VOLATILE ORGANICS INITIAL CALIBRATION DATA · 2019-12-01 · 7A VOLATILE CONTINUING CALIBRATION CHECK Lab Name: CHEMTECH . Contract: EPA REGION-in Project No. A671-S _____ Site: Location:

6AVOLATILE ORGANICS INITIAL CALIBRATION DATA

Lab Name: CHEMTECH Contract: EPA REGION-III

Project No.: A671-S_____ Site: ______ Location: ______ Group:

Instrument ID: VOA1______ Calibration Date(s): 12/1/95. 12/1/95

Heated Purge: (Y/N) _ ' Calibration Times: 0917 1249

GC Column DB624 ID: 0.53 (mm)

Lab File ID: RRF10 = L1385.D . RRF20 = L1384.DRRF50 = L1383.D RRFIOO = L1386.D . RRF200 = L1387.D

COMPOUNDDichlorodifluorometbaneChloromethaneBromomethaue *Vinyl Chloride *ChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dicliloroethene *1 , 1 -Dicliloroethaue *trans- 1 .2-Dichloroethenecis- 1 ,2-DichioroetheneChloroform *1,2-Dichloroechane *2-Butaiione1.1.1 -Trichloroethane *Carbon Tetrachloride *Btomodichloromethane '*1 ,2-Dicliloropropanecis-l,3-Dichloropropene *Irichloroethene *Dibromochloromethane *1,1,2-Trichloroethane *Benzene *trans- 1,3-Dichloropropene *Bromoform *4-Methyl-2-Pentanone2-HexanoneTetrachloroetbene *1,1,2,2-Tetrachloroethane *Toluene *Chlorobenzene *Ethylbenzene - *Styrene *m+ prXylenes *o-xylene *

RRFIO1.8460.5760.8260.7450.5941.7420.5253.2582.0082.7192.0671.7763.3071.6540.1240.4400.4280.5230.3830:4850.3360.4700.3410.8170.3990.2970.4390.2520.4600.7171.2700.9171.4140.8330.4830.979

RRF201.8630.5750.9000.8770.5811.7910.6263.6962.2582.9732.4152.0803.6701.8930.1650.4660.4850.5720.4140.5130.3630.5220.3700.8720.4490.3680.5210.3150.5070.8261.3360.9791.5650.9730.5431.129

RRF501.9100.6080.9330.9390.6181.8770.4733.9812.3523.2642.4622.3273.9251.9690.1360.4690.4600.5690.3970.5040.3810.5270.3530.8750.4350.3600.4170.2670.4880.6961.2480.9281.424

L0.9180.4841.015

RRFIOO1.6950.5230.8430.8300.4621.6510.3483.5082.1042.9992.1612.0053.5031.8190.1240.4540.4480.5490.3870.4860.3500.4880.3400.8210.4330.3200.3990.2700.4600.6681.2040.9061.4160.9060.5171.048

RRF2001.6780.4940.7530.8010.3811.5920.3233.3181.9902.7992.1431.9643.3661.6920.1180.428 _0.4210.5190.3610.4660.3290.4580.3210.7630.4090.3110.3610.2420.4200.6111.0840.8511.3180.8580.4770.983

RRF1.7980.5550.8510.8380.5271.7310.4593.5522.1432.9512.2502.0303.5541.805•0.1340.4510.4480.5470.3880-4910.3520.4930.3450.8300.4250.3310.4270.2690.4670.7041.2280.9161.4270.8970.5011.031

%RSD5.88.28.28.819.26.527.48.37.47.17.9 '9.97.07.314.13.85.74.55.03.76.06.35.25.64.89.513.910.47.011.37.65.06.26.15.66.0

*Compounds with required minimum RRF and maximum %RSD values.All other compounds must meet a minimum RRF of 0.010. . .» t\ A * Q A.«eiof2 AR3I8H3 OOOU*H M O | O H 4 J FQRM VQA 3/90


Lab Name: CHEMTECH_________ Contract: EPA REGION-III

Project No.: A671-S_____ Site: • Location: ________ Group:

Instrument ID: VOA1 Calibration Date(s): 12/1/95 12/1/95

Heated Purge: (Y/N) _ Calibration Times: 0917 1249


Lab File ID: " RRF10 = L1385.D RRF20 - L1384.DRRF50 = L1383.D RRFIOO = L1386.D RRF200 = L1387.D

COMPOUND

'

Toluene-d8Bromofluorobenzene *1 ,2-DichIoroethane-d4

RRF10

1.2620.6981.544

RRF20

1.1690.6841.525

RRF50

1.1390.6421.560

RRFIOO

1.0530.5801.382

RRF200

• 1.0410.5911.502

RRF

""-

1.1330.6391.503

%RSD

•

8.08.34.7

* Compounds with required minimum RRF and maximum %RSD values.All other compounds must meet a minimufn RRF of 0.010.

Page2of2 000135FORMVIVOA

7AVOLATILE CONTINUING CALIBRATION CHECK _ w so


Project No. A671-S_____ Site: _____ Location: ______ Group:

Instrument ID: VOA1 Calibration Date: 12/6/95 Time: 1425

Lab File ID: L1395.D Init. Calib. Date(s): 12/1/95 12/1/95

Heated Purge: (Y/N) ___ Init. Calib. Times: 0917 1249

GC Column: DB624 ID: 0.53 (mm)

COMPOUNDDichlorodifluoromethane

. ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethyleue ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroetliene1,1-Dichloroe thanetrans- 1 ,2-Dichloroedienecis- 1 ,2-DichloroetlieneChloroform1 ,2-Dichloroethane2-Butanone1,1,1 -TrichloroedianeCarbon TetrachlorideBromodichloromediane1 ,2-Dichloropropanecis- 1 ,3-DichloropropeneTrichloroediene'Dibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans- 1 ,3-DichloropropeueBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroediene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem+ p-Xyleneso-xylene

RRF1.7980.5550.8510.8380.5271.7310.4593.5522.1422.9512.2502.0303.5541.8050.1340.4510.4480.5470.3880.4910.3520.4930.3450.830 .0.4250.3310.427 '0.2690.4670.7041.2280.9161.4270.8970.5011.031

RRF501.3810.4130.7310.6730.3721.5420.4322.8631.8122.6762.0551.8163.2501.7150.1640.4070.4170.5120.3630.4650.3280.4820.3420.7880.4260.3570.5010.3310.4380.7801.1430.8721.3830.8840.4881.028

MINRRF

0.1000.100

0.1000.200

0.2000.100

0.1000.1000.200

0.2000.3000.1000.1000.5000.1000.100

0.2000.5000.4000.5000.1000.3000.3000.300

%D23.2

r25.6j>14.119.7

C29.4310.95.919.415.49.38.710.5-8.65.0-22.49.86.96.46.45.36.82.20.95.1-0.2-7.9-17.3-23.06.2-10.86.94.83.11.42.60.3

MAX%D

25.025.0

25.025.0

25.025.0

25.025.025.0

25.025.025.025.025.025.025.0'

25.025.025.025.025.025.025.025.0

SAMPLE NO.VSTDOSOVBLK0118I1128W341811128W411811128W421811128W1318H128W46181112834A1811129W47I18H129W48181112948A1811127W201811127W20MS181H27W20MS18H12918B

Page I of2

All other compounds must meet a minimum RRF of 0.010.

AR3

7AVOLATILE CONTINUING CALIBRATION CHECK



Instrument ID: VOA1 . Calibration Date: 12/6/95 Time: 1425


Heated Purge: (Y/N) ____ Init. Calib. Times: 0917 1249


COMPOUND

Toiuene-d8Bromofluorobenzene1 ,2-Dichloroethane-d4

RRF

1.1330.6391.503

RRF50

1.1250.6811.521

MINRRF

<

-

•

0.200

%D

*

_

0.7-6.6-1.2

MAX%D

'

25.0


Page 2 of 2 /» R 3 I 8 !* l» 6



Project No. A671-S _____ Site: _____ Location: _ _____ Group:

Instrument ID: VOA1 Calibration Date: 12/9/95 Tune: 0858

Lab File ID: L1456.D . Init. Calib. Date(s): 12/1/95 12/1/95

Heated Purge: (Y/N) ___ Init. Calib. Times: 0917 1249


COMPOUNDDichlorodifiuoromedianeChloromethaneBrbmomethaneVinyl ChlorideChloroethane 'Methyleue ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-DichIoroe thanetrans- 1 , 2-DichIoroethenecis-1 ,2-DichloroedieneChloroform1 ,2-Dichloroethane2-Butanone1,1,1 -TrichloroedianeCarbon TetrachiorideBromodichloromediane1 ,2-Dichloropropanecis- 1 ,3-DichloropropeneTrichloroedieneDibromochlororaediaiie1 , 1 ,2-TrichloroedianeBenzenetrans- 1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroediene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem+ p-Xyleneso-xylene

•<

RRF1.7980.5550.8510.8380.5271.7310.4593.5522.1422.9512.2502.0303.5541.8050.1340.4510.4480.5470.3880.4910.3520.4930.3450.8300.4250.3310.4270.2690.4670.7041.2280.9161.4270.8970.5011.031

RRF502.1610.6911.0681.150 •0.5081.4270.3713.1051.8702.3581.8641.5942.9231.4300.1510.4470.4200.5530.3500.4790.3210.4570.3200.8170.4020.2890.4560.3020.447

. 0.6901.1940.8401.3770.8620.4921.017

MINRRF

0.1000.100

0.1000.200

0.2000.100

0.1000.1000.200

0.2000.3000.1000.1000.5000.1000.100

0.2000.5000.4000.5000.1000.3000.3000.300

%D-20.2-24.525.5C-37.23.617.619.212.612.720.117.121.517.820.8-12.75:96.3-1.19.82.48.87.37.21.65.412.7-6.8-12.34.32.02.88.33.53.91.81.4

MAX%D

25.025.0

25.025.0

25.0 •25.0

25.025.025.0

25.025.025.025.025.025.025.0

25.025.025.025.025.025.025.025.0

SAMPLE NO.VSTD050VBLK02181112947B1811129W18181H30W061811130WS1181113006A1811204W531811204W541811204W55181 120453 B

All orner compounds must meet a minimum RRF of 0.010. .

000155


Lab Name: CHEMTECH . Contract: EPA REGION-in

Project No. A671-S _____ Site: Location: ______ , Group:

Instrument ID: VOAI Calibration Date: 12/9/95 Time: . 0858



GC Column: DB624 ID: 0.53 (mm) "

COMPOUND

^

Toluene -d8BromoQuorobenzenel,2-Dichlorocdiane-d4

RRF

1.1330.6391.503.

RRF50

•

1.3870.7631.564

MINRRF

t

0.200

%D

•~.

-22.4-19.4-4.1

MAX%D

25.0


Page2of2FORM VH VOA 3/90


Lab Name: CHEMTECH Contract: EPA REGION III

Project No. A674-S _____ Site: _____ Location: ______ Group:

Instrument ID: VOA1 ' Calibration Date: 12/17/95 Time: 1419




COMPOUNDDichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroetliene1,1-Dichloroedianetrans- 1 .2-DichIoroedienecis-1 ,2-DichloroedieneChloroform1 ,2-Dichloroethane2-Butanone1,1,1 -TrichloroedianeCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroedieneDibromochloromediane1 , 1 ,2-TrichloroethaneBenzenetrans- 1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem+ p-Xyleneso-xylene

RRF1.7980.5550.8510.8380.5271.7310.4593.5522.1422.9512.2502.0303.5541.8050.1340.4510.4480.5470.3880.4910.3520.4930.3450.8300.4250.3310.4270.2690.4670.7041.2280.9161.4270.8970.5011.031

RRF501.3630.4450.8070.6610.4601.4920.3892.5481.6502.7361.9512.1903.4311.6860.1590.3690.4630.4650.4140.4030.3980.5470.3930.6780.3410.3680.4410.3020.5000.7511.0140.9111.1160.8150.4150.86S

MINRRF

0.1000.100

0.1000.200

0.2000.100

0.1000.1000.200

0.2000.3000.100 '0.1000.5000.1000.100

0.2000.5000.4000.5000.1000.3000.3000.300

%D24.219.85.221.112.713.815.36a.3323.07.313.3-7.93.56.6-18.713.2-3.315.0-6.717.9-13.1-11.0-13.918.319.8-11.2-3.3-12.3-7.1-6.717.40.521.89.117.216.1

MAX%D

25.025.0

25.025.0

25.025.0

25.025.025.0

25.025.025.025.025.025.025.0

25.025.025.0.25.025.025.025.025.0

1SAMPLE NO.VSTD050VBLK031811206P2B1811206W641811206W62181 1206 W651811206W661811207W041811213B011811213B02

•

All odier compounds must meet a minimum RRF of 0.010.AR3 I 81*1*9 000173

Page I of2


~ 3 .3 r*Lab Name: CHEMTECH________ Contract: EPA REGION IE

Project No. A674-S___ Site: Location: Group:


Lab File ID: L1499.D____________ Init- Calib. Date(s): 12/1/95 12/1/95

Heated Purge: (Y/N) ____ luit. Calib. Times: . 0917 1249

GC Column: DB624 ED: 0.53 (mm)

COMPOUND

'

V

Tolueoe-dSBromofluorobenzenc1 ,2-Dichloroethane-d4

RRF

1.1330.6391.503

RRF50

1.1100.6251.411

MINRRF

0.200

%D

""••

2.02.26.1

MAX%D

25.0

All other compounds must meet a minimm^ RRF of 0.010.

