Notes
Date:Time:
4/18/121:17 PM
Peak rt Height1 0.52 4302 1.12 963 2.48 347
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 7 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 160 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes22 A S B120642-BLK2 2 79 0.176 0.00 < HS accept
Notes
Date:Time:
4/18/121:24 PM
Peak rt Height1 0.52 5282 1.16 793 2.47 374
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes23 B S B120642-BLK3 2 76 0.165 0.00 < HS accept
Notes
Date:Time:
4/18/121:31 PM
Peak rt Height1 0.52 2792 1.12 763 2.45 194
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes24 C S B120642-BLK4 2 98 0.248 0.00 < HS accept
Notes
Date:Time:
4/18/121:37 PM
Peak rt Height1 0.52 4162 1.16 983 2.47 858
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 8 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 161 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes25 A S B120642-BS1 2 352 1.21 0.00 < HS accept
Notes
Date:Time:
4/18/121:44 PM
Peak rt Height1 0.52 4792 1.13 3523 2.46 326
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes26 B S B120642-BS2 2 388 1.34 0.00 < HS accept
Notes
Date:Time:
4/18/121:51 PM
Peak rt Height1 0.52 2762 1.12 3883 2.45 618
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes27 C S B120642-BS3 2 345 1.18 0.00 < HS accept
Notes
Date:Time:
4/18/121:57 PM
Peak rt Height1 0.52 4202 1.15 3453 2.47 589
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 9 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 162 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes28 A S B120642-BS4 2 364 1.25 0.00 < HS accept
Notes
Date:Time:
4/18/122:04 PM
Peak rt Height1 0.52 4502 1.14 3643 2.48 423
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes29 B S B120642-BS5 2 443 1.55 0.00 < HS accept
Notes
Date:Time:
4/18/122:11 PM
Peak rt Height1 0.52 3242 1.12 4433 2.46 2,620
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes30 C S B120642-BS6 2 302 1.02 0.00 < HS accept
Notes
Date:Time:
4/18/122:17 PM
Peak rt Height1 0.52 4042 1.15 3023 2.47 585
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 10 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 163 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes31 A CCV SEQ-CCV 2 6,910 25.9 104 67-133 accept
Notes
Date:Time:
4/18/122:24 PM
Peak rt Height1 0.52 4682 1.14 6,9103 2.48 332
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes32 B CCB SEQ-CCB u 23 0.0867 0.0867 < 1.4 accept
Notes
Date:Time:
4/18/122:31 PM
Peak rt Height1 0.53 2672 2.44 163u 1.10 23
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2u
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes33 C S B120642-BS7 2 358 1.23 0.00 < HS accept
Notes
Date:Time:
4/18/122:37 PM
Peak rt Height1 0.52 3982 1.15 3583 2.48 580
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 11 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 164 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes34 A S B120642-BS8 2 426 1.48 0.00 < HS accept
Notes
Date:Time:
4/18/122:44 PM
Peak rt Height1 0.52 4462 1.14 4263 2.48 958
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes35 B S B120642-BS9 2 2,384 8.87 0.00 < HS accept
Notes
Date:Time:
4/18/122:51 PM
Peak rt Height1 0.52 2532 1.12 2,3843 2.46 3624 4.62 15 4.64 1
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3 4 5
1 2 3 45
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes36 C S B120642-BSA 2 315 1.07 0.00 < HS accept
Notes
Date:Time:
4/18/122:57 PM
Peak rt Height1 0.52 4292 1.15 3153 1.75 24 1.78 15 2.48 6546 4.57 17 4.60 2
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 34 5 67
Page 12 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 165 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes37 A S B120642-BSB 2 621 2.22 0.00 < HS accept
Notes
Date:Time:
4/18/123:04 PM
Peak rt Height1 0.52 4452 1.14 6213 2.48 570
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes38 B S B120642-BSC 2 576 2.05 0.00 < HS accept
Notes
Date:Time:
4/18/123:11 PM
Peak rt Height1 0.52 2632 1.13 5763 2.47 315
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes39 C S B120642-BSD 2 659 2.36 0.00 < HS accept
Notes
Date:Time:
4/18/123:17 PM
Peak rt Height1 0.52 3692 1.15 6593 2.48 286
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3 4 5
1 2 3
Page 13 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 166 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes40 A S B120642-BSE 2 698 2.51 0.00 < HS accept
Notes
Date:Time:
4/18/123:24 PM
Peak rt Height1 0.52 4322 1.14 6983 2.48 626
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes41 B CCV SEQ-CCV 2 6,693 25.1 100. 67-133 accept
Notes
Date:Time:
4/18/123:31 PM
Peak rt Height1 0.52 2862 1.13 6,6933 2.46 406
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes42 C CCB SEQ-CCB 2 46 0.173 0.173 < 1.4 accept
Notes
Date:Time:
4/18/123:37 PM
Peak rt Height1 0.52 3672 1.16 463 2.48 172
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 14 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 167 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes43 A S B120565-BLK1 2 47 0.0553 0.00 < HS accept
Notes
Date:Time:
4/18/123:44 PM
Peak rt Height1 0.52 4452 1.13 473 2.48 245
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes44 B S B120565-BLK2 2 25 -0.0277 0.00 < HS accept
Notes
Date:Time:
4/18/123:51 PM
Peak rt Height1 0.52 2642 1.12 253 2.46 422
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes45 C S B120565-BLK3 2 74 0.157 0.00 < HS accept
Notes
Date:Time:
4/18/123:57 PM
Peak rt Height1 0.52 3602 1.14 743 2.48 335
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 15 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 168 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes46 A S B120565-BLK4 2 73 0.153 0.00 < HS accept
Notes
Date:Time:
4/18/124:04 PM
Peak rt Height1 0.52 3872 1.13 733 2.48 3544 3.45 38
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes47 B S B120565-BS1 2 5,491 20.6 0.00 < HS accept
Notes
Date:Time:
4/18/124:11 PM
Peak rt Height1 0.53 2912 1.13 5,4913 2.46 1,315
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes48 C S B120565-BS2 2 5,538 20.8 0.00 < HS accept
Notes
Date:Time:
4/18/124:17 PM
Peak rt Height1 0.52 3662 1.15 5,5383 2.50 383
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Page 16 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 169 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes49 A S 1212016-23RE1 2 391 1.35 0.00 < HS accept
Notes
Date:Time:
4/18/124:24 PM
Peak rt Height1 0.52 3782 1.14 3913 2.49 435
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes50 B S 1212016-25RE1 2 528 1.87 0.00 < HS accept
Notes
Date:Time:
4/18/124:31 PM
Peak rt Height1 0.53 3012 1.13 5283 1.65 294 2.47 2,087
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes51 C S 1213006-01RE1 2 166 0.504 0.00 < HS accept
Notes
Date:Time:
4/18/124:37 PM
Peak rt Height1 0.52 3482 1.15 1663 2.48 393
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 17 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 170 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes52 A S B120565-MS1 2 1,769 6.55 0.00 < HS accept
Notes
Date:Time:
4/18/124:44 PM
Peak rt Height1 0.52 3992 1.14 1,7693 2.48 622
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes53 B CCV SEQ-CCV 2 6,567 24.6 98.6 67-133 accept
Notes
Date:Time:
4/18/124:51 PM
Peak rt Height1 0.52 2632 1.13 6,5673 2.46 332
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes54 C CCB SEQ-CCB 2 48 0.181 0.181 < 1.4 accept
Notes
Date:Time:
4/18/124:57 PM
Peak rt Height1 0.53 3662 1.16 483 2.45 111
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 18 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 171 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes55 A S B120565-MSD1 2 1,698 6.28 0.00 < HS accept
Notes
Date:Time:
4/18/125:04 PM
Peak rt Height1 0.52 3892 1.14 1,6983 2.49 559
0
1,000
2,000
3,000
4,000
5,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes56 B S 1213006-03RE1 2 167 0.508 0.00 < HS accept
Notes
Date:Time:
4/18/125:11 PM
Peak rt Height1 0.53 2292 1.12 1673 2.46 693
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes57 C S 1213006-05RE1 2 157 0.470 0.00 < HS accept
Notes
Date:Time:
4/18/125:17 PM
Peak rt Height1 0.52 3422 1.15 1573 2.48 417
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 19 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 172 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes58 A S 1213006-07RE1 2 255 0.840 0.00 < HS accept
Notes
Date:Time:
4/18/125:24 PM
Peak rt Height1 0.52 3492 1.13 2553 2.48 569
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes59 B S 1214002-43 2 121 0.334 0.00 < HS accept
Notes
Date:Time:
4/18/125:31 PM
Peak rt Height1 0.53 2542 1.11 1213 2.45 344
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes60 C S B120565-MS2 2 6,381 23.9 0.00 < HS accept
Notes
Date:Time:
4/18/125:37 PM
Peak rt Height1 0.52 3322 1.15 6,3813 2.48 577
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Page 20 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 173 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes61 A S B120565-MSD2 2 6,107 22.9 0.00 < HS accept
Notes
Date:Time:
4/18/125:44 PM
Peak rt Height1 0.52 3492 1.14 6,1073 2.48 519
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes62 B S 1214002-49 3 85 0.199 0.00 < HS accept
Notes
Date:Time:
4/18/125:51 PM
Peak rt Height1 0.52 2072 0.85 13 1.13 854 2.46 506
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3 4
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes63 C S 1214002-50 2 186 0.580 0.00 < HS accept
Notes
Date:Time:
4/18/125:57 PM
Peak rt Height1 0.52 3202 1.15 1863 2.48 593
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Page 21 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 174 of 274
Peak ReportBatch Number: B120565, B120573, B120620
Method Number: CVAFS BR-0011Project Number(s): 1200272 Date Analyzed: 4/18/12Instrument ID: BR-09 Analyst Name: BJT
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes64 A S 1214002-51 2 84 0.195 0.00 < HS accept
Notes
Date:Time:
4/18/126:04 PM
Peak rt Height1 0.52 3372 1.13 843 2.48 371
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes65 B CCV SEQ-CCV 2 6,701 25.1 101 67-133 accept
Notes
Date:Time:
4/18/126:11 PM
Peak rt Height1 0.52 2362 1.12 6,7013 2.45 326
0
5,000
10,000
15,000
20,000
25,000
0 1 2 3 4 5
1 2 3
