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An investigation and enhancement of
thermal performance in a heat pipe and its
thermal modeling application
Yeu Yee Lee
Faculty of Engineering, Computing and Science (FECS)
Swinburne University of Technology
Sarawak Campus, Malaysia
Submitted for the degree of Doctor of Philosophy
2018
Dedicated to
my parents, siblings,
my beloved husband Alvin,
my delighted sons Finn and Fabian,
and my sweet daughter Francine.
ACKNOWLEDGEMENT
First and foremost, I would like to thank God for giving me the opportunity to undertake
this study and providing me with the strength to complete it with His grace.
In my journey towards this degree, I have found a mentor, a friend, an inspiration, and a
role model. I am deeply grateful to my principal coordinating supervisor, Prof. Alexander
Gorin, for his valuable advice and feedback. His detailed and constructive comments
helped me to improve the thesis in many ways. He was all the time available for fruitful
research discussions. His guidance and encouragement during these years are beneficial
contributions to this study. Finally, I appreciate his total confidence and the responsibility
granted me throughout this period.
I would also like to express my sincere gratitude and deep appreciation to my coordinating
supervisor, Prof. Anatoli Vakhguelt. His broad knowledge and his support throughout
this work have been of great value for me. His understanding, encouraging and personal
guidance have provided a good basis for the present thesis.
In addition, I thank my associate supervisor Adjunct Prof. Ioan Sauciuc for giving me the
opportunity and motivation to undertake this work.
My sincere thanks are due to my colleagues from Swinburne University of Technology
(Sarawak Campus), for their detailed review, constructive criticism and excellent advice
during the preparation of this thesis. Special thanks to Luk Tien Boh and Victor Bong for
helping me in the lab. I also acknowledge our lab officers and technicians for their
cooperation and friendship.
Furthermore, I wish to express my gratitude to Swinburne University of Technology
(Sarawak Campus) for my PhD studentship and the financial support in this research.
Finally, I owe my loving thanks to my family. They have lost a lot due to my research
abroad. Without their encouragement and understanding, it would be impossible for me
to finish this work.
Best Regards, Yeu Yee Lee, 2018
i
ABSTRACT Heat transfer in porous media has become increasingly important since last few decades.
The principles of heat transfer in porous media are widely used in many fields including
engineering and science. As the demand for higher heat transfer efficiency is increasing,
the use of porous media in heat pipe has vastly gained recognition. Heat pipe is the most
commonly used heat transfer device that involves the principles of conduction,
evaporation, and condensation in a porous medium. Thus, evaporation and condensation
heat transfer of porous medium play significant roles in heat pipe’s working principle.
However, there is only a handful of researches for condensation in porous media with the
effects of inertial, near-wall zone and two-phase zone. The experimental investigation of
the above-mentioned effects is complicated and remain challenging even with the
present-day advanced technology.
In this study, experimental and theoretical investigations have been done on the
evaporation and condensation heat transfer in porous media. The findings will help to
improve the performance of a heat pipe as the evaporation and condensation rates can
affect the heat transfer capacity and efficiency of the heat pipe.
Initially, experimental investigations of evaporation from porous media are conducted to
provide a deeper understanding of the mechanism heat transfer in porous media during
phase change process. An experimental setup used to study the fundamental of
evaporation mechanism in porous media is developed. The porous media is modelled by
using various sizes of brass balls, chrome steel balls, ceramic balls and river sand. The
porous media are tested at various temperatures with regards to different structures and
characteristics, such as porosity, particle size, pores size, porous layer thickness, and
particle material. Many positive results are achieved and successfully characterized
throughout this study. The experimental results obtained would enhance the thermal
performance of heat pipe. In addition, a physical model is developed for evaporation heat
transfer in porous media and fits well with experimental data.
Furthermore, the effective thermal conductivity for various porous samples is determined
experimentally. The comparison is made on the experimental results of effective thermal
conductivity and the models available. The effects of porous media parameters on
effective thermal conductivity are also studied.
ii
Next, the physico-mathematical models for film condensation on an inclined plate
embedded in porous media with the effects of inertial and near-wall region are developed.
The models developed are compared to the models and experimental data available. The
effective thermal conductivity, liquid film thickness, and convection heat transfer
coefficient were determined from experimental data available in published resources.
Finally, the theoretical model of liquid film condensation embedded in porous media with
two-phase region effect based on several assumptions was developed. The developed
model was compared to the models and experimental data available. It is found that the
model developed in this study show good agreement with both the model and
experimental results of previous researchers. The model of film condensation on an
inclined plate embedded in a porous medium with two-phase region introduces simple
analytical solutions to complex problems.
The model developed for film condensation on an inclined plate embedded in a porous
medium with two-phase region effect, as well as the modified solutions for film
condensation on an inclined plate embedded in a porous medium with inertial and near-
wall region effects, have formed the main novelty of this study. Overall, this study
contributes towards enhancing the thermal performance of heat pipe. It could lead to the
development of smaller yet efficient heat pipe. It allows control of “dry-outs” in the
evaporation section and “flooding” in the condensation section of heat pipes.
iii
DECLARATION
I declare that this thesis contains no material that has been accepted for the award of any
other degree or diploma and to the best of my knowledge contains no material previously
published or written by another person except where due reference is made in the text of
this thesis.
_________________
Yeu Yee Lee
iv
NOMENCLATURE
𝐴𝐴 Area, m2
𝑎𝑎 Thermal diffusivity, m2/s
𝑐𝑐𝑝𝑝 Specific heat capacity, J/kg.K
𝑐𝑐𝑣𝑣 Specific heat capacity at constant volume, J/kg·K
𝐶𝐶 Constant
𝒞𝒞 Concentration, mol/m3
𝐶𝐶𝑐𝑐 Coefficient of curvature
𝐶𝐶𝑢𝑢 Coefficient of uniformity
𝐸𝐸 Internal energy, J/kg
𝑑𝑑 Diameter, m
𝑑𝑑𝑑𝑑/𝑑𝑑𝑑𝑑 Temperature gradient (K/m)
𝐷𝐷𝐴𝐴𝐴𝐴 Diffusion coefficient of the molecule A in B
𝑔𝑔 Gravitational acceleration, m/s2
𝐺𝐺𝑠𝑠 Specific gravity of solids
𝑄𝑄 Heat energy, J
𝑞𝑞 Heat transfer rate, j/s or W
𝑞𝑞′′ Heat flux, W/m2
�̇�𝑞 Internal heat generation, W/m3
ℎ Mass transfer coefficient, m/s
ℎ𝑓𝑓𝑓𝑓 Latent heat of vaporization, J/kg
𝑗𝑗 Diffusive mass flux, g/m2⋅s
𝚥𝚥 ̅ Diffusive molar flux, mol/m2⋅s
𝑗𝑗𝑠𝑠 Leverett J-function
Nomenclature v
𝐾𝐾 Permeability, m2
𝐿𝐿 Length of plate or representative dimension, m
𝑚𝑚 Mass of substances, kg
�̇�𝑚 Rate of evaporation, kg/s
�̇�𝑚′′ Mass flux, kg/s⋅m2
𝑀𝑀 Molar mass, kg/mol
𝑁𝑁 Mass transfer rate, mol/s
𝑙𝑙 Porous layer thickness, m
𝐿𝐿𝑐𝑐 Characteristic length, m
𝑃𝑃 Pressure, pa or N/m2
𝑟𝑟 Radius, m
𝑟𝑟𝑐𝑐 Equivalent capillary radius, m
𝑅𝑅 Thermal resistance, K/w
𝑠𝑠 Saturation
𝑆𝑆𝑎𝑎 Surface area, m2
𝑑𝑑 Temperature, K
𝑡𝑡 Time, s
𝑈𝑈 𝑑𝑑-component velocity , m/s
𝑉𝑉 𝑦𝑦-component velocity , m/s
𝑣𝑣 Volume, m3
𝓋𝓋 Molecular volumes, m3/mol
𝑦𝑦 Mole fraction
𝛥𝛥𝛥𝛥 Enthalpy change in vaporization, J/kg
∆𝑆𝑆 Change in entropy, J
𝛥𝛥𝑑𝑑 Change in temperature, K
∇ Three-dimensional del operator
vi
Dimensionless Parameters
𝐴𝐴𝑟𝑟 Archimedes Number, 𝑓𝑓𝐿𝐿3
𝜈𝜈2�1 − 𝜌𝜌𝑣𝑣
𝜌𝜌𝑙𝑙� cos𝜑𝜑
𝐴𝐴𝑟𝑟∗ Modified Archimedes Number, 𝑓𝑓𝑔𝑔𝐿𝐿𝜈𝜈𝑙𝑙2 �1 −
𝜌𝜌𝑣𝑣𝜌𝜌𝑙𝑙� cos𝜑𝜑
𝐺𝐺𝑟𝑟 Grashof number, 𝑓𝑓𝐿𝐿3𝛽𝛽∆𝑇𝑇𝜈𝜈2
Ku Kutateladze number, 𝑟𝑟𝑖𝑖
𝑐𝑐𝑝𝑝(𝑇𝑇𝑤𝑤−𝑇𝑇𝑠𝑠𝑠𝑠𝑠𝑠)
𝑁𝑁𝑁𝑁 Nusselt number, 𝛼𝛼𝛼𝛼𝜆𝜆
𝑁𝑁𝑁𝑁���� Average Nusselt number, 𝛼𝛼�𝐿𝐿𝜆𝜆
𝑃𝑃𝑟𝑟 Prandtl number, 𝜈𝜈𝑎𝑎 𝑜𝑜𝑟𝑟𝜌𝜌𝑐𝑐𝑝𝑝𝜈𝜈𝜆𝜆
𝑅𝑅� Dimensionless group, 𝜎𝜎√𝑔𝑔𝐾𝐾𝜇𝜇𝑙𝑙𝑎𝑎𝑒𝑒
𝑅𝑅𝑅𝑅 Reynold’s number, 𝑈𝑈𝐿𝐿𝜈𝜈
𝑆𝑆𝑐𝑐 Schmidt number, 𝜈𝜈
𝐷𝐷𝐴𝐴𝐴𝐴
𝑆𝑆ℎ Sherwood number, ℎ𝑚𝑚𝐿𝐿𝐷𝐷𝐴𝐴𝐴𝐴
Greek symbols
𝛼𝛼 Convection heat transfer coefficient, w/m2·K
𝛽𝛽 Coefficient of expansion of the fluid, K−1
𝜉𝜉 Constant
𝜀𝜀 Porosity
𝐾𝐾 Permeability, m2
𝜌𝜌 Density, kg/m3
𝜆𝜆 Thermal conductivity, W/m·k
𝜎𝜎 Surface tension, N/m
𝛿𝛿 Film thickness, m
Nomenclature vii
𝜇𝜇 Dynamic viscosity, kg/m·s
𝜃𝜃 Contact angle
Subscripts
∞ Ambient
𝑏𝑏 Metal ball
𝐵𝐵 Bulk
𝑐𝑐 Capillary
𝑐𝑐𝑜𝑜𝑐𝑐 Container
cond Conduction
conv Convection
e Effective
evap Evaporation
𝑓𝑓 Fluid
ℎ Heat
𝑙𝑙 Liquid
loss Loss
m Porous Medium
mass Mass
max Maximum
min Minimum
o Overall
p Particle
r Relative
s Solid
sat Saturated
viii
set Set-point
T Total
t Two-phase
𝑣𝑣 Vapour
v Void space
𝑤𝑤 Wall or surface
ix
PUBLICATIONS ARISING FROM THIS
DOCTORAL STUDY
Y.L. Yeu, H. H. J. Tan, A. Gorin, A. Vakhguelt, "Experimental Study of the Rate of
Evaporation from Porous Media of Different Matrices", Defect and Diffusion Forum, Vol.
379, pp. 171-180, 2017
Y.L. Yeu, H. H. J. Tan, A. Gorin, A. Vakhguelt, Experimental Study of the Rate of
Evaporation from Porous Media of Different Matrices, Proc. 13th International
Conference on Diffusion in Solids and Liquids (DSL 2017), Vienna, Austria, 2017.
Y.L. Yeu, A. Vakhguelt, A. Gorin, An Experimental Study of Evaporation in Porous
Media, Proc. World Hybrid Technologies and Energy Conference (World Hybrid 2013),
Kuching, Malaysia, 2013.
Y.L. Yeu, A. Vakhguelt, Fundamental Study of Evaporation Heat Transfer in Porous
Media, Proc. 3rd International Conference of Institution of Engineering and Technology
(IETBIC)”, Brunei Darussalam, pp. 25, 2012.
Y.L. Yeu, A. Vakhguelt, An Experimental Study in the Fundamentals of Evaporation
from Porous Structure, Proc. 10th International Heat Pipe Symposium, Tamsui, New
Taipei City, Taiwan, pp. 54 - 60, 2011.
Vakhguelt A., Bong V., Yeu E., Study of Evaporation Mechanism using Porous Media,
Drying and Evaporation, Proc. 19th Int Cong. Chemical and Process Engineering, Prague,
Czech Republic, 2010.
Y.L. Yeu, N.S. Victor Bong, A. Vakhguelt, Evaporation Mechanism in Porous Medium,