Page2of2 A R 3 I 8 k 5 0FORM VH VOA 3/90

6A • " / ' . . " . VVOLATILE ORGANICS INITIAL CALIBRATION DATA

• •• •_Lab Name: CHEMTECH Contract: US EPA REGION PI

Project No.: A689-S _____ Site: _______ Location: _ Group:

Instrument ID: HP5971A Calibration Date(s): 12/20/95 12/20/95

Heated Purge: (Y/N) t__ ' Calibration Times: 0934 1221

GC Column DB624 _______ ID: 0.53 (mm)

Lab File ID: RRF1Q = L1516.D , RRF20 = L1515.DRRF50 = L1514.D RRFIOO - L1517.D RRF200 = L1518.D

COMPOUNDDichlorodifluoromethaneChloromethaneBromomethane •*.Vinyl Chloride *ChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene *1,1-Dichloroethane •*1,2-Dichloroediene (total)Chloroform *1,2-Dichloroethane *2-Butanone1,1,1-Trichloroethane *Carbon Tetrachloride *Bromodichlbromethane *1,2-Dichloropropanecis-1, 3-Dichloropropene *Trichloroethene *Dibromochloromethane *1,1,2-Trichloroethane *Benzene . *trans-1, 3-Dichloropropene *'Bromoform " *4-Methyl-2-Pentanooe2-HexanoneTetrachloroethene *1,1,2,2-Terrachloroethane *Toluene *Chlorobenzene *Ethylbenzene '*Styrene . » *01+ p-Xylenes *o-xylene *

RRF10L4671.3671.440.1.5620.7021.822.:;'0.561 I..3.8502.H33.3805.2095.3602.9570.1870.4960.4580.6120.409-0.5220.3510.4810.3550.8890.448.,0.2950.5260.341 .0.4330.7731.2790.9441.5580.9390.5681.204

RRF201.5421.2091.2151.5110.6101.799 >:•0.5563.7422.170 -3.9495.6075.3992.892.0.1720.4910.4700.6140.4040.5190.356 i •0.490,0.337 •0.8720.4440.304 r0.4770.32510.4490.7221.2700.9381.560,0.952?0.5701.192

RRF501.5061.2851.2021.709.0.530U8260.5873.8742.0913.6585.6295.701 '3.2410.1640.4930.475 ,0.6460.4140.5420.35L0.5270.3560.8790.480. :0.34$0.483, '0.3170.4490.7521.2480.9231.531.0.9510.564'-1.180

RRF.1001.4750.9431.2091.5230.443117820.460 >.3.9141.9723.1534.6104.9573.1140.1250.4630.4460.5880.3810.5010.32T10.4850.3190.8090.436;0.307,0.3870:2600.4190.6221.1370.856-L400,0.882-0.507Nvl.085

1 -

RRF200^ 0.9070.7590:7260.9500.4461.243"0.3092.7561.4542.3373.4133.6242.1270.0950.3590.360 ~0.4690.294013890.2680.3830.2440.629

V0.341-0.2410.2880.1900.3430.4690.9280.6891.124: 0:7100.4130.851

RRF1.3801.1131.1581.4510.5461.694 :

0.4953.6271.9603.2954.8945.0082.8660.1480.4600.4420.5860.3800.4940.3320.4730.3220.8160.4300.2990.4320.2860.4190.6671.172'0.8701.4350.887.0.5241.102

RSD19.322.822.620.120.314.923.213.514.918.618.916.315.225.512.610.711,713.112.311.011.414.513.312.212.622.021.710.618.812.612.312.911.6J2.913.4

* Compounds with required minimum RRF and maximum 56RSD values. ^00054All other compounds must meet a minimum RRF of 0.010. ~

Page 1 of 2 'FORM VI VGA AR3I8U5I 3/9°

6A .* :VOLATILE ORGANICS INITIAL CALIBRATION DATA — S 6-3

Lab Name: CHEMTECH_________ Contract: US EPA REGION m

Project No.: A689-S_____ Site: _____ Location: ______ Group:


Heated Purge: (Y/N) _N_ ' Calibration Times: 0934 1221

GC Column DB624_____ ID: 0153 (mm)

Lab File ID: RRF10 = L1516.D RRF20 = L1515.DRRF50 - L1514.D RRFIOO = L1517.D RRF200 = L1518.D

COMPOUND

.

. . . .

. ' - ' • " '

- <.- - - . /''Vi''.

Toluene-dS. • . - -"fBromofluorobenzene *l,2-Dichloroethane-d4

RRF10

-..-

- - •

••*'*<%&&£112840.8743.052

RRF20

-

i

:;-;,•:.<•".•:-

1.1140.7442.524

RRF50

-

\ - . ' - - •

•u-C H1.073*0.7202.718

RRFIOO

•,

" •' -

.

•« ^ 4-1.014 >0.6512.667

RRF200

t'ff ' '

. •

• - ,

' •--»'/' -,• _— i.- •]-

-• " •

••••&%>$&&0.859-•0.5351.887

RRF, V; '.

• - .-

'-":• • *".'»•*•,*"•

• •;,.•

,

».

,. - - • -, ,• ''• -' T %* *~ *~ • * *•*;

, .

:>.:i'!1.069,0.705 •:2.570

%RSD.r-

1 t

'- . ,

., •

. -..

• '

," ': '.-'<14.417.716.7

f,.

*

* Compounds with required minimum RRF and maTimum %RSD values. . 'All other compounds must meet a minimum RRF of 0.010. f

Page 2 of2FORM VI VOA AR 3 I 8U52 3/9°

, • 7A 'VOLATILE CONTINUING CALIBRATION CHECK

Lab Name: CHEMTECH . Contract: US EPA REGION ffl


Instrument ID: HP5971A Calibration Date: 12/20/95 time: 1445


Heated Purge: (Y/N) N Init. Calib. Times: 0934 1221


COMPOUND• DichlorodifluorometnaneChloromethaneBromomethaneVinyl ChlorideChloroetnaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroethane1 ,2-Dichloroethene (total)Chloroform1 ,2-Dichloroe thane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromediane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroethene"Dibromochloromediane1,1,2-TrichloroedianeBenzenetrans-1, 3-DichloropropeneBromoform ,4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEmylbenzeneStyrenem+ p-Xyleneso-xylene -

RRF1.3801.1121.1581.4510.5461.6940.4953.6271.9603.2954.8945.0082.8660.1480.4600.4420.5860.3800.4940.3320.4730.3220.8160.4300.2990.432-0.2860.4190.6671.1720.8701.4350.8870.5241.102

RRF501.4200.9861.3081.5580.6621.6590.5063.8421.9112.9984.5884.7613.1340.1810.4840,4230.6330.4010.5290.3030.4740.3330.861

• 0.4720.2880.5170.3400.3510.7521.1900.8201.4800.9360.5171.139

MINRRF

0.1000.100

0.1000.200

0.2000.100

0.1000.1000.200

0.2000.3000.1000.1000.5000.10001100

0.2000.5000.4000.5000.1000.3000.3000.300

%D-2.911.3-13.0

- -7.4-21.22.1-2.2-5.92.59.06.64.9-9.4-22.3-5.2~ 3-8.0-5.5-7.18.7-0.2-3.4-5.5-9.83.7-19.7-18.916.2-12.7-1.55.7-3.1-5.51.3-3.4

MAX%D

25.025.0

25.025.0

25.025.0

25.025.025.0

25.025.025.025.025.025.025.0

25.025.025.025.025.025.025.025.0

SAMPLE NO.VSTD050VBLK011811213B031811214B041811214T031811214W671811218W221811218W681811218T681811218T68MS1811218T68MSD

-

All other compounds must meet a minimum RRF of 0.010. ''00073

AR3I8U53FORM VH VOA 3/90

7A 'VOLATILE CONTINUING CALIBRATION CHECK

. .Lab Name: CHEMTECH Contract: US EPA REGION m

Project No. A689-S ____ Site: Location: ____ Group:

Instrument ID: HP5971A Calibration Date: 12/20/95 Tune: 1445

Lab File ID: L1520.D____________ Init. Calib. Date(s): 12/20/95 12/20/95

Heated Purge: (Y/N) N Init. Calib. Times: 0934 1221


COMPOUND

-.

-

. . «

- • - • - .

*'

- -' - . ----- -"'---Toluene-d8Bromofiuorobenzenel,2-Dichloroethane-d4

RRF

. •-•- • ,-

1.0690.7052.570

RRF50

. , \

,\

0.9650.6432.398

MENRRF

•

. .

'

.- ...-•..•

.

.

0.200

%D

•

, •9.78.86.7

MAX%D

25.0

All other compounds must meet a miniming RRF of 0.010. * ^ U U f 4

Page2of2 . A R 3 I 8 »* 51*FORM VH VOA 3/90


Lab Name: CHEMTECH . Contract: EPA REGION m


Instrument ID: VOA1_____ Calibration Date(s): 12/3/95 12/3/95

Heated Purge: (Y/N) _Y_ ' Calibration Times: 0738 1038


Lab File ID: RRF10 = L1391.D RRF20 = L1390.DRRF50 = L1389.D RRFIOO = L1392.D RRF200 = L1393.D

COMPOUNDDichlorodifluoromethaneChtoromethaneBroraomethaue *Vinyl Chloride *Chloroethahe • •Methyiene ChlorideAcetone - .Carbon Disulfide .1,1-Dichloroethene *1,1-Dichloroethane / *trans-1, 2-dichloroetbenecis-1 ,2-DichloroetheneChloroform - *1,2-Dichloroediane *2-Butanone1,1,1-Trichloroethane , *Carbon Terrachloride *Bromodkhlaromethane *1,2-Dichloropropane .- 'cis-1, 3-Dichloropropene *Frichloroethene , • -*Dibromochloromethane *1,1,2-Trichloroethane +•Benzene; ... .,' . . - ;*trans-1, 3-Dichloropropene • *iromoform . *4-Memyl-2-Pentanone2-Hexanone -retrachloroethene *1,1,2,2-Tetrachloroethane >Toluene ..*Chlorobenzene . • ,- > , *Ethylbenzene " ffc "'""'.SfeAStyrene '- • .. "r ••<'•--' >.*ta+ p-Xylenes , . • "; *o-xylene. *

RRF100.2410.4100.6950.6150.4571.664.0.736.'3.1171.886?2.8072.1721.9203.5071,7830.2750.4520.4180.531s0.4080.487

. 0.3580.4730.3800.846,'0.438- -0:3480.7630.4740.47,10.9361.2430.947,

:M34iI*?jJO.8701 .0.5311.043

. RRg20 :0,249;-0.454 , -0.770.-0.701 J

0.618."•'. IJS6S&:0:908£?3.219*1.965;3.2052.1612.0663.486.2.0510.3420.492f0.48370.609K0.435 K0.554-f;0;408f;0.552 c0.434.0.922,rOJ505l"0.4210.8350.617,0.4760.967.1.256.0.984;VtiS&K.-0.9390.5401.066

'

vRRFSO0.3000.453,0.7030,768-a5371 668';0.707 '3:3172.0983.1542.3222.1403.6851.9170.2830.4640.4740.5800.415 v.5160.380.0.531 :0.396;0.859SO.4770.4080.765.0.554-0.4770.9111.213:0.9603 456T0.919 r0,5141.046

RRFIOO.0.2120.4020.6950.6460.426.1.652-0.5522.9491.974 -2.8992.1512.0003.5541.9340.2410.4340.4200.5340.3810.4800.3580.5000.3660.8000.4480.378

> 0.6000.448

' 0.4250.7851.1250.865n.329 ;0.863.0.4820.981

"

RRF200.0.2100.4310.578 .0.6690.3561.4950.4962.5571.6862.7061.9381.9173.1431.8200.2500.395 .0.3920.4880.336

. 0.4330.3060.4730.3560.7230.421 '0.3660.6170.4580.405"0.7981.0610.837>1.140 -.0.8320.5050.932

RRF0.2420.4300.6880.6800.4791.6300.6803:0321.9222.9542.1492.0083.4751.9010.2780.4480.4370.5490.3950.4940.3620.5060.387018300.4580.3840.7160.5100.4510.8791.1790.9191.3680.885 .0.514L014

%RSD15.05.610.18.621.24.623.99.87.97.46.44.85.85.514.28.19.08.69.69.110.37.07.98.97.37.714.314.37.49.47.16.910.54.94'.45.5

* Compounds with required minimnni RRF and maximum %RSD values. . H A H 1 /( OAll other compounds must meet a minimum RRF of 0.010. U U U J. 4 O

Pagelof2. . AR3I81*55FORM VI VOA 3/90

6A , .' VOLATILE ORGAlNICS INITIAL CALIBRATION DATA ___ -^ g Q

- Lab Name: CHEMTECH _____ Contract: EPA REGION ffl

Project No.: A672-S Site: _____ Location: ______ Group: ___

Instrument ID: VOA1______ Calibration Date(s): 12/3/95 12/3/95

Heated Purge: (Y/N) _Y_ Calibration Tunes: 0738 1038


Lab File ID: ' RRF10 = LI39I.D RRF20 - L1390JDRRF50 = . LI389.D RRFIOO = L1392.D RRF200 - L1393.D

COMPOUND

,

-

-

•

, ,

' ,: " . • ' - • - •

Toluene-dSBromofluorobenzene ,. *1 ,2-Dichloroethane-d4

RRF10

1.2780.7271.802

RRF20

1

1.1360.6601.825

RRF50

,

1.0510.5951,728

RRFIOO

_

0.9940.5651.711

RRF200

'

^

. ••,0.9620.5391.587

RRF

•

— ••».,

'; , '/ _-,.

1.084O.6171.731

J£D.,'

,

• ,- ..

*

••:v'.11.712.45.4

-

*.

* Compounds with required minimum RRF and maTJmtmi %RSD values.All odier compounds must meet a minimum RRF of 0.010.

Page 2 of 2FORM VI VGA A R 3 j 8 k 5 6 3/90

000144

. , 7AVOLATILE CONTINUING CALIBRATION CHECK

Lab Name: CHEMTECH Contract: EPA REGION in

Project No. A672-S Site: • Location: Group:


Lab File ID: L1411.D ______ Init. Calib. Date(s): 12/3/95 12/3/95

Heated Purge: (Y/N) Y Init. Calib. Tunes: 0738 1038

GC Column: DB624 - ID: 0.53 (mm)

COMPOUNDDichlorodifluoromethaneChloromethaneBromometbaneVinyl ChlorideChloroethane .Methylene ChlorideAcetone ;Carbon Disulfide1,1-Dichloroethene1 , 1 -Dichloroethanetrans- 1 ,2-dichloroedienecis-1 ,2-DichloroetheneChloroform1 ,2-Dichloroediane2-Butanone1,1,1-TrichloroedianeCarbon TerrachldrideBromodichloromethane1 ,2-Dichloropropanecis-1, 3-DichloropropeneTrichloroedieneDibromochioromediane1 , 1 ,2-TrichloroedianeBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanbneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzene . . • ;- .Ethylbenzene. ' •Styrenem-l- p-Xylenes \ .o-xylene

-

RRF0.2420.4300.6880.6800.4791.6300.680 J3:0321.9222.9542.1492.0083.4751.9010.2780.4480.4370.5490.3950.4940.362 *0.5060.387"0.830:0.4580.3840.7160.5100.4510.8791.1790:9191.3680.8850.5141.013

RRF500.252 '0.4740.7500.7260.4211.9460.4413.5382.0462.9402.3422.0243.6161.8400.1860.5090.5080.6210.4400.5570.4030.5960.425

; 0:9070.4870.4500.522014590.5330.8781.240

•4 1.0261.5131.0400.5731.156

MINRRF

0.1000.100

0.1000.200

0.2000.100

0.1000.1000.200

0.2000.3000.1000.100*0.5000.1000.100

0.2000.5000.4000.5000.100:0.3000.3000.300

%D-4.1-10.2-9.0-6.812.1-19.4O5-O

-16.7-6.50.5-9.0>0.84.13.2

03.0-i3:&--16.2

. -13.1-11.4-12.8-11.3-17.8-9.8-9.3-6.3-17.2r27.G?10.0-18.20.1-5.2 .rll.6

-10.6* -17.5-11.5-14.1

MAX%D

25.025.0

25.025.0

25.025.0

25.025.025.0

25.025.025.025.025.025.025.0

25.025.025.025.025.025.025.025.0

I

SAMPLE NO.VSTD050VBLK011811127PD51811128D411811128D421811128D461811129D471811129D48 .I811127D201181I127D20MS1811127D20MSD

.

All other compounds must meet a mininmtn RRF of 0.010.flR3!8li57 Q00162

Page I of 2

, 7 AVOLATILE CONTINUING CALIBRATION CHECK _ N o

Lab Name: CHEMTECH -_____ , Contract: EPA REGION HI

Project No. A672-S Site: Location: Group: __



Heated Purge: (Y/N) Y Init. Calib. Times': 0738 1038


COMPOUND-

*¥

-

:

Toluene-d8; Bromofluorobenzene1 ,2-Dichloroethane-d4

RRF

-

1.0840.6171.731

RRF50

1.3330.8061.676

MINRRF

0.200

%D

~"--

,

-23.0C30.63.2

MAX%D

--

1)25.0

All other compounds must meet a minimum RRF of 0.010. n A n « n n000163Page2of2 AR3 181*58

FORM VH VOA 3/90

VOLATILE CONTINUING CALIBRATION CHECK-. .. ' . -

Lab Name: CHEMTECH_______ Contract: EPA REGION m

Project No. • A672-S Site: Location: ____ Group:


Lab File ID: L1427.D _______ Init. Calib. Date(s): 12/3/95 12/3/95

Heated Purge: (Y/N) Y Init. Calib. Times: 0738 1038


All other compounds must meet a minimum RRF of 0.010.AR3I81*59 000164

Page I of2

COMPOUNDDichlorodiiluoromedianeChloromethaneBromomethaneVinyl ChlorideChlbroethane . .