Run Trap Type Name/ID M B Peak Peak Height Analyzed Result Final Result QA Results Criteria Notes66 C CCB SEQ-CCB 2 33 0.124 0.124 < 1.4 accept
Notes
Date:Time:
4/18/126:17 PM
Peak rt Height1 0.52 3272 1.14 333 2.48 1304 4.80 28
0
200
400
600
800
1,000
0 1 2 3 4 5
1 2 3 4
Page 22 of 49 (Peak Report)
Mercury Guru ver 4.6 © 1995-2011 Brooks Rand LLC
BRL Report 1212016
Page 175 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200243
ICP-MS-2Instrument:
Batch # Source ID
Brooks Rand Labs
1200243-ICB1 QC 11200243 -
1200243-CAL1 QC 2 12120781200243 -
1200243-CAL2 QC 3 12120791200243 -
1200243-CAL3 QC 4 12120801200243 -
1200243-CAL4 QC 5 12120811200243 -
1200243-CAL5 QC 6 12120821200243 -
1200243-CAL6 QC 7 12120831200243 -
1200243-CAL7 QC 8 12120841200243 -
1200243-CAL8 QC 9 12120851200243 -
1200243-ICB2 QC 101200243 -
1200243-ICV1 QC 11 12020021200243 -
1200243-ICB3 QC 121200243 -
1200243-IBL1 QC 131200243 -
1200243-IBL2 QC 141200243 -
1200243-IBL3 QC 151200243 -
1200243-IBL4 QC 161200243 -
1200243-SCV1 QC 17 11340311200243 -
1200243-CCV1 QC 18 12120811200243 -
1200243-CCB1 QC 191200243 -
B120485-BLK1 QC 20B120485 -
B120485-BLK2 QC 21B120485 -
B120485-BLK3 QC 22B120485 -
B120485-BLK4 QC 23B120485 -
B120485-BS1 QC 24B120485 -
B120485-SRM1 QC 25B120485 -
B120485-SRM2 QC 26B120485 -
Page 1 of 6Printed: 4/12/2012 5:08:03PM
BRL Report 1212016
Page 176 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200243
ICP-MS-2Instrument:
Batch # Source ID
Brooks Rand Labs
B120485-SRM3 QC 27B120485 -
1200243-CCV2 QC 28 12120811200243 -
1200243-CCB2 QC 291200243 -
1211036-01 As-S-RARBomb-DRC 30B120485 ACF-SH1201 4/4/2012
1211036-01 Se-S-RARBomb-DRC 31B120485 ACF-SH1201 4/4/2012
B120485-DUP1 QC 32B120485 1211036-01
B120485-MS1 QC 33B120485 1211036-01
B120485-MSD1 QC 34B120485 1211036-01
1200243-CCV3 QC 35 12120811200243 -
1200243-CCB3 QC 361200243 -
B120537-BLK1 QC 37B120537 -
B120537-BLK2 QC 38B120537 -
B120537-BLK3 QC 39B120537 -
B120537-BLK4 QC 40B120537 -
B120537-BS1 QC 41B120537 -
B120537-SRM1 QC 42B120537 -
1212016-21 Se-FW-Oven-DRC-NoMB-TR 43B120537 AAL-MN1101 4/10/2012
1212016-22 Se-FW-Oven-DRC-NoMB-Diss 44B120537 AAL-MN1101 4/10/2012
1212016-01 Se-FW-Oven-DRC-NoMB-TR 45B120537 AAL-MN1101 4/10/2012
1212016-02 Se-FW-Oven-DRC-NoMB-Diss 46B120537 AAL-MN1101 4/10/2012
1200243-CCV4 QC 47 12120811200243 -
1200243-CCB4 QC 481200243 -
1212016-03 Se-FW-Oven-DRC-NoMB-TR 49B120537 AAL-MN1101 4/10/2012
1212016-04 Se-FW-Oven-DRC-NoMB-Diss 50B120537 AAL-MN1101 4/10/2012
1212016-05 Se-FW-Oven-DRC-NoMB-TR 51B120537 AAL-MN1101 4/10/2012
1212016-05 Se-FW-Oven-DRC-NoMB-Diss 52 BatchQCB120537 AAL-MN1101 1/1/1980
Page 2 of 6Printed: 4/12/2012 5:08:03PM
BRL Report 1212016
Page 177 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200243
ICP-MS-2Instrument:
Batch # Source ID
Brooks Rand Labs
B120537-DUP1 QC 53B120537 1212016-05
B120537-MS1 QC 54B120537 1212016-05
B120537-MSD1 QC 55B120537 1212016-05
1212016-06 Se-FW-Oven-DRC-NoMB-Diss 56B120537 AAL-MN1101 4/10/2012
1212016-07 Se-FW-Oven-DRC-NoMB-TR 57B120537 AAL-MN1101 4/10/2012
1200243-CCV5 QC 58 12120811200243 -
1200243-CCB5 QC 591200243 -
1212016-08 Se-FW-Oven-DRC-NoMB-Diss 60B120537 AAL-MN1101 4/10/2012
1212016-09 Se-FW-Oven-DRC-NoMB-TR 61B120537 AAL-MN1101 4/10/2012
1212016-09 Se-FW-Oven-DRC-NoMB-Diss 62 BatchQCB120537 AAL-MN1101 1/1/1980
B120537-DUP2 QC 63B120537 1212016-09
B120537-MS2 QC 64B120537 1212016-09
B120537-MSD2 QC 65B120537 1212016-09
1212016-10 Se-FW-Oven-DRC-NoMB-Diss 66B120537 AAL-MN1101 4/10/2012
1212016-11 Se-FW-Oven-DRC-NoMB-TR 67B120537 AAL-MN1101 4/10/2012
1212016-12 Se-FW-Oven-DRC-NoMB-Diss 68B120537 AAL-MN1101 4/10/2012
1212016-13 Se-FW-Oven-DRC-NoMB-TR 69B120537 AAL-MN1101 4/10/2012
1212016-14 Se-FW-Oven-DRC-NoMB-Diss 70B120537 AAL-MN1101 4/10/2012
1200243-CCV6 QC 71 12120811200243 -
1200243-CCB6 QC 721200243 -
1212016-15 Se-FW-Oven-DRC-NoMB-TR 73B120537 AAL-MN1101 4/10/2012
1212016-16 Se-FW-Oven-DRC-NoMB-Diss 74B120537 AAL-MN1101 4/10/2012
1212016-17 Se-FW-Oven-DRC-NoMB-TR 75B120537 AAL-MN1101 4/10/2012
1212016-18 Se-FW-Oven-DRC-NoMB-Diss 76B120537 AAL-MN1101 4/10/2012
1212016-19 Se-FW-Oven-DRC-NoMB-TR 77B120537 AAL-MN1101 4/10/2012
1212016-19 Se-FW-Oven-DRC-NoMB-Diss 78 BatchQCB120537 AAL-MN1101 1/1/1980
Page 3 of 6Printed: 4/12/2012 5:08:03PM
BRL Report 1212016
Page 178 of 274
ANALYSIS SEQUENCE
Analysis STD ID CommentsDueOrder BRL Project #Lab Number
1200243
ICP-MS-2Instrument:
Batch # Source ID
Brooks Rand Labs
B120537-DUP3 QC 79B120537 1212016-19
B120537-MS3 QC 80B120537 1212016-19
B120537-MSD3 QC 81B120537 1212016-19
1200243-CCV7 QC 82 12120811200243 -
1200243-CCB7 QC 831200243 -
1212016-20 Se-FW-Oven-DRC-NoMB-Diss 84B120537 AAL-MN1101 4/10/2012
1212016-23 Se-FW-Oven-DRC-NoMB-TR 85B120537 AAL-MN1101 4/10/2012
1212016-24 Se-FW-Oven-DRC-NoMB-Diss 86B120537 AAL-MN1101 4/10/2012
1212016-25 Se-FW-Oven-DRC-NoMB-TR 87B120537 AAL-MN1101 4/10/2012
1212016-26 Se-FW-Oven-DRC-NoMB-Diss 88B120537 AAL-MN1101 4/10/2012
1213006-01 Se-FW-Oven-DRC-NoMB-TR 89B120537 AAL-MN1101 4/18/2012
1213006-02 Se-FW-Oven-DRC-NoMB-Diss 90B120537 AAL-MN1101 4/18/2012
1200243-CCV8 QC 91 12120821200243 -
1200243-CCB8 QC 921200243 -
1213006-03 Se-FW-Oven-DRC-NoMB-TR 93B120537 AAL-MN1101 4/18/2012
1213006-04 Se-FW-Oven-DRC-NoMB-Diss 94B120537 AAL-MN1101 4/18/2012
1213006-05 Se-FW-Oven-DRC-NoMB-TR 95B120537 AAL-MN1101 4/18/2012
1213006-06 Se-FW-Oven-DRC-NoMB-Diss 96B120537 AAL-MN1101 4/18/2012
1213006-07 Se-FW-Oven-DRC-NoMB-TR 97B120537 AAL-MN1101 4/18/2012
1213006-08 Se-FW-Oven-DRC-NoMB-Diss 98B120537 AAL-MN1101 4/18/2012
1213006-09 Se-FW-Oven-DRC-NoMB-TR 99B120537 AAL-MN1101 4/18/2012
1213006-10 Se-FW-Oven-DRC-NoMB-Diss 100B120537 AAL-MN1101 4/18/2012
1213006-11 Se-FW-Oven-DRC-NoMB-TR 101B120537 AAL-MN1101 4/18/2012
1213006-12 Se-FW-Oven-DRC-NoMB-Diss 102B120537 AAL-MN1101 4/18/2012
1200243-CCV9 QC 103 12120821200243 -
1200243-CCB9 QC 1041200243 -
Page 4 of 6Printed: 4/12/2012 5:08:03PM
BRL Report 1212016
Page 179 of 274
BRL Report 1212016
Page 180 of 274
BRL Report 1212016
Page 181 of 274
BRL Report 1212016
Page 182 of 274
BRL Report 1212016
Page 183 of 274
BRL Report 1212016
Page 184 of 274
BRL Report 1212016
Page 185 of 274
BRL Report 1212016
Page 186 of 274
BRL Report 1212016
Page 187 of 274
Sample InformationReport Title: QUANTITATIVE ANALYSIS REPORT Batch ID: Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002 Tuning File: C:\Elandata\Tuning\Default.tun Optimization File: C:\Elandata\Optimize\Default.dac Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Calibration Type: External Calibration
Calibration Analyte MassCurve Type Slope Intercept Correlation Coefficient Std 1 Conc AsO 91Weighted Linear 0.004 -0.000 0.999232 0.025000 Se 78Weighted Linear 0.000 -0.000 0.999674 0.050000 Se 77Weighted Linear 0.000 -0.000 0.998008 0.050000> Rh 103Weighted Linear Br 79Weighted Linear Cl 35Weighted Linear C 13Weighted Linear
BRL Report 1212016
Page 188 of 274
Page 1 Sample ID: SEQ-ICB1 Report Date/Time: Friday, April 06, 2012 12:27:33
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-ICB1 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:07:39 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 1 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 2 20.4 ug/L Se 78 5 2 36.1 ug/L Se 77 2 1 31.2 ug/L>>>> Rh 103 398528 4323 1.1 ug/L Br 79 3 1 43.3 ug/L Cl 35 278 26 9.5 ug/L C 13 1493 46 3.1 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 Br 79 Cl 35 C 13
BRL Report 1212016
Page 189 of 274
Page 1 Sample ID: SEQ-CAL1 Report Date/Time: Friday, April 06, 2012 12:27:35
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CAL1 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:09:07 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 2 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CAL1.003 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 46 2 5.1 0.000088 0.0242 ug/L Se 78 5 11 1 13.2 0.000015 0.0491 ug/L Se 77 2 3 1 34.6 0.000005 0.0469 ug/L>>>> Rh 103 398528 391532 5558 1.4 391531.585266 ug/L Br 79 3 7 3 43.3 3.333336 ug/L Cl 35 278 276 24 8.8 -2.500095 ug/L C 13 1493 1464 15 1.0 -28.338860 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 Br 79 Cl 35 C 13
BRL Report 1212016
Page 190 of 274
Page 1 Sample ID: SEQ-CAL2 Report Date/Time: Friday, April 06, 2012 12:27:38
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CAL2 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:10:35 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 3 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CAL2.004 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 96 2 1.6 0.000215 0.0536 ug/L Se 78 5 19 2 12.3 0.000037 0.1045 ug/L Se 77 2 7 1 17.6 0.000012 0.1131 ug/L>>>> Rh 103 398528 393052 2018 0.5 393051.835812 ug/L Br 79 3 2 1 86.6 -1.666667 ug/L Cl 35 278 266 6 2.4 -12.500471 ug/L C 13 1493 1521 53 3.5 28.338917 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 Br 79 Cl 35 C 13
BRL Report 1212016
Page 191 of 274
Page 1 Sample ID: SEQ-CAL3 Report Date/Time: Friday, April 06, 2012 12:27:40
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CAL3 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:12:04 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 4 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CAL3.005 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 410 27 6.5 0.001023 0.2412 ug/L Se 78 5 41 1 2.0 0.000092 0.2451 ug/L Se 77 2 13 2 14.1 0.000028 0.2460 ug/L>>>> Rh 103 398528 390298 1792 0.5 390298.449467 ug/L Br 79 3 0 0 -3.333334 ug/L Cl 35 278 265 18 6.6 -13.333821 ug/L C 13 1493 1533 73 4.8 40.841507 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 Br 79 Cl 35 C 13
BRL Report 1212016
Page 192 of 274
Page 1 Sample ID: SEQ-CAL4 Report Date/Time: Friday, April 06, 2012 12:27:43
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CAL4 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:13:32 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 5 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CAL4.006 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 1682 35 2.1 0.004283 0.9983 ug/L Se 78 5 156 5 2.9 0.000387 0.9957 ug/L Se 77 2 47 4 7.8 0.000117 0.9988 ug/L>>>> Rh 103 398528 390152 2182 0.6 390152.198836 ug/L Br 79 3 5 3 50.0 1.666668 ug/L Cl 35 278 268 19 7.1 -10.833733 ug/L C 13 1493 1440 84 5.8 -52.509797 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 Br 79 Cl 35 C 13