Proc. 4th World Engineering Congress, Kuching, Malaysia, PP. 201-208, 2010.
x
TABLE OF CONTENTS
ACKNOWLEDGEMENT .............................................................................................. i
ABSTRACT .................................................................................................................... i
DECLARATION .......................................................................................................... iii
NOMENCLATURE ...................................................................................................... iv
PUBLICATIONS ARISING FROM THIS DOCTORAL STUDY ............................. ix
TABLE OF CONTENTS ............................................................................................... x
LIST OF FIGURES ...................................................................................................... xv
LIST OF TABLES .................................................................................................. xxviii
1. INTRODUCTION ................................................................................................... 1
1.1 Historical Development of Heat Pipes ................................................................... 2
1.2 Fundamental Working Principles of Heat Pipes .................................................... 4
1.3 Porous Media ......................................................................................................... 6
1.4 Evaporation in Porous Media ................................................................................. 8
1.5 Condensation in Porous Media .............................................................................. 9
1.6 Research Objectives and Contributions ............................................................... 10
1.7 Outline of the Thesis ............................................................................................ 12
2. LITERATURE REVIEW ..................................................................................... 14
2.1 Fundamental Definition in Heat and Mass Transfer ............................................ 14
2.1.1 Conduction Heat Transfer ............................................................................ 14
2.1.2 Convection Heat Transfer............................................................................. 16
2.1.3 Evaporation Heat Transfer ........................................................................... 17
2.1.4 Evaporation Mass Transfer .......................................................................... 20
2.2 Effective Thermal Conductivity ........................................................................... 23
Table of Content xi
2.3 Porous Media in Heat Pipe ................................................................................... 32
2.4 Evaporation Heat Transfer in Porous Media ........................................................ 34
2.5 Investigation on Porous Media and Wick Structure ............................................. 38
2.5.1 Various Wick Structure Characteristics ....................................................... 39
2.5.2 Bi-porous Wick Structure.............................................................................. 41
2.5.3 Microgroove Wick Structures ....................................................................... 41
2.6 Parametric Study of Evaporation Heat Transfer from Porous Media .................. 42
2.6.1 Particle Size .................................................................................................. 43
2.6.2 Pore Size .................................................................................................. 46
2.6.3 Porous/Wick Thickness ............................................................................ 50
2.6.4 Porosity ......................................................................................................... 53
2.7 Boiling in Porous Media ...................................................................................... 55
2.8 Film Condensation ............................................................................................... 61
2.9 Film Condensation in Porous Media .................................................................... 64
2.9.1 Liquid Film ................................................................................................... 69
2.9.2 Inertial Effect ................................................................................................ 73
2.9.3 Near-Wall Region Effect ............................................................................... 78
2.9.4 Two-phase region effect ................................................................................ 80
2.10 Summary ............................................................................................................ 88
3. METHODOLOGY OF EXPERIMENTAL STUDIES ...................................... 90
3.1 Experimental Setup for the Study of Evaporation from Porous Media ............... 90
3.2 Experimental Setup for the Effective Thermal Conductivity Investigation ....... 101
3.3 Experimental Working Procedure for Investigation of Effective Thermal
Conductivity ............................................................................................................... 105
3.4 Experimental Procedure for the Study of Evaporation from Porous Media ...... 107
3.5 Materials used to create porous structures ......................................................... 111
xii
3.6 Instrumentation and software used for data acquisition ..................................... 113
3.6.1 Heater Control Sub-system ......................................................................... 115
3.6.2 Water Temperature Logging sub-system .................................................... 116
3.6.3 Mass Logging Sub-system........................................................................... 117
3.6.4 Ambient Temperature and Humidity Logging Sub-System ......................... 119
4. RESULTS OF EFFECTIVE THERMAL CONDUCTIVITY ........................ 120
4.1 Results of Effective Thermal Conductivity ........................................................ 120
4.2 The effect of different nature/type of solid particles on effective thermal
conductivity ................................................................................................................ 132
4.3 Effect of particle size on effective thermal conductivity ................................... 133
5. EVAPORATION FROM POROUS MEDIA: EXPERIMENTAL RESULTS
AND PHYSICAL MODELS ...................................................................................... 135
5.1 Preliminary Experimental Results and Performance Analysis of the Experimental
Setup ........................................................................................................................... 135
5.1.1 Water Temperature ..................................................................................... 137
5.1.2 Ambient conditions ..................................................................................... 141
5.1.3 Porous structure ......................................................................................... 142
5.1.4 Summary ..................................................................................................... 146
5.2 Experimental Results for the Study of Evaporation from Porous Media ........... 147
5.3 Temporal Temperature Distribution of the Water Temperature ........................ 148
5.4 Temperature History across the Porous Samples ............................................... 157
5.5 Ambient Temperature Profile and Ambient Relative Humidity ........................ 164
5.6 Evaporation Rates from Porous Media .............................................................. 167
5.7 Water Level Change During Evaporation in Porous Media .............................. 180
5.8 Effect of Particle Size on Rate of Evaporation .................................................. 181
5.9 Effect of Porosity on Rate of Evaporation ......................................................... 193
5.10 Physical Model of Evaporation from Porous Media ........................................ 197
Table of Content xiii
6. FILM CONDENSATION ON AN INCLINED PLATE EMBEDDED IN A
POROUS MEDIUM ................................................................................................... 203
6.1 Classical solution of film condensation on an inclined plate embedded in a
porous medium ........................................................................................................... 204
6.1.1 Temperature distribution along the porous layer ....................................... 208
6.1.2 Determination of liquid film thickness ........................................................ 210
6.1.3 Determination of the effective thermal conductivity ................................... 217
6.2 Modified solution for film condensation on an inclined plate embedded in a
porous medium with inertial effects ........................................................................... 220
6.3 Modified solution for film condensation on an inclined plate embedded in a
porous medium with inertial effects and the near-wall region effects ....................... 222
6.4 Thin Film Condensation in Porous Media ......................................................... 228
6.4.1 Comparison of experimental data to predicted values ............................... 231
7. TWO-PHASE REGION EFFECT ON FILM CONDENSATION ON AN
INCLINED PLATE EMBEDDED IN A POROUS MEDIUM ............................... 233
7.1 Mathematical Formulation for film condensation on an inclined plate embedded in
a porous medium with two phase region effect .......................................................... 234
7.2 Comparison to models developed by other researchers. ...................................... 248
7.3 Comparison of experimental data to other models ............................................... 251
8. CONCLUSIONS AND RECOMMENDATIONS ............................................ 258
8.1 Conclusions ........................................................................................................ 258
8.2 Recommendations of Future Studies .................................................................. 260
REFERENCES ........................................................................................................... 262
APPENDICES ......................................................................................................... xxxiii