. Methylene Chloride .Acetone .Carbon Disulfide1 , l-Dichloroernene1 ; 1-Dichloroethane

. trans- 1.2-dichloroethenecis- 1 ,2-DichloroetheneChloroform1,2-Dichloroethane

• 2-Butanone1,1,1 -TrichloroethaneCarbon TetrachlorideBrbmodichloromethane1 ,2-Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochloromediane1 , 1 ,2-TrichloroethaneBenzene -trans-1 ,3-DichloropropeneBromoform4-Memyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneToluene -Chtorooenzene : •EthylbenzeneStyrenem-l- p-Xylenes • ,.o-xylene

RRF0.2420.4300.688 :0.6800.479 -: 1,630 '*•0,6803.0321.9222.9542.1492.0083.4751.9010.278,0.4480.4370.5490,3950:4940.362 .0.5060.387

~01S30~0.4580.384

- 0.716 -0.5100.4510:8791.179rO#19'•*!li368-.~:0.885015141.013

RRF500.212.0.4535o.83r-0.5080*415**la$?5 •• 0.751,:2:9241:8%2.7822.207

' 2.0893.5751.837 .0.3340.519'0.5430.688."0.465-0.572-0.4320.6280.427O.'SSS'0.4790.3970.7750.5560.5260.8361.250

~*QM1 -i sr0.9610.5131.053

MINRRF

-

0.-1000.100. :.;,

- -.,..,.-.....-...-- 1 .-.,

011000.200

0.2000.100

0.1000.1000.200

v .

0.2000.3000.1000.100•X):500-0.1000.100

0.2000.5000.4000.500.1000.3000.3000.300'

%D12.4-5.3-20.8 -.(25.3J13.4-2.8-10,43.61.45.8-2.7-4.0-2.93.4-20.1-isra--24.3C-25.&-17.7-15.8-19.3-24.1-10.3-7.0. --4.6 --3.4-8.2-9.0-16.64.9-6.0-3.0 --1.08.60.2-3.9

.MAX%D

25.025.0

25.025.0

•

25.025.0

25.0, 25:025.0

25.025.025.025.0-25.025.025.0

25.025.025.025.0.25.0.25.0-25.025.0

SAMPLE NO.VSTD050VBLK021811128D341811128D131811129D181811130D061811130D501811130D49181H30D511811204D531811204D541811204D551811204D561811204D57

-

' • • • • - " - • - . . - • T----7A .VOLATILE CONTINUING CALIBRATION CHECK

Lab Name: CHEMTECH Contract: EPA REGION ffl

Project No. A672-S_____ Site: Location: ___ Group:


Lab File ID: L1427.D __________ Init. Calib. Date(s): 12/3/95 12/3/95

Heated Purge: (Y/N) Y Ink. Calib. Times: 0738 1038


COMPOUND

.•

• ' ' , . • • - - . ». • • ' - - - .' • . .

• • •. - - •

,

.•

-

;.

i ~ . .*

' • • • • • • , • • ' ' • .•••" • • -: •_•„;*":• -

"

' V" '- " ' f

'•''-.-X? -.-:,>".'----v**-4-.>-<*»' J r?.• '• -•- . • .v- ,-..-;, -: <:: -SLxz-Toluene-d8 . ,>•••• •'••Bromofluorobenzene

. l,2-Dichloroethane-d4

RRF

•

•«-;. v- • •/• •-••

4e fes .'t. • , ff,. .*•-»•"*?**, '-'

- 1.084. 0.6171.731

RRF50,

,.-- •• -' •

•

.. .'. '. .-'--' -••'

V- •.-"..,r* • •' ' •

.1.2400.7361.721

MINRRF

1 ' '. --

-

..;• ' ''

....„_.

. •"•--'

0.200

%D

• > ' ,

~*~

v;'>' . "

,.,'i--.-. _ . ,

-14.4. -19.30.6

MAX%D

\

25.0.

All other compounds, must meet a minimum RRF of 0.010.

Page2of2 A R 3 I 8 1* 6 0FORM Vn VOA 3/90

. • " ' . 6A ' . ' ' '' .VOLATILE ORGANICS INITIAL-CALIBRATION DATA 33)6-

Lab Name: CHEMTECH _____ Contract: EPA REGION IIIf . . •


Instrument ID: VOA1 _____ Calibration Date(s): 12/3/95 12/3/95

Heated Purge: (Y/N) _Y_ ' Calibration Times: 0738 1038GC Column DB624 ID: 0.53 (mm)


COMPOUNDDichlorodifluoromethaneChloromethaneBromomediane *Vinyl Chloride *ChloroethaneMemylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene *1,1-Dicliloroethane *trans- 1 ,2-dichloroethenecis-1, 2-Dichloroethene "Chloroform *1,2-Dichloroethane, *2-Butanone1,1,1 -Trichloroethane *Carbon Tetrachloride *Bromodichloromethane *1 ,2-Dichloropropanecis-1, 3-Dichloropropene *Trichloroethene *Dibrbmochloromediane *1,1,2-Trichloroethane *Benzene *trans-1, 3-Dichloropropene •*Bromoform *4-Methyl-2-Pentanone2-Hexanoneretrachloroethene *1 , 1 ,2,2-Tetrachloroethane *Toluene *Chlorobenzene , *Ethylbenzene *Styrene *nr+ p-Xylenes - *o-xylene *

• • •

RRFIO0.2410.4100.6950.6150.4571.6640.7363.1171.8862.8072.1721.9203.5071.7830.2750.4520.4180.5310.4080;4870.3580.4730.3800.8460.4380.3480.7630.4740.4710.9361.2430.9471.411,0.8700.5311.043

RRF200.2490.4540.7700.701:0.618.1.6690.9083.2191.965'3.2052.1612.0663.4862.0510.3420.4920.4830.6090.4350.5540.4080.5520.4340.9220.505 =0.4210.8350.6170.4760.9671.2560.9841.505 '«0.9390.5401.066

RRF500.3000.4530.7030.768V0.5371.6680.7073.3172.0983.1542.3222.1403.6851.9170.2830.4640.4740.5800.4150.5160.3800.5310.3%0.8590.4770.4080.7650.5540.4770.9111.2130.9601.4560.9190.5141.046

RRFIOO0.2120.4020.6950.6460.426.1.6520.5522.9491.9742.8992.1512.0003.5541.9340.241.0.4340.4200.5340.3810.4800.3580.5000.3660.8000.4480.3780.6000.4480.4250.7851.1250.8651.3290.8630.4820.981

RRF2000.2100.4310.5780.6690.3561.4950.4962.5571.6862.7061.9381.9173.1431.820

. 0.2500.395 _0.3920.4880.3360.4330.3060.4730.3560.7230.4210.3660.6170.4580.4050.7981.0610.8371.1400.8320.5050.932

RRF0.2420.4300.6880.6800.4791.630.0.6803.0321.9222.9542.1492.0083.4751.9010.2780.4480.4370.5490.3950.494013620.5060.3870.8300.4580.3840.7160.5100.4510.8791.1790.9191.3680.8850.514'

_ 1.014

%RSD15.05.610.18.621.24.623.99.87.97.46.44.85.85.514.28.19.08/69.69.110.37.07.98.97.37.714.314.37.49.47.16.910.54.94.4515

**

**

**

4>

*

*

4>

4>

*

*

*

*

4i

*

*

*

*

*

*

4>

*

Compounds with required minimum RRF and mariiniiin %RSD values. U U U1 4All other compounds must meet a minimum RRF of 0.010. /} D o I o / r I

Page 1 of2 Hn •? i 0*40 IFORM VI VGA 3/90

. 6AVOLATILE ORGANICS INITIAL CALIBRATION DATA

Lab Name: CHEMTECH_________ Contract: EPA REGION m — ]>* — — ——• — —--—— _—-i-- ^ V_____BB____________________________.M^_^__MH_

Project No.: A673-S_____ Site: _____ Location: _____ Group:

Instrument ID: VOA1________ Calibration Date(s): 12/3/95 12/3/95

Heated Purge: (Y/N) _Y_ ' Calibration Tunes: 0738 1038


Lab File ID: RRF10 = L1391.D RRF20 = L1390.DRRF50 •=* L1389.D RRFIOO = L1392.D RRF200 = L1393.D

COMPOUND

•

t

•

•

•

1• - - • • - '

roiuene-dS 'Bromofluorobenzene *l,2-Dichloroethane-d4

RRF10

-

.1.2780.7271.802

RRF20

-

,.

1.1360.6601.825

RRF50

•»,

,'

1.0510.5951.728

RRFIOO

\

0.9940.5651.711

RRF200

^

-

0.9620.5391.587

RRF

•_

,

1.0840.6171.731

%RSD

x

11.712.45.4

* Compounds with required minimum RRF and maximmn %RSD values. A Q() 1 AAll Other compounds must meet a minimum RRF nf Q.Q1Q, •'-I**

Page 2 of2AR3I8l*62 3/9°

7A ..VOLATILE CONTINUING CALIBRATION CHECK


Project No. A673-S _____ Site: ' Location: _____ Group:


Lab File ID: L1442.D _________ Init. Calib. Date(s): 12/3/95 12/3/95

Heated Purge: (Y/N) Y hiit. Calib. Times: 0738 1038

GC Column: DB624 ID: 0.53 (nun)

COMPOUND• Dichlorodifluorouietl mi ieCnloromediarieBromomedianeVinyl ChlorideChjorocthane

. Medrylene ChlorideAcetoneCarbon Disul fide1,1-DicbJorpeiheiic1 , 1 -Dichlorocdiauc:trans-l,2-Dichlon)ctliciiccis-l,2-Dichkm>ctliciicChloroform1 ,2-Dichloroethanc2-Butanonel,l,l-Trichlonx:tlianeCarbon.TetrachlorkleBromodichloromethaiic1,2-Dichloropropaiic

. cis-1 ,3-DichloropropciicTrichloroetlieiieDibrbmoclilontmetliane1,1,2-TrichlonKJthaiic-

•iBenzene: 1'* • 'trans-1.3-DichloropropcticBromofbrm4-Methyl-2-Pentaiu)iie2-HexanoneTerrachloroetliene1 , 1 ,2,2-TetrachloroethaneToluene .ChlorbbenzeueEmylbenzeneStyrenem+ p-Xyleheso-xylene

RRF0.2420.4300.6880.6800.4791.6300.6803.0321.9222.9542.1492.0083.475 .1.901'0.278•0.4480.437

[ 0.549.0.3950.4940.3620.5060.3870.8300.4580.3840.7160.5100.4510.8791.1790.9191.3680.8850.5141.013

' •

.

RRF500.1220.2770.7530.4240.256!1.7130.7392.8562.0042.8972.2281.9483.5501.8640.3620.5380.4800.7480.4980.6150.3920.5780.4460.9750.5110.3840.7260.5730.459 .0.7501.2991.0081.4020.9680.5381.121

MINRRF

0.1000.100.

0.1000.200

. 0.2000.100

0.1000.1000.200

0.2000.3000.1000.1000.5000.1000.100

0.2000.5000.4000,5000.100 •0.3000.3000.300

•

*bC49C35J2

-9.4(37.6:)C46.6J)-5.1-8.7 . '5.8-4.31.9-3.73.0-2.21.9

C-30.2-20.T-9.8

<r36.23>

G?eX>-24.5-8.3

•-14.2-15.2-17.5-11.60.0-1.4-12.4-1.814.7-10.2-9.7-2.5'-9.4-4.7-10.7

MAX%D

25.025.0

25.025.0

25.025.0

25.025.025.0

25.025.025.025.025.025.025.0

25.025.025.025,025.025.025.025.0

j SAMPLE NO.VSTD050VBLK011811205D581811205DS91811205D601811205D63181 1205 DOS18112P5D03 1811206P02 '«.1811206D611811204D521811204D52MS1811204D52MSD

•

,

'

All other compounds must meet a minimum RRF of 0.010. 000166A n 3 I 8 k 6 3

Page I of2


Lab Name: CHEMTECH________ Contract: EPA REGION III . —j> S 2—

Project No. A673-S Site: Location: ___ Group:



Heated Purge: (Y/N) Y Init. Calih. Times: 0738 1038

GC Column: DB624 ID: 0.53 (nun)

COMPOUND

.

-

•

-

. '

t^

. . . .«

Toluene-d8Bromofluorobenzeuel,2-Diculoroedianc:-d4 .

RRF

1

•1.0840.6171.731

RRF50

,

-

,

:

1.4290.7061.980

MINRRF

1

'"

0.200

%D,

-. •

~ ~-

•

-

C3y_-14.4-14.4

MAX%D

1

"

25.0


Page2of2 'fl R 3 1 8 k 6 I*FORM VH VGA 3/90 II

• '• 7A• .VOLATILE CONTINUING CALIBRATION CHECK

Lab Name: CHEMTECH - Contract: EPA REGION III

Project No. A673-S' Site: Location: Group:


Lab File ID: L148S.D___________ I''"- Calib. Date(s): 12/3/95 12/3/95

Heated Purge: (Y/N) Y , Init. Calih. Times: 0738 1038

GC Column: DB624 ID: U53 (mm)

COMPOUNDDichlorodifluorometlunc .Chloromethaue ' 'BromomedianeVinyl ChlorideChloroediane • .Methylene Chloride •AcetoneCarbon Disuitide1,1-Dichloroethcnc1,1-Dichloroethanctrans- L2-Dichloroetlicnccis-1 ,2-DichloroedieiicChloroform1,2-Dichioroethahe2-Butanone1,1, 1-TrichloroethaiicCarbon TetrachlorideBromodichloroinetliaiic1,2-Dichloropropanecis-1 ,3-DichloropnipeneTrichloroediene ' 'Dibromochloronietliane1 , 1 »2-Trichlon>etliaiie

"-'•Benzene '.• • '*r •• , •trans-1, 3-DichloropropciieBromofbrm4-Memyl-2-PentaiK)iie24iexanoneTerrachloroedieueIrli2,2-Tetrachicm>etliaiicTolueneChlorobenzeneEthylbenzene <-.••'.'Styrenem+ p-Xylenes. •o-xylene

RRF0.2420.4300.6880.6800.4791.6300.6803.0321.9222.9542.1492.0083.4751.9010.2780.4480.4370.549U3950.4940.3620.5060.3870.8300.4580.3840.7160.5100.4510.8791.1790.919113680.8850.5141.013

RRF500.1060.4430.8010.4660.2741.6170.9012.8291.5872.7352.1172.3743.8541.9840.3560.4270.5270.5770.4690.4870.4570.6230.4390.7910.4230.4160.8040.590Q.5520.8391.1050.9841.2130.9400.4690/909

MINRRF

0.1000.100

0.1000.200

0.2000.100

0.1000.1000.200

0.2000.3000.1000.1000.5000.1000.100

0.2000.5000.4000.5000.1000.3000.3000.300

%D-_C56.2-3.0-16.4f3_1.5j)C42.8>>O.g.