BRL Report 1212016
Page 193 of 274
Page 1 Sample ID: SEQ-CAL5 Report Date/Time: Friday, April 06, 2012 12:27:45
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CAL5 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:15:00 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 6 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CAL5.007 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 8530 130 1.5 0.021999 5.1119 ug/L Se 78 5 780 9 1.1 0.002002 5.1055 ug/L Se 77 2 231 6 2.7 0.000591 5.0171 ug/L>>>> Rh 103 398528 387238 2410 0.6 387237.878237 ug/L Br 79 3 6 1 24.7 2.500001 ug/L Cl 35 278 282 34 12.2 3.333476 ug/L C 13 1493 1439 70 4.9 -53.343376 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 Br 79 Cl 35 C 13
BRL Report 1212016
Page 194 of 274
Page 1 Sample ID: SEQ-CAL6 Report Date/Time: Friday, April 06, 2012 12:27:48
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CAL6 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:16:28 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 7 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CAL6.008 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 42058 389 0.9 0.107749 25.0232 ug/L Se 78 5 3834 35 0.9 0.009812 24.9801 ug/L Se 77 2 1136 8 0.7 0.002906 24.6289 ug/L>>>> Rh 103 398528 390228 2403 0.6 390227.589768 ug/L Br 79 3 8 8 100.0 4.166672 ug/L Cl 35 278 278 21 7.7 -0.833374 ug/L C 13 1493 1424 124 8.7 -68.345711 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 Br 79 Cl 35 C 13
BRL Report 1212016
Page 195 of 274
Page 1 Sample ID: SEQ-CAL7 Report Date/Time: Friday, April 06, 2012 12:27:50
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CAL7 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:17:57 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 8 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CAL7.009 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 211131 1836 0.9 0.540921 125.6066 ug/L Se 78 5 19153 57 0.3 0.049061 124.8509 ug/L Se 77 2 5693 28 0.5 0.014583 123.5504 ug/L>>>> Rh 103 398528 390295 515 0.1 390294.820313 ug/L Br 79 3 9 3 31.5 5.833338 ug/L Cl 35 278 260 23 8.8 -18.333983 ug/L C 13 1493 1491 20 1.4 -1.667063 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 Br 79 Cl 35 C 13
BRL Report 1212016
Page 196 of 274
Page 1 Sample ID: SEQ-CAL8 Report Date/Time: Friday, April 06, 2012 12:27:53
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CAL8 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:19:25 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 9 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CAL8.010 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 817974 5959 0.7 2.086653 484.5287 ug/L Se 78 5 75373 399 0.5 0.192268 489.2528 ug/L Se 77 2 22481 55 0.2 0.057346 485.8193 ug/L>>>> Rh 103 398528 392001 817 0.2 392000.888961 ug/L Br 79 3 16 8 48.2 12.500018 ug/L Cl 35 278 252 22 8.7 -26.667595 ug/L C 13 1493 1442 71 4.9 -50.842900 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 Br 79 Cl 35 C 13
BRL Report 1212016
Page 197 of 274
Page 1 Sample ID: SEQ-ICB2 Report Date/Time: Friday, April 06, 2012 12:27:55
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-ICB2 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:20:54 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 1 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB2.011 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 224 245 109.3 0.000544 0.1300 ug/L Se 78 5 24 13 53.1 0.000048 0.1333 ug/L Se 77 2 10 6 60.4 0.000022 0.1950 ug/L>>>> Rh 103 398528 390853 1109 0.3 390852.989373 ug/L Br 79 3 6 3 49.5 2.500002 ug/L Cl 35 278 285 34 12.1 6.666932 ug/L C 13 1493 1488 28 1.8 -5.001027 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 98.074 Br 79 Cl 35 C 13
BRL Report 1212016
Page 198 of 274
Page 1 Sample ID: SEQ-ICV1 Report Date/Time: Friday, April 06, 2012 12:27:58
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-ICV1 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:22:48 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 10 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICV1.012 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 8795 250 2.8 0.021991 5.1100 ug/L Se 78 5 1621 21 1.3 0.004047 10.3082 ug/L Se 77 2 481 10 2.1 0.001201 10.1833 ug/L>>>> Rh 103 398528 399388 4643 1.2 399388.401925 ug/L Br 79 3 2 3 173.2 -1.666667 ug/L Cl 35 278 288 26 9.2 9.167003 ug/L C 13 1493 1507 90 5.9 14.169686 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 100.216 Br 79 Cl 35 C 13
BRL Report 1212016
Page 199 of 274
Page 1 Sample ID: SEQ-ICB3 Report Date/Time: Friday, April 06, 2012 12:28:01
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-ICB3 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:26:29 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 1 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB3.013 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 18 6 31.2 0.000017 0.0077 ug/L Se 78 5 7 1 12.5 0.000006 0.0265 ug/L Se 77 2 2 0 6.9 0.000001 0.0186 ug/L>>>> Rh 103 398528 387159 3903 1.0 387158.578003 ug/L Br 79 3 1 1 173.2 -2.500001 ug/L Cl 35 278 268 11 4.2 -10.000380 ug/L C 13 1493 1458 48 3.3 -35.006702 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 97.147 Br 79 Cl 35 C 13
BRL Report 1212016
Page 200 of 274
Page 1 Sample ID: SEQ-IBL1 Report Date/Time: Friday, April 06, 2012 12:28:03
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-IBL1 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:27:58 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 101 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-IBL1.014 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 13 1 9.1 0.000005 0.0048 ug/L Se 78 5 5 1 16.3 0.000002 0.0157 ug/L Se 77 2 3 2 54.6 0.000004 0.0392 ug/L>>>> Rh 103 398528 384312 1907 0.5 384312.241166 ug/L Br 79 3 2 1 86.6 -1.666667 ug/L Cl 35 278 272 5 1.9 -6.666934 ug/L C 13 1493 1490 98 6.6 -2.500159 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.433 Br 79 Cl 35 C 13
BRL Report 1212016
Page 201 of 274
Page 1 Sample ID: SEQ-IBL2 Report Date/Time: Friday, April 06, 2012 12:28:06
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-IBL2 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:29:27 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 102 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-IBL2.015 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 13 3 19.9 0.000004 0.0047 ug/L Se 78 5 5 1 18.9 0.000001 0.0135 ug/L Se 77 2 3 0 8.7 0.000004 0.0462 ug/L>>>> Rh 103 398528 385654 1435 0.4 385653.534773 ug/L Br 79 3 3 3 100.0 -0.833333 ug/L Cl 35 278 258 33 12.6 -20.834044 ug/L C 13 1493 1467 51 3.5 -25.838280 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.770 Br 79 Cl 35 C 13
BRL Report 1212016
Page 202 of 274
Page 1 Sample ID: SEQ-IBL3 Report Date/Time: Friday, April 06, 2012 12:28:08
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-IBL3 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:30:55 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 103 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-IBL3.016 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 12 4 32.8 0.000004 0.0045 ug/L Se 78 5 6 2 37.9 0.000003 0.0192 ug/L Se 77 2 2 0 21.7 0.000001 0.0172 ug/L>>>> Rh 103 398528 383832 8527 2.2 383831.908362 ug/L Br 79 3 3 3 86.6 0.000000 ug/L Cl 35 278 253 16 6.4 -25.000883 ug/L C 13 1493 1488 92 6.2 -4.167198 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.312 Br 79 Cl 35 C 13
BRL Report 1212016
Page 203 of 274
Page 1 Sample ID: SEQ-IBL4 Report Date/Time: Friday, April 06, 2012 12:28:11
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-IBL4 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:32:24 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 104 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-IBL4.017 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 11 3 28.6 -0.000001 0.0035 ug/L Se 78 5 7 1 21.8 0.000005 0.0250 ug/L Se 77 2 3 1 18.4 0.000003 0.0352 ug/L>>>> Rh 103 398528 385614 3229 0.8 385613.609464 ug/L Br 79 3 6 4 65.5 2.500002 ug/L Cl 35 278 267 31 11.8 -11.667068 ug/L C 13 1493 1481 30 2.0 -11.668974 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.760 Br 79 Cl 35 C 13
BRL Report 1212016
Page 204 of 274
Page 1 Sample ID: SEQ-SCV1 Report Date/Time: Friday, April 06, 2012 12:28:13
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-SCV1 Sample Description: 5x Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:33:52 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 1 Autosampler Position: 105 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-SCV1.018 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 20526 175 0.9 0.050813 59.0124 ug/L Se 78 5 394 11 2.8 0.000964 12.3193 ug/L Se 77 2 121 2 2.0 0.000295 12.5169 ug/L>>>> Rh 103 398528 403719 1303 0.3 403719.300106 ug/L Br 79 3 8 0 0.0 4.166670 ug/L Cl 35 278 273 14 5.3 -5.000201 ug/L C 13 1493 1445 13 0.9 -47.509154 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 101.303 Br 79 Cl 35 C 13
BRL Report 1212016
Page 205 of 274
Page 1 Sample ID: SEQ-CCV1 Report Date/Time: Friday, April 06, 2012 12:28:16
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCV1 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:38:44 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 5 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCV1.019 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 1642 36 2.2 0.004147 0.9666 ug/L Se 78 5 162 11 6.6 0.000400 1.0288 ug/L Se 77 2 46 1 3.0 0.000112 0.9608 ug/L>>>> Rh 103 398528 393152 4591 1.2 393151.594418 ug/L Br 79 3 3 4 114.6 0.000001 ug/L Cl 35 278 298 15 4.9 20.000729 ug/L C 13 1493 1474 63 4.2 -18.336791 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 98.651 Br 79 Cl 35 C 13
BRL Report 1212016
Page 206 of 274
Page 1 Sample ID: SEQ-CCB1 Report Date/Time: Friday, April 06, 2012 12:28:18
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCB1 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:40:13 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 1 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCB1.020 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 14 3 18.9 0.000008 0.0055 ug/L Se 78 5 7 1 14.4 0.000005 0.0247 ug/L Se 77 2 2 1 33.3 0.000002 0.0257 ug/L>>>> Rh 103 398528 389014 2686 0.7 389014.284380 ug/L Br 79 3 3 1 43.3 -0.000000 ug/L Cl 35 278 273 16 5.7 -5.833562 ug/L C 13 1493 1508 33 2.2 15.836377 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 97.613 Br 79 Cl 35 C 13