A. Detailed summary table of results obtained from the Evaporation heat transfer
in porous medium................................................................................................. xxxiv
B. Data of water temperatures obtained from LabVIEW Signal Express software
lii
xiv
C. Data of water mass changes obtained from RS key software .....................xcvi
D. Specification of Dvorovenko’s (1997) Test Samples ................................... cxx
E. Summary Table of Calculated Results for Film Condensation Heat Transfer of
Freon-12 on Inclined Plate Embedded in the Porous Medium .......................... cxxiv
F. Matlab Code ................................................................................................. clviii
G. Thermophysical Properties of Saturated Freon-12 (CCL2F2) .................. clxiv
xv
LIST OF FIGURES Figure 1.1 Schematic diagram of a conventional heat pipe ............................................. 5
Figure 1.2 The variation of the matrices of porous medium with (a) no sphere particles;
(b) large sphere particles; and (c) small sphere particles .................................................. 7
Figure 2.1 One-dimensional heat transfer by conduction (diffusion of energy) ............ 15
Figure 2.2 Model development pathways for molecular diffusion problems (Welty et al.,
2014) ............................................................................................................................... 22
Figure 2.3 A porous medium that comprise of series composite wall ........................... 24
Figure 2.4 A porous medium that comprises the parallel composite wall ..................... 24
Figure 2.5 Comparison between proposed model and data for porous media filled with
water (Florez et al., 2013) ............................................................................................... 26
Figure 2.6 Effective thermal conductivity vs. porosity for experimental data and values
calculated through literature models for porous media saturated with water (Florez et al.,
2013) ............................................................................................................................... 26
Figure 2.7 Comparison of effective thermal conductivity predicted by various analyses
of the experimental data of Nozad et al. (1985) (Kaviany, 2012)................................... 30
Figure 2.8 Comparison of the permeability and the capillary pumping for different wick
structure (Sauciuc et al., 2000) ........................................................................................ 40
Figure 2.9 Mean temperature of the heating block vs. imposed heat flux at ∆𝛥𝛥 =
4.0mm. (Cao et al., 2002) ............................................................................................... 48
Figure 2.10 Heat transfer coefficient vs. imposed heat flux at ∆𝛥𝛥 = 4.0mm. (Cao et al.,
2002) ............................................................................................................................... 48
Figure 2.11 Heat transfer coefficient with vaa rying heat flux of different mesh size and
pool boiling (Li and Peterson, 2006b) ............................................................................ 49
Figure 2.12 Wick thickness effect on the evaporating heat transfer coefficients (rb =
0.635mm; 𝜀𝜀 = 43%; LH = 0.01m; working fluid = water)(Hanlon and Ma, 2003) ........ 51
xvi
Figure 2.13 Effect of wick thickness on (a) the vapour temperature (Tv), (b), (c) and (d)
the pressure drop for OD=12.7mm, OD=20mm and OD=30mm respectively for
difference evaporator lengths. (Di Marco et al., 2014) ................................................... 52
Figure 2.14 Steady-state maximum temperature rise of the heat pipe temperature with
porosity for different wick structures (Hassan and Harmand, 2015). ............................. 54
Figure 2.15 Maximum heat pipe pressure difference at steady state with porosity for
different wick structures (Hassan and Harmand, 2015). ................................................. 54
Figure 2.16 Heat transfer from capillary wicking structure surfaces (Faghri, 1995) ..... 55
Figure 2.17 Heat transfer from a submerged wick (Faghri and Zhang, 2006) ............... 56
Figure 2.18 Coordinates and nomenclature for a thin vapour layer adjacent to a heated
vertical surface in a permeable medium. (Parmentier, 1979) ......................................... 57
Figure 2.19 Schematic diagram of a water-saturated porous bed with the two-phase zone
(Bau and Torrance, 1982a).............................................................................................. 59
Figure 2.20 Film boiling in porous media on a vertical wall (Cheng and Verma, 1981,
Faghri and Zhang, 2006) ................................................................................................. 61
Figure 2.21 Condensation formed on the surface. Dropwise condensation (left) and
Film condensation (Right). ............................................................................................. 62
Figure 2.22 Condensation curves for steam. (Tanasawa, 1991, Amanifard et al., 2007)
......................................................................................................................................... 62
Figure 2.23 Coordinate systems for film condensation along a wedge (n = 0) and a cone
(n = 1) (Cheng, 1981) ...................................................................................................... 66
Figure 2.24 Variation of the Nusselt number with the Jacob number for θ = 30 ° and ω
= 0.2 and various values of the anisotropic permeability ratio (Sanya et al., 2014) ...... 70
Figure 2.25 Effect of the derivation from the Darcy flow regime (Nakoryakov and
Gorin 1994) ..................................................................................................................... 77
Figure 2.26 Heat transfer with consideration for the inertial effects (Nakoryakov and
Gorin 1994) ..................................................................................................................... 78
Figure 2.27 Film condensation embedded in porous media for gravity-capillary
dominated (𝐵𝐵𝑜𝑜 ≃ 1) and capillary dominated(𝐵𝐵𝑜𝑜 < 1) flows ...................................... 81
List of Figures xvii
Figure 3.1 Schematic diagram of the experimental set up for the study of evaporation
from porous media .......................................................................................................... 91
Figure 3.2 Photo of actual experimental set up for the study of evaporation from porous
media ............................................................................................................................... 92
Figure 3.3 Cast Aluminium Heater with an integrated K-type thermocouple ............... 95
Figure 3.4 Uneven heat distribution on the top surface of the aluminium container
(Left) and an improved heat distribution with the use of a sand bath (Right) was
observed through the thermal imaging device. ............................................................... 96
Figure 3.5 Even heat distribution on the surface of the (Left) heater and (Right)
aluminium container was achieved using the aluminium thick block. ........................... 97
Figure 3.6 Heat sink compound to reduce contact resistance between two surfaces. (a)
RS Heat Sink Compound and (b) Wakefield Thermal Compound. ................................ 98
Figure 3.7 Fairly even heat distribution observed in the aluminium container ............. 98
Figure 3.8 Superwool 607 paper thermal insulation sheet ............................................. 99
Figure 3.9 Temperature control system with temperature controller, solid state relay
(SSR) and pulse width modulation (PWM). ................................................................. 100
Figure 3.10 (a) Temperature-Humidity Sensors chip and (b) Temperature-Humidity
logging system .............................................................................................................. 101
Figure 3.11 Thermal network of heat transfer in porous medium ............................... 102
Figure 3.12 Equipment used to determine the thermal conductivity of the materials 103
Figure 3.13 Schematic diagram of Armfield linear heat conduction accessory (model:
HT 11). .......................................................................................................................... 104
Figure 3.14 Decagon KD2 Pro Thermal Properties Analyser...................................... 104
Figure 3.15 Points of temperature distribution in composite solids............................. 106
Figure 3.16 Heat transfer through composite wall (test section) ................................. 107
Figure 3.17 Thermocouples position............................................................................. 109
Figure 3.18 View of surface area change as the water level drops .............................. 110
Figure 3.19 Various sizes of Brass balls used in the experiment ................................. 112
xviii
Figure 3.20 Overview of the data acquisition and control system ............................... 113
Figure 3.21 Block diagram of heater control sub-system ............................................ 115
Figure 3.22 Pulse-width modulation driver ................................................................. 116
Figure 3.23 Block diagram of the water temperature logging sub-system .................. 116
Figure 3.24 NI 9211 Thermocouple input module with NI USB 9162 Hi-Speed USB
Carrier ........................................................................................................................... 117
Figure 3.25 Block diagram of the mass logging sub-system ....................................... 117
Figure 3.26 A&D GF-10K Electronic balance ............................................................ 118
Figure 3.27 WinCT Data Communication RsKey software interface ......................... 118
Figure 3.28 Block diagram of the ambient temperature and humidity logging sub-
system............................................................................................................................ 119
Figure 4.1 Physical contact points between brass balls and heated surface ................. 122
Figure 4.2 Temperature distribution along the simple plane wall of uniform material
(Brass) and constant cross sectional area (0.00049m2). ................................................ 126
Figure 4.3 Temperature distribution along the composite wall of Brass – Ceramic –
Brass .............................................................................................................................. 126