C-32.5J6.717.47.41.5-18.2-10.9-4.4

C-28.J >4.7---20.6-5.1-18.71.4

&6.£>-23.1-13.44.77.6-8.3-12.3-15.7-22.44.66.3-7.111.3-6.28.810.3

MAX%D

25.025.0

25.025.0

25.025.0

25.025.025.0

25.025.025.025.025.025.025.0

25.025.025.025.025.025.025.025.0

1SAMPLE NO.VSTD050VBLK021811206P02RE181I206D6418112060621811206D6S1811206D661811207D041811213G011811213G021811213G031811214G041811214D67

All other compounds must meet a minimum RRF of 0.010.AR3!8i*65

Page 1 of 2

7 AVOLATILE CONTINUING CALIBRATION CHECK

Lab Name: CHEMTECH . Contract: EPA REGION III

Project No. A673-S _____ Site: __ Location: __ Group:



Heated Purge: (Y/N) Y Iiiit. Calib. Times: 0738 1038

GC Column: DB624 ID: 0!5? (nun) .

COMPOUND

Toluene-d8Bromofiuorobenzene1 ,2-Dichloroethane-d4

-RRF

•*

1.0840.6171.731

RRF50

- /

•

1.2290.7001.582

MINRRF

0.200

%D

B

""" "

'

'

-13.4-13.58.6

MAX%D

•

25.0

All odier compounds must meet a minimum RRF of 0 010. U U U 1 D O

Page2of2 A R 3 I 8 'I* 6 6FORM VH VOA 3/90

' . ' ; . " • - • ' . • . - - • . 6 AVOLATILE ORGANICS INITIAL CALIBRATION BATA '

Lab Name: CHEMTECH_____. Contract: US EPA REGION ffl .

Project No.: A695-S_____ Site: Location: ______ Group:


Heated Purge: (Y/N) _Y_ " Calibration Times: 1034 1401

GC Column DB624 ID: 0.53 (mm) -

Lab File ID: RRF10 = L1534.D RRF20 - L1533.DRRF50 = L1532.D RRFIOO = L1535.D RRF200 = L1536.D

COMPOUNDDicMorodiflaoromethaneChloromethaneBromomethane . *Vinyl Chloride • *ChloroethaneMethylene Chloride 'AcetoneCarbon Disulfide '1,1-Dichloroethene *1,1-Dichloroethane *1,2-Dichloroethene (total)Chloroform. . *1,2-Dichloroethane *2-Butanone1,1, 1-Trichloroethane *Carbon Tetrachloride *Bromodichloromethane *1,2-Dichldropropanecis-113-DichIoropropene" *rrichloroediene - . *Dibromochloromethane • *1,1,2-Trichloroethane *Benzene *trans-1, 3-Dichloropropene ,. *Bromoform ' - ' - *4-Methyl-2-Pentanone2-HexanoneTetrachloroethene *1,1,2,2-Tetrachloroethane *Toluene *Chlorobenzene , *Ethylbenzene *Styrerie ,'•' ::-^--: • -';/&$*m+ p-Xylenes . o- *o-xylene ' • ' • . - ' *

RRF101.0600.9420.9511.2150.3511.757 ,0.9403.8662.0303.1974.7075.9563.1380.3090.5090.4750.6720.4300.540 '0.4150.5250.3930.909

, 0.480 ;0:344;0.7600.5210.4360.7241.2080.9211.5090.9250.5491.200

RRF201.2461.3071.0231.2600.3381.7640.8823.7552.097,311614.8245.4633.0630.2810.4870.4710.6470.4110.5190.3980.5270.3710.862.0.467.;0.3610.763 -t0.554

i 0.4580.7271.2320.9301.5290.938 h0.5571.178

RRFSO^0.9831.1220.760.1.0000.301,Iv372 :.0.683 ..-,.3.0321.576 :2.4033.7473.8262.4780.2180.4000.3790,5030.3160.4110.3320.4340.291.0.6810.3670.315*:0.5700.3900.3660.571 v0.951 .0.7111.134,0.723$0.412 '-ft.0.876• . . ' -- >','

RRFIOO'0 8571.0080.781a%20.28113810:6 73.084 -r1.6482.3413.512-3.4292.6520.2640.477'0.45501621 :D1402 ;0.520"013930.509-

.0.3650.830 r-

0.473;}.••*O361$i*0.6760.4%0.4050.641 .1,108. 0.845.1.340 „*&&$&*•vOi494f,1.056

RRF2000.7250.9360.784

_• 1.0000.260

v:l:l%-U'582;;2.8021.343

, 1.9963.7723.5532.2330.2100.372.0.355-,0.478>0 3110.4070.3110.400.0.2860.644

;fc0.373E?o:290'0.5380.3950.321 •0.5050.8620.668

- 1;0330:674 •-,"

* 0.388 '0.798i

RRF0.9741.0630.8601.0870.3061.4940.7573.3081.7392.6204,1194.4452.7130.2560.4490.4270.5840.3740.4790.3700,4790.3410.7850.4320.3340.6620.4710.3970.6331.0720.8151.3090.8220.480 *1.022

• •• '>

.%RSD20,314.613.912.812.517.019.714.318.320.414.626.414.216.513.313.1-15.015.013.512.312.214.514.813.19.315.815.913.815.315.114.816.914.516.117.6

**

**

**

**4>

4>

*

41

*

*

*

*

*

41

4r.

*

*

*

*

4>

* Compounds with required minimum RRF and maximum %RSD values.All other compounds must meet a minimum RRF of 0.010. . .. • 000044

Page 1 of 2 • '/I R Q f O/. C 7FORM VI VGA '^ H 0 j 0 4 b / 3/90


Lab Name: CHEMTECH Contract: US EPA REGION m



Heated Purge: (Y/N) _Y_ " Calibration Times: 1034 1401



COMPOUND

X

• - • -; V'-V '?'<#**•' " • *::* •?;-

**'• '•- " ,r

." - ••-,:.•

' . '. "V

.

• •- --.v . '.-••.• • ,',.'.:„,-: - z~, ''*': .--V"

. - ,

. - ••• . iij$ c**?'9S -%*-$&

ToIuene-dS ^ ' '*• ' ;f- r* '~Bromofluorobenzene . *l,2TDichloroetnane-d4

RRFIO

;

I/

..--

• -\ '

' X - >•

..*•'• • : •'-

,-

.• r ;--*-1.423.1.0023.727

RRF20

•

. • ••

i

••".?:• 3$?%;

1.117 r0.7612.649

RRF50

,

.;.^ J-1.0160.651

' 2.388

RRFIOO

_

1.0130.6502.253

RRF200

.

0.8170.5082.131

RRF

1.0770.7142.629

%RSD

•

20.625.724.5

* Compounds with required minimum RRF arid mflyiimnn %RSD values. . 000045All other compounds must meet a miniminn RRF of 0.010.

Page 2 of 2 • ' - - A D O I O I C oFORM VI VOA H (1 O I O «4 D O 3/90

• • ' ' : ' • ' '' 7A • •' ' ,VOLATILE CONTINUING CALIBRATION CHECK

Lab Name: CHEMTECH Contract: US EPA REGION m

Project No, A695-S _____ Site: Location: _____ Group:


Lab File ID: L1538.D________ Init. Calib. Date(s): 12/21/95 12/21/95



COMPOUNDDichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethane . -Methylene ChlorideAcetone , •Carbon Disulfide1,1-Dichloroethenc1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane -2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzene ;trans-1 ,3-DichloropropeneBromofbrm '4~Methyl-2-Pentanone .

. 2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEmylbenzene • ; , .Styrene .m+ p-Xyleneso-xylene

^RRF0.9741.0630.8601.0870.3061.4940.7573.3081.7392.6204.1194.4452.7130.2560.4490.4270.5840.3740.4790.3700.4790.3410.7850.4320.3340.6620.4710.3970.633L0720.815,1.3090.8220.4801.022

RRF501.0360.8890.8661.0690.2841.580 -0.7713.3481.8652.8614.3854.4082.9470.2530.4800.4470.6250.3940.5210.3930.4970.3570.8480.4690.3460.6490.4760.4140.6231.1490.8561.4000.8220.5081.104

MINRRF

0.1000.100

0.1000.200

0.2000.100

0.1000.1000.200

0.2000.3000.1000.1000.5000.1000.100

0.2000.5000.4000.5000.1000.3000.3000.300

•

%D-6.416.4-0.71.77.2-5.8 .-1.8-1.2-7.2-9.2-7.40.8-8.61.2-6.9-4.?-7.0-5.3-8.8-6.2.-3.8-4.7-8.0-8.6 -•„••-3.62.0-LI-4.31.6-7.2-5.0-7:00.0-5.8 '•-8.0 -

MAX%D

25.0 ,25.0

.-'

25.025.0

25.025.0

25.025.025.0

25.025.025.025.025.025.025.0

25.025,025.025.0.,25.0,25.025.025.0

All odier compounds must meet a minimum RRF of 0.010. '•

SAMPLE NO.VSTD050VBLK011811218D691811218D22 -1811218D681811218D68MS1811218D68MSD1811218D69RE1811218D68RE

10062

Pagelof2 ' AR3l&l»69FORM VH VOA 3/90


' 'LabName: CHEMTECH Contract: US EPA REGION ffl

'

Project No. A69S-S _____ Site: Location: _____ Group:


Lab File ID: L1538.D___________ Init. Calib. Date(s): 12/21/95 12/21/95


GC Column: DB624 • ID: 0.53 (mm)

COMPOUND

.

1

•*

• • " ' • - ' . , (-''•..". *"• .

' ., " "

Toluene-d8Bromofluorobenzene . .l,2-DicbloroethaiK-d4

RRF

-. ' !'•-? < '• ''

•,'••.'.;,•%'•"•-'

1.0770.7142.629

RRF50

r~

- •

0.9870.6552.4%

MIN.RRF

T.

0.200

%D

,

---.

•

8.48.35.1

MAX%D

V

.,

25.0

All other compounds must meet a minimum RRF of 0.010. 000063

Page2of2 A R 3 I 8 k 7 0FORM VH VGA 3/90

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SDG 181-1127-W20

AR3l8tf87

OEmiECH

Report Number: A671-S Dase Number: R3181

a. Number of Samples and Date of Sample Receipt:

20 water samples were received intact on November 29.30, and December 1.1995. .

b. Parameters:

These samples were analyzed for TCL Volatile + Dichlorodifluoromethahe.t • - -

c. Analytical Techniques:

Samples were purged and analyzed by EPA GLP SOW OLM03.0 Method.

d. QA/QC's:

The surrogate recoveries of each sample is found on Form II-A. The Internal Standard Area counts for eaSample is found on Form VIII-A, and Initial Calibration results are. found on Form VI-A. Both ContinuiCalibrations and Instrument Tuning Information are located on Form V-A. Data for the Blank and associatsamples are reported on Form "IV-A". The 1811127W20 is reported on Form HI A and all %R's are within tcontrol limits.

I certify that the data package is in compliance with the terms and conditions of the contract, both technically and icompleteness, for other/than the conditions detailed above. Release of the data contained in this hard copy data packahas been authorized by thejaboratory manager or his designed, as verified by the following signature.

Name: Divyajit Mehta

Tide: Lab Manager

AR3I8488.

Gannett Fleming GANNETT FLEMING, INC.Suite 200

ENGINEERS AND PLANNERS ow KeysBaltimore. MD 21210

. . Fax: (410) 433-6520Office: (410) 433-8832

December 19, 1995

Mr. Emmanuel HedvatChemtech Consulting Group1 1 0 Route 4Englewood, New Jersey 07631

Re: EPA Contract No.: 68-W8-0037EPA Work Assignment: 37-34-3JZZEPA Region III DAS Case Number R3181Shipping Dates: November 28, November 29, and December 4, 1995Federal Express Airbill Nos.: 4405012183, 4405012113, and 4405011800,

Dear Mr. Hedvat:

The purpose of this letter is to correct errors in the Station Number column on the EPA Chain ofCustody Forms (COCs) for the referenced shipments of samples to Chemtech Consulting Group.

The following table provides the correct Sample Numbers. The Station Location column on theCOCs and the EPA Sample #s were correct:

coc#3-16043

3-16049

3-16049

3-16049

3-16058

3-16058

ShippingDate11/28/95

1 1 /29/95

1 1 /29/95

11/29/95

12/04/95

12/04/95 .

IncorrectStationNumber

SW-34

SW-18

SW-47

SW-48

SW-53

SW-53

CorrectStationNumberSW-34A

SW-18B

SW-47B

SW-48A

SW-53B

SW-53A .

FedExAirbillNumber

4405012183

4405012113

4405012113

4405012113

4405011800

4405011800

•CommentsSample was a trip blank.Sample location and EPASample # were correct.

Sample was a field blank.Sample location and EPASample # were correct.Sample was a field blank.Sample location and EPASample # were correct.Sample was a trip blank.Sample location and EPASample # were correct.

Sample was a field blank.Sample location and EPASample # were cprrect.Sample was a trip blank.Sample location and EPASampfe i were correct.

A Tradition of Excellence Since 1915 A R 3 | 8 l| 8 9

Corrected copies of the COCs referenced above are enclosed.

We apologize for any inconvenience these discrepancies may have caused.

Sincerely,GANNETT FLEMING, INC.

Sidney J. Curran

Enclosures

cc: Annette Lage (CRL) >Christopher Corbert (EPA Region III) (w/o enclosures)Rayo Bhumgara (GF (w/o enclosures)William Wentworth (HNUSI .

File: 9529.001/4.0.

flR3l8l»90

1A >'. SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

1811127W20MSLab Name: CHEMTECH . Contract: EPA REGION-HI

Project No.: A671-S Site: _____ Location: •_______ Group:

Matrix: (soil/water) WATER Lab Sample ID: t)48162

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L1407.D

Level: (low/med) Date Received: 11/29/95

% Moisture: not dec. ______ Date Analyzed: 12/6/95

GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0

Page Iof2

Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)

Concentration Units:-CAS No. Compound (ug/L or ug/Kg) ug/L Q

75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-3- '71-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571 -43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChlorometiiaueBromoniethaneVinyl ChlorideChloroetlianeMethylene ChlorideAcetoneCarbon Disulfide1 , i -Dichloroethene1, 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis- 1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans- 1 , 3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachioroethene1 , 1,2,2-TetrachloroethaneTolueneChJorobenzeneEthylbenzeneStyrene

10.10101010

- 10r2.6}1064101010 ^101010101010-10511010581010

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Project No.: A671-S Site: Location:

Matrix: (soil/water) WATER

Sample wt/voi: 5.0 ' (g/mL) ML

Level: (low/med)

% Moisture: not dec.

Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:

GC Column: DB624 ID: 0.53 (mm) Dilution Factor:

Soil Extract Volume: (uL) Soil Aliquot Volume:

Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L

>

0 m+ p-Xylenes1330-20-7 o-xylene

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SAMPLE NO.

1811127W20MS

Group:

048162

L1407.D

11/29/95'

12/6/95

1.0

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Page 2 of 2 . .