BRL Report 1212016
Page 207 of 274
Page 1 Sample ID: B120485-BLK1 Report Date/Time: Friday, April 06, 2012 12:28:21
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120485-BLK1 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 17:41:43 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 106 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120485-BLK1.021 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 8 2 21.7 -0.000007 0.1014 ug/L Se 78 5 7 1 17.0 0.000006 1.3014 ug/L Se 77 2 4 2 52.8 0.000005 2.6562 ug/L>>>> Rh 103 398528 377606 3375 0.9 377605.689269 ug/L Br 79 3 8 4 45.8 5.000004 ug/L Cl 35 278 341 53 15.7 62.502609 ug/L C 13 1493 1403 22 1.5 -89.183524 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 94.750 Br 79 Cl 35 C 13
BRL Report 1212016
Page 208 of 274
Page 1 Sample ID: B120485-BLK2 Report Date/Time: Friday, April 06, 2012 12:28:23
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120485-BLK2 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 17:43:12 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 107 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120485-BLK2.022 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 8 2 25.0 -0.000007 0.1047 ug/L Se 78 5 6 0 2.5 0.000004 1.1030 ug/L Se 77 2 2 1 29.0 0.000002 1.1136 ug/L>>>> Rh 103 398528 372145 1398 0.4 372145.289624 ug/L Br 79 3 12 6 53.9 8.333343 ug/L Cl 35 278 326 38 11.5 47.501896 ug/L C 13 1493 1400 15 1.1 -92.517475 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 93.380 Br 79 Cl 35 C 13
BRL Report 1212016
Page 209 of 274
Page 1 Sample ID: B120485-BLK3 Report Date/Time: Friday, April 06, 2012 12:28:26
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120485-BLK3 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 17:44:40 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 108 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120485-BLK3.023 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 7 1 17.3 -0.000010 0.0651 ug/L Se 78 5 7 0 4.3 0.000006 1.3821 ug/L Se 77 2 2 0 13.9 0.000001 1.0381 ug/L>>>> Rh 103 398528 369200 3892 1.1 369199.683948 ug/L Br 79 3 13 1 10.8 10.000011 ug/L Cl 35 278 318 48 15.0 39.168251 ug/L C 13 1493 1362 75 5.5 -130.857459 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 92.641 Br 79 Cl 35 C 13
BRL Report 1212016
Page 210 of 274
Page 1 Sample ID: B120485-BLK4 Report Date/Time: Friday, April 06, 2012 12:28:28
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120485-BLK4 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 17:46:09 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 109 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120485-BLK4.024 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 4 1 26.6 -0.000017 -0.0088 ug/L Se 78 5 7 1 8.0 0.000007 1.4606 ug/L Se 77 2 3 1 16.4 0.000004 2.2699 ug/L>>>> Rh 103 398528 370004 4155 1.1 370003.719634 ug/L Br 79 3 10 3 25.0 6.666673 ug/L Cl 35 278 308 8 2.5 30.001116 ug/L C 13 1493 1355 58 4.3 -137.525396 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 92.843 Br 79 Cl 35 C 13
BRL Report 1212016
Page 211 of 274
Page 1 Sample ID: B120485-BS1 Report Date/Time: Friday, April 06, 2012 12:28:31
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120485-BS1 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 17:47:37 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 110 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120485-BS1.025 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 557 35 6.3 0.001464 17.1794 ug/L Se 78 5 147 14 9.6 0.000381 49.0341 ug/L Se 77 2 46 2 3.5 0.000118 50.3421 ug/L>>>> Rh 103 398528 373483 1730 0.5 373482.876139 ug/L Br 79 3 15 5 33.3 11.666682 ug/L Cl 35 278 335 26 7.9 56.668925 ug/L C 13 1493 1348 38 2.8 -145.026800 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 93.716 Br 79 Cl 35 C 13
BRL Report 1212016
Page 212 of 274
Page 1 Sample ID: B120485-SRM1 Report Date/Time: Friday, April 06, 2012 12:28:33
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120485-SRM1 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 17:49:06 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 111 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120485-SRM1.026 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 1500 18 1.2 0.003871 45.1245 ug/L Se 78 5 28 1 5.2 0.000060 8.2531 ug/L Se 77 2 12 1 4.7 0.000027 12.0435 ug/L>>>> Rh 103 398528 384833 2791 0.7 384833.348723 ug/L Br 79 3 17 1 8.7 13.333351 ug/L Cl 35 278 330 43 13.1 51.668761 ug/L C 13 1493 1361 46 3.4 -131.691087 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.564 Br 79 Cl 35 C 13
BRL Report 1212016
Page 213 of 274
Page 1 Sample ID: B120485-SRM2 Report Date/Time: Friday, April 06, 2012 12:28:36
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120485-SRM2 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 17:50:34 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 112 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120485-SRM2.027 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 238415 1421 0.6 0.587618 6822.4945 ug/L Se 78 5 21 1 2.9 0.000040 5.6380 ug/L Se 77 2 9 2 22.0 0.000018 8.2181 ug/L>>>> Rh 103 398528 405714 1384 0.3 405714.444939 ug/L Br 79 3 29 9 30.1 25.833391 ug/L Cl 35 278 293 28 9.6 15.000561 ug/L C 13 1493 1296 91 7.0 -196.702046 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 101.803 Br 79 Cl 35 C 13
BRL Report 1212016
Page 214 of 274
Page 1 Sample ID: B120485-SRM3 Report Date/Time: Friday, April 06, 2012 12:28:38
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120485-SRM3 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 17:52:03 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 113 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120485-SRM3.028 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 3534 107 3.0 0.009252 107.6071 ug/L Se 78 5 23 2 9.8 0.000048 6.6763 ug/L Se 77 2 13 1 5.3 0.000029 12.5545 ug/L>>>> Rh 103 398528 380725 3429 0.9 380724.779370 ug/L Br 79 3 32 6 18.2 28.333399 ug/L Cl 35 278 333 40 12.0 55.002225 ug/L C 13 1493 1415 103 7.3 -77.514283 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 95.533 Br 79 Cl 35 C 13
BRL Report 1212016
Page 215 of 274
Page 1 Sample ID: SEQ-CCV2 Report Date/Time: Friday, April 06, 2012 12:28:41
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCV2 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:53:32 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 5 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCV2.029 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 1556 10 0.6 0.004086 0.9526 ug/L Se 78 5 147 7 4.4 0.000377 0.9701 ug/L Se 77 2 44 3 5.8 0.000111 0.9473 ug/L>>>> Rh 103 398528 378189 1627 0.4 378188.794431 ug/L Br 79 3 3 1 43.3 -0.000000 ug/L Cl 35 278 269 18 6.7 -9.167009 ug/L C 13 1493 1412 50 3.5 -80.848579 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 94.896 Br 79 Cl 35 C 13
BRL Report 1212016
Page 216 of 274
Page 1 Sample ID: SEQ-CCB2 Report Date/Time: Friday, April 06, 2012 12:28:44
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCB2 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 17:55:02 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 1 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCB2.030 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 11 8 72.2 0.000001 0.0039 ug/L Se 78 5 4 1 26.7 -0.000002 0.0052 ug/L Se 77 2 2 1 43.3 0.000002 0.0253 ug/L>>>> Rh 103 398528 378030 1434 0.4 378030.430960 ug/L Br 79 3 8 3 33.3 4.166670 ug/L Cl 35 278 248 8 3.2 -30.001055 ug/L C 13 1493 1448 50 3.5 -45.008583 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 94.857 Br 79 Cl 35 C 13
BRL Report 1212016
Page 217 of 274
Page 1 Sample ID: 1211036-01 Report Date/Time: Friday, April 06, 2012 12:28:46
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1211036-01 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 17:56:31 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 114 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1211036-01.031 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 3329 73 2.2 0.008615 100.2022 ug/L Se 78 5 23 4 16.5 0.000048 6.6211 ug/L Se 77 2 13 1 10.0 0.000028 12.4885 ug/L>>>> Rh 103 398528 385110 4316 1.1 385110.484174 ug/L Br 79 3 28 1 5.1 25.000051 ug/L Cl 35 278 322 16 5.0 43.335004 ug/L C 13 1493 1437 101 7.0 -55.843612 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.633 Br 79 Cl 35 C 13
BRL Report 1212016
Page 218 of 274
Page 1 Sample ID: B120485-DUP1 Report Date/Time: Friday, April 06, 2012 12:28:49
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120485-DUP1 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 17:58:00 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 115 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120485-DUP1.032 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 3268 12 0.4 0.008502 98.8992 ug/L Se 78 5 22 4 16.9 0.000044 6.1717 ug/L Se 77 2 11 2 17.3 0.000024 10.6308 ug/L>>>> Rh 103 398528 383065 2957 0.8 383064.986644 ug/L Br 79 3 20 4 21.7 16.666693 ug/L Cl 35 278 330 3 0.8 51.668680 ug/L C 13 1493 1398 31 2.2 -94.184414 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.120 Br 79 Cl 35 C 13
BRL Report 1212016
Page 219 of 274
Page 1 Sample ID: B120485-MS1 Report Date/Time: Friday, April 06, 2012 12:28:51
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120485-MS1 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 17:59:28 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 116 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120485-MS1.033 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 3078 42 1.4 0.008011 93.1882 ug/L Se 78 5 139 2 1.7 0.000351 45.2573 ug/L Se 77 2 44 2 5.3 0.000111 47.2427 ug/L>>>> Rh 103 398528 382835 691 0.2 382835.299025 ug/L Br 79 3 28 7 24.1 24.166717 ug/L Cl 35 278 324 20 6.2 45.835116 ug/L C 13 1493 1369 17 1.2 -123.356357 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.062 Br 79 Cl 35 C 13
BRL Report 1212016
Page 220 of 274
Page 1 Sample ID: B120485-MSD1 Report Date/Time: Friday, April 06, 2012 12:28:54