Figure 4.4 Temperature distribution along the composite wall of Brass – Dry River
Sand (0.6-1.2mm) – Brass ........................................................................................... 127
Figure 4.5 Temperature distribution along the Composite Wall of Brass – Dry River
Sand (1.2-2.4mm) – Brass ........................................................................................... 127
Figure 4.6 Temperature distribution along the composite call of Brass – Dry River
Sand (2.4-4.8mm) – Brass ........................................................................................... 128
Figure 4.7 Temperature distribution along the composite call of Brass – Brass 2mm
balls (Randomly packed) – Brass ............................................................................... 128
Figure 4.8 Temperature distribution along the composite wall of Brass – Brass 3mm
balls (Randomly packed) – Brass ............................................................................... 129
Figure 4.9 Temperature distribution along the composite wall of Brass – Brass 4mm
balls (Randomly packed) – Brass ............................................................................... 129
List of Figures xix
Figure 4.10 Temperature distribution along the composite wall of Brass – Brass 5mm
balls (Randomly packed) – Brass ............................................................................... 130
Figure 4.11 Temperature distribution along the composite wall of Brass – Brass
2,3,4,5mm balls (Randomly packed) – Brass ............................................................ 130
Figure 4.12 Comparison between literature models and experimental data for a porous
structure made up of Brass Ball 2mm. .......................................................................... 131
Figure 4.13 Comparison of thermal conductivity for Brass Balls samples.................. 134
Figure 5.1 Transient temperature response of the water temperature(Yeu and Vakhguelt,
2011) ............................................................................................................................. 138
Figure 5.2 Thermal resistance for initial experiment setup (Yeu and Vakhguelt, 2011)
....................................................................................................................................... 139
Figure 5.3 The balls arrangement for Mix all sample during the preliminary test ...... 141
Figure 5.4 The relation between evaporation rate and relative humidity (Yeu and
Vakhguelt, 2011) ........................................................................................................... 141
Figure 5.5 The relations between evaporation rate and room temperature (Yeu and
Vakhguelt, 2011). .......................................................................................................... 142
Figure 5.6 The relations between porosity and evaporation rate at different heater
temperatures for Loose Random Packing Test Samples. .............................................. 144
Figure 5.7 Graph of evaporation rate for simple cubic samples with ball size of 20mm,
heater temperature of 60°C and porous layer thickness of 40mm (Yeu et al., 2010). .. 144
Figure 5.8 The evaporated water mass for the first hour at steady state. (single sizes
samples with loose random packing)(Yeu and Vakhguelt, 2011). ............................... 145
Figure 5.9 The evaporated water mass for the first hour at steady state. (mix sizes
samples with loose random packing)(Yeu and Vakhguelt, 2011). ............................... 145
Figure 5.10 Chrome steel balls rusted during the heating process ............................... 146
Figure 5.11 Temporal temperature distribution of the water temperature at a different
position for all test samples ........................................................................................... 149
xx
Figure 5.12 Temporal temperature distribution of the water temperature at different
position for River sand (with a grain size of 0.6 – 1.2mm, 1.2 – 2.4mm, and 2.4 –
4.8mm) and Ceramic Carbon Balls samples ................................................................. 149
Figure 5.13 Temporal temperature distribution of the water temperature at a different
position for Non-porous sample sets ............................................................................. 150
Figure 5.14 Temporal temperature distribution of the water temperature at a different
position for Brass2rp1 sample sets (2mm Brass Balls with random packing and porous
thickness of 1.9cm) ....................................................................................................... 150
Figure 5.15 Temporal temperature distribution of the water temperature at a different
position for Brass4hcp1 sample sets (4mm Brass Balls with hexagonal closed packing
and porous thickness of 1.95cm) ................................................................................... 151
Figure 5.16 Temporal temperature distribution of the water temperature at a different
position for Brass5sc1 sample sets (5mm Brass Balls with simple cubic packing and
porous thickness of 1.9cm) ........................................................................................... 151
Figure 5.17 Temporal temperature distribution of the water temperature at a different
position for Brass4rp2 sample sets (4mm Brass Balls with random packing and porous
thickness of 2.93cm) ..................................................................................................... 152
Figure 5.18 Temporal temperature distribution of the water temperature at a different
position for Brassmrp2 sample sets (2,3,4,5 mm Brass Balls with random packing and
porous thickness of 2.9cm) ........................................................................................... 152
Figure 5.19 Temporal temperature distribution of the water temperature at a different
position for Brassmrp3 sample sets (2,3,4,5 mm Brass Balls with random packing and
porous thickness of 3.1cm) ........................................................................................... 153
Figure 5.20 Temporal temperature distribution of the water temperature at a different
position for Brass23rp sample sets (2,3 mm Brass Balls with random packing and
porous thickness of 3.1cm) ........................................................................................... 153
Figure 5.21 Temporal temperature distribution of the water temperature at a different
position for RS1 sample sets (River sand with a grain size of 0.6 – 1.2mm) ............... 154
Figure 5.22 Temporal temperature distribution of the water temperature at a different
position for RS2 sample sets (River sand with a grain size of 1.2 – 2.4mm) ............... 155
List of Figures xxi
Figure 5.23 Temporal temperature distribution of the water temperature at a different
position for RS4 sample sets (River sand with a grain size of 2.4 – 4.8mm) ............... 155
Figure 5.24 Temporal temperature distribution of the water temperature at a different
position for CCB porous sample sets (8mm ceramic carbon balls packed randomly) . 156
Figure 5.25 Temporal temperature distribution of the water temperature at a different
position for HCP porous sample sets (5mm brass balls with Hexagonal Closed packing)
....................................................................................................................................... 156
Figure 5.26 Temporal temperature distribution of the water temperature at a different
position for BCC porous sample sets (5mm brass balls with Body Cubic Cantered
packing) ......................................................................................................................... 157
Figure 5.27 Temporal temperature distribution of the water temperature at a different
position for Random porous sample sets (5mm brass balls with Random packing). ... 157
Figure 5.28 Temperature History across the Plain Media (Water only) Sample ......... 159
Figure 5.29 Temperature History across the Porous Sample of Brass2rp1 ................. 159
Figure 5.30 Temperature History across the Porous Sample of Brass4hcp1 ............... 159
Figure 5.31 Temperature History across the Porous Sample of Brass5sc1 ................. 160
Figure 5.32 Temperature History across the Porous Sample of Brass4rp2 ................. 160
Figure 5.33 Temperature History across the Porous Sample of Brassmrp2 ................ 160
Figure 5.34 Temperature History across the Porous Sample of Brassmrp3 ................ 161
Figure 5.35 Temperature History across the Porous Sample of Brass23rp ................. 161
Figure 5.36 Temperature History across the Porous Sample of RS1 ........................... 161
Figure 5.37 Temperature History across the Porous Sample of RS2 ........................... 162
Figure 5.38 Temperature History across the Porous Sample of RS4 ........................... 162
Figure 5.39 Temperature History across the Porous Sample of CCB.......................... 162
Figure 5.40 Temperature History across the Porous Sample of Brass5Hcp ................ 163
Figure 5.41 Temperature History across the Porous Sample of Brass5Bcc ................ 163
Figure 5.42 Temperature History across the Porous Sample of Brass5Rp .................. 163
xxii
Figure 5.43 Comparison of Steady-State Temperature Distribution for all test samples
....................................................................................................................................... 164
Figure 5.44 Ambient temperature and relative humidity for porous sample of Brass2rp1
....................................................................................................................................... 165
Figure 5.45 Ambient temperature and relative humidity for porous sample of
Brass4hcp1 .................................................................................................................... 165
Figure 5.46 Ambient temperature and relative humidity for porous sample of Brass5sc1
....................................................................................................................................... 166
Figure 5.47 Ambient temperature and relative humidity for porous sample of Brass4rp1
....................................................................................................................................... 166
Figure 5.48 Ambient temperature and relative humidity for porous sample of
Brassmrp2 ..................................................................................................................... 166