AR3I8I»92 FORMIVOA 3/9°

1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: EPA REGION-IE1811127W20MSD

Project No.: A671-S Site: _____ Location: _________ Group:

Matrix: (soil/water) WATER Lab Sample ID: O48163

Sample wt/vol: 5.Q (g/mL) ML Lab File ID L1408.D



GC Column: DB624_________ ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ______(uL) Soil Aliquot Volume: ____' (uL)

Concentration Units:CAS No. Compound (ug/L or ug/Kg) . ug/L Q

75-71-874-87-3 •74-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478 87-510061-01-579-01-6124-48-179-00-57M3-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5-108-88-3108-90-7100-41-4100-42-5

DichlorodifluorometnaneCWoromethaneBromometlianeVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroetheue1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 ,2-Dichloroediane2-Butanone1,1,1 -TrichloroethaneCarbon TetrachJorideBromodichloromethane1 ,2-Dtchloropropanecis- 1 ,3-DichloropropeneTrichloroetheneTDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans- 1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroetfaene1 ,1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

101010101010$*J1060101010101010101010105310106110101010e**j1058511010

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LA " . SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET




Sample wt/vol: 5.0 (g/mL) ML

Level: (low/med)


Lab Sample ID:

1811127W20MSD

Group:

048163

Lab File ID: L1408.D

Date Received:v

Date Analyzed:

GC Column: DB624 ID:' 0.53 (mm) Dilution Factor:


Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L -

1

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Lab Name: CHEMTECH Contract: EPA REGION-IH


VBLK01

Project No.: A671-S Site: _____ Location: __________ Group:

Matrix: (soil/water) WATER . Lab Sample ID: PBLK01

Sample wt/vol: 5.0 (g/mL) ML . Lab File ID: L1396.D

Level: (low/med) • -Date Received: ____

% Moisture: not dec. ______' Date Analyzed: 12/6/95



Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L • Q

75-71-874-87-374-83-975-OM »75-00-375-09-2 .67-64-175-15-075-35 475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-5 -75-27-478-87-510061-01-5

DichlorodifluoromethaneChloromethaneBromomedianeVinyl ChlorideChloroedianeMemylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichlotoethene1,1-Dichloroethane -1,2-Dichlproethene (total)Chloroform • -,'-1 ,2-Dich!6roethane2-Butanone1,111-Trichloroediane '.Carbon TetrachlorideBromodichloromethane1,2-Dichloropropanccis- 1, 3-Dichloropropene ,

79-01--6 ''r-'* • TnchlotoeaieiS? -'' •-*'>—•124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-

Dibromochloromethane1 , 1 ,2-TrichlbroethaneBenzene - ,nans-l ,"3-DicnloropropeneBromoform4-Memyl-2-Pentanone. 2-Hexanone p ; r

127fl8 ^ «$*<Didi tgt iaafc <f-~ ••*••*#**••79-34-5 ! *Lfl , Tca cnlotocthane108-88-3108-90-7100-41-4 .100-42-5

TolueneChlorobenzeneEthylbenzeneStyrene

10 .101010101010101010101010101010101010

,1010101010101010

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Lab Name: CHEMTECH Contract: EPA REGION-IE




Level: (low/med)


Lab Sample ID:

SAMPLE NO.

VBLK01

Group:

PBLK01


Date Received:

Date Analyzed:



Concentration Units:CAS No. Compound (ug/L Or ug/Kg) ug/L

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IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

VBLK01TENTATIVELY'IDENTIFIED COMPOUNDSLab Name: CHEMTECH Contract: EPA REGION-III

Project No. A671 Site: _____ Location: __________ Group:

Matrix: (soil/water) WATER • Lab Sample ID: PBLK01

Sample wt/vol: 5.0 (g/mL) ML Lab File II): L1396.D

Level: (low/med) Date Received:

% Moisture: not dec. ________ . Date Analyzed; 12/6/95

GC Column: DB624 ID: 0.53 (mm) Dilution Facton 1.0

Soil Extract Volume: ________(uL) Soil Aliquot Volume: ______ (uL)

Concentration Units:Number TICs found: 0 (ug/Lorug/Kg) .ug/L

|£A£ Number1.2.3.4.5.6.7.8.9.10.H.

•12.13.14.15. -'16.17.18..19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

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1A .. SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

VBLK02Lab Name: CHEMTECH Contract: EPA, REGION-HI

Project No.: A671-S Site: _____ Location: ________' Group:

Matrix: (soil/water) WATER Lab Sample ID: PBLK02

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L14S7.D


% Moisture: not dec. ______ Date Analyzed: 12/9/95.



Concentration Units:CASNo. -Compound (ug/Lorug/Kg) . ug/L Q

75-71-874-87-374-83-975-01-475-00-375-09-267-64-1 .75-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-5-10061-01-579-01-6124-18-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-710CW1-4100-42-5

Dichlorodi fluoromethaneChloromethaneBroraometlianeVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfidel.i-Dichloroethene1 , 1 -Dichloroethane1,2-Dicbloroethene (total)Chloroform1,2-DichJoroethane .2-Butanone1 , 1 , 1 -TrichloroedianeCarbon Tetrachloride

, Bromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroetnaneBenzenetrans-1 ,3-DichloropropeneBromoform .4-MethyI-2-Pentanone2-HexanoneTetrachloroethene1, 1.2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

101010101010101010to10101016 x1010101010101010101010101010 : •1010101010

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Page 1 of 2FORM IVOA ' 3/90

M3I8498 OOOltS •






Level: (low/med)


Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:

GC Column: DB624 , ID: 0.53 (mm) Dilution Factor:


Concentration Units:CAS No. Compound (ug/L or ug/Kg) . ug/L

0 m+ p-Xy4enes1330-20-7 o-xyiene

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Page 2 of 2HH 3 18*49 9 FORMIVOA Y 3/9°

IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: CHEMTECH Contract: EPA REGION-HI

VBLK02

Project No. A671 Site: _____ Location: ____________ Group:



Level: (low/med) . Date Received:

% Moisture: not dec. ________ Date Analyzed: 12/9/95

GC Column: DB624_____ ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ._____'(uL) Soil Aliquot Volume: _____ (uL)

Concentration Units:Number TICs found: ___0___ (ug/L or ug/Kg) ug/L

CAS Number1.2- •3.4.5.6.7.8.9.10.11.12.13.14.15. -16.17.18.19.20.21.22.23.24. ^25.26.27.28.29.30.

Compound Name

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SDG 181-1204-53A

flR3!850

ChEmiECH7'.'jSiJLTING GSOUP iNC

Report Number: \674-S . Dase Number: R3181/ * . . _ - • -

a. Number ef Samples and Date of Sample Receipt:

20 water samples were received intact on December 5, 6, 8, and 15, 1995.

b. Parameters:

These samples were analyzed for TCL Volatile + Dichlorodifluoromethane.


Samples were purged and analyzed by EPA CLP SOW OLM03.0 Method.

d. QA/QC's:"--—. *

The surrogate recoveries of each sample is found on Form II-A. The Internal Standard Area counts for eacSample is found on Form VIII-A, and Initial Calibration results are found on Form VI-A. Both ContinuirCalibrations and Instrument Tuning Information are located on Form V-A. Data for the Blank and associat<samples are reported on Form "IV-A". The. 1811204W52 is reported on Form HI A and all %R'sare within t!control limits. •

I certify that the data package is in compliance with the terms and conditions of the contract, both technically and fcompleteness, for othe than the conditions detailed above. Release of the data contained in this hard copy data packajhas been authorized! y thejabojatory manager or his designed, as verified by the following signature.

: Divyajit Mehta

Title: Lab Manager ,

AR3I8502 00000?

3AWATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: CHEMTECH ___________ Contract: EPA REGION III

Project No. A674-S Site: _______ Location: ________ Group: _

Matrix Spike - Sample No.: 1811204W52

COMPOUND1,1-DichloroethcneTrichloroetheneBenzene •TolueneChlorobenzene

SPIKEADDED(ug/L)

5050505050

SAMPLECONCENTRATION

(ug/L)00000

MSCONCENTRATION

(ug/L)5752634743

MS%

REC #1141041269486

QC. 'LIMITSREC.

(61-145)(71-120)(76-127)(76-125)(75-130)

COMPOUND1 , 1-DichioroetheneTrichloroetheneBenzeneTolueneChlorobenzene

SPIKEADDED(ug/L)

5050505050

MSDCONCENTRATION

(ug/L).67SO655545

MS%

REC #134100130 *no •90

%RPD #

16 *4316 *5

QC LRPD1414111313

IMITSREC.

(61-145)(71-120)(76-127)(76-125)(75-130)

# Column to be used to flag recovery and RPD values with an asterisk

* Values outside of QC limits

RPD: 2 out of 5 outside limitsSpike Recovery: 1 out of 10 outside limits

Comments:

FORMin. VOA-I AR3I8503

1A __SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

1811204W52MSLab Name: CHEMTECH Contract: EPA REGION

Project No.: A674-S , Site: _____ .' Location: __________ Group:

Matrix: (soil/water) WATER Lab Sample ID: O48324

Sample wt/vol: 5.0 (g/mL) ML Lab File ID:L1481.D


Page 1 of2 FORMIVOA AR3I850I*

% Moisture:. not dec. ,,___. . Date Analyzed: 12/10/95

GC Column: DB624,________ ID: 0.53 (mm) , Dilution Factor: . 1.0

Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)

Concentration Units:CAS No, Compound (ug/L or ug/Kg) ug/L Q

75-71-874-87,374-83-9,75-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethane •BromomethaneVinyl ChlorideChloroedianeMediylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroetlieue1,1-Dichloroetbane1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1 , 1 , 1 -TrichloroethaneCarbon TetrachlonW

- Bromodichloronietbane1 ,2-Dichloropropanccis- 1 ,3-DichloropropeneTrichloroetheneDibromochlorometbane1,1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene ._. .1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

. 1010

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Lab Name: CHEMTECH - . Contract: EPA REGION HI .1811204W52MS

Project No.: A674-S Site: Location: Group:



Level: (low/med)


Lab Sample ID: 048324


Date Received:

Date Analyzed:



Concentration Units:CAS No. Compound (ug/L or ug/Kg) ' ug/L

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Page 2 of2FORMIVOA AR3I8505 00 22

1A 'SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: EPA REGION III1811204W52MSD

Project No.: A674-S Site: • Location: ___________ Group:

Matrix: (soil/water) WATER . Lab Sample ID: 048325

Sample \yt/vol: 5.0 (g/mL) ML Lab File ID: L1482.D


% Moisture: not dec. ' Date Analyzed: 12/10/95.

GC Column: DB624 ID: 0-.53 (mm) Dilution Factor IJO

Soil Extract Volume:. ______-(uL) Soil Aliquot Volume: ______ (uL)

Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L Q

75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18?*79-34-5 .108-88-3108-90-7100-41-4100-42-5

Dichlorodifluorumethane 'ChlorotnethaneBrbmomethane •.Vinyl ChlorideChloroethaneMediylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene *1 , 1 -Dichloroethane1,2-Dichloroediene (total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1-Trichloroediane .Carbon TctrachloridcBromodicbJoromeoiane1,2-Dichloropropanecis-1, 3-DichloropropeneTrichloroethene •Dibromochloromethane1 , 1 ,2-TrichloroetbaneBenzenetrans-l,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-Hexanone :.Tetrachlproethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEtfaylbenzeneStyrene

1010101010no 310106710101010

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Page 1 of 2 ftooiocnrFORMIVOA ARvl I 8506


Lab Name: CHEMTECH Contract: EPA REGION m




Level: (low/med)


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Date Received:t

Date Analyzed:

GC Column: DB624 ID: 0.53. .(mm) Dilution Factor:



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Sample wt/vol: , 5.0 (g/mL) ML Lab File ID: L1457.D

Level: (low/med) • Date Received:

% Moisture: not dec. ___. Date Analyzed: 12/9/95

GC Column: DB624______ ID: 0.53 (mm) Dilution Facton 1.0

Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)'i

Concentration Units:CASNo. . Compound (ug/L Or ug/Kg) ug/L Q

75-71-8 Dichlorodifluoromethane74-57-3 Chloromediane •74-83-975-0.1-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-3 ..'71-55-6 .56-23-575-27-478-87-510061.-01-579-01*124-48-179-00-371-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

BroniomediaheVinyl ChlorideCfaJoroethaneMediylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroethene1,1 -Dichloroethane1.2-Dichloroediene (total)Chloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1, 3-Dichloropropene

-TrichloroetheneDibromocbJoromethane1, 1 ,2-Tn'chloroethane

• Benzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-Hexanone

'v Tetrachloroethehe '.'•-•1,1,2,2-TetrachlbroethaneTolueneChlorobenzeneEthylbenzeneStyrene

101010101010101010101010101010101010101010101010101010101010101010

uuuuuuuuuuuuuuuu ,uuuu-

. uuuuuuuuuuuuu

Page 1 of 2 •FORMIVOA AR3I8508 000 &3

1A .VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH - Contract: EPA REGION ffi

SAMPLE NO.

VBLK01

Project No.: A674-S Site: Location: Group: VH



Level: (low/med)


Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:



Concentration Units:CAS No. Compound . (ug/L or ug/Kg) ug/L

Page 2 ol


,

• . , i

t

, 1010

s

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12/9/95

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'2FORMIVOA AR3 18509 000*04

IE ' SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: CHEMTECH * Contract: EPA REGION IH

VBLK01

Project No. A674 Site: _____ Location: _________ Group:

Matrix: (soil/water) WATER " Lab Sample ID: PBLK01


Level: (low/med) , Date Received:



Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ______ (uL)

Concentration Units:'Number TICs found: 0 (ug/L or ug/Kg) ug/L

CAS Number1.2. .3.4.5.6.7.8.9.10.11.12.13.14.15. .16.17.18. ' <. •19.20.21.22.23. .24.25.36.O?A-& .-'.-v27. '.;.'•..; •:•:28. "•'29.30.

' . Compound Name

" . ' ' • ' . '

-

'*'-•' , ' ••

l

RT

-

• " • _•

Est. Cone.

"**--

Q

FORM I VOATTIC AR3 I 85 10 3/90000205


VBLK02Lab Name: CHEMTECH Contract: EPA REGION ffl






GC Column: DB624 - ID: 0.53 (mm) Dilution Factor: 1.0

Page 1 of 2FORM I VGA



75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66 3107-06-2 •78-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

Dichlorodi fluoromedianeChloromedianeBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroethene1 , 1 -Dichloroethane1,2-Dichloroethene (total)Chloroform1 ,2-Dichloroediane2-Butanone1,1,1-Trichloroethane -Carbon TetrachlorideBromodichloromethane1,2-Dichloropropane .cis- 1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroetnaneBenzenetrans-1 ,3-DichloropropeneBromofonn4-MethyI-2-Pentanone2-HexanoneTetrachloroethene1,1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

101010101010101010101010 "--101010101010101010101010101010101010101010

uuu_uuuuuuuuuuuuuu •uuuuuuuuuuU-uuuuu

A R 3 I 8 5 I I 00?j?Q9

' -'•-...: ' •. • - • • ' • 1A • ' ' :' VOLATILE ORGANICS ANALYSIS DATASHEET

Lab Name: CHEMTECH Contract: EPA REGION IH

Project No.: A674-S Site: ' Location:



Level: (low/med)

% Moisture: .not dec.

Lab Sample ID:

SAMPLE NO.

VBLK02

Group:

PBLK02

LabFileID:L1471.D

Date Received:

Date Analyzed:

GC Column: DB624 , ID: 0.53 (mm) . Dilution Factor

Soil Extract Volume: (uL)' Soil Aliquot Volume:

Concentration Units:CAS No. Compound . (ug/L or ug/Kg) ug/L

0 '•.-', .:.-•'" m+ p-Xylenes1330-2fc7r. r. :0-*y'cne

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Page 2 of2FORMIVOA AR3I85I2 ood'fio

IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS VBLK02

Lab Name: CHEMTECH___________' Contract: EPA REGION. HI

Project No. A674 Site: _______ Location: '_______ Group:



Level: (low/med) . Date Received:

% Moisture: not dec. ________ Date Analyzed: 12/9/95

GC Column: DB624_______ ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ________(uL) • Soil Aliquot Volume: ______ (uL)

Concentration Units:Number TICs found; .0 v (ug/L or ug/Kg) ug/L

CAS Number•1. , ' ' . •2.3.4.5.6.7.8.9.10.11.12. .13.14. .15.16.17.18.19.20.21.22. ,23.24.25. ,>&&**?+.:;--. •; -27..28.29.30.