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120485-MSD1 Sample Description: 50x Batch ID: B120485 Sample Date/Time: Thursday, April 05, 2012 18:00:57 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 117 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120485-MSD1.034 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 3028 24 0.8 0.007841 91.2184 ug/L Se 78 5 134 4 3.1 0.000336 43.3220 ug/L Se 77 2 44 1 1.4 0.000111 47.5497 ug/L>>>> Rh 103 398528 384732 1581 0.4 384732.438021 ug/L Br 79 3 22 1 6.7 18.333363 ug/L Cl 35 278 340 11 3.4 61.669120 ug/L C 13 1493 1408 51 3.6 -84.182519 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.538 Br 79 Cl 35 C 13
BRL Report 1212016
Page 221 of 274
Page 1 Sample ID: SEQ-CCV3 Report Date/Time: Friday, April 06, 2012 12:28:56
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCV3 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 18:02:27 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 5 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCV3.035 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 1590 47 3.0 0.004196 0.9780 ug/L Se 78 5 148 3 1.8 0.000381 0.9801 ug/L Se 77 2 47 4 8.7 0.000120 1.0284 ug/L>>>> Rh 103 398528 376549 2650 0.7 376548.886432 ug/L Br 79 3 4 3 69.3 0.833334 ug/L Cl 35 278 244 17 6.8 -34.167845 ug/L C 13 1493 1459 85 5.8 -33.339510 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 94.485 Br 79 Cl 35 C 13
BRL Report 1212016
Page 222 of 274
Page 1 Sample ID: SEQ-CCB3 Report Date/Time: Friday, April 06, 2012 12:28:59
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCB3 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 18:03:56 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 1 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCB3.036 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 13 5 35.3 0.000007 0.0052 ug/L Se 78 5 5 1 15.9 0.000002 0.0151 ug/L Se 77 2 2 1 45.4 0.000001 0.0205 ug/L>>>> Rh 103 398528 372498 9667 2.6 372497.950297 ug/L Br 79 3 7 4 57.3 3.333336 ug/L Cl 35 278 253 24 9.5 -25.000869 ug/L C 13 1493 1501 40 2.7 8.334934 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 93.468 Br 79 Cl 35 C 13
BRL Report 1212016
Page 223 of 274
Page 1 Sample ID: B120537-BLK1 Report Date/Time: Friday, April 06, 2012 12:29:01
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-BLK1 Sample Description: Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:05:27 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 201 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-BLK1.037 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 7 1 8.7 -0.000011 0.0012 ug/L Se 78 5 4 1 15.3 -0.000000 0.0101 ug/L Se 77 2 2 1 44.1 -0.000000 0.0065 ug/L>>>> Rh 103 398528 379677 1857 0.5 379677.016211 ug/L Br 79 3 0 0 -3.333334 ug/L Cl 35 278 268 27 10.0 -10.000354 ug/L C 13 1493 1550 45 2.9 57.511370 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 95.270 Br 79 Cl 35 C 13
BRL Report 1212016
Page 224 of 274
Page 1 Sample ID: B120537-BLK2 Report Date/Time: Friday, April 06, 2012 12:29:04
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-BLK2 Sample Description: Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:06:56 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 202 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-BLK2.038 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 5 3 52.9 -0.000015 0.0002 ug/L Se 78 5 4 1 32.2 -0.000001 0.0089 ug/L Se 77 2 3 2 62.2 0.000003 0.0304 ug/L>>>> Rh 103 398528 380814 204 0.1 380813.543342 ug/L Br 79 3 3 3 100.0 -0.833333 ug/L Cl 35 278 282 26 9.3 3.333454 ug/L C 13 1493 1514 27 1.8 21.670842 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 95.555 Br 79 Cl 35 C 13
BRL Report 1212016
Page 225 of 274
Page 1 Sample ID: B120537-BLK3 Report Date/Time: Friday, April 06, 2012 12:29:06
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-BLK3 Sample Description: Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:08:24 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 203 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-BLK3.039 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 8 2 30.1 -0.000008 0.0018 ug/L Se 78 5 4 0 10.6 -0.000003 0.0046 ug/L Se 77 2 2 1 50.9 0.000002 0.0232 ug/L>>>> Rh 103 398528 378828 2151 0.6 378828.388241 ug/L Br 79 3 3 0 0.0 -0.833334 ug/L Cl 35 278 240 5 2.1 -38.334654 ug/L C 13 1493 1469 122 8.3 -23.337277 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 95.057 Br 79 Cl 35 C 13
BRL Report 1212016
Page 226 of 274
Page 1 Sample ID: B120537-BLK4 Report Date/Time: Friday, April 06, 2012 12:29:09
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-BLK4 Sample Description: Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:09:52 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 204 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-BLK4.040 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 8 4 50.0 -0.000007 0.0020 ug/L Se 78 5 5 1 13.4 0.000000 0.0123 ug/L Se 77 2 2 1 28.4 0.000001 0.0139 ug/L>>>> Rh 103 398528 379763 1771 0.5 379762.750677 ug/L Br 79 3 2 1 86.6 -1.666667 ug/L Cl 35 278 237 9 3.7 -41.668089 ug/L C 13 1493 1486 31 2.1 -6.668008 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 95.291 Br 79 Cl 35 C 13
BRL Report 1212016
Page 227 of 274
Page 1 Sample ID: B120537-BS1 Report Date/Time: Friday, April 06, 2012 12:29:11
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-BS1 Sample Description: Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:11:21 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 205 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-BS1.041 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 6635 46 0.7 0.017091 3.9724 ug/L Se 78 5 622 7 1.1 0.001594 4.0663 ug/L Se 77 2 189 2 1.1 0.000482 4.0953 ug/L>>>> Rh 103 398528 387549 1502 0.4 387548.647335 ug/L Br 79 3 2 3 173.2 -1.666667 ug/L Cl 35 278 269 29 10.8 -9.166987 ug/L C 13 1493 1477 71 4.8 -15.836261 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 97.245 Br 79 Cl 35 C 13
BRL Report 1212016
Page 228 of 274
Page 1 Sample ID: 1212016-21 Report Date/Time: Friday, April 06, 2012 12:29:14
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-21 Sample Description: Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:12:49 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 206 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-21.042 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 12 2 17.8 0.000002 0.0042 ug/L Se 78 5 4 1 21.7 -0.000001 0.0086 ug/L Se 77 2 2 1 56.8 0.000001 0.0133 ug/L>>>> Rh 103 398528 384740 1985 0.5 384739.503245 ug/L Br 79 3 6 1 24.7 2.500001 ug/L Cl 35 278 234 23 9.7 -44.168146 ug/L C 13 1493 1520 23 1.5 27.505317 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.540 Br 79 Cl 35 C 13
BRL Report 1212016
Page 229 of 274
Page 1 Sample ID: 1212016-22 Report Date/Time: Friday, April 06, 2012 12:29:16
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-22 Sample Description: Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:14:18 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 207 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-22.043 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 8 3 33.1 -0.000008 0.0019 ug/L Se 78 5 4 2 51.4 -0.000001 0.0075 ug/L Se 77 2 2 1 57.1 0.000000 0.0114 ug/L>>>> Rh 103 398528 385103 1840 0.5 385102.834988 ug/L Br 79 3 3 3 100.0 -0.833333 ug/L Cl 35 278 248 18 7.1 -30.834404 ug/L C 13 1493 1507 39 2.6 14.169403 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.631 Br 79 Cl 35 C 13
BRL Report 1212016
Page 230 of 274
Page 1 Sample ID: 1212016-01 Report Date/Time: Friday, April 06, 2012 12:29:19
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-01 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:15:46 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 208 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-01.044 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 65 3 4.4 0.000163 2.0785 ug/L Se 78 5 6 0 5.7 0.000004 1.0781 ug/L Se 77 2 2 1 48.3 0.000003 1.5373 ug/L>>>> Rh 103 398528 341272 3502 1.0 341272.389490 ug/L Br 79 3 1344 122 9.1 1340.951428 ug/L Cl 35 278 294 15 5.1 15.833902 ug/L C 13 1493 1563 109 7.0 70.847826 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 85.633 Br 79 Cl 35 C 13
BRL Report 1212016
Page 231 of 274
Page 1 Sample ID: 1212016-02 Report Date/Time: Friday, April 06, 2012 12:29:22
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-02 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:17:15 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 209 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-02.045 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 50 6 12.5 0.000115 1.5206 ug/L Se 78 5 4 1 21.0 0.000001 0.6395 ug/L Se 77 2 2 0 16.4 0.000003 1.4841 ug/L>>>> Rh 103 398528 348606 169 0.0 348605.834814 ug/L Br 79 3 1367 46 3.4 1363.454840 ug/L Cl 35 278 354 15 4.3 75.836431 ug/L C 13 1493 1637 60 3.7 144.196059 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 87.473 Br 79 Cl 35 C 13
BRL Report 1212016
Page 232 of 274
Page 1 Sample ID: SEQ-CCV4 Report Date/Time: Friday, April 06, 2012 12:29:24
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCV4 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 18:18:46 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 5 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCV2.046 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 1753 45 2.6 0.004272 0.9956 ug/L Se 78 5 166 5 3.3 0.000395 1.0176 ug/L Se 77 2 48 3 6.3 0.000114 0.9701 ug/L>>>> Rh 103 398528 407669 3671 0.9 407669.302835 ug/L Br 79 3 18 11 65.5 14.166691 ug/L Cl 35 278 314 29 9.2 35.834719 ug/L C 13 1493 1714 91 5.3 221.713148 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 102.294 Br 79 Cl 35 C 13
BRL Report 1212016
Page 233 of 274
Page 1 Sample ID: SEQ-CCB4 Report Date/Time: Friday, April 06, 2012 12:29:27
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCB4 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 18:20:16 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 1 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCB2.047 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 9 1 6.7 -0.000007 0.0021 ug/L Se 78 5 3 1 23.0 -0.000004 0.0008 ug/L Se 77 2 2 1 28.6 0.000000 0.0094 ug/L>>>> Rh 103 398528 406098 3029 0.7 406097.509894 ug/L Br 79 3 15 11 76.4 11.666686 ug/L Cl 35 278 295 33 11.1 16.667304 ug/L C 13 1493 1740 54 3.1 247.552047 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 101.899 Br 79 Cl 35 C 13