Figure 5.49 Comparison of Evaporation Rates for non-porous sample and various
porous samples every 10 minutes interval .................................................................... 167
Figure 5.50 Comparison of Evaporation Rates for Brass4hcp1 sample and Brass4rp2
sample every 10 minutes interval .................................................................................. 168
Figure 5.51 the changes of surface area with respect to the porous height. .................. 169
Figure 5.52 Liquid receding during evaporation ......................................................... 170
Figure 5.53 Comparison of Evaporated Water Mass ................................................... 171
Figure 5.54 Evaporated Water Mass for Non-porous samples .................................... 173
Figure 5.55 Evaporated Water Mass for Brass2rp1 samples ....................................... 173
Figure 5.56 Evaporated Water Mass for Brass4hcp1 samples ..................................... 174
Figure 5.57 Evaporated Water Mass for Brass5sc1 samples ....................................... 174
Figure 5.58 Evaporated Water Mass for Brass4rp2 samples ....................................... 175
Figure 5.59 Evaporated Water Mass for Brassmrp2 samples ...................................... 175
Figure 5.60 Evaporated Water Mass for Brassmrp3 samples ...................................... 176
Figure 5.61 Evaporated Water Mass for Brass23rp samples ....................................... 176
Figure 5.62 Evaporated Water Mass for RS1 samples ................................................ 176
List of Figures xxiii
Figure 5.63 Evaporated Water Mass for RS2 samples ................................................ 177
Figure 5.64 Evaporated Water Mass for RS4 samples ................................................ 177
Figure 5.65 Evaporated Water Mass for CCB samples ............................................... 177
Figure 5.66 Observed Liquid Water Evaporation Rate for all test samples................. 178
Figure 5.67 Water Level Changes during Evaporation ................................................ 180
Figure 5.68 Observed Liquid Water Evaporation Rate for Non-porous and Brass Balls
Porous Samples ............................................................................................................. 181
Figure 5.69 Mass changes of sample Brass2rp1 for the first hour after achieving steady
state ............................................................................................................................... 183
Figure 5.70 Mass changes of sample Brass4hcp1 for the first hour after achieving
steady state .................................................................................................................... 183
Figure 5.71 Mass changes of sample Brass5sc1 for the first hour after achieving steady
state ............................................................................................................................... 184
Figure 5.72 Water mass changes of sample Brass4rp2 for the first hour after achieving
steady state .................................................................................................................... 184
Figure 5.73 Mass changes of sample Brassmrp2 for the first hour after achieving steady
state ............................................................................................................................... 185
Figure 5.74 Mass changes of sample Brassmrp3 for the first hour after achieving steady
state ............................................................................................................................... 185
Figure 5.75 Mass changes of sample Brass23rp for the first hour after achieving steady
state ............................................................................................................................... 186
Figure 5.76 Water mass changes of sample Non-porous for the first hour after
achieving steady state .................................................................................................... 186
Figure 5.77 Effect of Particle Size for Brass Balls samples on Rate of Evaporation .. 187
Figure 5.78 Observed Liquid Water Evaporation Rate for River Sand and Ceramic
Carbon Balls Porous Samples ....................................................................................... 188
Figure 5.79 Water mass changes of sample RS1 for the first hour after achieving steady
state ............................................................................................................................... 188
xxiv
Figure 5.80 Water mass changes of sample RS2 for the first hour after achieving steady
state ............................................................................................................................... 189
Figure 5.81 Water mass changes of sample RS3 for the first hour after achieving steady
state ............................................................................................................................... 189
Figure 5.82 Effect of Particle Size for River Sand samples on Rate of Evaporation .. 190
Figure 5.83 Effect of Particle Size for River Sand samples on amount of water
evaporated in 60minutes & 120 minutes. ...................................................................... 191
Figure 5.84 Evaporated mass changes for porous samples used to test the effect of
particle size on the rate of evaporation ......................................................................... 192
Figure 5.85 Effect of porosity on the rate of evaporation for brass balls samples ....... 194
Figure 5.86 Effect of porosity on water temperature at liquid-vapor interface for brass
balls samples ................................................................................................................. 194
Figure 5.87 Effect of porosity on rate of evaporation for river sand samples ............. 196
Figure 5.88 Effect of porosity on water temperature at liquid-vapour interface for river
sand samples ................................................................................................................. 196
Figure 5.89 overview of heat pipe construction and its working principle.................. 197
Figure 5.90 Leverett J-Function versus water saturation. ............................................ 199
Figure 5.91 Comparison between experimental results with the developed models for
various brass balls sample at Tw=80°C and saturation, s ≈ 0.98. ................................ 201
Figure 5.92 Comparison between experimental results with the developed models for
various sizes of randomly packed brass balls sample at Tw=100°C and saturation, s ≈
0.96. ............................................................................................................................... 202
Figure 6.1. Schematic diagram of film condensation on an inclined plate embedded in a
porous medium. ............................................................................................................. 205
Figure 6.2 Comparison of the experimental data of Dvorovenko (1997) with the
theoretical model of Nakoryakov and Gorin (1994) for film condensation on an inclined
plate embedded in a porous medium............................................................................. 208
List of Figures xxv
Figure 6.3 Temperature profile of condensation film in a porous medium with a grain
diameter of d=1.1mm and grain porosity of ε=0.38 with plate length of (a) L=250mm,
(b) L=500mm, (c) L=750mm and (d) L=1000mm (Dvorovenko, 1997) ...................... 209
Figure 6.4 Temperature profile of condensation film in a porous medium with a grain
diameter of d=0.8mm and grain porosity of ε=0.38 with plate length of (a) L=250mm,
(b) L=500mm, (c) L=750mm and (d) L=1000mm (Dvorovenko, 1997) ...................... 210
Figure 6.5 Determination of liquid film thickness from the E-3f (d=1.1mm, L=750mm,
cos φ=0.01784) temperature profile graph .................................................................... 211
Figure 6.6 Determination of liquid film thickness from the E-4b (d=1.1mm, L=500mm,
cos φ = 0.45008) temperature profile graph .................................................................. 212
Figure 6.7 Relations between the liquid film thicknesses with the Rayleigh number. 215
Figure 6.8 Relations between the liquid film thicknesses with the Rayleigh number and
G-parameter................................................................................................................... 217
Figure 6.9 Correlation between effective thermal conductivity and Rayleigh Number
....................................................................................................................................... 219
Figure 6.10 Correlation between effective thermal conductivity and Rayleigh Number
for film condensation on a inclined plate with an inclination angle of 𝑐𝑐𝑜𝑜𝑠𝑠𝜑𝜑 = 0.2 ..... 219
Figure 6.11 Comparison of experimental results (Dvorovenko, 1997) with the
theoretical model for film condensation on an inclined plate embedded in a porous
medium with inertial effects.......................................................................................... 222
Figure 6.12 Film condensation in porous media with near-wall region effects ........... 223
Figure 6.13 Film condensation heat transfer of Freon-12 on inclined plate embedded in
the grain layer with near-wall region effects for samples E-4 (d=1.1mm, ε=0.38, and
L=1000mm) .................................................................................................................. 224
Figure 6.14 Film condensation heat transfer of Freon-12 on inclined plate embedded in
the grain layer with near wall region effects for samples E-4 (d=1.1mm, L=1000mm,
ε=0.38). ......................................................................................................................... 225
Figure 6.15 Comparison of experimental results with the theoretical model for film
condensation on an inclined plate embedded in a porous medium with inertial effects
....................................................................................................................................... 228
xxvi
Figure 6.16 Thin condensate film forms on the surface .............................................. 229
Figure 6.17 Void fraction distribution (Johnson and Kapner, 1990) ........................... 229
Figure 6.18 Comparison of experimental data to predicted values for thin film
condensation on an inclined plate embedded in porous media with grain size of 3.2mm.