: Compound Name

•

•

. -• • • • • '

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RT Est. Cone

•

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Q

FORM I VOA-TIC $ R 3 I 8 5 I 3


VBLK03Lab Name: CHEMTECH , Contract: EPA REGION ffl

Project No.: A674-S Site: _____ Location: ._______ Group:




% Moisture: not dec. ______ . Date Analyzed: 12/17/95

GC Column: DB624______ ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ______(uL) . Soil Aliquot Volume: ______ (uL)


75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06r278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloronietnane 'Bromomethane-Vinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroetbene1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform • • - • • •1.2-Dichloroethane2-Butanone '1.1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroethene - •Dibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-L3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene ••••v«f--.1,1,2,2-TetrachloroedianeTolueneChlorobenzeneEthylbenzeneStyrene

1010101010101010101010101010

- 101010101010101010101Q1010

~1Q10 ,

f 10101010

' Uuuuuuuuuuuuuuuuuuuuuuu

.-uuuuy . -uuu .uu

Page 1 of 2 'FORMIVOA AR3I85U 00021R


Lab Name: CHEMTECH Contract: EPA REGION in

1

VBLK03

Project No.: A674-S Site: Location: Group:



Level: (low/med)


Lab Sample ID: PBLK03

Lab File ID:

Date Received:

Date Analyzed:

GC Column: DB624 ID: 0.53 (mm) Dilution Factor:\




,_.

-

\

1

... -

-

. - - • • • • . . - . ........•; ' ' . . , . • • - - . .

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Page 2 of 2 fl p o j p r i rFORM i VGA H n o i o a i 9 ^ 3/9Q*

- - ' ' • • " .,* •" "" -Zr£\ " T*J\ ' 'V'"' ' • " " ' - '



VBLK03

Project No. A674 Site: _____ Location: •______ Group:




% Moisture: • not dec. ____' Date Analyzed: 12/17/95


Soil Extract Volume: ________(uL) " Soil Aliquot Volume: ____' (uL)

Concentration Units:Number TICs found: 0 ' (ug/L or ug/Kg) ug/L

CAS Number1. • '2.3.4.5. •6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28. .29.30.

Compound Name

1

t

. RT-

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~"~

•

•

Q

. . • •. •

FORMI VOA-TICAR3 I 85 I 6 000 1?

GPO 605-924

ANALYSESQ

Preservative:Yes 0 No D

BOD. AnionsSolids (TSS) (TOS) (SS)

COD. TOC, NutrientsPhenolicsMercuryMetalsCyanideOil and GreaseOrganics GC/MSPriority PollutantsVolatile OrganicsPesticidesMutagenicityBacteriology

TagNa UbSamptoNa

3-1.Oft51.T5

A R 3 I 8 5 I 7

SDG 181-1213-B03

flR3l85!8

AfOEmiECH

NSULTING GROUPS,

Report Number: A689-S Dase Number: R3181

a. Number of Samples and Date of Sample Receipt: ]•

. /7 water samples were received intact on December IS and 19.1995.

v " '• ' ' * ' ' ' • ' ' " . * * ' *

b. Parameters:


c. Analytical Techniques: , , , '


QA/QC's:

The surrogate recoveries of each sample is found on Form II-A. ,The Internal Standard Area counts for eacSample is found on Form VTJI-A, and Initial Calibration results are'found on Form VI-A. Both ContinuinCalibrations and Instrument Tuning Information are located onForm V-A: Data for the Blank and associatesamples are reported on Form "IV-A". The 1811218T68 is reported oh Form HI A and all %R's are within thcontrol limits. ' ' . ' ,, •' . : .

I certify that the data package is in compliance with the terms and conditions of the contract, both technically and fccompleteness, for other than the conditions detailed above. Release of the data, contained in this hard copy data packaghas been authorizedjjby the laboratory manager or his designed, as verified by the following signature.

. Name: Dryyajfr Mehta r.-_ . .,'...:' .;

Tnie: Lab Manaeer

AR3I85I9-


1S11218T68MSLab Name: CHEMTECH - Contract: US EPA REGION H

Project No.: A689-S Site: _____ Location: _________ Group: ___

Matrix: (soil/water) WATER . Lab Sample ID: O48948MS


Level: (low/med) _________ Date Received: 12/19/95

% Moisture: not dec. 100 Date Analyzed: 12/20/95

GC Column: DB624________ ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: ______(uL) Soil Aliquot Volume: ____ • (liL)

Concentration Units:CAS No. Compound . . (ug/L or ug/Kg) ug/L Q

75-71-874-87-374-83-975-01-475-00-375-09-2.67-64-175-15-075-35-475-34-4540-39-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-5

DichlorodifiuoromemaneChloromethane •BromomethaneVinyl ChlorideChloroetfaancMethylenc ChlorideAcetoneCarbon Disulfide1 , 1-DichloFoethene1 , 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1,2-Dichioroethane,2-Butanonc ~ . • - - . - -• - -1,1,1-TrichloroethaneCarbon-TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloroprDpcne

79-01-6 ' Tricoldrjbeaiene~* '*& r* ' ' •124-48-179-00-571-43-2.10061-02-675-25-2108-10-1591-78-6127-18-4 ^79-34-5108-88-3108-90-7100-41-4KXM2-5 '

DibFomochldromethane1,1,2-TrichlotoethaoeBenzene ,,trans-1 , j-uicuioropropene

' Bromofbrm4-Methyl-2-Pentanone24iexanone. .•,.-->•

* -'-•"f_'t ...nl.'f.-i'^jl.a.. a..-'.' - • ' ff- ......,.- >ueinciuoiucuicQC ';*'•'.; - ..14,2 -TettachloroethaneToluene "ChlorobenzeneEmylbenzeneStyrene

10101010101010

. 1054101010 ^1010101010101053 "10104810101010101048481010

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uU 1 00090

Page 1 of2FORMIVOA -AR3I8520 3/9°

Lab Nam

Project N

Matrix:

Sample \v

Level:

% Moisti

GCColui

SoilExtrj


e: CHEMTECH , Contract: US EPA REGION H

o.: A689-S Site: Location:

(soil/water) WATER

t/vol: 5.0 (g/mL) ML

(low/med)

ire: not dec. 100

Lab Sample ID:

SAMPLE NO.

181L218T68MS

Group:

O48948MS


Date Received:

Date Analyzed:

nn: DB624 ID: 0.53 (mm) Dilution Factor

act Volume: ' . (uL) Soil Aliquot Volume:

Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/L

/

Page 2 of

0 m+ p-Xylenes1330-20-J o-xylene v V

t;•

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' - - - - -

. . . . • . . . .

I

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(uL)

^

000913/90


Lab Name: CHEMTECH Contract: US EPA REGION H1811218T68MSD

Project No.: A689-S Site: _____ Location: ____________ Group:

Matrix: (soil/water) WATER . Lab Sample ID: O48948MD


Level: (low/med) ______ Date Received: 12/19/95





75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-0 -75-35-475-34-4540-59-067-66-3107-06-278-93-3 '71-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroethene1 , LJDichloroethane1,2-Dichloroethene (total)Chloroform •• .1,2-Dichloroe thane

. 2-Butanone .1,1,1-TrichloroethaneCarbon Tetrachloride

• Bromodichloromethane' 1,2-Dichloropropane<&•! ,3-DichloropropeneTrichloroethene .Dibromochloromethane1,1,2-TrichloroethaneBenzene . 'trans-1, 3-DichloropropeneBromofotm4-Methyl-2-Pentanone,2-Hexanone .. . -: ,

127™Io"i4 * , -0*"' _-j nTctlTKinlOrOCtlvrPiff- .»**", '79-34-5 .108-88-3108-90-710O41-4100-42-5

1,1,2,2-TetrachloroethaneToluene .ChlorobenzeneEthylbenzene

• Styrenc

101010101010101052101010101010101010105710105310101010101051521010

UuuuuuU t

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uU . f

Page 1 of2 FORMIVOA AR3I8522 3/90

1A .SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: US EPA REGION H




Level: (low/med)

% Moisture: not dec. 100

Lab Sample ID:

1811218T68MSD

Group:

O48948MD


Date Received:

Date Analyzed:

GC Column: DB624 ID: 0.53 (mm) Dilution Factor.



•


.

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CM09!Page 2 of2

FORMIVOA AR3 18523 3/9°


"•• VBLK01Lab Name: CHEMTECH Contract: US EPA REGION IT


Matrix: (soil/water) WATER . Lab Sample ID: VBLK01



% Moisture:, not dec. 100 Date Analyzed: 12/20/95

GC Column: DB624________ ID: 0.53 (mm) Dilution Factor: 1.0



75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-2778-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-4M100-42-5

Dichlorodifluoromethane .. .Chloromethane ' • - ' :BromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-DichlOroethene1 , 1 -Dichloroethane1,2-Dichloroethene (total)Chloroform •1 ,2-Dichloroethane2-Butanone ' ' •1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromcthanc .1 ,2-Dichloropropanetis-l,3-DichloropropeneTrichloroemene ' '- "Dibromochloromethane ,1,1,2-TrichloroethaneBenzene ,trans-1, 3-DichloropropeneBromoform4-Methyl-2-Pentanone2-Hexanone

"•' Tetrachloroethene .1,1,2,2-TetrachlorocthaneTolueneChlorobenzeneEthylbenzeneStyrene

1010

. 1 010101010101010

. 101010101010101010 .10101010 '1010101010 .1010101010

.uuu .uU'uuuu .uuuuuu-uuuu

, uuu .

-'• U- u

- uuu

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-. uu

Page 1 of 2 • • ' .FORMIVOA AR3I8521* OOW84.


Lab-Name: CHEMTECH . . Contract: US EPA REGION IE

Project N

Matrix:

Sample v

Level:i

% Moisti

fo.: A689-S Site: Location:

(soil/water) WATER

rt/vol: 5.0 (g/mL) ML

(low/med)

are: not dec. 100

Lab Sample ID:

SAMPLE NO.

VBLK01

Group:

VBLK01

LabFileID:L1521.D

Date Received:

Date Analyzed:


Soil Extract Volume: ___ (uL) Soil Aliquot Volume:


Page 2 of

0 m-f p-Xylenes1330-20-7 o-xylene

/- - ' '

-

1010 ,

-

• , '•

,

12/20/95

1.0

QUU

FORM I VOA fl R 3 1 8 5 2 5

(uL)

»

>000853/90


Lab Name: CHEMTECH_____________________1 Contract: US EPA REGION ffl

Project No. A689 Site: _____ Location: _________ Group:

Matrix: (soil/water) WATER " " Lab Sample ID: VBLK01

Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L1521.Dk

Level: (low/med) ________ Date Received:




Concentration Units:Number TICs found: __ 0 ___ (ug/L or ug/Kg) ug/L

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

.