BRL Report 1212016
Page 234 of 274
Page 1 Sample ID: 1212016-03 Report Date/Time: Friday, April 06, 2012 12:29:29
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-03 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:21:47 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 210 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-03.048 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 66 2 2.3 0.000159 2.0310 ug/L Se 78 5 5 1 12.2 0.000003 0.9363 ug/L Se 77 2 2 1 63.5 0.000002 1.2653 ug/L>>>> Rh 103 398528 350424 794 0.2 350424.075379 ug/L Br 79 3 1363 118 8.7 1360.121427 ug/L Cl 35 278 341 31 9.0 62.502525 ug/L C 13 1493 1634 30 1.8 141.695411 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 87.930 Br 79 Cl 35 C 13
BRL Report 1212016
Page 235 of 274
Page 1 Sample ID: 1212016-04 Report Date/Time: Friday, April 06, 2012 12:29:32
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-04 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:23:16 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 211 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-04.049 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 51 7 14.1 0.000117 1.5444 ug/L Se 78 5 5 0 9.5 0.000003 0.8969 ug/L Se 77 2 3 1 36.1 0.000003 1.6707 ug/L>>>> Rh 103 398528 350629 1033 0.3 350628.952726 ug/L Br 79 3 1461 64 4.4 1457.638902 ug/L Cl 35 278 331 15 4.4 52.502058 ug/L C 13 1493 1710 45 2.6 217.545279 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 87.981 Br 79 Cl 35 C 13
BRL Report 1212016
Page 236 of 274
Page 1 Sample ID: 1212016-05 Report Date/Time: Friday, April 06, 2012 12:29:34
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-05 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:24:44 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 212 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-05.050 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 73 6 7.5 0.000181 2.2884 ug/L Se 78 5 5 0 7.9 0.000002 0.7806 ug/L Se 77 2 2 1 27.0 0.000002 1.4723 ug/L>>>> Rh 103 398528 349936 1076 0.3 349935.945010 ug/L Br 79 3 1414 75 5.3 1410.963580 ug/L Cl 35 278 327 6 1.8 48.335205 ug/L C 13 1493 1628 25 1.6 135.027319 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 87.807 Br 79 Cl 35 C 13
BRL Report 1212016
Page 237 of 274
Page 1 Sample ID: B120537-DUP1 Report Date/Time: Friday, April 06, 2012 12:29:37
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-DUP1 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:26:13 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 213 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-DUP1.051 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 67 3 4.5 0.000164 2.0855 ug/L Se 78 5 5 1 28.7 0.000002 0.8478 ug/L Se 77 2 3 0 8.3 0.000004 2.2928 ug/L>>>> Rh 103 398528 348868 2498 0.7 348868.431879 ug/L Br 79 3 1480 121 8.2 1476.809694 ug/L Cl 35 278 338 15 4.3 60.002384 ug/L C 13 1493 1673 36 2.2 180.037002 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 87.539 Br 79 Cl 35 C 13
BRL Report 1212016
Page 238 of 274
Page 1 Sample ID: B120537-MS1 Report Date/Time: Friday, April 06, 2012 12:29:39
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-MS1 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:27:41 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 214 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-MS1.052 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 63 9 13.6 0.000150 1.9308 ug/L Se 78 5 153 5 3.1 0.000422 54.2521 ug/L Se 77 2 47 5 11.3 0.000128 54.7212 ug/L>>>> Rh 103 398528 352348 2972 0.8 352347.690446 ug/L Br 79 3 1411 21 1.5 1407.629410 ug/L Cl 35 278 320 8 2.3 41.668259 ug/L C 13 1493 1680 83 4.9 187.538878 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 88.412 Br 79 Cl 35 C 13
BRL Report 1212016
Page 239 of 274
Page 1 Sample ID: B120537-MSD1 Report Date/Time: Friday, April 06, 2012 12:29:42
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-MSD1 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:29:10 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 215 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-MSD1.053 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 68 12 16.9 0.000166 2.1115 ug/L Se 78 5 150 10 6.6 0.000415 53.3690 ug/L Se 77 2 49 3 7.0 0.000136 57.9508 ug/L>>>> Rh 103 398528 351723 1744 0.5 351723.159891 ug/L Br 79 3 1381 30 2.2 1377.623985 ug/L Cl 35 278 359 33 9.2 80.836700 ug/L C 13 1493 1720 28 1.7 227.547456 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 88.256 Br 79 Cl 35 C 13
BRL Report 1212016
Page 240 of 274
Page 1 Sample ID: 1212016-06 Report Date/Time: Friday, April 06, 2012 12:29:44
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-06 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:30:38 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 216 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-06.054 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 62 3 5.2 0.000148 1.8987 ug/L Se 78 5 5 0 10.0 0.000002 0.8080 ug/L Se 77 2 2 2 66.5 0.000003 1.5680 ug/L>>>> Rh 103 398528 350389 647 0.2 350389.197388 ug/L Br 79 3 1426 67 4.7 1422.632349 ug/L Cl 35 278 321 11 3.5 42.501630 ug/L C 13 1493 1639 87 5.3 145.863250 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 87.921 Br 79 Cl 35 C 13
BRL Report 1212016
Page 241 of 274
Page 1 Sample ID: 1212016-07 Report Date/Time: Friday, April 06, 2012 12:29:47
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-07 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:32:07 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 217 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-07.055 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 72 10 13.6 0.000176 2.2340 ug/L Se 78 5 5 1 16.1 0.000003 0.9731 ug/L Se 77 2 2 1 45.1 0.000001 1.0482 ug/L>>>> Rh 103 398528 352969 966 0.3 352969.074627 ug/L Br 79 3 1445 68 4.7 1441.802600 ug/L Cl 35 278 351 23 6.6 72.502958 ug/L C 13 1493 1667 33 2.0 174.202391 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 88.568 Br 79 Cl 35 C 13
BRL Report 1212016
Page 242 of 274
Page 1 Sample ID: SEQ-CCV5 Report Date/Time: Friday, April 06, 2012 12:29:49
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCV5 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 18:33:38 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 5 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCV3.056 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 1776 33 1.9 0.004248 0.9900 ug/L Se 78 5 167 12 7.1 0.000389 1.0010 ug/L Se 77 2 50 4 7.6 0.000117 0.9995 ug/L>>>> Rh 103 398528 415296 1923 0.5 415296.084903 ug/L Br 79 3 25 7 26.5 21.666708 ug/L Cl 35 278 308 9 3.1 30.001117 ug/L C 13 1493 1774 94 5.3 280.893248 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 104.208 Br 79 Cl 35 C 13
BRL Report 1212016
Page 243 of 274
Page 1 Sample ID: SEQ-CCB5 Report Date/Time: Friday, April 06, 2012 12:29:52
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCB5 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 18:35:07 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 1 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCB3.057 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 11 2 19.5 -0.000003 0.0031 ug/L Se 78 5 4 1 13.3 -0.000002 0.0065 ug/L Se 77 2 1 1 48.0 -0.000002 -0.0049 ug/L>>>> Rh 103 398528 414362 1356 0.3 414361.758092 ug/L Br 79 3 13 1 10.8 10.000011 ug/L Cl 35 278 306 43 14.1 27.501094 ug/L C 13 1493 1655 76 4.6 162.533412 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 103.973 Br 79 Cl 35 C 13
BRL Report 1212016
Page 244 of 274
Page 1 Sample ID: 1212016-08 Report Date/Time: Friday, April 06, 2012 12:29:54
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-08 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:36:38 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 218 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-08.058 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 55 5 8.9 0.000128 1.6707 ug/L Se 78 5 4 0 8.8 0.000000 0.5828 ug/L Se 77 2 2 1 34.4 0.000002 1.4439 ug/L>>>> Rh 103 398528 353804 1134 0.3 353803.647677 ug/L Br 79 3 1500 33 2.2 1496.812977 ug/L Cl 35 278 369 10 2.8 90.837131 ug/L C 13 1493 1705 61 3.6 212.544241 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 88.778 Br 79 Cl 35 C 13
BRL Report 1212016
Page 245 of 274
Page 1 Sample ID: 1212016-09 Report Date/Time: Friday, April 06, 2012 12:29:57
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-09 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:38:07 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 219 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-09.059 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 84 8 9.2 0.000209 2.6080 ug/L Se 78 5 4 1 29.0 0.000000 0.5807 ug/L Se 77 2 3 1 54.1 0.000003 1.8254 ug/L>>>> Rh 103 398528 355679 443 0.1 355678.845948 ug/L Br 79 3 1548 68 4.4 1545.156042 ug/L Cl 35 278 328 25 7.7 50.001969 ug/L C 13 1493 1754 78 4.5 260.888545 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 89.248 Br 79 Cl 35 C 13
BRL Report 1212016
Page 246 of 274
Page 1 Sample ID: B120537-DUP2 Report Date/Time: Friday, April 06, 2012 12:29:59
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-DUP2 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:39:35 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 220 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-DUP2.060 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 72 7 9.6 0.000172 2.1769 ug/L Se 78 5 7 1 22.4 0.000006 1.3715 ug/L Se 77 2 2 2 62.4 0.000003 1.4931 ug/L>>>> Rh 103 398528 360119 905 0.3 360119.313339 ug/L Br 79 3 1454 34 2.3 1450.970845 ug/L Cl 35 278 333 37 11.1 54.168846 ug/L C 13 1493 1694 79 4.7 200.875106 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 90.362 Br 79 Cl 35 C 13
BRL Report 1212016
Page 247 of 274
Page 1 Sample ID: B120537-MS2 Report Date/Time: Friday, April 06, 2012 12:30:02
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-MS2 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:41:04 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 221 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-MS2.061 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 75 5 6.7 0.000180 2.2755 ug/L Se 78 5 159 2 1.3 0.000433 55.6491 ug/L Se 77 2 46 5 11.3 0.000125 53.2596 ug/L>>>> Rh 103 398528 358215 2165 0.6 358215.251597 ug/L Br 79 3 1628 54 3.3 1624.338979 ug/L Cl 35 278 308 5 1.7 30.001115 ug/L C 13 1493 1746 32 1.8 253.386619 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 89.885 Br 79 Cl 35 C 13