....................................................................................................................................... 232
Figure 7.1 Schematic diagram of film condensation on an inclined plate embedded in a
porous medium that has two-phase region. ................................................................... 234
Figure 7.2 Leverett J-Function varies with water saturation. ...................................... 237
Figure 7.3 Relative permeability of liquid phase and vapour phase. ........................... 238
Figure 7.4 Nusselt number as function of 𝐴𝐴𝑟𝑟 ∗ 𝑃𝑃𝑟𝑟𝐾𝐾𝑁𝑁 for porosity 𝜀𝜀 = 0.38, permeability
K = 0.0005075 mm2, γ = 0.025 and 𝜉𝜉= 1. ..................................................................... 245
Figure 7.5 The effect of Kutateladze number, 𝐾𝐾𝑁𝑁. ...................................................... 246
Figure 7.6 The condensation heat transfer results for porosity 𝜀𝜀 = 0.38, permeability K
= 0.0005075 mm2, γ = 0.025 and 𝜉𝜉 = 1. ........................................................................ 246
Figure 7.7 Dimensionless heat transfer coefficient with surface tension effect for
porosity 𝜀𝜀 = 0.38, permeability K = 0.0005075 mm2,𝛾𝛾 = 0.025 and 𝜉𝜉 = 1 ................. 247
Figure 7.8 The effect of 𝛾𝛾 for porosity 𝜀𝜀 = 0.38, permeability K = 0.0005075 mm2,
L = 250mm, 𝐵𝐵𝑜𝑜 = 0.1 and 𝜉𝜉 = 1. ................................................................................. 248
Figure 7.9 Film condensation embedded in porous media with glass beads size of
900𝜇𝜇m. .......................................................................................................................... 250
Figure 7.10 Comparison of the predicted model developed by Majumdar and Tien
(1990), Plumb (1984) to the present model (with 𝜉𝜉 = 1) and experimental data with no
two-phase region effect (𝐵𝐵𝑜𝑜 ≫ 1) for film condensation on an inclined plate with a
length of 500mm embedded in porous media with a grain size of 800μm. .................. 252
Figure 7.11 Comparison of experimental results with the theoretical model for film
condensation on an inclined plate embedded in porous media with a grain size of 800μm
and plate length of 250mm............................................................................................ 253
List of Figures xxvii
Figure 7.12 Temperature profile of condensation film in a porous medium with a grain
diameter of d=800μm and grain porosity of ε=0.38 on an inclined plane with an angle of
cos φ=0.10343 and plate length of L=250mm (Dvorovenko, 1997). ........................... 254
Figure 7.13 Comparison of temperature difference between wall temperature and
saturation temperature with different heat flux for various samples of film condensation
on an inclined plate with angle cos φ=0.10343 embedded in porous media with grain
size of 800μm and plate length of 250mm, 500mm, 750mm and 1000mm. ................ 255
Figure 7.14 Comparison of liquid film thickness for various samples of film
condensation on an inclined plate with angle cos φ=0.10343 embedded in porous media
with grain size of 800μm and plate length of 250mm, 500mm, 750mm and 1000mm.
....................................................................................................................................... 255
Figure 7.15 Comparison of experimental data to numerical values for film condensation
on an inclined plate with inclination angle of 𝑐𝑐𝑜𝑜𝑠𝑠𝜑𝜑 = 0.10343 and length of 250mm
embedded in porous media with grain size of 800𝜇𝜇m. ................................................. 256
Figure 7.16 Film condensation on an inclined plate with inclination angle of 𝑐𝑐𝑜𝑜𝑠𝑠𝜑𝜑 =
0.10343 and length of 250mm embedded in porous media with grain size of 800𝜇𝜇m.
....................................................................................................................................... 257
xxviii
LIST OF TABLES Table 2.1 Existing mass transfer-based evaporation equations use (Singh and Xu, 1997)
......................................................................................................................................... 18
Table 2.2 Models and correlations for the effective thermal conductivity of the
composed material (Hahne et al., 1991, Bird et al., 2007, Pietrak and Wisniewski, 2015)
......................................................................................................................................... 27
Table 2.3 Experimental results of 𝜆𝜆𝑅𝑅 of various dry sands with different densities 𝜌𝜌 and
porosities 𝜀𝜀 at 20℃. (Hahne et al., 1991) ....................................................................... 31
Table 2.4 Maximum porosity for different packing arrangements ................................ 37
Table 2.5 Comparison of Permeability analysed by using Carman-Kozeny equation and
Ergun equation. ............................................................................................................... 38
Table 2.6 Porous sample developed by Mwaba et al. (2006) ........................................ 47
Table 2.7 Porous example developed by Cao et al. ( 2002)........................................... 47
Table 2.8 Typical values of Bo and 𝑅𝑅 for various fluids and porous media (Majumdar
and Tien, 1990, Vargaftik, 1975) .................................................................................... 84
Table 2.9 Relative permeability suggested by various researchers. (Chung et al., 1992,
Gudjonsdottir et al., 2015, Pruess et al., 1999) ............................................................... 86
Table 3.1 List of Materials, Apparatus, and Equipment ................................................. 92
Table 3.2 HT11 Insulated Composite Wall Specification ........................................... 105
Table 3.3 Distance of thermocouples relative to T1 ..................................................... 105
Table 3.4 Various packing types for porous structure ................................................. 108
Table 3.5 Specification of Test Samples ...................................................................... 109
Table 3.6 Thermophysical Properties of Selected Materials ....................................... 112
Table 3.7 Instrumentation and software used for data acquisition .............................. 114
Table 4.1. Experimental measurements for heat conduction in the composite solids of
Brass – test samples – Brass. ....................................................................................... 123
List of Tables xxix
Table 4.2 Comparison of measurement between Armfield HT11 and Decagon KD2 Pro
for effective thermal conductivity ................................................................................. 131
Table 4.3 Experimental Results of River Sand ............................................................. 132
Table 5.1 Specification of Simple Cubic Packing Test Samples for Preliminary Test. 136
Table 5.2 Specification of Loose Random Packing Test Samples for Preliminary Test
....................................................................................................................................... 137
Table 5.3 The void fraction and packing density value for various random packed
structure (Dullien and Brenner 2012) ........................................................................... 143
Table 5.4 A comparison between the experimental porosity and theoretical porosity for
all three matrix arrangements ........................................................................................ 148
Table 5.5 Mass fraction of liquid water in brass balls porous samples........................ 179
Table 5.6 Mass fraction of remaining water in 2 river sand and ceramic carbon balls
porous samples .............................................................................................................. 179
Table 5.7 Summary of the average evaporation rates for brass balls samples after steady
state ............................................................................................................................... 187
Table 5.8 Summary of the steady state for River sands mass versus time .................. 190
Table 5.9 The rate of evaporation for various particle size samples ............................ 193
Table 6.1 Determination of liquid film thickness from the E-3f (d=1.1mm, L=750mm,
cos φ=0.01784) samples ................................................................................................ 211
1
1. INTRODUCTION New technology of electronic component using innovative materials is getting smaller,
faster and more energy efficient. As a result, the heat generated in electronic devices and
systems is critically high. Heat is an inevitable by-product of every electronic component.