1

RT Est. Cone.

~~~ —

,

Q

•

nft

(

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FORM I VOA-TIC A R 3 ! 8 5 2 6 3/9°

SDG 181-1127-D20

AR3I8527

OEimECH

Report Number: A672-S Dase Number: '_ R3181

a. Number of Samples and Date of Sample Receipt:

19 soil samples were received intact on November 29,30, December 1, and S, 1995.

b. Parameters:f




d. QA/QC's:

The surrogate recoveries of each sample is foundôn Form II-A. The Internal Standard Area counts for eachSample is found oh Form VIII-A, and Initial Calibration results are found on Form VI-A. Both ContinuingCalibrations and Instrument Tuning Information are located on Form V-A. Data for the Blank and associatedsamples are reported on Form "IV-A". The 1811127D20 is reported on Form HI A and all %R's are within thecontrol limits. , ,

I certify that the data pcompleteness, for otherhas been authorized bj

~ \<Signature: \

Date:

ickage is in compliance with the terms and conditions of the contract, both technically and forthan the conditions detailed above. Release of the data contained in this hard copy data packagethe laboratory manager or his designed, as verified by the following signatureT~~~ ~^^ ' . ...C )r / ^ - ^ OJame: Diwaiit Mehta

J#& &*Y. Title: LakManager/


1811127D20MSLab Name: CHEMTECH Contract: EPA REGION III

Project No. :• A672-S Site: _______ Location: '_____ Group: ___

Matrix: (soil/water) SOIL Lab Sample ID: O48177

Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1424.D

Level: (low/med) LOW Date Received: 11/29/95

% Moisture: not dec. 27 ' Date Analyzed: 12/7/95

GC Column: DB624 ______ ID: 0.53 .(mm) Dilution Factor: 1.0


Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q

75-71-874-87-374-83-975-01-475-00-375-09-267-64- 1'75-15-075-35-4 -75-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-57941-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-S108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBroniomethaneVinyl ChlorideChloroetliaiieMethyiene ChlorideAcetoneCarbon Disulfide1 . 1 -Dichloroethene1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 ,2-Dichloroethane2-Butahone1.1,1 -TrichloroethaueCarbon Tetrachloridc .Bromodichloromethane1,2-Dichloropropanecis- 1 ,3-Dichloropropene

. TrichloroetheneDibromochloromethaoe1,1,2-Trichloroediane "Benzenetrans- 1 ,3-DichloropropeneBromofbnn4-Methyl-2-Pentanone2-HcxanoncTetrachloroetnene1,1,2,2-TctrachIoroethane .TolueneChlorobenzeneEthylbenzeneStyrcnc

141414141414

r™j>~~~1489141414141414141414145914147114141414141468531414

UUUuuu

u

uuuuuuuuuu

uu

uuuuuu

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Page 1 of 2FORMIVOA 000194 3/90

AR3I8529


Lab Name: CHEMTECH Contract: EPA REGION, HI


Matrix: (soil/water) SOILi *

Sample wt/vol: 5.0 (g/mL) G

Level: (low/med) LOW

% Moisture: not deq. 27

•Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:



Concentration Units:CAS No. . Compound (ug/L or ug/Kg) ug/Kg

0 m-f- p-Xylenes1330-20-7 o-xylene

'

; l

-'

.

• . ' • ' ' -• • ,

'

1414

•'

-

~~->-

- •:

--

SAMPLE NO. T

1811127D20MS

Group:

048177

L1424.D

11/29/95

12/7/95

1.0

Quu

- •

•

(uL)

Page2of2 ««*»-*»—FORMIVOA 000195 3/90

AR3I8530

1A " SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

1811127D20MSDLab Name: -CHEMTECH . Contract: EPA REGION III


Matrix: (soil/water) SOIL Lab Sample ID: O48178•


Level: (low/med) LOW . Date Received: 11/29/95




Concentration Units:CASNo. Compound . (ug/L or ug/Kg) ug/Kg Q

75-71-874-87-3 .74-83-975-0 1-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-2778-87-510061-01-579-01-6 :124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41r4100-42-5

DichlorodifluommethaneChloromethaneBromomethaneVinyl ChlorideChloroediane .Metbylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroethene1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 ,2-Dichloroethane2-Butanone . • .'1,1,1 -TrichloroedianeCarbon TetrachlorideBromodichloromcthaue1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetbeneDibromochloromethanc1 , 1 ,2-TrichloroethaneBenzene

. trans-1 ,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-Hexanone , -

"Tetrachloroethene- . -...• .*-_£1,1,2,2-TetrachloroethaneToluene. > -ChlorobenzeneEthylbenzeneStyrene

1414

: . 14141414

S*4?~1485141414141414 .141414145714146714141414

.:,,..-,,-; ,;l- -t14«- •;,<:,.

1468531414

UU •Uuuu

u-uu

"-• uuuuuuuu

uu

uuu

, ur., U

r. U

U -u

Page 1 of 2 _*_».,.-_«FORM I VGA 000198 3/90

AR3I853I

1A .- SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH . , Contract: EPA REGION HI.


Matrix: (soil/water) SOIL




Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:


Soil Extract Volume: • (uL) Soil Aliquot Volume:

Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg

1

0 • m+ p-Xylenes1330-20-7 o-xylene

-

•'' ... " • . '

.

1414

•

.

.

1811127D20MSD

Group:

048178

L1425.D

11/29/95

12/7/95

1.0

Quu

--

x

-

(uL)

Page 2 of 2FORMIVOA 3/90

AR3J8532

4 IA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

VBLK01Lab Name: CHEMTECH * Contract: EPA REGION HI


Matrix: (soil/water) SOIL - Lab Sample ID: PBLK01


Level: (lo\v/med) LOW Date Received:



Soil Extract Volume: ___ (uL) Soil Aliquot Volume: _______ (uL)


75-71-874-87-374-83-975-01-475-00-375-09-2 .67-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-2778-87-510061-01-5 .79-01-6124-48-179-00-571-43-2 '10061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichiorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1 , 1 -Dichloroethane1,2-Dichlorocthenc (total)Chloroform1 ,2-Dichlorocthane2-Butanone1,1,1-TrichJoroethane .Carbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis- 1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-1, 3-DichloropropeneBromoform4-MethyI-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

101010101010101010101010101010101010101010101010101010101010101010

uuuuuu

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Page 1 of2FORM IVOA 3/90

AR.3I8533 00018?

Lab Narn

Project N

Matrix:

Sample w

Level:

% Moisti

GCColui

Soil Extr


e: CHEMTECH " <• Contract: " EPA REGlbN ffl


(soil/water) SOIL - -

t/vol: 5.0 (g/mL) G

(low/med) LOW

ire: not dec. 0 . , • ' '

Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:

Tin: DB624 ID: 0.53 (mm) Dilution Factor:

act Volume: (uL) Soil Aliquot Volume:


/

Page 2 of

0 m+ p-Xytenes t •-. .:.,; '.„. ..1330-20-7 o-xylene : ., •' \'-A?

. .. = •' ;

\

- ' •• • , ;*

' - ' '' -i' '">- * . , - - . . -.;..'.--7

*

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• . . , .- . . ' . . , - . . -. -* •"' --•-«! V\-J, i;..*"1*". •ji i-t '-V.i '-i ••-• V,.r-r': «~'-V. / t*1 •.. %*.*'**.'

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: -

. • . - . - 1 010

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. . .

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~

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:

SAMPLE NO.

VBLK01

Group: .

PBLK01

L1412.D

12/7/95

1,0

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'2FORM I VGA , 3/90

AR3,I8531* 000183


VBLK01TENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: CHEMTECH Contract: EPA REGION HI

Project No. A672 Site: _____ Location: __________ Group:

Matrix: (soil/water) SOIL ' Lab Sample ID: PBLK01

Sample wt/vol: 5.0 (g/mL) G_____ Lab File ID: L1412.D

Level: (low/med) LOW Date Received: _____

% Moisture: not dec. ___0____ . Date Analyzed: 12/7/95

GC Column: DB624_______ ID: 0.53 (mm) Dilution Factor: 1.0


Concentration Units:Number TICs found: 0____ (ug/L or ug/Kg) ug/Kg

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

Compound Name

•

- .

RT

.

-

Est. Cone.

~"~-

.

Q

FORM I VOA-TIC 3/90

AR3I8535 000184


VBLK02Lab Name: CHEMTECH Contract: EPA REGION ffl

Project No.: A672-S Site: _____ Location: _______'' Group:

Matrix: (soil/water) SOIL . Lab Sample ID: PBLK02


Level: (low/med) LOW Date Received:

% Moisture: not dec. 0 . Date Analyzed: 12/7/95


Soil Extract Volume: _______(uL) Soil Aliquot Volume: _______ (uL)

Concentration Units: •CASNo. Compound (ug/L or ug/Kg) ug/Kg Q

75-71-874-87-374-83-975-01-475-00-375-09-2 .67-64-175-15-075-35-475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061r01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78r6127:18-4.79-34-5108-88-3 .108-90-7100-41-4100-42-5

• Dichlorodi fluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene Chloride

. AcetoneCarbon Disulfide1,1-Dichloroethene1,1 -Dichloroethane1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloroprqpanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzene •trans-l',3-DichloropropcneBromoform4-Methyl-2-Pcntanone2-HexanoneTettachloroethene v r '1,1,2,2-TetrachloroedianeTolueneChlorobenzene.EmylbenzeneStyrene

101010101010101010101010 '101010101010101010101010101010101010101010

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/1R3I8536

Page 1 o f 2 . . .FORM I VGA 3/9°

Lab Nam

Project N

Matrix:

Sample v,

Level:

% Moisti

GCColui

Soil Extr

IAVOLATILE ORGANICS ANALYSIS DATA SHEET

e: CHEMTECH ' Contract: EPA REGION IH


(soil/water) SOIL

t/vol: 5.0 (g/mL) G

(low/med) LOW

ire: not dec. 0

Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:

:nn: DB624 ID: 0.53 (mm) Dilution Factor:

act Volume: (uL) Soil Aliquot Volume:


/


^

»

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*

f

*

1010

SAMPLE NO.

VBLK02

Group:

PBLK02

L1428.D

12/7/95

1.0

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Page2of2 FORMIVOA lOj 3/90

AR3I8537

.


Lab Name: CHEMTECH " Contract: EPA REGION HI

VBLK02

Project No. A672 . Site: • Location: __________ Group:



Level: (low/med) LOW . Date Received:

% Moisture: not dec. ___0___ Date Analyzed: 12/7/95


Soil Extract Volume: ________(uL) Soil Aliquot Volume: .______ (uL)

Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/Kg

CAS Number1.2.3.4.5.6.7. '8.9.10.11.12.13. .14.15. •16.17.18.19.20.21.22.23.24.25.26.27.28.29. '30.

Compound Name

,

••

••

.'' '

,

RT

-

Est.Conc.

"~- -

Q

-

FORM I VOA-TIC 000190 3/90

AR3I8538

SDG 181-1204-D52

AR3I8539

ctEimECH•4S--L* NGGSGL'P -NC

Report Number: A673-S Dase Number: R3181\

a. Number of Samples and Date of Sample Receipt:_r

19 soil samples were received intact on December 5. 6. 8, and 15. 1995.

b . Parameters: ' - . ' . . . -

These samples were analyzed for TCL Volatile.* Dichlorodifluoromethane.

c. Analytical Techniques: .


"3. QA/QC's:

The surrogate recoveries of each sample is found on Form II-A. The Internal Standard Area counts for eachSample is found on Form VIII-A, and Initial Calibration results are found on Form VI-A, Both ContinuingCalibrations and Instrument Tuning Information are located on Form V-A. Data for the Blank and associatedsamples are reported on Form "IV-A". The 1811204D52 is reported on Form III A and all %R's are within thecontrol limits.'

I certify that the data package is in compliance with the terms and conditions of the contract, both technically and forcompleteness, for other than the conditions detailed above. Release of the data contained in this hard copy data packagehas been authorized by fhe laboratory manager or his designed, as verified by the following signature.

Name: Pivyaiit Mehta

Title: Lab Manager

000001AR3I85UO

8AVOLATILE INTERNAL STANDARD AREA AND RT SUMMARY



Lab File ID (Standard): L1442.D_____ Date Analyzed: 12/8/95

Instrument ID: VQA1____ Time Analyzed: L700

GC Column: DB624 ID: 0.53 (mm) Heated Purge (Y/N). Y

010203040506070809101112131415161718192021•22

12 HOUR STDUPPER LIMITLOWER LIMIT, SAMPLE

NO.VBLK01181I205D581811205D591811205D601811205D631811205D08 .181 1205D03- I3lfca4 Dfl31811206P021811206D611811204D5218H204D52MS1811204D52MSD

.

ISI (BCM)AREA tt42301:846024211506

373607252697277X3S2750442358762442 IS .2327 vX1 7659S *

RT #9.67

.10/179.17

9.719.800.889.92' • .9.95 "l>.9710.02 .10.05

260056 i 111.03276477 • 10.04IOS5S") » | 10.09230325 • 10.10

1

IS2 (DFB) .AREA #,16550123310024827506

/

1366457,.11)68825,1145151 .1307885108856311940359042416620% *10643621129319810083 *900395

RT M13.8314.3313.33

13.8413,9414.0214.0814.0914.1014.1514.1714.1614.1714.2014.23

IS3 (CBZ)AREA #10921202184240546060

809550667599716112819922685438785056601440408806 *712519

. 752369483455 *5(56126 •*

v

RT '#24.0924.5923.59

24.0724.2024.2724.3124.3024.3324.3724.3924.3724.4024.4324.43

ISI (BCM) - Bromochlorome?haiicIS2 (DFB) - 1,4-DifluorobenzeiieIS3 (CBZ) = Chlorobenzeiie-d5

AREA UPPER LIMIT = +1005? of internal standard area . .AREA LOWER LIMIT =-50% of internal standard areaRT UPPER LIMIT = 4-0.50 minutes of internal standard RTRT LOWER LIMIT = -0.50 minutes of internal standard RT

# Column used to flag values outside QC limits with an asterisk- * Values outside of QC limits. . 0 fl fl f Q ft

Page lofl RD o l o C I 1FORM VIH VGA H n O I O J H I 3/90

' . . . - . 8AVOLATILE INTERNAL STANDARD AREA AND RT SUMMARY

Lab Name: CHEMTECH Contract: EPA REGION IH

Project No.: A673-S_____ Site: ______ Location: _______ Group:

Lab File ID (Standard): L1485.D____ Date Analyzed: 12/16/95

Instrument ID: VOA1 Time Analyzed: 0847

GC Column: DB624 ID: 0.53 (mm) Heated Purge (Y/N) Y

01020304050607080910111213141516171819202122

12 HOUR STDUPPER LIMITLOWER LIMITSAMPLE

NO.VBLK021811206P02RE1811206D641811206D62181 1206D651811206D661811207D041811213G011811213G021811213G031811214G04 .18U214D67

,

' - /• - '.

r

.•

ISI (BCM)AREA #427211854422213606

- 396408 ,223364 . '3i3i2f.- •.;.351734 .

. 269036249065327359353304242971302404.273829382659 •

."'. • - ' '

" * . ..- - .... -1. +ff •„ .

RT #9.8610.369.36

9.93,,,-IQ.QO .10.0110.02 .10.0710.0910.1110.1110.1310.1610.1310.13 •

IS2 (DFB)AREA #19355453871090967773

1186239791568 *1329994127176112615791364497136551417566721153952120253916430441824922

RT #14.0314.5313.53

14.0514.1314. 1414.17-14.2014.2114.2014.2214.2514.2714.26.14.26

IS3 (CBZ)AREA #13320172664034666009

828539539651 *73519868971774557167980080284011606707004627104381103462U35971

RT #24.2824.7823.78

24.31. 24.3524.3724.3924.4224.4224.4324.4424.4524.4724.4724.47

ISI (BCM) = Bromochloromethaiie . 'IS2 (DFB) - 1,4-DifluorobenzeneIS3 (CBZ) — Chlorobenzeue-dS

AREA UPPER LIMIT. +100$ôfimenial standard areaAREA LOWER LIMTf5= 50% ofimeniai standard areaRT UPPER LIMIT = +0.50 minutes of internal standard RTRT LOWER UMTT = -0.50 minutes of internal standard RT

. i' , . • ~ - - '# Column used to Sag values, outside QC limits with an asterisk* Values outside of QC limits. - '" ftftft T fl *

Page 1 of 1FORMVffl VOA 3/90

1A __ SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: EPA REGION III181L204D52MSD_____ 4.


Matrix: (soil/water) SOIL - Lab Sample ID: O48322


Level: (low/med) LOW . . Date Received: 12/5/95


GC Column: DB624_________ ID: 0.53 (mm) Dilution Factor: t.O



75-71-8 ,74-87-374-83-975-01 -475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

Dichlorodi fluorometlianeChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroetheue1 , 1 -Dichloroethanc1,2-Dichloroethene (total)Chloroform1 ,2-Dichloroethanc2-Butanone '1,1.1 -TrichloroethaneCarbon TetrachloridcBromodichloromethane1 ,2-Dichloropropanecis-1. 3-DichloropropeneTrichloroetheneDibromochloromcthanc1 , 1 ,2-TrichloroethaneBenzene

, trans-1, 3-DichloropropeneBromofonn4-MethyI-2-Pentanone2-HexanoneTetrachloroetnene1,1,2,2-TetrachIoroetbaneTolueneChlorobenzeneEthylbenzeoeStyrene

202020202020202012020202020202020202020%2020110202020202020120842020

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FORM I VGA 3/90AR3I851*3

. • SAMPLEVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: EPA REGION HI18H204D52MSD

Project No.: A673-S Site: ____ Location: ___________ Group:


Sample wt/vol: 5.0 (g/mL) G , Lab File ID: L1454.D

Level: (low/med) . LOW Date Received: 12/5/95

% Moisture: not dec. 49 . Date Analyzed: 12/9/95

GC Column: DB624 ' ID: 0.53 (mm) Dilution Factor 1.0

Soil Extract Volume: . (uL) Soil Aliquot Volume: (uL)

Concentration Units:CAS No. Compound > (ug/L or ug/Kg) ug/Kg

0 v m+ p-Xylenes1330-20-7'. o-xylene

• ' ' . - • • • - . . . : . . - .

•

i

' ;

.. ' . • • .,- ~ ~ '. ' . ' - ' ' . ' •

4

. 2 020

•

-~. , -. •

.• . • •

•'•' • . - • ' •

• .--. .T -. - . - " . • • ' ' ' . • . - •• •• ' . • • .' •": • . \ '

QU . ,u

1

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-

— fr30203Page 2 of 2

FORM I VGA 3/90

1A , SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

1811204D52MSLab Name: CHEMTECH - Contract: EPA REGION III




Level: (low/med) LOW. Date Received: 12/5/95


GC Column: DB624___________ ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: " ______(uL) Soil Aliquot Volume: _______ (uL)


75-7 ITS74-87-374-83-975-OM75-00-375-09-267-64-175-15-075-35-475-34-4 -540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-5 ,10061-01r5

79-016.,.124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6

. DichiorodifluoromeuianeChloromethane :BromomethaneVinyl Chloride .ChloroetiianeMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1 . 1 -Dichloroethane1 .2-Dichloroethene (total)Chloroform1,2-Dichlorocihane2-Butanone. 1 . 1 , 1 -TrichloroeihaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanc

. cis-1, 3-Dichloropropene: - TrichloroedieneV;? • ;Dibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans- 1 ,3-DichloropropeneBromoform4-Methyl-2-Pentahone2-Hexanone ... '

127-18-4 i e*t oroedie:ne -: :f .-£x. £'.79-34-5 i ....108-88-3108-90-7100-41-4100-42-5

. ! iri,l;2 TetrachjoroedianeTolueneChlorobenzeneEthylbenzeneStyrene

20-20 >

, 20202020202010020202020202020202020

. 90 .202011020202020202011078 <2020

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Page 1 of 2FORM I VOA 3/90

AR3i85l*5

" 1A. VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: EPA REGION HI






Lab Sample ID:

Lab File ID:

Date' Received:

Date Analyzed:



Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg

>

0 tn+ p-Xylenes1330-20-7 o-xylene .

•

* " ' " • . . " . ' •

•

,

' 2020 '

""***-

• . •

'

•

, . . ' ; . .

•

SAMPLE NO.

1811204D52MS

Group:

048321

L1453.D

12/5/95

12/9/95

1.0

QUU

' f- '

(uL)

0001Page 2 of 2

FORMIVOA 3/90

AR3l.85if6


VBLK01Lab Name: CHEMTECH Contract: EPA REGION III


Matrix: (soil/water) SOIL • Lab Sample ID: PBLK01

Sample wt/vol: 5.0 (g/mL) G Lab File ID:L1443.D


% Moisture: not dec. 0 Date Analyzed: • 12/8/95


Page 1 of 2

F°RMIVOA AR3I85U7



75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-4.79-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoroniedianeChloromethaneBromoniethaneVinyl ChlorideChloroetltaneMethylene ChlorideAcetoneCarbon Disulfide1 . 1 -Dichldroethene1 . 1 -Dichloroethanc1,2-Dichloroethene (total)Chloroform1.2-Dichloroethane2-Butanone-1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-DichIoropropanecis- 1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-Trichloroethane -Benzenetrans-1, 3-DichloropropeneBromofbrm4-Methyl-2-Pentanone

. 2-Hexanone- - Tetrachloroethene . * .'

1,1,2,2-Tetrachlorocthane'- Toluene

ChlorobenzeneEmylbenzeneStyrene

101010,1010 •10101010101010101010101010101010101010101010

,101010101010

uuuuuuuuuuuuuuuuuuuuuuuuuuuuU 'uuuu

Lab Nam

Project N

Matrix:

Sample w

Level:

% Moisn

GCColui

Soil Extr


e: CHEMTECH Contract: EPA REGION IH


(soil/water) SOIL

t/vol: 5.0 (g/mL) G

(low/med) LOW

ire: not dec. 0

Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:

mn: DB624 ID: 0.53 (mm) Dilution Factor:

act Volume: (uL)f

Soil Aliquot Volume:


0 m+ p'Xylenes1330-20-7 o-xylene

10 - ,10