BRL Report 1212016
Page 248 of 274
Page 1 Sample ID: B120537-MSD2 Report Date/Time: Friday, April 06, 2012 12:30:04
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-MSD2 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:42:32 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 222 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-MSD2.062 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 74 9 12.3 0.000177 2.2393 ug/L Se 78 5 155 8 5.0 0.000419 53.8128 ug/L Se 77 2 52 2 4.3 0.000142 60.4333 ug/L>>>> Rh 103 398528 358855 2118 0.6 358854.878881 ug/L Br 79 3 1543 37 2.4 1540.154896 ug/L Cl 35 278 366 11 3.1 87.503639 ug/L C 13 1493 1664 86 5.2 170.868612 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 90.045 Br 79 Cl 35 C 13
BRL Report 1212016
Page 249 of 274
Page 1 Sample ID: 1212016-10 Report Date/Time: Friday, April 06, 2012 12:30:07
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-10 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:44:01 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 223 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-10.063 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 58 10 16.8 0.000130 1.6991 ug/L Se 78 5 5 2 30.3 0.000002 0.7728 ug/L Se 77 2 3 1 26.5 0.000003 1.5609 ug/L>>>> Rh 103 398528 363274 2301 0.6 363273.571337 ug/L Br 79 3 1561 96 6.2 1557.658771 ug/L Cl 35 278 370 11 3.1 91.670505 ug/L C 13 1493 1743 90 5.2 250.052837 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 91.154 Br 79 Cl 35 C 13
BRL Report 1212016
Page 250 of 274
Page 1 Sample ID: 1212016-11 Report Date/Time: Friday, April 06, 2012 12:30:09
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-11 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:45:29 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 224 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-11.064 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 71 12 17.3 0.000167 2.1259 ug/L Se 78 5 5 1 28.6 0.000001 0.7104 ug/L Se 77 2 2 1 32.9 0.000000 0.4875 ug/L>>>> Rh 103 398528 364989 2018 0.6 364989.451268 ug/L Br 79 3 1590 114 7.2 1586.831572 ug/L Cl 35 278 344 19 5.5 65.835983 ug/L C 13 1493 1628 79 4.9 135.027562 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 91.584 Br 79 Cl 35 C 13
BRL Report 1212016
Page 251 of 274
Page 1 Sample ID: 1212016-12 Report Date/Time: Friday, April 06, 2012 12:30:12
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-12 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:46:58 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 225 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-12.065 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 39 7 17.2 0.000077 1.0787 ug/L Se 78 5 4 1 36.0 -0.000002 0.3547 ug/L Se 77 2 2 1 37.8 0.000001 0.6673 ug/L>>>> Rh 103 398528 366688 2996 0.8 366688.494003 ug/L Br 79 3 1545 84 5.4 1541.822141 ug/L Cl 35 278 356 38 10.7 77.503227 ug/L C 13 1493 1765 120 6.8 272.558237 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 92.011 Br 79 Cl 35 C 13
BRL Report 1212016
Page 252 of 274
Page 1 Sample ID: 1212016-13 Report Date/Time: Friday, April 06, 2012 12:30:14
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-13 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:48:26 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 226 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-13.066 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 56 6 9.9 0.000122 1.6052 ug/L Se 78 5 5 0 8.4 0.000003 0.8904 ug/L Se 77 2 2 1 37.7 0.000000 0.5595 ug/L>>>> Rh 103 398528 369282 836 0.2 369282.085059 ug/L Br 79 3 1548 92 5.9 1545.156206 ug/L Cl 35 278 350 22 6.2 71.669584 ug/L C 13 1493 1789 88 4.9 296.730204 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 92.662 Br 79 Cl 35 C 13
BRL Report 1212016
Page 253 of 274
Page 1 Sample ID: 1212016-14 Report Date/Time: Friday, April 06, 2012 12:30:17
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-14 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:49:55 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 227 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-14.067 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 58 1 1.0 0.000128 1.6680 ug/L Se 78 5 5 2 34.9 0.000000 0.6132 ug/L Se 77 2 3 0 15.7 0.000003 1.7660 ug/L>>>> Rh 103 398528 373604 1248 0.3 373604.342017 ug/L Br 79 3 1637 30 1.8 1633.507503 ug/L Cl 35 278 353 41 11.7 74.169751 ug/L C 13 1493 1715 24 1.4 222.546329 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 93.746 Br 79 Cl 35 C 13
BRL Report 1212016
Page 254 of 274
Page 1 Sample ID: SEQ-CCV6 Report Date/Time: Friday, April 06, 2012 12:30:20
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCV6 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 18:51:25 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 5 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCV4.068 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 1872 18 1.0 0.004256 0.9918 ug/L Se 78 5 172 9 5.0 0.000380 0.9793 ug/L Se 77 2 53 1 1.9 0.000117 0.9971 ug/L>>>> Rh 103 398528 437041 2155 0.5 437040.878284 ug/L Br 79 3 28 11 39.6 24.166720 ug/L Cl 35 278 291 4 1.3 12.500433 ug/L C 13 1493 1852 32 1.7 359.244704 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 109.664 Br 79 Cl 35 C 13
BRL Report 1212016
Page 255 of 274
Page 1 Sample ID: SEQ-CCB6 Report Date/Time: Friday, April 06, 2012 12:30:22
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCB6 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 18:52:54 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 1 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCB4.069 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 9 2 24.0 -0.000008 0.0018 ug/L Se 78 5 5 0 3.4 -0.000002 0.0074 ug/L Se 77 2 2 1 38.5 0.000001 0.0170 ug/L>>>> Rh 103 398528 432832 1549 0.4 432831.685815 ug/L Br 79 3 19 5 27.2 15.833358 ug/L Cl 35 278 303 9 2.9 24.167552 ug/L C 13 1493 1867 44 2.4 374.248371 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 108.608 Br 79 Cl 35 C 13
BRL Report 1212016
Page 256 of 274
Page 1 Sample ID: 1212016-15 Report Date/Time: Friday, April 06, 2012 12:30:25
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-15 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:54:25 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 228 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-15.070 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 72 2 2.1 0.000165 2.1069 ug/L Se 78 5 5 1 27.4 0.000002 0.8289 ug/L Se 77 2 2 0 19.9 0.000001 0.8448 ug/L>>>> Rh 103 398528 369559 1082 0.3 369559.110587 ug/L Br 79 3 1634 113 6.9 1631.007491 ug/L Cl 35 278 351 4 1.1 72.502935 ug/L C 13 1493 1709 72 4.2 216.711897 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 92.731 Br 79 Cl 35 C 13
BRL Report 1212016
Page 257 of 274
Page 1 Sample ID: 1212016-16 Report Date/Time: Friday, April 06, 2012 12:30:27
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-16 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:55:54 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 229 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-16.071 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 57 18 31.6 0.000124 1.6196 ug/L Se 78 5 5 1 10.3 0.000001 0.7183 ug/L Se 77 2 2 1 34.4 0.000002 1.2875 ug/L>>>> Rh 103 398528 374798 1600 0.4 374797.892374 ug/L Br 79 3 1624 65 4.0 1621.004999 ug/L Cl 35 278 343 36 10.5 64.169282 ug/L C 13 1493 1673 16 0.9 180.036956 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 94.046 Br 79 Cl 35 C 13
BRL Report 1212016
Page 258 of 274
Page 1 Sample ID: 1212016-17 Report Date/Time: Friday, April 06, 2012 12:30:30
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-17 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:57:22 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 230 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-17.072 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 71 3 4.9 0.000161 2.0518 ug/L Se 78 5 4 2 44.1 -0.000000 0.5164 ug/L Se 77 2 2 0 15.7 0.000001 0.7178 ug/L>>>> Rh 103 398528 375247 1241 0.3 375247.319493 ug/L Br 79 3 1644 19 1.2 1640.175569 ug/L Cl 35 278 356 30 8.4 77.503203 ug/L C 13 1493 1747 51 2.9 254.220212 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 94.158 Br 79 Cl 35 C 13
BRL Report 1212016
Page 259 of 274
Page 1 Sample ID: 1212016-18 Report Date/Time: Friday, April 06, 2012 12:30:32
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-18 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 18:58:51 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 231 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-18.073 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 63 4 5.7 0.000138 1.7914 ug/L Se 78 5 4 1 17.4 -0.000002 0.3384 ug/L Se 77 2 3 0 13.3 0.000004 2.2927 ug/L>>>> Rh 103 398528 377777 443 0.1 377776.667335 ug/L Br 79 3 1723 32 1.9 1719.359587 ug/L Cl 35 278 383 9 2.3 104.171114 ug/L C 13 1493 1784 25 1.4 290.895206 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 94.793 Br 79 Cl 35 C 13
BRL Report 1212016
Page 260 of 274
Page 1 Sample ID: 1212016-19 Report Date/Time: Friday, April 06, 2012 12:30:35
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-19 Sample Description: 40x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 19:00:19 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.125 Autosampler Position: 232 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-19.074 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 85 10 11.6 0.000198 1.9864 ug/L Se 78 5 5 1 28.6 0.000001 0.5719 ug/L Se 77 2 3 1 16.9 0.000004 1.7027 ug/L>>>> Rh 103 398528 375472 1323 0.4 375472.073219 ug/L Br 79 3 1774 74 4.2 1771.038190 ug/L Cl 35 278 390 26 6.8 111.671517 ug/L C 13 1493 1760 75 4.3 267.556715 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 94.215 Br 79 Cl 35 C 13
BRL Report 1212016
Page 261 of 274
Page 1 Sample ID: B120537-DUP3 Report Date/Time: Friday, April 06, 2012 12:30:37
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-DUP3 Sample Description: 40x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 19:01:48 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.125 Autosampler Position: 233 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-DUP3.075 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 77 7 9.4 0.000176 1.7868 ug/L Se 78 5 6 2 25.7 0.000004 0.8224 ug/L Se 77 2 3 1 30.0 0.000004 1.6243 ug/L>>>> Rh 103 398528 375852 1311 0.3 375852.491138 ug/L Br 79 3 1738 25 1.4 1734.362944 ug/L Cl 35 278 353 11 3.3 74.169683 ug/L C 13 1493 1686 30 1.8 193.373228 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 94.310 Br 79 Cl 35 C 13
BRL Report 1212016
Page 262 of 274
Page 1 Sample ID: B120537-MS3 Report Date/Time: Friday, April 06, 2012 12:30:40
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-MS3 Sample Description: 40x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 19:03:16 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.125 Autosampler Position: 234 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-MS3.076 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 79 8 10.2 0.000181 1.8279 ug/L Se 78 5 182 1 0.4 0.000468 48.0618 ug/L Se 77 2 53 3 5.5 0.000135 46.2205 ug/L>>>> Rh 103 398528 379063 1229 0.3 379062.727436 ug/L Br 79 3 1896 43 2.2 1892.733729 ug/L Cl 35 278 384 35 9.2 105.837915 ug/L C 13 1493 1711 47 2.8 218.378807 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 95.116 Br 79 Cl 35 C 13
BRL Report 1212016
Page 263 of 274
Page 1 Sample ID: B120537-MSD3 Report Date/Time: Friday, April 06, 2012 12:30:42
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: B120537-MSD3 Sample Description: 40x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 19:04:45 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.125 Autosampler Position: 235 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\B120537-MSD3.077 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 77 12 16.1 0.000174 1.7664 ug/L Se 78 5 176 1 0.5 0.000453 46.5596 ug/L Se 77 2 56 5 8.8 0.000143 48.7990 ug/L>>>> Rh 103 398528 378024 4128 1.1 378024.066383 ug/L Br 79 3 1789 53 3.0 1786.041550 ug/L Cl 35 278 391 28 7.1 112.504896 ug/L C 13 1493 1741 84 4.8 248.385748 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 94.855 Br 79 Cl 35 C 13
BRL Report 1212016
Page 264 of 274
Page 1 Sample ID: SEQ-CCV7 Report Date/Time: Friday, April 06, 2012 12:30:45
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCV7 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 19:06:16 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 5 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCV5.078 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 1921 25 1.3 0.004211 0.9814 ug/L Se 78 5 183 2 1.3 0.000391 1.0057 ug/L Se 77 2 54 2 3.9 0.000114 0.9747 ug/L>>>> Rh 103 398528 453157 809 0.2 453156.764602 ug/L Br 79 3 26 10 39.1 22.500047 ug/L Cl 35 278 355 36 10.2 76.669849 ug/L C 13 1493 1885 53 2.8 392.586213 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 113.708 Br 79 Cl 35 C 13
BRL Report 1212016
Page 265 of 274
Page 1 Sample ID: SEQ-CCB7 Report Date/Time: Friday, April 06, 2012 12:30:47
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCB7 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 19:07:45 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 1 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCB5.079 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 12 2 16.7 -0.000002 0.0033 ug/L Se 78 5 4 1 20.0 -0.000002 0.0052 ug/L Se 77 2 1 1 47.2 -0.000001 -0.0018 ug/L>>>> Rh 103 398528 446813 3419 0.8 446813.467576 ug/L Br 79 3 18 9 51.5 14.166689 ug/L Cl 35 278 301 19 6.3 22.500832 ug/L C 13 1493 1901 124 6.5 408.423990 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 112.116 Br 79 Cl 35 C 13
BRL Report 1212016
Page 266 of 274
Page 1 Sample ID: 1212016-20 Report Date/Time: Friday, April 06, 2012 12:30:50
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-20 Sample Description: 40x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 19:09:17 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.125 Autosampler Position: 236 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-20.080 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 15 4 27.6 0.000004 0.1881 ug/L Se 78 5 4 0 9.5 -0.000003 0.1267 ug/L Se 77 2 1 0 20.4 -0.000001 -0.0094 ug/L>>>> Rh 103 398528 447871 5572 1.2 447870.634921 ug/L Br 79 3 13 4 28.6 10.000011 ug/L Cl 35 278 328 35 10.8 49.168626 ug/L C 13 1493 1842 83 4.5 349.242560 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 112.381 Br 79 Cl 35 C 13
BRL Report 1212016
Page 267 of 274
Page 1 Sample ID: 1212016-23 Report Date/Time: Friday, April 06, 2012 12:30:52
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-23 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 19:10:46 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 237 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-23.081 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 79 12 14.5 0.000178 2.2550 ug/L Se 78 5 5 0 3.0 0.000000 0.6025 ug/L Se 77 2 4 1 13.3 0.000006 2.7883 ug/L>>>> Rh 103 398528 383776 1740 0.5 383775.559999 ug/L Br 79 3 1717 51 3.0 1713.525020 ug/L Cl 35 278 382 22 5.9 103.337758 ug/L C 13 1493 1774 81 4.6 281.726679 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.298 Br 79 Cl 35 C 13
BRL Report 1212016
Page 268 of 274
Page 1 Sample ID: 1212016-24 Report Date/Time: Friday, April 06, 2012 12:30:55
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-24 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 19:12:14 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 238 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-24.082 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 53 4 7.2 0.000107 1.4253 ug/L Se 78 5 5 1 20.9 -0.000001 0.4833 ug/L Se 77 2 2 0 17.3 0.000000 0.4605 ug/L>>>> Rh 103 398528 389477 1853 0.5 389476.671012 ug/L Br 79 3 1739 92 5.3 1736.030326 ug/L Cl 35 278 348 10 2.9 69.169454 ug/L C 13 1493 1708 9 0.5 215.044639 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 97.729 Br 79 Cl 35 C 13
BRL Report 1212016
Page 269 of 274
Page 1 Sample ID: 1212016-25 Report Date/Time: Friday, April 06, 2012 12:30:58
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-25 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 19:13:43 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 239 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-25.083 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 80 8 10.5 0.000177 2.2407 ug/L Se 78 5 5 1 20.2 0.000001 0.6592 ug/L Se 77 2 2 1 24.0 0.000001 1.0158 ug/L>>>> Rh 103 398528 387773 590 0.2 387772.786653 ug/L Br 79 3 1833 39 2.1 1829.385031 ug/L Cl 35 278 384 18 4.6 105.837874 ug/L C 13 1493 1751 14 0.8 258.387721 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 97.301 Br 79 Cl 35 C 13
BRL Report 1212016
Page 270 of 274
Page 1 Sample ID: 1212016-26 Report Date/Time: Friday, April 06, 2012 12:31:00
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1212016-26 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 19:15:11 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 240 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1212016-26.084 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 49 3 5.1 0.000099 1.3390 ug/L Se 78 5 5 1 31.7 -0.000000 0.5351 ug/L Se 77 2 2 1 36.7 0.000001 0.9241 ug/L>>>> Rh 103 398528 386135 7913 2.0 386135.082957 ug/L Br 79 3 1796 83 4.6 1792.709950 ug/L Cl 35 278 365 30 8.3 86.670300 ug/L C 13 1493 1744 45 2.6 251.719618 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 96.890 Br 79 Cl 35 C 13
BRL Report 1212016
Page 271 of 274
Page 1 Sample ID: 1213006-01 Report Date/Time: Friday, April 06, 2012 12:31:03
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1213006-01 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 19:16:40 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 241 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1213006-01.085 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 72 6 8.7 0.000154 1.9783 ug/L Se 78 5 5 1 28.5 0.000001 0.6677 ug/L Se 77 2 2 1 41.7 0.000000 0.6243 ug/L>>>> Rh 103 398528 393798 2575 0.7 393797.844787 ug/L Br 79 3 1778 134 7.5 1774.372835 ug/L Cl 35 278 387 26 6.9 108.338016 ug/L C 13 1493 1747 65 3.7 254.220282 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 98.813 Br 79 Cl 35 C 13
BRL Report 1212016
Page 272 of 274
Page 1 Sample ID: 1213006-02 Report Date/Time: Friday, April 06, 2012 12:31:05
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: 1213006-02 Sample Description: 50x Batch ID: B120537 Sample Date/Time: Thursday, April 05, 2012 19:18:08 Diluted To Volume (mL): 5.00 Aliquot Volume (mL): 0.1 Autosampler Position: 242 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\1213006-02.086 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 53 10 18.0 0.000106 1.4151 ug/L Se 78 5 6 1 11.1 0.000003 0.9255 ug/L Se 77 2 2 1 37.7 0.000000 0.4376 ug/L>>>> Rh 103 398528 394473 1037 0.3 394472.575294 ug/L Br 79 3 1763 46 2.6 1759.368696 ug/L Cl 35 278 383 16 4.3 104.171122 ug/L C 13 1493 1786 83 4.6 293.396056 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 98.982 Br 79 Cl 35 C 13
BRL Report 1212016
Page 273 of 274
Page 1 Sample ID: SEQ-CCV8 Report Date/Time: Friday, April 06, 2012 12:31:08
Quantitative Analysis - Brooks Rand Labs ICP-MS Summary Report
Sample ID: SEQ-CCV8 Sample Description: Batch ID: Sample Date/Time: Thursday, April 05, 2012 19:19:39 Diluted To Volume (mL): Aliquot Volume (mL): Autosampler Position: 6 Sample File: C:\Elandata\Sample\2012\4-12\1200243.sam Method File: C:\Elandata\Method\2012\4-12\1200243-0062-ICPMS2-mel.mth Dataset File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-CCV6.087 Calibration File: C:\Elandata\System\2012\4-12\1200243.cal Blank File: C:\Elandata\DataSet\Data\2012\4-12\1200243\SEQ-ICB1.002
Concentration Results Analyte Mass Blank Int Mean Meas Int Mean Meas Int SD Meas Int RSD Net Int Mean Conc Mean Sample Unit AsO 91 11 9811 52 0.5 0.021163 4.9179 ug/L Se 78 5 977 18 1.8 0.002099 5.3522 ug/L Se 77 2 293 9 3.2 0.000628 5.3252 ug/L>>>> Rh 103 398528 462969 1903 0.4 462968.559868 ug/L Br 79 3 33 9 27.7 29.166738 ug/L Cl 35 278 324 19 5.8 45.835113 ug/L C 13 1493 1934 43 2.2 440.931503 ug/L
Int Std % Recovery Analyte Mass Int Std % Recovery AsO 91 Se 78 Se 77> Rh 103 116.170 Br 79 Cl 35 C 13
BRL Report 1212016
Page 274 of 274