It is usually unfavourable to the performance and reliability of an electric component. The
reduced size high-performance electric components lead to higher heat generation density,
therefore causing the component temperature to increase, resulting in the shortened
lifetime, and higher probabilities of malfunction and failure. Therefore, thermal
management should be taken seriously.
One of the examples is modern microprocessor core. It is found on general-purpose
computing platform and accelerated graphic cards which produce a high amount of heat
during its operation. This heat must be dissipated to keep these components within the
required safe operating temperature. Intel co-founder Gordon Moore (1965) stated that
“the number of transistors on a chip will double about every two years”. This law has
become known as Moore’s law (Moore, 1965). Today, microprocessor technology
continues to evolve, microprocessor with 4.3 billion transistors is launched by Intel in the
first quarter of the year 2014. The International Business Machines Corporation (IBM)
launched its neuromorphic TrueNorth chip with 5.4 billion transistors dated 7 August
2014 (Modha). Three years later, IBM researchers introduced the world's first 5-
nanometre chip with 30 billion transistors packed in it (Nield, 2017). Intel not to lag
behind, surprised the market with new technology named Intel’s hyper-scaling process.
With this new technology, Intel can fit 100 million transistors per square millimetre of
chip “for the first time in our industry’s history,” said Kaizad Mistry, a vice president and
co-director of logic technology at the company (Courtland, 2017). On the other side,
Advanced Micro Devices, Inc. (AMD) claimed that they are preparing to launch a new
AMD 32-core 64-thread CPU end of the year 2018 (Hruska, 2018).
Furthermore, the clock speed of processors are measured in Gigahertz and not in
Megahertz anymore, lead to a heat dissipation approaching 100 W (Tadayon, 2000). The
higher the amount of transistor, the smaller the transistor size and higher the clock speed,
this causes the heat flux to be critically high. Therefore, cooling of the microprocessor is
to be taken seriously. NEC Corporation developed a silent liquid cooling system for use
2 Chapter 1. Introduction
in the desktop personal computer in the year 2007. The prominent feature of the system
is the "multiple-heat-source cooling capability," which cools the microprocessor with the
liquid (Uno, 2007). IBM Corporation uses a network of copper pipes that sit just above
the new Power6 processor and carry cold water to them and warm water away. According
to IBM, Water cooling is 4,000 times more efficient than air cooling (Nicoolai, 2008).
The conventional cooling method uses the fan cooling or the combination with the heat
sink. However, these conventional cooling methods generate acoustic noise and have
limitations in confined space. Thus, the well-known alternative way is the use of heat
pipe. Heat pipe is a highly effective thermal conductance device. It has an ability to
transport large quantities of heat against gravity through a small cross-sectional area over
a relatively long length with a comparatively small temperature difference by an
evaporation-condensation cycle with no additional power input to the system.
Heat pipe is widely used in heat-generating components such as computer central
processing unit (CPU) for heat withdrawal. As electronic devices are shifting towards a
more compact form factor (i.e. a design that is smaller than other similar designs in its
field), heat pipe has attracted increasing interest in the research community. Heat pipe has
an advantage, as it can vary its geometrical properties. Hence, heat pipe can be easily
constructed in the available space around the electronics needed to be cooled.
Other than computer industry, heat pipe has numerous applications in automotive industry
such as vehicle brake system cooling, aeronautical industry such as airplane anti-icing
system, aerospace industry such as iso-thermalization of large surfaces, manufacturing
industry such as die casting and injection molding, nuclear power plants, road and bridge
de-icing, and human body temperature control.
1.1 Historical Development of Heat Pipes
The development of the heat pipe began in 1831 when Jacob Perkins and Angier March
Perkins patented their hermetic tube boiler (UK Patent No. 6146) which applied in central
heating system. The hermetic tube boiler works on the principle of single-phase working
fluid circulating in tubes between the furnace and the steam drum at high pressure
(Skempton, 2002). The hermetic tube boiler was produced commercially for over 100
years under A.M. Perkins & Sons Ltd (Reay et al., 2013). In 1839, Angier March Perkins
patented his hot water hermetic heating tubes in UK Patent No. 8311.
Chapter 1. Introduction 3
In the nineteenth century, Perkins family invented Perkins tube through a series of patents
in the United Kingdom. The Perkins tube was the first use and described as a device that
contains only a small quantity of water and operating like a two-phase thermosyphon in
UK Patent No. 7059, dated April 1936. Perkins tube predates the heat pipe for several
decades and plays an essential part in the history of heat pipe (Perkins, 1836).
Thermosyphon is a passive refrigeration device also known as wickless gravity-assisted
heat pipes. It is helpful to understand the operation of thermosyphon before discussing
the heat pipe as heat pipe is similar to thermosyphon in some respects. Thermosyphon
consists of a small quantity of working fluid and a majority the vapour phase, placed in a
closed, sealed tubular vessel. The working principle of the thermosyphon system is that
the working fluid is heated and vaporized at the lower end of the tube called evaporator.
The vaporized working fluid which has lower density travels up to the cold end of the
tube called condenser and condensed back to the liquid. The condensate which has a
higher density drains back down the sides of the vessels interior wall to the hot end by
gravity. The circulation of the working fluid is due to the density difference between cold
temperature fluid (liquid) and hot temperature fluid (vapour).
Gaugler (1944) of the General Motors Corporation who was working on the refrigeration
problems in the mid of the twentieth century invented a heat transfer device. This heat
transfer device would evaporate the liquid to a point above the place where condensation
would take place with no additional work required to raise the liquid. This heat transfer
device introduced the concept of heat pipe and applied for a patent on 21 December 1942.
The patent was then published as US Patent No. 2350348, dated 6 June 1944. The concept
of heat pipe was re-evaluated by Trefethen (1962). However, the heat pipe concept
received relatively little attention until Grover (1966) at Los Alamos National Laboratory
in New Mexico filed his evaporation-condensation heat transfer device patent on behalf
of the US Atomic Energy Commission on 2 December 1963. Grover referred his device
to a heat pipe and described the device as a “synergistic engineering structure which is
equivalent to a material having thermal conductivity greatly exceeding that of any known
metal.
The heat pipe was then recognized as a reliable thermal device based largely on the work
of Cotter (1965) who works at Los Alamos as well. Research on heat pipe began
worldwide after Cotter publication. Many laboratories initiated efforts in this regard. The
United Kingdom Atomic Energy Laboratory at Harwell investigated the use of sodium
4 Chapter 1. Introduction
heat pipes as thermionic diode converters (Bainton, 1965). A similar research was started
at the Joint Nuclear Research Centre in Ispra, Italy (Grover et al., 1965). Others country
such as Germany and France are also actively involved in heat pipe research.
Initially, an emphasis for the use of heat pipe in space application is due to its lighter
weight, higher heat flux, and has capillary driven wicks on its inner pipe wall, which can
operate in zero gravity environment without any external force field. The first flight of
heat pipes which were used for satellite thermal control on Geodetic Earth Orbiting
Satellite (GEOS-B) was launched from Vandenburg Air Force Base in 1968. Heat pipes
were considerable growth in the terrestrial application by early 1970. Feldman and
Whiting (1967, 1968), Eastman (1968), and Katzoff (1966) discussed the terrestrial
applications of heat pipes in air conditioning, engine cooling, and electronics cooling.
A large number of research and development works had been published over the last four
decades. Today, the number of publication in the areas of heat pipe continue to grow.
Many researchers are actively involved in research and development of heat pipes. The
industrial community began to look for a solution in energy savings due to the high cost
of energy. Various types of heat pipes were invented and developed. Among the broad
variety of heat pipes, the commonly found heat pipes are variable conductance heat-pipes,
loop heat pipes, miniature heat pipes, and micro heat pipes. These heat pipes are matured
enough for the use in various applications like power engineering, chemical engineering,
space technology, and many other engineering fields. Heat pipes are also used in many
everyday applications, such as laptops, electronics, games consoles, air conditioner,
refrigeration, television, and much more because of their low weight, high reliability,
operating self-sufficiency, and high effective thermal conductivity which approximately
5,000 W/m⋅K to 200,000 W/m⋅K . Heat pipe has the ability to transfer and dissipate a
large amount of heat with a very small temperature difference between the hot and cold
end. Hence heat pipe will continue to play a crucial role in cooling technology.
1.2 Fundamental Working Principles of Heat Pipes
Heat pipes are characteristically straight and round but not restricted to cylindrical
geometry. It can be bend and flatten into a different form even in other complex shapes.
The schematic diagram of a conventional heat pipe is shown in Figure 1.1 below. Heat
pipe is made up of an evaporator, adiabatic and condenser section. The adiabatic section
separates the evaporator and condenser section. Some of the heat pipes might not have
Chapter 1. Introduction 5
the adiabatic section, and some heat pipes might have multiple heat sources and heat sinks.
The design of heat pipe depends on specific applications. There are three main
components of a heat pipe: the sealed container, small amount of working fluid, and the
wick or capillary structure.
The working principle of heat pipe is similar to “reverse thermosyphon” due to its ability
to transport heat against gravity by an evaporation-condensation cycle. The difference
between heat pipe and thermosyphon is that heat pipe consists of wick on the inner pipe
wall. A two-phase closed thermosyphon is a gravity-assisted wickless heat pipe (Faghri,
1995).
Wick is a type of porous medium. The porous medium is a solid matrix that consists of
many pores or voids filled by fluid (liquid or gas) and permeate in between the solid.
There are many naturally existing porous media such as rocks, soils, and biological tissue
while materials such as ceramics, foam and metal wick in the heat pipe are considered as
man-made.
Figure 1.1 Schematic diagram of a conventional heat pipe
The wick lined on the inner wall of a heat pipe is functioned to generate capillary pressure
that drives the working fluid from the condenser back to the evaporator. Other than
providing a mechanism for the working fluid return to the evaporator, the wick in the heat
pipe also facilitates the working fluid to distribute evenly over the evaporator surface.
Since the wick exerts capillary force the return of the condensate back to the evaporator,
Evaporator
section Condenser
section Adiabatic
section
Heat Source Heat Sink
Condenser end cap
Evaporator end cap
Wick
Vapour flow Liquid flow
Container
6 Chapter 1. Introduction
hence the position for evaporator section can be in any orientation and not restricted to be
at the lower end of the heat pipe. In addition, the wick lined in the inner tube of heat pipe
increases the surface area for better evaporative heat transfer and leads to a high effective
thermal conductance of the heat pipe and efficient in heat transfer.
The heat pipe container consists of a pipe wall and the end caps on both ends. The
container is usually made of high thermal conductivity metals like copper and aluminium.
The working fluid is in equilibrium with its vapour. Usually, water, acetone, nitrogen,
methanol, ammonia or sodium is used as working fluid based on the operating
temperature. One of the main incentives for using the heat pipe is the working fluids in
its cooling system has the ability to absorb heat that closes to the heat generating regions
in microscale. Then, it will move arbitrary distances to locations where more convenient
to reject heat to the surrounding environment.
Heat pipe employed the evaporative cooling to transfer the energy in the form of heat
from the hot end (or known as the evaporator) through evaporation to the cold end (or
known as the condenser) where condensation happens. The heat is applied to the external
wall of the heat pipe and conduct through the pipe wall and the wick structure at the
evaporator section. The working fluid at the evaporator section absorbs the heat and
vaporizes. The vapour then travels through the adiabatic section to the condenser section,
driven by the resulting vapour pressure. At the condenser section, the vapour condensed,
releasing a large amount of latent heat of vaporization to the heat sink. The condensate
then flows back to the evaporator using capillary action, also known as capillarity,
capillary motion or wicking. Capillary action is the ability of a liquid to flow within the
void spaces of a porous medium due to the adhesion of the liquid to the sides of the tube
and cohesion between particular liquid molecules and surface tension that acts to hold the
liquid surface intact. If the liquid flow in a sufficiently narrow tube and the adhesion of
the liquid to the tube walls is sufficiently strong, the interaction between these two
phenomena causes the liquid to work in opposition to the gravity and to be drawn upward
in the tube.
1.3 Porous Media
Porous media is a material which consists of a solid matrix with an interconnected void.
The interconnectedness of the void, which sometimes called the pores, allows one or more
fluids to flow through the material. The void is saturated by single fluid (liquid or gas)
Chapter 1. Introduction 7
in single-phase flow. While in multiphase flow, liquid and gases share the void space.
When the fluid filled the voids completely, the porous media is saturated.
The porous media has been used in many applications, especially in the science and
engineering field. One of the examples is the use of wick structure in heat pipe cooling
application. It is attached to the inner linings of the heat pipe’s tube to enhance and aid
the evaporative heat transfer rate. The materials of wick structure are either made of
aluminum, steel, copper or nickel in the various range of pore sizes. Fibrous materials,
like ceramics, have also been used widely. Recently, the interest of wick material has
turned to carbon fiber. Carbon fiber filaments are chemically stable and have many fine
longitudinal grooves on their surface results in higher capillary pressures.
The porous medium with matrices composed of smaller sphere particles has a more solid-
liquid contact surface area and solid-solid contact point compared to plain media as
illustrated in Figure 1.2. One can say the porous medium with matrices composed of
smaller sphere particles has a larger effective area for heat to transfer and hence the rate
of heat transfer will be higher.
(a)
(b)
(c)
Figure 1.2 The variation of the matrices of porous medium with (a) no sphere particles; (b) large sphere particles; and (c) small sphere particles
To improve the heat transfer rate through a porous medium in a heat pipe, many
researchers (Lu et al., 1999, Levkov and Kulkov, 2016, Woodside and Messmer, 1961,
Florez et al., 2013, Ren et al., 2007a, Hanlon and Ma, 2003, Li et al., 2006, Li and
Peterson, 2006b, Li and Peterson, 2006a, Li and Peterson, 2007, Deng et al., 2017)
examined in depth the porous properties and characteristics through experimental and
theoretical investigation.
Porous media is most often characterized by its porosity. The porous structure has a
significant effect on heat conduction in porous media. The higher the porosity, the lower
the thermal conductivity will be. In general, the overall thermal conductivity of porous
media depends on the geometry of the medium and the properties of liquid and solid. So
8 Chapter 1. Introduction
this overall thermal conductivity is known as effective thermal conductivity. It is in a
function of porosity and thermal conductivity of solid and liquid.
Deng (2017) applied fractal geometry to characterize the pore distribution of porous
material. He stated that the effective thermal conductivity is also affected by the fractal
dimensions of the porous material, even when porosity remains constant.
By examining the porous structure and its properties such as porosity, pore size, particle
size, porous layer thickness, total solid-liquid contact surface area and heat flux, a deeper
understanding of the heat transfer mechanism in a porous media can be achieved to
innovate and improve the heat pipes.
1.4 Evaporation in Porous Media
When a liquid sits in one place, for example, a puddle, its molecules will escape into a
gas. This is the process called evaporation. Evaporation can happen either when liquids
are cold or when they are warm, but the higher rate of evaporation is with warmer liquids.
It is because when the matter has a higher temperature, its molecules have more energy
to move and vibrate quicker, and the space between them also increases. When the energy
in specific molecules reaches a certain level, they would escape into the sur