~~~~-

'

: SAMPLE NO. '

VBLK01-%i

Group:

PBLK01

L1443.D

12/8/95

1.0

Q

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VBLK01TENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: CHEMTECH * Contract: EPA REGION UI

Project No. A673 Site: _____ Location: _______, Group:


Sample wt/vol: 5.0 (g/mL) G____ Lab File ID: L1443.D





Concentration Units:Number TICs found: __ 0 .(ug/L or ug/Kg) ug/Kg

CAS Number1. c2.'3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26. ' .27.28.29.30.

Compound Name.• „.

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FORMIVOA-TIC


VBLK02Lab Name: CHEMTECH Contract: EPA REGION III


Matrix: (soil/water) SOIL - Lab Sample ID: PBLK02

Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1486.O

Level: (low/med) LOW Date Received: ___

% Moisture: not dec. 0 , Date Analyzed: 12/16/95

. GC Column; DB624 ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: _____(uL) Soil Aliquot Volume: ______ (uL)~

Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q

75-71-874-87-374-83-9 .75-01-475-00-3 .75-09-267-64-175-15-075-35-475.34-4540-59-067-66-3107-06-2 .78 93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48rl79-00-571-43-210061-02-675-25-2108-10-1591r78-6

' DichlorodifluoromethaneChloromethaneBromomedianeViayl Chloride

. ChloroethaneMethylene ChlorideAcetoneCarbon Disulfide '1,1-Dichloroediene1 , 1 -Dichloroethane1,2-Dichloroethene (total).Chloroform1,2-Dichldroethane2-Butanone1 , 1 . 1 -TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropane -

, cis-1, 3-DichloropropeneTricntoroetheneDibromochloromethane1,1,2-TrichloroediancBenzenetrans-1, 3-DichloropropeneBromoform. 4-Methyl-2-Pentanone24Iexanone

l2/T*o*"4 • * ~ * "T "TCtTftCnloroCincnff - • *79-34-5108-88-3108-90-7100-41-4100-42-5

.. 1,1,2,2-TetnichloroethaneToluene. ..ChlorobenzeneEthylbenzeneStyrene

1010 '10101010101010101010101010101010101010101010101010101010101010

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Page 2 of


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ire: not dec. 0

Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed: .

un: DB624 ID: 0.53 (mm) Dilution Factor

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VBLK02

Project No. A673___ Site: ' Location: __________ Group:

Matrix: (soil/water) SOIL ; Lab Sample ID: PBLK02

Sample wt/vol: 5.0 (g/mL) G Lab File ID: LI486.D

Level: (low/med) LOW Date Received:

% Moisture: . not dec. 0___ Date Analyzed: 12/16/95


Soil Extract Volume: ________(uL) ' Soil Aliquot Volume: _____ (uL)

Number TICs found:d: 0

CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14. ~15. '.16.17.18.19.20.21.22.23.24.25.26;h "\ •'• ', •27,.28.29.30.

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000194FORM I VOA-TIC 3/90

AR3I8552


U8H20SD03"Lab Name: CHEMTECH Contract: EPA REGION III




Level: (tow/med) LOW Date Received: 12/6/95




Concentration Units:CASNo. Compound , (ug/L or ug/Kg) ug/Kg Q

MD03 'J""«-*" • |

75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-S10061-01-579-01-6124-48-t79-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethancChloromethaneBromomethane

' Vinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroetbene1 , 1-Dichlorocdune

' 1,2-Dichloroethene (total)Chlorofonn1 ,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon Tetrachioride •Bromodichloromethane1 ,2-Dichloropropane. cis-1, 3-DichloropropeneTrichloroetheneDibromochloromcdutne1 , 1 ,2-TrichloroethaneBenzenetnns- 1. 3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-HexanoneTetnchkHoethene1, 1,2,2-TetnchIoroetittneTolueneChlorobeozeneBthylbenzeneStyrene

22222222222222222222222222

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' AR3I8553 000052

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AR3I8557

In Reference to c ** N'o(s): -_.

REGIONAL/LABORATORY COMMUNICATION SYSTEMTelephone Record Log

' / MDate of Call:

Laboratory Name:Lab Contact: ' &. A'. O Tj

Region: ____Regional Contact: fivS'* S^Q..

Call Initiated By: __ M.afaora:ory __ Region

In reference to data for the following sample numbeKs):•• t

Summary of Questions/Issues Discussed:'" A/O

; O.C. * *•

Summary of Resolution:0 V-tS .*/-.'.£

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Signature . Date

000096Distribution: (1) Lab Copy, (2) Region Copy, (3) flpCopy. ' AR3I8558

CffimtECH

mmReport Number: A695-S Dase Number: R3I81

*-• • i

a. Number of Samples and Date or Sample Receipt:

3 soil samples were received intact on December 19. 1995.

b. Parameters:




d. QA/QC's:

The surrogate recoveries of each sample is found on Form H-A. The Internal Standard Area counts for eacSample is found on Form VIII-A, and Initial Calibration results are found on Form VI-A. Both ContinuinCalibrations and Instrument Tuning Information are located on Form V-A. Data for the Blank and associatesamples are reported on Form "IV-A". The 1811218D68 is reported on Form HI A and all %R's are within tl' control limits. '

I certify that the data package is in compliance with the terms and conditions of the contract, both technically, and ftcompleteness, for other than the conditions detailed above. Release of the data contained in this hard copy data packaghas been authorized b the laboratory manager or his designed, as verified by the following signature.

Name; Divyajit Mehta

Title* Lab Manacer

0 0001V-.,

flR3!8559 *'"J

8AVOLATILE INTERNAL STANDARD AREA AND RT SUMMARY

Lab Name: CHEMTECH Contract: US EPA REGION

Project No.: A695-S_____ Site: _______ Location: ______ Group:

Lab File ID (Standard): L1538.D_____ Date Analyzed: 12/22/95

Instrument ID: HPS971A . Time Analyzed: 1034

GC Column: DB624 ID: 0.53 (mm) Heated Purge (Y/N) Y

01020304050607080910111213141516171819202122

. .'. .12 HOUR STDUPPER LIMITLOWER LIMITSAMPLE .NO.

VBLK01 ' '••1811218D691811218D221811218D681811218D68MS1811218D68MSD1811218D69RE1811218D68RE'

ISI (BCM)AREA #14585329170672927

128896 ::.v,- 67543'*,8174739794 *51070 *49954 *51685 *32973 *

'•

RT #8.488.987.98

8.508.5,18.488.478.518.48 .8.498.52

IS2(DFB) .AREA' #11990732398146599537

1100764 :563445 ' *:656093357948 *471954 *469587 *454387 .*302625 *

L. •- w * - ,.

RT #12.6713.1712;17

.•-.«12367S3£gS-w.;32a»rr:>.- 12.168 "'12.6812.6812.6712.67

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IS3(CBZ)AREA #930524

' 1861048465262

' 894891•* 403223 •:•:*489752 ,258238 *343078 *361770 *316248 *198248 *

~^ -

RT' #23.0823.5822.58

23.0823.0823.0823.0923.0723.0823.0823.08

ISI (BCM) « Bromocfaloromethane 'IS2 (DFB) = 1,4-DifluorobenzeneIS3 (CBZ) = Chlorobenzene-dS

AREA UPPER LIMIT =? +10056 of internal standard ana. .v .-i, :*:5v7 =v" ,AREA LOWER UMTT•«* -30% of imemal stiidaid area: ; * ' V;"-'-". '* ,RT UPPER LIMIT = +0.50 minuteslof internal standard RTRT LOWER LtMTT = -0.50 minutes of internal standard RT ,

# Column used to flag values outside QC limits with an asterisk -* Values outside of QC limits. 0 00069

Page 1 o f 1 - . - . ' -FORMvmvoA I1R3J8560 3/9°


1811218D68MSLab Name: CHEMTECH - Contract: US EPA REGION H

75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-5 .71-43-210061-02-675-25-2108-10-1591-78-6

DichlorodifluotomcthancChloromethane; -•• ; - '•.BromomethaneVinyl Chloride ~ChloroethaneMethytene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform ;1,2-Dichloroethane2-Butanone .'•1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanetis-l,3-DichioropropeneTiicWcooethene t:J: 'DibromochloromethaiH. 1,1,2-TrichloroethaneBenzene ,trans-l,3-Dichloropropene

. Bromoform4-Methyl-2-Pentanone2-Hexanone" ..v;

127-184, T«ti3»i ilbnje11iene : ,' ".:- ~.79-34-5108-88-3108-90-7100-41-4100-42-5

1,1,2,2-TetrichloroethaneToluene* .-'ChlorobenzeneEthylbenzeneStyrene

2020

. 2 020202020,2015020202020.20202020202086202011020202020

;•••<*'. - 20 A .20110942020

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Project No.: A695-S ' Site: _____ Location: __________ Group: ___

Matrix: (soil/water) SOIL . Lab Sample ID: O48951MS

Sample wt/vol: 5.0 (g/mL) G Lab File ID: LJ543.D

Level: (low/med) LOW . ' Date Received: 12/19/95 •




Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q.

00007?Page 1 of2

v FORMIVOA 3/90AR3I856I

Lab Nam

Project N

Matrix:

Sample w

Level:

% Moisti

GCColui

Soil Extr


e: CHEMTECH Contract: US EPA REGION H

o.: A695-S Site: Location: .

(soil/water) SOIL

t/vol: 5.0 (g/mL) G

(low/med) LOW

ire: not dec. 51

Lab Sample ID:

SAMPLE NO.

1811218D68MS

Group:

O48951MS


Date Received:

Date Analyzed:

inn: DB624 ID: 0.53 (mm) Dilution Factor:

act Volume: • (uL) Soil. Aliquot Volume:


0 m-Kp-Xylenes1330-20-7 . o-xylene

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Page 2 of 2FORMIVOA

AR3I8562

1A . SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: CHEMTECH Contract: US EPA REGION H1811218D68MSD


Matrix: (soil/water) SOIL Lab Sample ID: O48951MD


Level: (low/med) LOW Date Received: 12/19/95


GC Column: DB624_________ ID: 0.53 (mm) Dilution Factor 1.0

Soil Extract Volume: (uL) Soil Aliquot Volume: ___________ (uL)

Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q

75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067r66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5

DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1,1-Dichloroethane

. 1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichioroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzene

Bromoform4-Methyl-2-Pentanonc2-Hexanone

•» - Tetrachloroethenc1,1,2,2-TetrachloroethaneToluene .ChlorobenzeneEthylbenzencStyrene

20202020202020201602020202020202020202011020201302020202020201301002020

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flR3!8563


Lab Name: CHEMTECH - Contract: US EPA REGION H






Lab Sample ID:

1811218D68MSD

Group:

O48951MD


Date Received:

Date Analyzed:




-0 m+ pOCylenes

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12/22/95

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FORM I VGA 3/90

HR3I8561*


VBLK01Lab Name: CHEMTECH , ... Contract: US EPA REGION tti

Project No.: A695-S Site: _____ Location: ____________ Group:

Matrix: (soil/water) SOIL . Lab Sample ID: VBLK01

Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1S39.D

Level: (low/med) LJDW_ Date Received: ______



GC Column: DB624 _________ ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: __________ ("*-) Soil Aliquot Volume: _______ (uL)

75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2 .108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41 *100-42-5

DichlorodifluoromethaneChloromethane "BromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetbneCarbon Disulfide1 , 1-Dichloroethene1 , 1 -Dichloroethane1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-Trichloroe thaneCarbon TetrachlorideBromodichlbromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromcthane1 , 1 ,2-TrichloroethaneBenzene ,trans-1 ,3-DichloropropeneBromoform4-Methyi-2-Pentanone2-HexanoneTetrachloroethene .1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene

10101010101010101010101010101010101010io10101010101010101010101010

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Page 1 of 2FORMIVOA H D O I O C C C 3/9°AnJ I 8565


Lab Name: CHEMTECH - Contract: US EPA REGION H



Sample wt/vol: . 5.0 (g/mL) G



Lab Sample ID:

SAMPLE NO.t

VBLK01

Group:

VBLK01


Date Received:

Date Analyzed:




Page 2 of

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1330-20-7 . o-xylene

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AR3I8566


Lab Name: CHEMTECH________________ Contract: US EPA REGION ffl -

Project No. A695 Site: _____ Location: ______________ Group:

Matrix: (soil/water) SOIL Lab Sample ID: VBLK01

Sample wt/vol: 5.0 (g/mL) G____ Lab File ID: L1539.D

Level: (low/med) LOW Date Received: __

% Moisture: not dec. ___0___ Date Analyzed: 12/22/95

GC Column: DB624________ ID: 0.53 (mm) Dilution Factor 1.0


Concentration Units:Number TICs found: ._______ (ug/L or ug/Kg) ug/Kg

CAS Number1.2.3..4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29. .30.

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Documents

VOLATILE ORGANICS INITIAL CALIBRATION DATA · 2019-12-01 · 7A VOLATILE CONTINUING CALIBRATION CHECK Lab Name: CHEMTECH . Contract: EPA REGION-in Project No. A671-S _____ Site: Location: